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Subpart X—Secondary Precious Metals Subcategory

Source:

50 FR 38365, Sept. 20, 1985, unless otherwise noted.

§ 421.260 Applicability: Description of the secondary precious metals subcategory.

The provisions of this subpart are applicable to discharges resulting from the production of precious metals at secondary precious metals facilities.

§ 421.261 Specialized definitions.

For the purpose of this subpart:

(a) Except as provided below, the general definitions, abbreviations, and methods of analysis set forth in 40 CFR part 401 shall apply to this subpart.

(b) The term precious metals shall mean gold, platinum, palladium, rhodium, iridium, osmium, and ruthenium.

(c) The term Combined Metals, shall mean the total of gold, platinum and palladium.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31705, Aug. 3, 1990]

§ 421.262 Effluent limitations guidelines representing the degree of effluent reduction attainable by the application of the best practicable control technology currently available.

Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart shall achieve the following effluent limitations representing the degree of effluent reduction attainable by the application of the best practicable technology currently available:

(a) Furnace wet air pollution control.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper 136.400 71.800
Cyanide (total) 20.820 8.616
Zinc 104.800 43.800
Ammonia (as N) 9,571.000 4,207.000
Combined metals 21.54
Total suspended solids 2,944.000 1,400.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(b) Raw material granulation.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metal in the granulated raw material
Copper 12.050 6.340
Cyanide (total) 1.839 0.761
Zinc 9.256 3.867
Ammonia (as N) 845.100 371.500
Combined metals 1.902
Total suspended solids 259.900 123.600
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(c) Spent plating solutions.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper 1.900 1.000
Cyanide (total) 0.290 0.120
Zinc 1.460 0.610
Ammonia (as N) 133.300 58.600
Combined metals 0.300
Total suspended solids 41.000 19.500
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(d) Spent cyanide stripping solutions.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper 7.030 3.700
Cyanide (total) 1.073 0.444
Zinc 5.402 2.257
Ammonia (as N) 493.200 216.800
Combined metals 1.110
Total suspended solids 151.700 72.150
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(e) Refinery wet air pollution control.[2]

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 39.900 21.000
Cyanide (total) 6.090 2.520
Zinc 30.660 12.810
Ammonia (as N) 2,799.000 1,231.000
Combined metals 6.300
Total suspended solids 861.000 409.500
pH (1) (1)
1 Within the range of 7.5 to 10.0 at alltimes.

(f) Gold solvent extraction raffinate and wash water.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper 1.197 0.630
Cyanide (total) 0.183 0.076
Zinc 0.920 0.384
Ammonia (as N) 83.980 36.920
Combined metals 0.189
Total suspended solids 25.830 12.290
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(g) Gold spent electrolyte.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper 0.017 0.009
Cyanide (total) 0.003 0.001
Zinc 0.103 0.005
Ammonia (as N) 1.160 0.510
Combined metals 0.003
Total suspended solids 0.357 0.170
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(h) Gold precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper 8.360 4.400
Cyanide (total) 1.276 0.528
Zinc 6.424 2.684
Ammonia (as N) 586.500 257.800
Combined metals 1.320
Total suspended solids 180.400 85.800
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(i) Platinum precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 9.880 5.200
Cyanide (total) 1.508 0.624
Zinc 7.592 3.172
Ammonia (as N) 693.200 304.700
Combined metals 1.560
Total suspended solids 213.200 101.400
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(j) Palladium precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper 11.400 6.000
Cyanide (total) 1.740 0.720
Zinc 8.760 3.660
Ammonia (as N) 799.800 351.600
Combined metals 1.800
Total suspended solids 246.000 117.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(k) Other platinum group metals precipitation and filtration.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper 9.880 5.200
Cyanide (total) 1.508 0.624
Zinc 7.592 3.172
Ammonia (as N) 693.200 304.700
Combined metals 1.560
Total suspended solids 213.200 101.400
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(l) Spent solution from PGC salt production.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper 1.710 0.900
Cyanide (total) 0.261 0.108
Zinc 1.314 0.549
Ammonia (as N) 120.000 52.740
Combined metals 0.270
Total suspended solids 36.900 17.550
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(m) Equipment and floor wash.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 0.000 0.000
Cyanide (total) 0.000 0.000
Zinc 0.000 0.000
Ammonia (as N) 0.000 0.000
Combined metals 0.000 0.000
Total suspended solids 0.000 0.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(n) Preliminary treatment.

BPT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of total precious metals produced through this operation
Copper 95.000 50.000
Cyanide (Total) 14.500 6.000
Zinc 73.000 30.500
Ammonia (as N) 6665.000 2930.000
Combined Metals 15.000
Total Suspended Solids 2050.000 975.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31705, 31706, Aug. 3, 1990]

§ 421.263 Effluent limitations guidelines representing the degree of effluent reduction attainable by the application of the best available technology economically achievable.

Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart shall achieve the following effluent limitations representing the degree of effluent reduction attainable by the application of the best available technology economically achievable:

(a) Furnace wet air pollution control.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper 5.760 2.745
Cyanide (total) 0.900 0.360
Zinc 4.590 1.890
Combined metals 1.350
Ammonia (as N) 599.900 263.700

(b) Raw material granulation.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper 0.819 0.390
Cyanide (total) 0.128 0.051
Zinc 0.653 0.269
Combined metals 0.192
Palladium 0.064
Platinum 0.064
Ammonia (as N) 85.310 37.500

(c) Spent plating solutions.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Gold
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(d) Spent cyanide stripping solutions.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper 4.736 2.257
Cyanide (total) 0.740 0.296
Zinc 3.774 1.554
Combined metals 1.110
Ammonia (as N) 493.200 216.800

(e) Refinery wet air pollution control[2] .

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(f) Gold solvent extraction raffinate and wash water.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper 0.806 0.384
Cyanide (total) 0.126 0.050
Zinc 0.643 0.265
Combined metals 0.189
Ammonia (as N) 83.980 36.920

(g) Gold spent electrolyte.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper 0.0111 0.0053
Cyanide (total) 0.0017 0.0007
Zinc 0.0089 0.0037
Combined metals 0.0030
Ammonia (as N) 1.1600 0.5100

(h) Gold precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper 5.632 2.684
Cyanide (total) 0.880 0.352
Zinc 4.488 1.848
Combined metals 1.320
Ammonia (as N) 586.500 257.800

(i) Platinum precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 0.560
Ammonia (as N) 693.200 304.700

(j) Palladium precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper 7.680 3.660
Cyanide (total) 1.200 .480
Zinc 6.120 2.520
Combined metals 1.800
Ammonia (as N) 799.800 351.600

(k) Other platinum group metals precipitation and filtration.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700

(l) Spent solutions from PGC salt production.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper 1.152 0.549
Cyanide (total) 0.180 0.072
Zinc 0.918 0.378
Combined metals 0.270
Ammonia (as N) 120.000 52.740

(m) Equipment and floor wash.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 0.000 0.000
Cyanide (total) 0.000 0.000
Zinc 0.000 0.000
Combined metals 0.000
Ammonia (as N) 0.000 0.000

(n) Preliminary treatment.

BAT Limitations for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
Mg/troy ounce of total precious metals produced through this operation
Copper 64.000 30.500
Cyanide (Total) 10.000 4.000
Zinc 51.000 21.000
Combined metals 15.000
Ammonia (as N) 6665.000 2930.000

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31706, Aug. 3, 1990; 55 FR 36932, Sept. 7, 1990]

§ 421.264 Standards of performance for new sources.

Any new source subject to this subpart shall achieve the following new source performance standards:

(a) Furnace wet air pollution control.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper 5.760 2.745
Cyanide (total) 0.900 0.360
Zinc 4.590 1.890
Combined metals 1.350
Ammonia (as N) 599.900 263.700
Total suspended solids 67.500 54.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(b) Raw material granulation.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper 0.819 0.390
Cyanide (total) 0.128 0.051
Zinc 0.653 0.269
Combined metals 0.192
Ammonia (as N) 85.310 37.500
Total suspended solids 9.600 7.680
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(c) Spent plating solutions.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600
Total suspended solids 15.000 12.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(d) Spent cyanide stripping solutions.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper 4.736 2.257
Cyanide (total) 0.740 0.296
Zinc 3.774 1.554
Combined metals 1.11
Ammonia (as N) 493.200 216.800
Total suspended solids 55.500 44.400
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(e) Refinery wet air pollution control[2] .

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600
Total suspended solids 15.000 12.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(f) Gold solvent extraction raffinate and wash water.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper 0.806 0.384
Cyanide (total) 0.126 0.050
Zinc 0.643 0.265
Combined metals 0.189
Ammonia (as N) 83.980 36.920
Total suspended solids 9.450 7.560
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(g) Gold spent electrolyte.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper 0.011 0.005
Cyanide (total) 0.002 0.001
Combined metals 0.003
Zinc 0.009 0.004
Ammonia (as N) 1.160 0.510
Total suspended solids 0.131 0.104
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(h) Gold precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper 5.632 2.684
Cyanide (total) 0.880 0.352
Zinc 4.488 1.848
Combined metals 1.320
Ammonia (as N) 586.500 257.800
Total suspended solids 66.00 52.800
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(i) Platinum precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700
Total suspended solids 78.000 62.400
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(j) Palladium precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper 7.680 3.660
Cyanide (total) 1.200 0.480
Zinc 6.1200 2.520
Combined metals 1.800
Ammonia (as N) 799.800 351.600
Total suspended solids 90.000 72.000
pH (1) (1)
1 Within the range of 7.5 to 10.00 at all times.

(k) Other platinum group metals precipitation and filtration.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700
Total suspended solids 78.000 62.400
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(l) Spent solution from PGC salt production.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper 1.152 0.549
Cyanide (total) 0.180 0.072
Zinc 0.918 0.378
Combined metals 0.270
Ammonia (as N) 120.000 52.740
Total suspended solids 13.500 10.800
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(m) Equipment and floor wash.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 0.000 0.000
Cyanide (total) 0.000 0.000
Zinc 0.000 0.000
Combined metals 0.000
Ammonia (as N) 0.000 0.000
Total suspended solids 0.000 0.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

(n) Preliminary treatment.

NSPS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of total precious metals produced through this operation
Copper 64.000 30.500
Cyanide (Total) 10.000 4.000
Zinc 51.000 21.000
Combined metals 15.000
Ammonia (as N) 6665.000 2930.000
Total Suspended Solids 750.000 600.000
pH (1) (1)
1 Within the range of 7.5 to 10.0 at all times.

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31708, Aug. 3, 1990]

§ 421.265 Pretreatment standards for existing sources.

Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for existing sources. The mass of wastewater pollutants in secondary precious metals process wastewater introduced into a POTW must not exceed the following values:

(a) Furnace wet air pollution control.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper 5.760 2.745
Cyanide (total) 0.900 0.360
Zinc 4.590 1.890
Combined metals 1.350
Ammonia (as N) 599.900 263.700

(b) Raw material granulation.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals in the granulated raw material
Copper 0.819 0.390
Cyanide (total) 0.128 0.051
Zinc 0.653 0.269
Combined metals 0.192
Ammonia (as N) 85.310 37.500

(c) Spent plating solutions.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw material
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(d) Spent Cyanide stripping solutions.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper 4.736 2.257
Cyanide (total) 0.740 0.296
Zinc 3.774 1.554
Combined metals 1.110
Ammonia (as N) 493.200 216.800

(e) Refinery wet air pollution control.[1]

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(f) Gold solvent extraction raffinate and wash water.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper 0.806 0.384
Cyanide (total) 0.126 0.050
Zinc 0.643 0.265
Combined metals 0.189
Ammonia (as N) 83.980 36.920

(g) Gold spent electrolyte.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper 0.011 0.005
Cyanide (total) 0.002 0.001
Zinc 0.009 0.004
Combined metals 0.003
Ammonia (as N) 1.160 0.510

(h) Gold precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper 5.632 2.684
Cyanide (total) 0.880 0.352
Zinc 4.488 1.848
Combined metals 1.320
Ammonia (as N) 586.500 257.800

(i) Platinum precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700

(j) Palladium precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of palladium precipitated
Copper 7.680 3.660
Cyanide (total) 1.200 0.480
Zinc 6.120 2.520
Combined metals 1.800
Ammonia (as N) 799.800 351.600

(k) Other platinum group metals precipitation and filtration.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700

(l) Spent solution from PGC salt production.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper 1.152 0.549
Cyanide (total) 0.180 0.072
Zinc 0.918 0.378
Combined metals 0.270
Ammonia (as N) 120.000 52.740

(m) Equipment and floor wash.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 0.000 0.000
Cyanide (total) 0.000 0.000
Zinc 0.000 0.000
Combined metals 0.000
Ammonia (as N) 0.000 0.000

(n) Preliminary Treatment.

PSES for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
Mg/troy ounce of total precious metals produced through this operation
Copper 64.000 30.500
Cyanide (Total) 10.000 4.000
Zinc 51.000 21.000
Combined Metals 15.000
Ammonia (as N) 6665.000 2930.000

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31710, 31711, Aug. 3, 1990]

§ 421.266 Pretreatment standards for new sources.

Except as provided in 40 CFR 403.7, any new source subject to this subpart which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources. The mass of wastewater pollutants in secondary precious metals process wastewater introduced into a POTW shall not exceed the following values:

(a) Furnace wet air pollution control.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, incinerated or smelted
Copper 5.760 2.745
Cyanide (total) 0.900 0.360
Zinc 4.590 1.890
Combined metals 1.350
Ammonia (as N) 599.900 263.700

(b) Raw material granulation.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, in the granulated raw material
Copper 0.819 0.390
Cyanide (total) 0.128 0.051
Zinc 0.653 0.269
Combined metals 0.192
Ammonia 85.310 37.500

(c) Spent plating solutions.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/liter of spent plating solution used as a raw materail
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(d) Spent cyanide stripping solutions.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by cyanide stripping
Copper 4.736 2.257
Cyanide (total) 0.740 0.296
Zinc 3.774 1.554
Combined metals 1.110
Ammonia (as N) 493.200 216.800

(e) Refinery Wet Air Pollution Control.[1]

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 1.280 0.610
Cyanide (total) 0.200 0.080
Zinc 1.020 0.420
Combined metals 0.300
Ammonia (as N) 133.300 58.600

(f) Gold solvent extraction raffinate and wash water.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by solvent extraction
Copper 0.806 0.384
Cyanide (total) 0.126 0.050
Zinc 0.643 0.265
Combined metals 0.189
Ammonia (as N) 83.980 36.920

(g) Gold spent electrolyte.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold produced by electrolysis
Copper 0.011 0.005
Cyanide (total) 0.002 0.001
Zinc 0.009 0.004
Combined metals 0.300
Ammonia (as N) 1.160 0.510

(h) Gold precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold precipitated
Copper 5.632 2.684
Cyanide (total) 0.880 0.352
Zinc 4.488 1.848
Combined metals 1.320
Ammonia (as N) 586.500 257.800

(i) Platinum precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700

(j) Palladium precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of platinum precipitated
Copper 7.680 3.660
Cyanide (Total) 1.200 0.480
Zinc 6.120 2.520
Combined Metals 1.800
Ammonia (as N) 799.800 351.600

(k) Other platinum group metals precipitation and filtration.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of other platinum group metals precipitated
Copper 6.656 3.172
Cyanide (total) 1.040 0.416
Zinc 5.304 2.184
Combined metals 1.560
Ammonia (as N) 693.200 304.700

(l) Spent solution from PGC salt production.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of gold contained in PGC product
Copper 1.152 0.549
Cyanide (total) 0.180 0.072
Zinc 0.918 0.378
Combined metals 0.270
Ammonia (as N) 120.000 52.740

(m) Equipment and floor wash.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly average
mg/troy ounce of precious metals, including silver, produced in refinery
Copper 0.000 0.000
Cyanide (total) 0.000 0.000
Zinc 0.000 0.000
Combined metals 0.000
Ammonia (as N) 0.000 0.000

(n) Preliminary treatment.

PSNS for the Secondary Precious Metals Subcategory

Pollutant or pollutant property Maximum for any 1 day Maximum for monthly averge
mg/troy ounce of total precious metals produced through this operation
Copper 64.000 30.500
Cyanide (Total) 10.000 4.000
Zinc 51.000 21.000
Combined Metals 15.000
Ammonia (as N) 6665.000 2930.000

[50 FR 38365, Sept. 20, 1985, as amended at 55 FR 31711, Aug. 3, 1990]

§ 421.267 [Reserved]