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Title 40

Displaying title 40, up to date as of 8/06/2026. Title 40 was last amended 8/06/2026.
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Subpart C—Specific Tolerances

§ 180.101 Specific tolerances; general provisions.

(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from their application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms of parts by weight of the pesticide chemical per one million parts by weight of the raw agricultural commodity.

(b) The poisonous and deleterious substances for which tolerances are established by the regulations in this subpart C are named by their common names wherever practicable, otherwise by their chemical names.

(c) The analytical methods to be used for determining whether pesticide residues, including negligible residues, in or on raw agricultural commodities are in compliance with the tolerances established in this part 180 are identified among the methods contained or referenced in the Food and Drug Administration's “Pesticide Analytical Manual” which is available from the Food and Drug Administration, Department of Health, Education, and Welfare, 200 C Street SW., Washington, DC 20204.

§ 180.103 Captan; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) in or on the following commodities:

Commodity Parts per million
Almond 0.25
Almond, hulls 75.0
Animal feed, nongrass, group 18 0.05
Apple 25.0
Apricot 10.0
Blueberry 20.0
Caneberry, subgroup 13A 25.0
Cherry, sweet 50.0
Cherry, tart 50.0
Cotton, undelinted seed 0.05
Dill, seed 0.05
Flax, seed 0.05
Grape 25.0
Grain, cereal, forage, fodder and straw, group 16 0.05
Grain, cereal, group 15 0.05
Grass, forage 0.05
Grass, hay 0.05
Nectarine 25.0
Okra 0.05
Peach 15.0
Peanut 0.05
Peanut, hay 0.05
Pear 25.0
Plum, prune, fresh 10.0
Rapeseed, forage 0.05
Rapeseed, seed 0.05
Safflower, seed 0.05
Sesame, seed 0.05
Strawberry 20.0
Sunflower, seed 0.05
Vegetable, brassica leafy, group 5 0.05
Vegetable, bulb, group 3 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, foliage of legume, group 7 0.05
Vegetable, fruiting, group 8 0.05
Vegetable, leafy, except brassica, group 4 0.05
Vegetable, leaves of root and tuber, group 2 0.05
Vegetable, legume, group 6 0.05
Vegetable, root and tuber, group 1 0.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at THPI, in or on the following commodities:

Commodity Parts per million
Cattle, fat 0.15
Cattle, meat 0.20
Cattle, meat byproducts 0.30
Goat, fat 0.15
Goat, meat 0.20
Goat, meat byproducts 0.30
Hog, fat 0.15
Hog, meat 0.20
Hog, meat byproducts 0.30
Horse, fat 0.15
Horse, meat 0.20
Horse, meat byproducts 0.30
Milk 0.10
Sheep, fat 0.15
Sheep, meat 0.20
Sheep, meat byproducts 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52016, Sept. 12, 2007]

§ 180.106 Diuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food commodities, as follows:

Commodity Parts per million
Alfalfa, forage 3.0
Alfalfa, hay 2.0
Apple 0.1
Artichoke, globe 1
Asparagus 7
Banana 0.1
Berry group 13 0.1
Cattle, fat 1
Cattle, meat 1
Cattle, meat byproducts 1
Citrus, oil 3.0
Corn, field, grain 0.1
Corn, pop, grain 0.1
Cotton, undelinted seed 0.2
Fish - freshwater finfish, farm raised 2.0
Fruit, citrus, group 10, except lemon 0.05
Goat, fat 1
Goat, meat 1
Goat, meat byproducts 1
Grain, aspirated fractions 5.0
Grape 0.05
Grass, forage, except bermudagrass 2
Grass, hay, except bermudagrass 2
Hazelnut 0.1
Hog, fat 1
Hog, meat 1
Hog, meat byproducts 1
Horse, fat 1
Horse, meat 1
Horse, meat byproducts 1
Lemon 0.5
Nut, macadamia 0.05
Olive 1
Papaya 0.5
Peach 0.1
Pear 1
Pea, field, seed 0.1
Pea, field, vines 2
Pea, field, hay 2
Pecan 0.05
Peppermint, tops 1.5
Pineapple 0.1
Pineapple, process residue 0.4
Sheep, fat 1
Sheep, meat 1
Sheep, meat byproducts 1
Sorghum, grain, forage 2
Sorghum, grain, grain 0.5
Sorghum, grain, stover 2
Spearmint, tops 1.5
Sugarcane, cane 0.2
Sugarcane, molasses 0.7
Walnut 0.05
Wheat, bran 0.7
Wheat, forage 2
Wheat, grain 0.5
Wheat, hay 2
Wheat, straw 1.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in § 180.1(l) are established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:

Commodity Parts per million
Barley, bran 0.7
Barley, grain 0.2
Barley, hay 2
Barley, straw 1.5
Cactus 0.05
Clover, forage 0.1
Clover, hay 1.0
Oat, forage 2
Oat, grain 0.1
Oat, hay 2
Oat, straw 1.5
Trefoil, forage 0.1
Trefoil, hay 1.5
Vetch, forage 0.1
Vetch, hay 1.5

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June 13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

§ 180.107 Triflumezopyrim; tolerance for residues.

(a) General. Tolerances are established for residues of the insecticide triflumezopyrim, including its metabolites and degradates, in or on the following food commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only triflumezopyrim (2,4-dioxo-1-(5-pyrimidinylmethyl)-3-[3-(trifluoromethyl)phenyl]-2H-pyrido[1,2-a] pyrimidinium inner salt) in or on the commodity.

Commodity Parts per
million
Rice, grain * 0.40
Rice, hulls * 1.0
* There are no U.S. registrations for the use of triflumezopyrim on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48005, Oct. 16, 2017]

§ 180.108 Acephate; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity 1 Parts per million
Bean, dry, seed 3.0
Brussels sprouts 3.0
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Cauliflower 2.0
Celery 10
Cotton, hulls 1.0
Cotton, meal 1.0
Cotton, undelinted seed 0.5
Cranberry 0.5
Egg 0.1
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Hog, fat 0.1
Hog, meat 0.1
Hog, meat byproducts 0.1
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Lettuce, head 10
Milk 0.1
Peanut 0.2
Pepper 4.0
Peppermint, tops 27
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Spearmint, tops 27
Soybean, seed 1.0
1 Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on all food items (other than those already covered by a higher tolerance as a result of use on growing crops) in food handling establishments where food and food products are held, processed, prepared and served, including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, where application of acephate shall be limited solely to spot and/or crack and crevice treatment (a coarse, low-pressure spray shall be used to avoid atomization or splashing of the spray for spot treatments; equipment capable of delivering a pin-stream of insecticide shall be used for crack and crevice treatments). Spray concentration shall be limited to a maximum of 1.0 percent active ingredient. Contamination of food or food-contact surfaces shall be avoided. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

(3) Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, including its metabolites and degradates, in or on the commodities in the following table as a result of the application of acephate. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the commodity.

Commodity Parts per million
Bean, dry, seed 1
Brussels sprouts 0.5
Cauliflower 0.5
Celery 1
Cranberry 0.1
Lettuce, head 1
Pepper 1
Peppermint, tops 1
Spearmint, tops 1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity1 Parts per million
Nut, macadamia 0.05
1 Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010; 81 FR 34905, June 1, 2016]

§ 180.109 Fenpicoxamid; Tolerances for residues.

(a) General. Tolerances are established for residues of fenpicoxamid including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels for fenpicoxamid is to be determined by measuring only fenpicoxamid ([[4-methoxy-2-[[[(3S,7R,8R,9S)-9-methyl-8-(2-methyl-1-oxopropoxy)-2,6-dioxo-7-(phenylmethyl)-1,5-dioxonan-3-yl]amino]carbonyl]-3-pyridinyl]oxy]methyl 2-methylpropanoate) in or on the commodity.

Commodity Parts per
million
Banana* 0.15
Wheat, grain* 0.60
Rye, grain* 0.60
*There are no U.S. registrations for use of fenpicoxamid on this commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48000, Oct. 16, 2017]

§ 180.111 Malathion; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage 135
Alfalfa, hay 135
Almond, hulls 50
Almond, postharvest 8
Apple 8
Apricot 8
Asparagus 8
Avocado 8
Barley, grain, postharvest 8
Bean, dry, seed 8
Bean, succulent 8
Beet, garden, roots 8
Beet, garden, tops 8
Beet, sugar, roots 1
Beet, sugar, tops 8
Blackberry 8
Blueberry 8
Boysenberry 8
Carrot, roots 8
Chayote, fruit 8
Chayote, roots 8
Cherry 8
Chestnut 1
Clover, forage 135
Clover, hay 135
Corn, field, forage 8
Corn, field, grain, postharvest 8
Corn, pop, grain, postharvest 8
Corn, sweet, forage 8
Corn, sweet, kernel plus cob with husks removed 2
Cowpea, forage 135
Cowpea, hay 135
Cranberry 8
Cucumber 8
Currant 8
Date, dried fruit 8
Dewberry 8
Eggplant 8
Fig 8
Flax, seed 0.1
Garlic, bulb 8
Gooseberry 8
Grape 8
Grapefruit 8
Guava 8
Hazelnut 1
Hop, dried cones 1
Horseradish 8
Kumquat 8
Leek 8
Lemon 8
Lentil, seed 8
Lespedeza, hay 135
Lime 8
Loganberry 8
Lupin, seed 8
Mango 8
Melon 8
Mushroom 8
Nectarine 8
Nut, macadamia 1
Oat, grain, postharvest 8
Okra 8
Onion, bulb 8
Onion, green 8
Orange 8
Papaya 1
Parsnip 8
Passionfruit 8
Pea 8
Pea, field, hay 8
Pea, field, vines 8
Peach 8
Peanut, hay 135
Peanut, postharvest 8
Pear 8
Pecan 8
Pepper 8
Peppermint, tops 8
Pineapple 8
Plum 8
Plum, prune 8
Potato 8
Pumpkin 8
Quince 8
Radish 8
Raspberry 8
Rice, grain, postharvest 8
Rice, wild 8
Rutabaga 8
Rye, grain, postharvest 8
Safflower, seed 0.2
Salsify, roots 8
Salsify, tops 8
Shallot, bulb 8
Sorghum, grain, forage 8
Sorghum, grain, grain, postharvest 8
Soybean, forage 135
Soybean, hay 135
Soybean, seed 8
Soybean, vegetable, succulent 8
Spearmint, tops 8
Squash, summer 8
Squash, winter 8
Strawberry 8
Sunflower, seed, postharvest 8
Sweet potato, roots 1
Tangerine 8
Tomato 8
Trefoil, forage 135
Trefoil, hay 135
Turnip, greens 8
Turnip, roots 8
Vegetable, brassica, leafy, group 5 8
Vegetable, leafy, except brassica, group 4 8
Vetch, hay 135
Walnut 8
Wheat, grain, postharvest 8

(2) Tolerances are established for the combined residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) and its metabolite, malaoxon (O,O-dimethyl thiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

Commodity Parts per million
Barley, straw 50
Corn, field, stover 30.0
Cotton, undelinted seed 20.0
Grass, forage 200
Grass, hay 270
Oat, forage 4.0
Oat, straw 50
Rye, forage 4.0
Rye, straw 50
Watercress 0.2
Wheat, forage 4.0
Wheat, straw 50

(3) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

Commodity Parts per million
Cattle, fat 4
Cattle, meat1 4
Cattle, meat byproducts1 4
Egg 0.1
Goat, fat 4
Goat, meat1 4
Goat, meat byproducts1 4
Hog, fat 4
Hog, meat1 4
Hog, meat byproducts1 4
Horse, fat 4
Horse, meat1 4
Horse, meat byproducts1 4
Milk, fat 0.5
Poultry, fat 4
Poultry, meat1 4
Poultry, meat byproducts1 4
Sheep, fat 4
Sheep, meat1 4
Sheep, meat byproducts1 4
1 The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, poultry, or sheep.

(4) Malathion may be safely used in accordance with the following conditions:

(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot.

(ii) Treated paper trays are intended for use only in the drying of grape (raisins).

(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to grape before harvest shall not exceed 12 parts per million on processed ready-to-eat raisins.

(5) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not exceed 0.6 parts per million.

(6) Malathion may be safely used for the control of insects during the drying of grape (raisins) in compliance with paragraph (a)(4) of this section by incorporation into paper trays in amounts not exceeding 100 milligrams per square foot.

(7) Malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in accordance with the following conditions.

(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle feed, when present as the result of the application of the pesticide to bagged citrus pulp during storage. Whether or not tolerances for residues of malathion on the fresh fruit have been established under section 408 of the Act, the total residue of malathion in the citrus, dried pulp shall not exceed 50 parts per million.

(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate blocks resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle feed concentrate blocks.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, 2010]

§ 180.114 Ferbam; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date
Apple 4.0 1 None
Bean 7.0 1 10/27/07
Cabbage 7.0 1 10/27/07
Cherry 4.0 1 None
Cranberry 4.0 1 None
Fruit, citrus, group 10 4.0 1 None
Grape 4.0 1 None
Lettuce 7.0 1 10/27/07
Nectarine 4.0 1 None
Peach 4.0 1 None
Pear 4.0 1 None
Raspberry 7.0 1 10/27/07
1 Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(l), are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

Commodity Parts per million
Mango 4.0 1
1 This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

§ 180.116 Ziram; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate), including its metabolites and degradates, in or on the commodities in the table below as a result of the application of ziram. Compliance with the tolerance levels specified below is to be determined by measuring total dithiocarbamates, determined as CS2, evolved during acid digestion and expressed as zinc ethylenebisdithiocarbamate.

Commodity Parts per million
Almond 1 0.10
Apple 1 7.0
Apricot 1 7.0
Blueberry 1 7.0
Cherry, sweet 1 7.0
Cherry, tart 1 7.0
Grape 7.0
Hazelnut 0.10
Huckleberry 7.0
Peach 7.0
Pear 1 7.0
Pecan 0.10
Quince 1 7.0
Strawberry 7.0
Tomato 1 7.0
1 Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly § 180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Public Law 518, 83d Congress (68 Stat. 511).

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008; 77 FR 59123, Sept. 26, 2012; 82 FR 57860, Dec. 8, 2017]

§ 180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl dipropylthiocarbamate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of S-ethyl dipropylthiocarbamate, S-ethyl (2-hydroxypropyl)propylcarbamothioate, S-(2-hydroxyethyl)dipropylcarbamothioate, and S-ethyl (3-hydroxypropyl)propylcarbamothioate, calculated as the stoichiometric equivalent of S-ethyl dipropylthiocarbamate, in or on the commodity.

Commodity Parts per million
Alfalfa, forage 0.2
Alfalfa, hay 0.6
Almond 0.08
Almond, hulls 0.08
Bean, dry, seed 0.08
Bean, succulent 0.08
Beet, garden, tops 0.5
Beet, sugar, molasses 0.4
Beet, sugar, tops 0.5
Clover, forage 0.1
Clover, hay 0.1
Corn, field, forage 0.08
Corn, field, grain 0.08
Corn, field, stover 0.08
Corn, pop, grain 0.08
Corn, pop, stover 0.08
Corn, sweet, forage 0.08
Corn, sweet, kernel plus cob with husks removed 0.08
Corn, sweet, stover 0.08
Cotton, gin byproducts 0.20
Cotton, undelinted seed 0.08
Fruit, citrus, group 10 0.1
Grass, forage 0.60
Grass, hay 0.50
Lespedeza, forage 0.1
Lespedeza, hay 0.1
Pea, succulent 0.08
Safflower, seed 0.08
Sunflower, seed 0.08
Tomato 0.08
Trefoil, forage 0.1
Trefoil, hay 0.1
Vegetable, root 0.1
Walnut 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60239, Sept. 29, 2010, as amended at 82 FR 42952, Sept. 13, 2017]

§ 180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on the following food commodities which have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest (with the exception of strawberry):

Commodity Parts per million Expiration/Revocation Date
Alfalfa, hay, postharvest 50.0 10/31/11
Almond, postharvest 200.0 None
Apple, postharvest 5.0 None
Apricot, postharvest 20.0 None
Artichoke, jerusalem, postharvest 30.0 None
Asparagus, postharvest 100.0 None
Avocado, postharvest 75.0 None
Barley, grain, postharvest 50.0 None
Bean, lima, postharvest 50.0 None
Bean, postharvest 50.0 None
Bean, snap, succulent, postharvest 50.0 None
Bean, succulent, postharvest 50.0 None
Beet, garden, roots, postharvest 30.0 None
Beet, sugar, roots, postharvest 30.0 None
Blueberry, postharvest 20.0 None
Butternut, postharvest 200.0 None
Cabbage, postharvest 50.0 None
Cacao bean, roasted bean, postharvest 50.0 None
Cantaloupe, postharvest 20.0 None
Carrot, roots, postharvest 30.0 None
Cashew, postharvest 200.0 None
Cherry, sweet, postharvest 20.0 None
Cherry, tart, postharvest 20 None
Chestnut, postharvest 200.0 None
Cippolini, bulb, postharvest 50.0 None
Citron, citrus, postharvest 30.0 None
Coconut, copra, postharvest 100.0 None
Coffee, bean, green, postharvest 75.0 None
Corn, field, grain, postharvest 50.0 None
Corn, pop, postharvest 240.0 None
Corn, sweet, kernel plus cob with husks removed, postharvest 50.0 None
Cotton, undelinted seed, postharvest 200.0 10/31/11
Cucumber, postharvest 30.0 None
Cumin, seed, postharvest 100.0 None
Eggplant, postharvest 20.0 None
Garlic, postharvest 50.0 None
Ginger, postharvest 100.0 None
Grape, postharvest 20.0 None
Grapefruit, postharvest 30.0 None
Hazelnut, postharvest 200.0 None
Horseradish, postharvest 30.0 None
Kumquat, postharvest 30.0 None
Lemon, postharvest 30.0 None
Lime, postharvest 30.0 None
Melon, honeydew, postharvest 20.0 None
Muskmelon, postharvest 20.0 None
Nectarine, postharvest 20.0 None
Nut, brazil, postharvest 200.0 None
Nut, hickory, postharvest 200.0 None
Nut, macadamia, postharvest 200.0 None
Oat, postharvest 50.0 None
Okra, postharvest 30.0 None
Onion, bulb, postharvest 20.0 None
Onion, green, postharvest 20.0 None
Orange, postharvest 30.0 None
Parsnip, roots, postharvest 30.0 None
Peach, postharvest 20.0 None
Peanut, postharvest 200.0 None
Pear, postharvest 5.0 None
Pea, blackeyed, postharvest 50.0 None
Pea, postharvest 50.0 None
Pecan, postharvest 200.0 None
Pepper, postharvest 30.0 None
Pimento, postharvest 30.0 None
Pineapple, postharvest 20.0 None
Pistachio, postharvest 200.0 None
Plum, postharvest 20.0 None
Pomegranate, postharvest 100.0 None
Potato, postharvest 75.0 None
Pumpkin, postharvest 20.0 None
Quince, postharvest 5.0 None
Radish, postharvest 30.0 None
Rice, grain, postharvest 50.0 None
Rutabaga, roots, postharvest 30.0 None
Rutabaga, tops, postharvest 30.0 None
Rye, grain, postharvest 50.0 None
Salsify, roots, postharvest 30.0 None
Sorghum, grain, grain, postharvest 50.0 None
Soybean, postharvest 200.0 None
Squash, summer, postharvest 30.0 None
Squash, winter, postharvest 20.0 None
Squash, zucchini, postharvest 20.0 None
Strawberry, postharvest 60.0 None
Sweet potato, postharvest 75.0 None
Tangerine, postharvest 30.0 None
Timothy, hay, postharvest 50.0 10/19/10
Tomato, postharvest 20.0 None
Turnip, roots, postharvest 30.0 None
Walnut, postharvest 200.0 None
Watermelon, postharvest 20.0 None
Wheat 50.0 None

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the following conditions:

(i) When inorganic bromide residues are present as a result of fumigation of the processed food with methyl bromide or from such fumigation in addition to the authorized use of methyl bromide on the source raw agricultural commodity, as provided for in this part, the total residues of inorganic bromides (calculated as Br) shall not exceed the following levels:

(A) 400 parts per million in or on egg, dried and herb, processed and spice.

(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.

(C) 250 parts per million in or on tomato, concentrated products and fig, dried fruit.

(D) 125 parts per million in or on processed food other than those listed above.

(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR 172.730(a)(2), the amount shall not exceed 25 parts per million (calculated as Br).

(iii) Where tolerances are established on both the raw agricultural commodities and processed food made therefrom, the total residues of inorganic bromides in or on the processed food shall not be greater than those designated in paragraph (a)(2) of this section, unless a higher level is established elsewhere in this part.

(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:

(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.

(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley, corn, grain sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or from carryover and concentration of residues of inorganic bromides from fumigation of the grains with methyl bromide.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(l), is established for residues of inorganic bromides (calculated as Br) in or on the following food commodity grown in soil fumigated with methyl bromide.

Commodity Parts per million
Ginger, postharvest 100

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74812, Dec. 13, 2006, as amended at 75 FR 60239, Sept. 29, 2010]

§ 180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been used as feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will contribute considerable residues of inorganic bromides to the meat and milk.

(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such peanut hulls as animal feed. Peanut hulls containing residues of inorganic bromides from the use of methyl bromide are unsuitable as an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.

[58 FR 65555, Dec. 15, 1993]

§ 180.124 Methyl bromide; tolerances for residues.

(a) General. A tolerance is established for residues of the fumigant methyl bromide, including metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be determined by measuring only methyl bromide.

Commodity Parts per
million
Cotton, undelinted seed 150

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fumigant methyl bromide, including its metabolites and degradates, in or on the specified agricultural commodities in Table 2 to this paragraph (b). Compliance with the tolerance levels specified in Table 2 to this paragraph (b) is to be determined by measuring only methyl bromide, in or on the commodities, resulting from use of the pesticide pursuant to Federal Insecticide, Fungicide, Rodenticide Act (FIFRA) section 18 emergency exemptions. The tolerances expire and are revoked on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation date
Berry and small fruit, group 13-07 5.0 12/31/26
Cactus 3.0 12/31/26
Coconut, copra 8.0 12/31/26
Coffee, green bean 150 12/31/26
Cola, seed 150 12/31/26
Cucurbit, seed 150 12/31/26
Fig 10 12/31/26
Fruit, citrus, group 10-10 2 12/31/26
Fruit, stone, group 12-12 5.0 12/31/26
Fruit, tropical and subtropical, edible peel, group 23 10 12/31/26
Fruit, tropical and subtropical, inedible peel, group 24 5.0 12/31/26
Herb and spice, group 19 35 12/31/26
Hibiscus, seed 150 12/31/26
Ivy gourd 5.0 12/31/26
Kaffir lime, leaves 0.50 12/31/26
Kenaf, seed 150 12/31/26
Oilseed group 20 150 12/31/26
Peppermint, tops 35 12/31/26
Pointed gourd 5.0 12/31/26
Spearmint, tops 35 12/31/26
Vegetable, bulb, group 3-07 2.0 12/31/26
Vegetable, cucurbit, group 9 5.0 12/31/26
Vegetable, foliage of legume, group 7 0.50 12/31/26
Vegetable, fruiting, group 8-10 7.0 12/31/26
Vegetable, head and stem Brassica, group 5-16 1.0 12/31/26
Vegetable, leafy, group 4-16 0.50 12/31/26
Vegetable, leaves of root and tuber, group 2 0.50 12/31/26
Vegetable, legume, group 6 3.0 12/31/26
Vegetable, root and tuber, group 1 3.0 12/31/26
Vegetable, stalk, stem and leaf petiole, group 22 0.50 12/31/26

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 35298, June 13, 2012, as amended at 83 FR 8763, Mar. 1, 2018; 85 FR 65734, Oct. 16, 2020; 86 FR 8703, Feb. 9, 2021; 88 FR 75505, Nov. 3, 2023]

§ 180.127 Piperonyl butoxide; tolerances for residues.

(a) General.

(1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl piperonyl)ether] are established in or on the following food commodities:

Commodity Parts per million
Almond, postharvest 8
Apple, postharvest 8
Barley, postharvest 20
Bean, postharvest 8
Birdseed, mixtures, postharvest 20
Blackberry, postharvest 8
Blueberry, postharvest 8
Boysenberry, postharvest 8
Buckwheat, grain, postharvest 20
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Cherry, sweet, postharvest 8
Cherry, tart, postharvest 8
Cacoa bean, roasted bean, postharvest 8
Coconut, copra, postharvest 8
Corn, field, grain, postharvest 20
Corn, pop, postharvest 20
Cotton, undelinted seed, postharvest 8
Crabapple, postharvest 8
Currant, postharvest 8
Dewberry, postharvest 8
Egg 1
Fig, postharvest 8
Flax, seed, postharvest 8
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Gooseberry, postharvest 8
Grape, postharvest 8
Guava, postharvest 8
Hog, fat 0.1
Hog, meat 0.1
Hog, meat byproducts 0.1
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Loganberry, postharvest 8
Mango, postharvest 8
Milk, fat 0.25
Muskmelon, postharvest 8
Oat, postharvest 8
Orange, postharvest 8
Peach, postharvest 8
Peanut, postharvest 8
Pea, postharvest 8
Pear, postharvest 8
Pineapple, postharvest 8
Plum, prune, fresh, postharvest 8
Potato, postharvest 0.25
Poultry, fat 3
Poultry, meat 3
Poultry, meat byproducts 3
Raspberry, postharvest 8
Rice, postharvest 20
Rye, postharvest 20
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Sorghum, grain, postharvest 8
Sweet potato, postharvest 0.25
Tomato, postharvest 8
Walnut, postharvest 8
Wheat, postharvest 20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of piperonyl butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the formulation.

(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for food, dried.

(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are constructed with waxed paper liners and are to be used only for food, dried that contain 4 percent fat or less.

(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it is incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl butoxide per square foot (538 milligrams per square meter). Such treated bags are to be used only for packaging plum, prune, dried; grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12 milligrams of piperonyl butoxide per ounce of fruit (0.10 milligram of piperonyl butoxide per gram of product).

(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to such use.

(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide for insect control in accordance with 21 CFR 178.3730.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:

(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(C) Food treated in accordance with 21 CFR 178.3730.

(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the cloth of cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(v) Where tolerances are established on both raw agricultural commodities and processed food made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot.

(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth. Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried that contain 4 percent fat or less.

(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as the result of migration:

(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency.

(v) Where tolerances are established on both the raw agricultural commodities and food, processed made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74813, Dec. 13, 2006]

§ 180.128 Pyrethrins; tolerances for residues.

(a) General.

(1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (pyrethrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl-2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (jasmolin 1), and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles of Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1, and jasmolin 1 are not to exceed the following:

Commodity Parts per million
Almond, postharvest 1.0
Apple, postharvest 1.0
Barley, grain, postharvest 3.0
Bean, succulent, postharvest 1.0
Birdseed, mixtures, postharvest 3.0
Blackberry, postharvest 1.0
Blueberry, postharvest 1.0
Boysenberry, postharvest 1.0
Buckwheat, grain, postharvest 3.0
Cacao bean, roasted bean, postharvest 1.0
Cattle, fat 1.0
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Cherry, sweet, postharvest 1.0
Cherry, tart, postharvest 1.0
Coconut, copra, postharvest 1.0
Corn, field, grain, postharvest 3.0
Corn, pop, grain, postharvest 3.0
Cotton, undelinted seed, postharvest 1.0
Crabapple, postharvest 1.0
Currant, postharvest 1.0
Dewberry, postharvest 1.0
Fig, postharvest 1.0
Flax, seed, postharvest 1.0
Goat, fat 1.0
Goat, meat 0.05
Goat, meat byproducts 0.05
Gooseberry, postharvest 1.0
Grape, postharvest 1.0
Guava, postharvest 1.0
Hog, fat 1.0
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 1.0
Horse, meat 0.05
Horse, meat byproducts 0.05
Loganberry, postharvest 1.0
Mango, postharvest 1.0
Milk, fat (reflecting negligible residues in milk) 0.05
Muskmelon, postharvest 1.0
Oat, grain, postharvest 1.0
Orange, postharvest 1.0
Pea, dry, seed, postharvest 1.0
Peach, postharvest 1.0
Peanut, postharvest 1.0
Pear, postharvest 1.0
Pineapple, postharvest 1.0
Plum, prune, fresh, postharvest 1.0
Potato, postharvest 0.05
Raspberry, postharvest 1.0
Rice, grain, postharvest 3.0
Rye, grain, postharvest 3.0
Sheep, fat 1.0
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Sorghum, grain, grain, postharvest 1.0
Sweet potato, postharvest 0.05
Tomato, postharvest 1.0
Walnut, postharvest 1.0
Wheat, grain, postharvest 3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions derived from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served. Food must be removed or covered prior to use.

(4) Where tolerances are established on both the raw agricultural commodities and processed foods made there-from, the total residues of pyrethrins in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

§ 180.129 o-Phenylphenol and its sodium salt; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide o-phenylphenol and sodium o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or on the following food commodities:

Commodity Parts per million
Apple 25
Cantaloupe (NMT 10 ppm in edible portion) 125
Carrot, roots 20
Cherry 5
Citrus fruits 10
Cucumber 10
Lemon 10
Nectarine 5
Orange 10
Pepper, bell 10
Peach 20
Pear 25.0
Pineapple 10
Plum, prune, fresh 20
Sweet potato, roots 15
Tomato 10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54960, Sept. 24, 2008]

§ 180.130 Hydrogen Cyanide; tolerances for residues.

(a) General. Tolerances are established for residues of sodium cyanide, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance level specified in table 1 to this paragraph (a) is to be determined by measuring only hydrogen cyanide in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Fruit, citrus, group 10-10 50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999, as amended at 91 FR 21388, Apr. 22, 2026]

§ 180.132 Thiram; tolerances for residues.

(a) General.

(1) A tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only thiram.

Commodity Parts
per million
Avocado 1 15
1 No U.S. registrations as of September 23, 2009.

(2) Tolerances are established for residues of the fungicide thiram, tetramethyl thiuram disulfide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those thiram residues convertible to and expressed in terms of the degradate carbon disulfide, in or on the commodity.

Commodity Parts
per million
Apple 5
Banana 1 2.0
Peach 7.0
Strawberry 13
1 There are no U.S. registrations as of September 23, 2009.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 49615, July 31, 2002, as amended at 74 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015; 80 FR 72597, Nov. 20, 2015]

§ 180.142 2,4-D; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Almond hulls 0.1
Asparagus 5.0
Barley, bran 4.0
Barley, grain 2.0
Barley, straw 50
Berry, group 13 0.2
Cattle, fat 0.3
Cattle, kidney 4.0
Cattle, meat 0.3
Cattle, meat byproducts, except kidney 0.3
Corn, field, forage 6.0
Corn, field, grain 0.05
Corn, field, stover 50
Corn, pop, grain 0.05
Corn, pop, stover 50
Corn, sweet, forage 6.0
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 50
Cotton, gin byproducts 1.5
Cotton, undelinted seed 0.08
Cranberry 0.5
Fish 0.1
Fruit, citrus, group 10 3.0
Fruit, pome, group 11 0.05
Fruit, stone, group 12 0.05
Goat, fat 0.3
Goat, kidney 4.0
Goat, meat 0.3
Goat, meat byproducts, except kidney 0.3
Grain, aspirated fractions 40
Grape 0.05
Grass, forage 360
Grass, hay 300
Hop, dried cones 0.2
Horse, fat 0.3
Horse, kidney 4.0
Horse, meat 0.3
Horse, meat byproducts, except kidney 0.3
Milk 0.05
Millet, forage 25
Millet, grain 2.0
Millet, straw 50
Nut, tree, group 14 0.2
Oat, forage 25
Oat, grain 2.0
Oat, straw 50
Pistachio 0.05
Potato 0.4
Rice, grain 0.5
Rice, hulls 2.0
Rye, bran 4.0
Rye, forage 25
Rye, grain 2.0
Rye, straw 50
Sesame, seed 0.05
Sheep, fat 0.3
Sheep, kidney 4.0
Sheep, meat 0.3
Sheep, meat byproducts, except kidney 0.3
Shellfish 1.0
Sorghum, grain, forage 0.2
Sorghum, grain, grain 0.2
Sorghum, grain, stover 0.2
Soybean, forage 0.02
Soybean, hay 2.0
Soybean, seed 0.02
Strawberry 0.05
Sugarcane, cane 0.05
Sugarcane, molasses 0.2
Teff, bran 4.0
Teff, forage 25.0
Teff, grain 2.0
Teff, straw 50.0
Vegetable, leaves of root and tuber, group 2 0.1
Vegetable, root and tuber, except potato, group 1 0.1
Wheat, bran 4.0
Wheat, forage 25
Wheat, grain 2.0
Wheat, straw 50
Wheatgrass, intermediate, bran 4
Wheatgrass, intermediate, forage 30
Wheatgrass, intermediate, grain 2
Wheatgrass, intermediate, straw 50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the follow commodities:

Commodity Parts per million
Rice, wild, grain 0.05

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerances levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

Commodity Parts per million
Animal feed, nongrass, group 18 0.2
Avocado 0.05
Dill, seed 0.05
Okra 0.05
Vegetable, brassica leafy, group 5 0.4
Vegetable, bulb, group 3 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, foliage of legume, group 7 0.2
Vegetable, fruiting, group 8 0.05
Vegetable, leafy, except brassica, group 4 0.4
Vegetable, legume, group 6 0.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, 2009; 76 FR 55817, Sept. 9, 2011; 80 FR 72597, Nov. 20, 2015; 82 FR 9529, Feb. 7, 2017; 85 FR 82943, Dec. 21, 2020]

§ 180.145 Fluorine compounds; tolerances for residues.

(a) General.

(1) Tolerances are established for combined residues of the insecticidal fluorine compounds cryolite and synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:

Commodity Parts per million
Apricot 7
Blackberry 7
Blueberry 7
Boysenberry 7
Broccoli 7
Brussels sprouts 7
Cabbage 7
Cauliflower 7
Collards 7
Cranberry 7
Cucumber 7
Dewberry 7
Eggplant 7
Fruit, citrus 7
Grape 7
Kale 7
Kohlrabi 7
Lettuce, head 7
Lettuce, leaf 7
Loganberry 7
Melon 7
Nectarine 7
Peach 7
Pepper 7
Plum, prune, fresh 7
Pumpkin 7
Raspberry 7
Squash, summer 7
Squash, winter 7
Strawberry 7
Tomato 7
Youngberry 7

(2) Tolerances are established for residues of fluoride in or on the following commodities from the postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity Parts per million
All processed food commodities not otherwise listed 70
Barley, bran, postharvest 45.0
Barley, flour, postharvest 45.0
Barley, grain, postharvest 15.0
Barley, pearled barley, postharvest 45.0
Cattle, meat, dried 40
Cheese 5.0
Cacao bean, roasted bean, postharvest 20
Coconut, postharvest 40
Coffee, bean, green, postharvest 15
Corn, field, flour, postharvest 35.0
Corn, field, grain, postharvest 10.0
Corn, field, grits, postharvest 10.0
Corn, field, meal, postharvest 30.0
Corn, pop, grain, postharvest 10.0
Cotton, undelinted seed, postharvest 70
Egg, dried 900
Fruit, dried, except grape, raisin, postharvest 3.0
Ginger, postharvest 70
Grain, aspirated fractions, postharvest 55.0
Grape, raisin, postharvest 7.0
Hog, meat 20
Herbs and spices group 19, postharvest 70
Milk, powdered 5.0
Millet, grain, postharvest 40.0
Nut, pine, postharvest 20
Nut, tree, Group 14, postharvest 10.0
Oat, flour, postharvest 75.0
Oat, grain, postharvest 25.0
Oat, groats/rolled oats 75.0
Peanut, postharvest 15
Pistachio, postharvest 10.0
Rice, bran, postharvest 31.0
Rice, flour, postharvest 45
Rice, grain, postharvest 12.0
Rice, hulls, postharvest 35.0
Rice, polished rice, postharvest 25.0
Rice, wild, grain, postharvest 25.0
Sorghum, grain, postharvest 40.0
Triticale, grain, postharvest 40.0
Vegetable, legume, group 6, postharvest 70
Wheat, bran, postharvest 40.0
Wheat, flour, postharvest 125.0
Wheat, germ, postharvest 130.0
Wheat, grain, postharvest 40.0
Wheat, milled byproducts, postharvest 130.0
Wheat, shorts, postharvest 40.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by § 180.1(l), are established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic cryolite (sodium aluminum fluoride), in or on the following raw agricultural commodities:

Commodity Parts per million
Kiwifruit 15

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011]

§ 180.151 Ethylene oxide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene oxide, when used as a postharvest fumigant in or on the following food commodities:

Commodity Parts per million
Herb and spice, group 19, dried, except basil 7
Licorice, roots 7
Peppermint, tops, dried 7
Sesame, seed 7
Spearmint, tops, dried 7
Vegetable, dried 7
Walnut 50

(2) Tolerances are established for residues of the ethylene oxide reaction product, 2-chloroethanol, commonly referred to as ethylene chlorohydrin, when ethylene oxide is used as a postharvest fumigant in or on food commodities as follows:

Commodity Parts per million
Herb and spice, group 19, dried, except basil 940
Licorice, roots 940
Peppermint, tops, dried 940
Sesame, seed 940
Spearmint, tops, dried 940
Vegetable, dried 940

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009]

§ 180.153 Diazinon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide diazinon, O,O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity Parts per million
Almond, hulls 3.0
Apple 0.50
Apricot 0.20
Bean, lima 0.50
Bean, snap, succulent 0.50
Beet, garden, roots 0.75
Beet, garden, tops 0.70
Blueberry 0.50
Caneberry subgroup 13-07A 0.75
Carrot, roots 0.75
Cattle, fat 0.50
Cherry, sweet 0.20
Cherry, tart 0.20
Cranberry 0.50
Endive 0.70
Fig 0.50
Ginseng 0.75
Grape 0.75 2
Hazelnut 0.50
Kiwifruit 1 0.75
Lettuce 0.70
Melon 0.75
Mushroom 0.75 2
Nectarine 0.20
Onion, bulb 0.75
Onion, green 0.75
Pea, succulent 0.50
Peach 0.20
Pear 0.50
Pineapple 0.50
Plum, prune, fresh 0.20
Radish 0.50
Rutabaga 0.75
Spinach 0.70
Strawberry 0.50
Tomato 0.75
Vegetable, brassica, leafy, group 5 0.70
Watercress 0.05
1 There are no domestic registrations for kiwifruit as of March 6, 2002.
2 The expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the insecticide diazinon, O, O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]-phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity Parts per million
Almond 0.50
Banana 0.20
Celery 0.70
Cucumber 0.75
Parsley, leaves 0.75
Parsnip 0.50
Pepper 0.5
Potato 0.10
Squash, summer 0.50
Squash, winter 0.75
Sweet potato, roots 0.10
Swiss chard 0.70
Turnip, roots 0.50
Turnip, tops 0.75

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 42738, Sept. 29, 1982]

§ 180.155 1-Naphthaleneacetic acid; tolerances for residues.

(a) General. Tolerances are established for the residues of 1-naphthaleneacetic acid, including its metabolites and degradates in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring only 1-naphthaleneacetic acid and its conjugates, calculated as the Stoichiometric equivalent of 1-naphthaleneacetic acid, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Avocado 0.05
Cherry, sweet 0.1
Fruit, pome, group 11-10 0.15
Mango 0.05
Olive 0.7
Orange 0.1
Pineapple1 0.05
Pomegranate 0.05
Potato 0.01
Rambutan 2
Sapote, mamey 0.05
Tangerine 0.1
1 There are no U.S. registrations for this commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 30218, May 22, 2013, as amended at 80 FR 77260, Dec. 14, 2015; 91 FR 21388, Apr. 22, 2026]

§ 180.163 Dicofol; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicofol as the sum of its p,p-dicofol and o,p-dicofol isomers: 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

Commodity Parts per million Expiration/revocation date
Apple, wet pomace 38.0 10/31/16
Bean, dry, seed 0.5 10/31/16
Bean, succulent 3.0 10/31/16
Butternut 0.1 10/31/16
Caneberry subgroup 13A 5.0 10/31/16
Chestnut 0.1 10/31/16
Citrus, dried pulp 12.0 10/31/16
Citrus oil 200.0 10/31/16
Cotton, refined oil 0.5 10/31/16
Cotton, undelinted seed 0.1 10/31/16
Fruit, citrus, group 10 6.0 10/31/16
Fruit, pome, group 11 10.0 10/31/16
Fruit, stone, group 12 5.0 10/31/16
Grape 5.0 10/31/16
Grape, raisin 20.0 10/31/16
Hazelnut 0.1 10/31/16
Hop, dried cones 65.0 10/31/16
Nut, hickory 0.1 10/31/16
Nut, macadamia 0.1 10/31/16
Pecan 0.1 10/31/16
Peppermint, oil 30.0 10/31/16
Peppermint, tops 25.0 10/31/16
Spearmint, oil 30.0 10/31/16
Spearmint, tops 25.0 10/31/16
Strawberry 10.0 10/31/16
Tea, dried 50.0 None
Tea, plucked leaves 30.0 None
Vegetable, cucurbit, group 9 2.0 10/31/16
Vegetable, fruiting, group 8 2.0 10/31/16
Walnut 0.1 10/31/16

(2) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, its isomer o,p-dicofol, 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, and its metabolites 4-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol, calculated as the stoichiometric equivalent of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date
Cattle, fat 50.0 10/31/16
Cattle, liver 5.0 10/31/16
Cattle, meat 3.0 10/31/16
Cattle, meat byproducts, except liver 3.0 10/31/16
Egg 0.05 10/31/16
Goat, fat 50.0 10/31/16
Goat, liver 5.0 10/31/16
Goat, meat 3.0 10/31/16
Goat, meat byproducts, except liver 3.0 10/31/16
Hog, fat 50.0 10/31/16
Hog, liver 5.0 10/31/16
Hog, meat 3.0 10/31/16
Hog, meat byproducts, except liver 3.0 10/31/16
Horse, fat 50.0 10/31/16
Horse, liver 5.0 10/31/16
Horse, meat 3.0 10/31/16
Horse, meat byproducts, except liver 3.0 10/31/16
Milk, fat (reflecting 0.75 ppm in whole milk) 22.0 10/31/16
Poultry, fat 0.1 10/31/16
Poultry, meat 0.1 10/31/16
Poultry, meat byproducts 0.1 10/31/16
Sheep, fat 50.0 10/31/16
Sheep, liver 5.0 10/31/16
Sheep, meat 3.0 10/31/16
Sheep, meat byproducts, except liver 3.0 10/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007; 77 FR 59124, Sept. 26, 2012]

§ 180.169 Carbaryl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date
Alfalfa, forage 50 None
Alfalfa, hay 75 None
Almond, hulls 50 None
Apple, wet pomace 15 None
Asparagus 15 None
Banana 5.0 None
Beet, sugar, roots 0.5 None
Beet, sugar, tops 25 None
Bushberry subgroup 13-07B 3.0 None
Cabbage 21 None
Cactus, fruit 5.0 None
Cactus, pads 12 None
Caneberry subgroup 13-07A 12.0 None
Citrus, oil 20 None
Clover, forage 50 None
Clover, hay 70 None
Corn, field, forage 30 None
Corn, field, grain 0.02 None
Corn, field, stover 20 None
Corn, pop, grain 0.02 None
Corn, pop, stover 20 None
Corn, sweet, forage 185 None
Corn, sweet, kernel plus cob with husks removed 0.1 None
Corn, sweet, stover 215 None
Cotton, undelinted seed 5.0 10/31/09
Cranberry 3.0 None
Dandelion, leaves 22 None
Endive 10 None
Flax, seed 0.5 None
Fruit, citrus, group 10 10 None
Fruit, pome, group 11 12 None
Fruit, stone, group 12 10 None
Grain, aspirated fractions 70 None
Grape 10 None
Grape, raisin 12 None
Grass, forage 100 None
Grass, hay 15 None
Leaf petiole subgroup 4B 3.0 None
Lettuce 10 None
Millet, proso, grain 1.0 None
Millet, proso, straw 20 None
Nut, tree group 14, except walnut 0.1 None
Okra 4.0 None
Olive 10 None
Oyster 0.25 None
Parsley, leaves 22 None
Pea and bean, dried shelled, except soybean, subgroup 6C 1.0 None
Peanut 0.05 None
Peanut, hay 20 None
Pineapple 2.0 None
Pistachio 0.1 None
Rice, grain 15 None
Rice, hulls 30 None
Sorghum grain, forage 30 None
Sorghum grain, grain 10 None
Sorghum grain, stover 30 None
Soybean, forage 15 None
Soybean, hay 15 None
Soybean, seed 0.5 None
Spinach 22 None
Strawberry 4.0 None
Sunflower, seed 0.5 None
Sweet potato, roots 0.2 None
Trefoil, forage 15 None
Trefoil, hay 25 None
Vegetable, brassica, leafy, group 5, except cabbage 10 None
Vegetable, cucurbit, group 9 3.0 None
Vegetable, foliage of legume, subgroup 7A, except soybean 60 None
Vegetable, fruiting, group 8 5.0 None
Vegetable, leaves of root and tuber, group 2, except sugar beet tops 75 None
Vegetable, legume, edible podded, subgroup 6A 10 None
Vegetable, root and tuber, group 1, except sugar beet and sweet potato 2.0 None
Walnut 1.0 None
Wheat, forage 30 None
Wheat, grain 1.0 None
Wheat, hay 30 None
Wheat, straw 20 None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate, including its metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6-dihydrodihydroxy naphthol, calculated as 1-naphthyl N-methylcarbamate and the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 5-methoxy-6-hydroxy carbaryl, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date
Cattle, fat 0.5 None
Cattle, meat 1.0 None
Cattle, meat byproducts 3.0 None
Egg 0.5 10/31/09
Goat, fat 0.5 None
Goat, meat 1.0 None
Goat, meat byproducts 3.0 None
Hog, fat 0.5 None
Hog, meat 1.0 None
Hog, meat byproducts 3.0 None
Horse, fat 0.5 None
Horse, meat 1.0 None
Horse, meat byproducts 3.0 None
Milk 1.0 None
Poultry, fat 5.0 10/31/09
Poultry, meat 5.0 10/31/09
Sheep, fat 0.5 None
Sheep, meat 1.0 None
Sheep, meat byproducts 3.0 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(l), are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

Commodity Parts per million
Dillweed, fresh leaves 0.2

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009; 80 FR 72597, Nov. 20, 2015]

§ 180.172 Dodine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dodine, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 is to be determined by measuring only dodine, N-dodecylguanidine acetate; in or on the following commodities.

Table 1 to Paragraph (a)

Commodity Parts
per million
Almond, hull 30.0
Apple, wet pomace 15.0
Banana 0.50
Fruit, pome, group 11-10 5
Fruit, stone, group 12-12 5
Nut, tree, group 14-12 0.3
Olive, with pit 0.4
Peanut 0.013
Strawberry 5.0

(b)-(d) [Reserved]

[88 FR 86273, Dec. 13, 2023]

§ 180.176 Mancozeb; tolerances for residues.

(a) General. Tolerances are established for residues of mancozeb (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts
per million
Almond 0.1
Almond, hulls 4
Apple 0.6
Asparagus 0.1
Atemoya 3.0
Banana 2
Barley, bran 2
Barley, flour 1.2
Barley, grain 1
Barley, hay 30
Barley, pearled barley 20
Barley, straw 25
Beet, sugar, dried pulp 3.0
Beet, sugar, roots 1.2
Beet, sugar, tops 60
Broccoli 7
Cabbage 9
Canistel 15.0
Cattle, kidney 0.5
Cattle, liver 0.5
Cherimoya 3.0
Corn, field, forage 40
Corn, field, grain 0.06
Corn, field, stover 15
Corn, pop, grain 0.1
Corn, pop, stover 40
Corn, sweet, forage 70
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 40
Cotton, undelinted seed 0.5
Crabapple 0.6
Cranberry 5
Custard apple 3.0
Fennel 2.5
Flax, seed 0.15
Ginseng 1.2
Goat, kidney 0.5
Goat, liver 0.5
Grape 1.5
Hog, kidney 0.5
Hog, liver 0.5
Horse, kidney 0.5
Horse, liver 0.5
Lettuce, head 3.5
Lettuce, leaf 18
Mango 15.0
Oat, flour 1.2
Oat, grain 1
Oat, groats/rolled oats 20
Oat, hay 30
Oat, straw 25
Onion, bulb 1.5
Papaya 9
Peanut 0.1
Peanut, hay 65
Pear 0.6
Pepper 12
Potato 0.2
Poultry, kidney 0.5
Poultry, liver 0.5
Quince 0.6
Rice, grain 0.06
Rye, bran 2
Rye, flour 1.2
Rye, grain 1
Rye, straw 25
Sapodilla 15.0
Sapote, mamey 15.0
Sapote, white 15.0
Sheep, kidney 0.5
Sheep, liver 0.5
Sorghum, grain, forage 0.15
Sorghum, grain, grain 0.25
Sorghum, grain, stover 0.15
Star apple 15.0
Sugar apple 3.0
Tangerine 1 10
Tomato 2.5
Vegetable, cucurbit, group 9 2.0
Walnut 0.70
Wheat, bran 2
Wheat, flour 1.2
Wheat, germ 20
Wheat, grain 1
Wheat, hay 30
Wheat, middlings 20
Wheat, shorts 2
Wheat, straw 25
1 There are no U.S. registrations for use of mancozeb on tangerine.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registrations, as defined in § 180.1(l), is established for residues of the fungicide mancozeb, (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodity in the following table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts per million
Carrot, roots 1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, May 14, 2014; 80 FR 72597, Nov. 20, 2015]

§ 180.178 Ethoxyquin; tolerances for residues.

(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:

Commodity Parts per million
Pear 3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57073, Oct. 26, 1998]

§ 180.181 Chlorpropham; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) in or on the following food commodities:

Commodity Parts per million
Potato 30
Potato, wet peel 40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic acid (4-HSA) in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.20
Cattle, kidney 0.30
Cattle, meat 0.06
Cattle, meat byproducts except kidney 0.06
Goat, fat 0.20
Goat, kidney 0.30
Goat, meat 0.06
Goat, meat byproducts except kidney 0.06
Hog, fat 0.20
Hog, kidney 0.30
Hog, meat 0.06
Hog, meat byproducts except kidney 0.06
Horse, fat 0.20
Horse, kidney 0.30
Horse, meat 0.06
Horse, meat byproducts except kidney 0.06
Milk 0.30
Sheep, fat 0.20
Sheep, kidney 0.30
Sheep, meat 0.06
Sheep, meat byproducts except kidney 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

§ 180.184 Linuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity:

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 1
Alfalfa, hay 3
Asparagus 7.0
Carrot, roots 1.0
Cattle, fat 0.2
Cattle, kidney 2.0
Cattle, liver 2.0
Cattle, meat 0.1
Cattle, meat byproducts except kidney and liver 0.1
Celeriac 1.0
Cilantro, dried leaves 10
Cilantro, fresh leaves 3.0
Coriander, seed 0.01
Corn, field, forage 1.0
Corn, field, grain 0.1
Corn, field, stover 6.0
Corn, sweet, forage 1.0
Corn, sweet, kernel plus cob with husks removed 0.25
Corn, sweet, stover 6.0
Cotton, gin byproducts 5.0
Cotton, undelinted seed 0.25
Dill, oil 2.0
Dill, seed 0.5
Dillweed, dried leaves 5.0
Dillweed, fresh leaves 1.5
Goat, fat 0.2
Goat, kidney 2.0
Goat, liver 2.0
Goat, meat 0.1
Goat, meat byproducts except kidney and liver 0.1
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.1
Horse, fat 0.2
Horse, kidney 2.0
Horse, liver 2.0
Horse, meat 0.1
Horse, meat byproducts except kidney and liver 0.1
Horseradish 0.05
Milk 0.05
Parsley, dried leaves 9.0
Parsley, leaves 4.0
Parsnip, roots 0.05
Parsnip, tops 0.05
Pea, dry, seed 0.09
Rhubarb 0.5
Sheep, fat 0.2
Sheep, kidney 2.0
Sheep, liver 2.0
Sheep, meat 0.1
Sheep, meat byproducts except kidney and liver 0.1
Sorghum, grain, forage 1.0
Sorghum, grain, grain 0.25
Sorghum, grain, stover 1.0
Soybean, seed 1.0
Soybean, vegetable 1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide linuron [3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea], including its metabolites and degradates, in or on the commodities in the table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3.4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity. The tolerance expires and is revoked on the date specified in the table.

Commodity Parts per
million
Expiration/revocation date
Lentil 0.1 12/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(l), are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity.

Commodity Parts per million
Celery 0.5
Potato 0.2
Wheat, forage 0.5
Wheat, grain 0.05
Wheat, hay 0.5
Wheat, straw 2.0

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Feb. 12, 2014; 89 FR 4200, Jan. 23, 2024]

§ 180.185 DCPA; tolerances for residues.

(a) General. Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid (TCP) (calculated as dimethyl tetrachloroterephthalate) are established in or on the following food commodities:

Commodity Parts per million
Cantaloupe 1.0
Garlic 1.0
Ginseng 2.0
Horseradish 2.0
Muskmelon 1.0
Onion, bulb 1.0
Onion, green 1.0
Strawberry 2.0
Tomato 1.0
Vegetable, brassica, leafy, group 5 5.0
Watermelon 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

Commodity Parts per million
Radish, roots 2.0
Radish, tops 15.0

(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

Commodity Parts per million
Basil, dried leaves 20.0
Basil, fresh leaves 5.0
Bean, dry 2.0
Bean, mung, seed 2.0
Bean, snap, succulent 2.0
Celeriac 2.0
Chicory, roots 2.0
Chicory, tops 5.0
Chive 5.0
Coriander, leaves 5.0
Corn, field, forage 0.4
Corn, field, grain 0.05
Corn, field, stover 0.4
Corn, pop, forage 0.4
Corn, pop, grain 0.05
Corn, pop, stover 0.4
Corn, sweet, forage 0.4
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.4
Cotton, undelinted seed 0.2
Cucumber 1.0
Dill 5.0
Eggplant 1.0
Lettuce 2.0
Marjoram 5.0
Parsley, dried leaves 20.0
Parsley, leaves 5.0
Pea, blackeyed, seed 2.0
Pepper 2.0
Pimento 2.0
Potato 2.0
Radicchio 5.0
Radish, oriental, roots 2.0
Radish, oriental, tops 2.0
Rutabaga 2.0
Soybean 2.0
Squash, summer 1.0
Squash, winter 1.0
Sweet potato 2.0
Turnip, roots 2.0
Turnip, tops 5.0
Yam, true, tuber 2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008; 74 FR 14744, Apr. 1, 2009]

§ 180.189 Coumaphos; tolerances for residues.

(a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphorothioate and its oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphate) in or on food commodities as follows:

Commodity Parts per million
Cattle, fat 1.0
Cattle, meat 1.0
Cattle, meat byproducts 1.0
Goat, fat 1.0
Goat, meat 1.0
Goat, meat byproducts 1.0
Hog, fat 1.0
Hog, meat 1.0
Hog, meat byproducts 1.0
Honey 0.15
Honeycomb 45.0
Horse, fat 1.0
Horse, meat 1.0
Horse, meat byproducts 1.0
Milk, fat ( = n in whole milk) 0.5
Sheep, fat 1.0
Sheep, meat 1.0
Sheep, meat byproducts 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, May 23, 2007]

§ 180.190 Diphenylamine; tolerances for residues.

(a) General. Tolerances are established for residues of diphenylamine, including its metabolites and degradates, in or on the commodities in Table 1 to Paragraph (a). Compliance with the tolerance levels specified in Table 1 to Paragraph (a) is to be determined by measuring only diphenylamine, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Apple 10
Apple, wet pomace 30
Pear 5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007; 76 FR 34885, June 15, 2011; 91 FR 8086, Feb. 20, 2026]

§ 180.191 Folpet; tolerances for residues.

(a) General. Tolerances are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on raw agricultural commodities as follows:

Commodity Parts per million
Apple 1 5.0
Cranberry 1 15.0
Cucumber 1 2.0
Grape 1 50.0
Grape, raisin 1 80.0
Hop, dried cones 120.0
Lettuce 1 50.0
Melon 1 3.0
Onion,bulb 1 2.0
Strawberry 1 5.0
Tomato 1 25.0
1 No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in § 180.1(l) are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on the following raw agricultural commodity:

Commodity Parts per million
Avocado 25.0

(d) Indirect or inadvertent residues. [Reserved]

[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72 FR 41928, Aug. 1, 2007]

§ 180.198 Trichlorfon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1-hydroxyethyl) phosphonate) in or on the following food commodities:

Commodity Parts per million
Cattle, fat 1 0.5
Cattle, meat 1 0.2
Cattle, meat byproducts 1 0.1
1 There are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

§ 180.200 Dicloran; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dicloran, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicloran, 2,6-dichloro-4-nitroaniline, in or on the commodity.

Commodity Parts per
million
Expiration/revocation date
Apricot 20 None
Bean, snap, succulent 20 None
Carrot, roots 10 11/2/11
Celery 15 None
Cherry, sweet 20 None
Cucumber 5 None
Endive 10 None
Garlic 5 None
Grape 10 None
Lettuce 10 None
Nectarine 20 None
Onion 10 None
Peach 20 None
Plum, prune, fresh 15 None
Potato 0.25 12/31/14
Rhubarb 10 None
Sweet potato, roots 10 None
Tomato 5 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

§ 180.202 p-Chlorophenoxyacetic acid; tolerances for residues.

(a) General. A tolerance is established for residues of the plant regulator p-chlorophenoxyacetic acid, including its metabolites and degradates, in or on the commodity in the table in this paragraph (a). Compliance with the tolerance level specified in this paragraph (a) is to be determined by measuring only p-chlorophenoxyacetic acid, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Bean, mung, sprouts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006; 88 FR 46083, July 19, 2023]

§ 180.204 Dimethoate; tolerances for residues.

(a) General. Tolerances are established for total residues of the insecticide dimethoate (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorodithioate) including its oxygen analog (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorothioate) in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage 2.0
Alfalfa, hay 2.0
Bean, dry, seed 2.0
Bean, lima 2.0
Bean, snap, succulent 2.0
Blueberry 1 1.0
Broccoli 2.0
Cattle, meat byproducts 0.02
Cauliflower 2.0
Celery 2.0
Citrus, dried pulp 5.0
Corn, field, forage 1.0
Corn, field, grain 0.1
Corn, field, stover 1.0
Corn, pop, grain 0.1
Corn, pop, stover 1.0
Corn, sweet, forage 1.0
Cotton, undelinted seed 0.1
Egg 0.02
Endive 2.0
Goat, meat byproducts 0.02
Grapefruit 2.0
Hog, meat byproducts 0.02
Horse, meat byproducts 0.02
Kale 2.0
Lemon 2.0
Lettuce, leaf 2.0
Melon 1.0
Milk 0.002
Mustard greens 2.0
Orange 2.0
Pea 2.0
Pear 2.0
Pecan 0.1
Pepper 2.0
Potato 0.2
Poultry, meat byproducts 0.02
Safflower, seed 0.1
Sheep, meat byproducts 0.02
Sorghum, grain, forage 0.1
Sorghum, grain, grain 0.1
Sorghum, grain, stover 0.1
Soybean, forage 2.0
Soybean, hay 2.0
Soybean, seed 0.05
Swiss chard 2.0
Tangerine 2.0
Tomato 2.0
Turnip, roots 0.2
Turnip, tops 2.0
Wheat, forage 2.0
Wheat, grain 0.04
Wheat, hay 2.0
Wheat, straw 2.0
1 There are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for total residues of dimethoate including its oxygen analog in or on the following food commodities:

Commodity Parts per million
Asparagus 0.15
Brussels sprouts 5.0
Cherry, sweet 2.0
Cherry, tart 2.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

§ 180.205 Paraquat; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat (1,1′-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity Parts per million
Acerola 0.05
Almond, hulls 0.5
Animal feed, nongrass, group 18, forage 75.0
Animal feed, nongrass, group 18, hay 210.0
Artichoke, globe 0.05
Asparagus 0.5
Atemoya 0.05
Avocado 0.05
Banana 0.05
Barley, grain 0.05
Barley, hay 3.5
Barley, straw 1.0
Beet, sugar, roots 0.5
Beet, sugar, tops 0.05
Berry group 13 0.05
Biriba 0.05
Cacao bean, bean 0.05
Canistel 0.05
Carrot, roots 0.05
Cattle, fat 0.05
Cattle, kidney 0.5
Cattle, meat 0.05
Cattle, meat byproducts, except kidney 0.05
Cherimoya 0.05
Coffee, bean, green 0.05
Corn, field, forage 3.0
Corn, field, grain 0.1
Corn, field, stover 10.0
Corn, pop, grain 0.1
Corn, pop, stover 10.0
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, gin byproducts 110.0
Cotton, undelinted seed 3.5
Cowpea, forage 0.1
Cowpea, hay 0.4
Cranberry 0.05
Custard apple 0.05
Egg 0.01
Endive 0.05
Feijoa 0.05
Fig 0.05
Fruit, citrus, group 10 0.05
Fruit, pome, group 11 0.05
Fruit, stone, group 12 0.05
Goat, fat 0.05
Goat, kidney 0.5
Goat, meat 0.05
Goat, meat byproducts, except kidney 0.05
Grain, aspirated fractions 65.0
Grape 0.05
Grass, forage 90.0
Grass, hay 40.0
Guar, seed 0.5
Guava 0.05
Hog, fat 0.05
Hog, kidney 0.5
Hog, meat 0.05
Hog, meat byproducts, except kidney 0.05
Hop, dried cones 0.5
Horse, fat 0.05
Horse, kidney 0.5
Horse, meat 0.05
Horse, meat byproducts, except kidney 0.05
Ilama 0.05
Jaboticaba 0.05
Kiwifruit 0.05
Lentil, seed 0.3
Lettuce 0.05
Longan 0.05
Lychee 0.05
Mango 0.05
Milk 0.01
Nut, tree, group 14 0.05
Okra 0.05
Olive 0.05
Onion, bulb 0.1
Onion, green 0.05
Papaya 0.05
Passionfruit 0.2
Pawpaw 0.05
Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean 0.3
Pea and bean, succulent shelled, subgroup 6B 0.05
Pea, field, hay 0.8
Pea, field, vines 0.2
Peanut 0.05
Peanut, hay 0.5
Peppermint, tops 0.5
Persimmon 0.05
Pineapple 0.05
Pineapple, process residue 0.25
Pistachio 0.05
Pomegranate 0.05
Pulasan 0.05
Rambutan 0.05
Rhubarb 0.05
Rice, grain 0.05
Safflower, seed 0.05
Sapodilla 0.05
Sapote, black 0.05
Sapote, mamey 0.05
Sapote, white 0.05
Sheep, fat 0.05
Sheep, kidney 0.5
Sheep, meat 0.05
Sheep, meat byproducts, except kidney 0.05
Sorghum, forage, forage 0.1
Sorghum, grain, forage 0.1
Sorghum, grain, grain 0.05
Soursop 0.05
Soybean, forage 0.4
Soybean, hay 10.0
Soybean, hulls 4.5
Soybean, seed 0.7
Spanish lime 0.05
Spearmint, tops 0.5
Star apple 0.05
Starfruit 0.05
Strawberry 0.25
Sugar apple 0.05
Sugarcane, cane 0.5
Sugarcane, molasses 3.0
Sunflower, seed 2.0
Turnip, greens 0.05
Turnip, roots 0.05
Vegetable, brassica, leafy, group 5 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, fruiting, group 8 0.05
Vegetable, legume, edible podded, subgroup 6A 0.05
Vegetable, tuberous and corm, subgroup 1C 0.50
Wax jambu 0.05
Wheat, forage 0.5
Wheat, grain 1.1
Wheat, hay 3.5
Wheat, straw 50.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in § 180.1(l), are established for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity Parts per million
Pea, pigeon, seed 0.05
Taro, corm 0.1
Tyfon 0.05

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 51614, Oct. 21, 1981]

§ 180.206 Phorate; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide phorate (O,O-diethyl S (ethylthio) methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen analog, phorate oxygen analog sulfoxide, and phorate oxygen analog sulfone in or on the following food commodities:

Commodity Parts per million
Bean, dry, seed 0.05
Bean, succulent 0.05
Beet, sugar, roots 0.3
Beet, sugar, tops 3.0
Coffee, green bean 1 0.02
Corn, field, forage 0.5
Corn, field, grain 0.05
Corn, sweet, forage 0.5
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, undelinted seed 0.05
Hop, dried cones 2.0
Peanut 0.1
Potato 0.2
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.1
Soybean, seed 0.05
Sugarcane, cane 0.05
Wheat, forage 1.5
Wheat, grain 0.05
Wheat, hay 1.5
Wheat, straw 0.05
1 There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008]

§ 180.207 Trifluralin; tolerances for residues.

(a) General. Tolerances are established for residues of trifluralin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only trifluralin (2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)benzenamine).

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 3.0
Alfalfa, hay 2.0
Almond, hulls 0.05
Asparagus 0.05
Barley, grain 0.05
Barley, hay 0.05
Barley, straw 0.05
Bean, mung, sprouts 2.0
Carrot, roots 1.0
Celery 0.05
Corn, field, forage 0.05
Corn, field, grain 0.05
Corn, field, stover 0.05
Cotton, gin byproducts 0.05
Endive 0.05
Fruit, citrus, group 10 0.05
Fruit, stone, group 12 0.05
Grape 0.05
Hop, dried cones 0.05
Nut, tree, group 14 0.05
Oilseed, crop group 20 0.05
Okra 0.05
Peanut 0.05
Peanut, hay 0.05
Peppermint, oil 2.0
Peppermint, tops 0.05
Rosemary, dried leaves 0.10
Rosemary, fresh leaves 0.10
Rosemary, oil 3.0
Sorghum, grain, forage 0.05
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.05
Spearmint, oil 2.0
Spearmint, tops 0.05
Sugarcane, cane 0.05
Tea, dried 1 0.05
Tea, instant 1 0.05
Vegetable, brassica, leafy group 5 0.05
Vegetable, bulb, group 3 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, foliage of legume, group 7 0.05
Vegetable, fruiting, group 8 0.05
Vegetable, leaves of root and tuber, group 2 0.05
Vegetable, legume, group 6 0.05
Vegetable, root and tuber, group 1, except carrot 0.05
Wheat, grain 0.05
Wheat, straw 0.05
1 There are no U.S. registrations as of August 24, 2023.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006; 78 FR 46274, July 31, 2013; 84 FR 4351, Feb. 15, 2019; 88 FR 57898, Aug. 24, 2023]

§ 180.208 Benfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide benfluralin, N-butyl-N-ethyl-ααα-trifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage 0.05
Alfalfa, hay 0.05
Clover, forage 0.05
Clover, hay 0.05
Lettuce 0.05
Trefoil, forage 0.05
Trefoil, hay 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

§ 180.209 Terbacil; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide terbacil, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only the sum of terbacil (5-chloro-3-(1,1-dimethylethyl)-6-methyl-2,4(1H,3H)-pyrimidinedione) and its metabolites 3-tert-butyl-5-chloro-6-hydroxymethyluracil, 6-chloro-2,3-dihydro-7-hydroxymethyl 3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one, and 6-chloro-2,3-dihydro-3,3,7-trimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one, calculated as the stoichiometric equivalent of terbacil, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 1
Alfalfa, hay 2
Apple 0.3
Asparagus 0.4
Blueberry 0.2
Caneberry subgroup 13A 0.2
Peach 0.2
Peppermint, fresh leaves 2
Spearmint, fresh leaves 2
Strawberry 0.1
Sugarcane, cane 0.4
Watermelon 1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 30818, May 31, 2006, as amended at 91 FR 8104, Feb. 20, 2026]

§ 180.210 Bromacil; tolerances for residues.

(a) General. Tolerances are established for residues of bromacil, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only bromacil, 5-bromo-6-methyl-3-(1-methylpropyl)-2,4(1H,3H)-pyrimidinedione, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Fruit, citrus, group 10-10 0.1
Pineapple 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 91 FR 8104, Feb. 20, 2026]

§ 180.211 Propachlor; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propachlor (2-chloro-N-isopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloro-N-isopropylacetanilide, in or on the raw agricultural commodities found in the table in this paragraph. The tolerances listed in the table will expire on January 19, 2024.

Table 1 to Paragraph (a)

Commodity Parts per million
Cattle, fat 0.05
Cattle, kidney 0.2
Cattle, meat 0.02
Cattle, meat byproducts, except kidney 0.05
Corn, field, forage 3.0
Corn, field, grain 0.2
Corn, field, stover 1.0
Corn, sweet, forage 3.0
Goat, fat 0.05
Goat, kidney 0.2
Goat, meat 0.02
Goat, meat byproducts, except kidney 0.05
Hog, fat 0.02
Hog, meat 0.02
Hog, meat byproducts 0.02
Horse, fat 0.05
Horse, kidney 0.2
Horse, meat 0.02
Horse, meat byproducts, except kidney 0.05
Milk 0.02
Sheep, fat 0.05
Sheep, kidney 0.2
Sheep, meat 0.02
Sheep, meat byproducts, except kidney 0.05
Sorghum, forage, forage 8.0
Sorghum, grain, forage 8.0
Sorghum, grain, grain 0.25
Sorghum, grain, stover 12.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007; 88 FR 46083, July 19, 2023]

§ 180.212 S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl cyclohexylethylthiocarbamate in or on the following food commodities:

Commodity Parts per million
Beet, garden, roots 0.05(N)
Beet, garden, tops 0.05(N)
Beet, sugar, roots 0.05(N)
Beet, sugar, tops 0.05(N)
Spinach 0.05(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

§ 180.213 Simazine; tolerances for residues.

(a) General. Tolerances are established residues of the herbicide simazine, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only the sum of simazine, 6-chloro-N,N′-diethyl-1,3,5-triazine-2,4-diamine, and its metabolites 6-chloro-N-ethyl-1,3,5-triazine-2,4-diamine, and 6-chloro-1,3,5-triazine-2,4-diamine, calculated as the stoichiometric equivalent of simazine, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond 1 0.25
Almond, hulls 3
Apple 1 0.20
Avocado 0.20
Blackberry 0.20
Blueberry 0.20
Cattle, meat 0.03
Cattle, meat byproducts 0.03
Cherry 1 0.25
Corn, field, forage 0.20
Corn, field, grain 0.20
Corn, field, stover 0.25
Corn, pop, grain 0.20
Corn, pop, stover 0.25
Corn, sweet, forage 0.20
Corn, sweet, kernel plus cob with husks removed 0.25
Corn, sweet, stover 0.25
Cranberry 0.25
Currant 0.25
Egg 0.03
Fruit, citrus, group 10-10 0.04
Fruit, pome, group 11-10 0.03
Fruit, stone, group 12-12 0.1
Goat, meat 0.03
Goat, meat byproducts 0.03
Grape 0.20
Grapefruit 1 0.25
Hazelnut 1 0.20
Horse, meat 0.03
Horse, meat byproducts 0.03
Lemon 1 0.25
Loganberry 0.20
Milk 0.03
Nut, macademia 1 0.25
Nut, tree, group 14-12 0.05
Olive 0.20
Orange 1 0.25
Peach 1 0.20
Pear 1 0.25
Pecan 1 0.20
Plum 1 0.20
Raspberry 0.20
Sheep, meat 0.03
Sheep, meat byproducts 0.03
Strawberry 0.25
Walnut 1 0.2
1 This tolerance expires on June 22, 2023.

(b)-(d) [Reserved]

[87 FR 78567, Dec. 22, 2022]

§ 180.215 Naled; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as naled, resulting from the application of the pesticide to growing crops or from direct application to livestock and poultry, in or on the following raw agricultural commodities:

Commodity Parts per million
Almond, hulls 0.5
Almond 0.5
Bean, dry, seed 0.5
Bean, succulent 0.5
Beet, sugar, roots 0.5
Beet, sugar, tops 0.5
Broccoli 1
Brussels sprouts 1
Cabbage 1
Cauliflower 1
Celery 3
Collards 3
Cotton, undelinted seed 0.5
Cucumber 0.5
Eggplant 0.5
Grape 0.5
Grapefruit 3
Grass, forage 10
Hop, dried cones 0.5
Kale 3
Legume, forage 10
Lemon 3
Melon 0.5
Orange, sweet 3
Peach 0.5
Pea, succulent 0.5
Pepper 0.5
Pumpkin 0.5
Safflower, seed 0.5
Spinach 3
Squash, summer 0.5
Squash, winter 0.5
Strawberry 1
Swiss chard 3
Tangerine 3
Tomato 0.5
Turnip, greens 3
Walnut 0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural commodities, except those otherwise listed in this section, from use of the pesticide for area pest (mosquito and fly) control.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, Sept. 26, 2012]

§ 180.217 Metiram; tolerances for residues.

(a) General. Tolerances are established for residues of a metiram (a mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those metiram residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts per million
Apple 0.5
Apple, pomace, wet 2
Banana 1 3
Grape, wine 1 5
Potato 0.2
1 There are no U.S. registrations on bananas and grape, wine as of April 29, 2011.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57074, Oct. 26, 1998, as amended at 76 FR 23891, Apr. 29, 2011]

§ 180.220 Atrazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4-ethylamino-6-isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylamino-s-triazine, 2-amino-4-chloro-6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the following food commodities:

Commodity Parts per
million
Cattle, fat 0.02
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Corn, field, forage 1.5
Corn, field, grain 0.20
Corn, field, stover 0.5
Corn, pop, forage 1.5
Corn, pop, grain 0.20
Corn, pop, stover 0.5
Corn, sweet, forage 15
Corn, sweet, kernel plus cob with husks removed 0.20
Corn, sweet, stover 2.0
Goat, fat 0.02
Goat, meat 0.02
Goat, meat byproducts 0.02
Grass, forage 4.0
Grass, hay 4.0
Guava 0.05
Horse, fat 0.02
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.02
Nut, macadamia 0.20
Sheep, fat 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.02
Sorghum, forage, forage 0.25
Sorghum, grain, forage 0.25
Sorghum, grain, grain 0.20
Sorghum, grain, stover 0.50
Sugarcane, cane 0.20
Wheat, forage 1.5
Wheat, grain 0.10
Wheat, hay 5.0
Wheat, straw 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of atrazine, 2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural commodity when present therein as a result of application of atrazine to the growing crops in paragraph (a) of this section:

Commodity Parts per million
Vegetable, leafy, except brassica, group 4 0.25

[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011]

§ 180.222 Prometryn; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities:

Commodity Parts per million
Bean, snap, succulent 0.05
Carrot, roots 0.45
Celeriac, roots 0.05
Celeriac, tops 0.20
Celtuce 0.50
Cilantro, leaves 3.5
Coriander, dried leaves 9.0
Cotton, gin byproducts 1.0
Cottonseed subgroup 20C 0.25
Dill, oil 1.3
Dillweed, dried leaves 1.1
Dillweed, fresh leaves 0.30
Fennel, Florence, fresh leaves and stalk 0.50
Leaf petiole vegetable subgroup 22B 0.50
Okra 0.05
Parsley, dried leaves 1.5
Parsley, leaves 0.60
Pea, pigeon, seed 0.25
Sesame, seed 0.05
Swiss chard 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities.

Commodity Parts per million
Barley, forage 0.3
Barley, hay 1.0
Barley, straw 0.3
Oat, forage 0.3
Oat, hay 1.0
Oat, straw 0.3
Rye, forage 0.3
Rye, hay 1.0
Rye, straw 0.3
Triticale, forage 0.3
Triticale, hay 1.0
Triticale, straw 0.3
Wheat, forage 0.3
Wheat, hay 1.0
Wheat, straw 0.3

[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013; 82 FR 57144, Dec. 4, 2017]

§ 180.225 Phosphine; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of phosphine in or on the following raw agricultural commodities (RACs) resulting from post-harvest fumigation for the control of insects with phosphine gas or phosphide compounds that produce phosphine gas.

Commodity Parts per million
Almond 0.1
Avocado 0.01
Banana 0.01
Barley, grain 0.1
Cabbage, Chinese, bok choy 0.01
Cabbage, Chinese, napa 0.01
Cacao bean, dried bean 0.1
Cashew 0.1
Citron, citrus 0.01
Coffee, bean, green 0.1
Corn, field, grain 0.1
Corn, pop, grain 0.1
Cotton, undelinted seed 0.1
Date, dried fruit 0.1
Dill, seed 0.01
Eggplant 0.01
Endive 0.01
Grapefruit 0.01
Hazelnut 0.1
Kumquat 0.01
Lemon 0.01
Lettuce 0.01
Lime 0.01
Mango 0.01
Millet, grain 0.1
Mushroom 0.01
Nut, brazil 0.1
Oat, grain 0.1
Okra 0.01
Orange, sweet 0.01
Papaya 0.01
Peanut 0.1
Pecan 0.1
Pepper 0.01
Persimmon 0.01
Pistachio 0.1
Rice, grain 0.1
Rye, grain 0.1
Safflower, seed 0.1
Salsify, tops 0.01
Sesame, seed 0.1
Sorghum, grain 0.1
Soybean, seed 0.1
Sunflower, seed 0.1
Sweet potato, roots 0.01
Tangelo 0.01
Tangerine 0.01
Tomato 0.01
Vegetable, legume, group 6, except soybean 0.01
Walnut 0.1
Wheat, grain 0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest treatment of pest burrows in agricultural and non-crop land areas.

Commodity Parts per million
All raw agricultural commodities resulting from preharvest treatment of pest burrows 0.01

(3) Residues resulting from fumigation of processed food:

Commodity Parts per million
Processed food 0.01

(4) Residues resulting from fumigation of animal feed :

Commodity Parts per million
Animal feed 0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that registered by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a restriction to aerate the finished food/feed for 48 hours before it is offered to the consumer, unless EPA specifically determines that a different time period is appropriate. Where appropriate, a warning shall state that under no condition should any formulation containing aluminum or magnesium phosphide be used so that it will come in contact with any processed food, except processed brewer's rice, malt, and corn grits stored in breweries for use in the manufacture of beer.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007; 74 FR 46372, Sept. 9, 2009]

§ 180.226 Diquat; tolerances for residues.

(a) General.

(1) Tolerances are established for the residues of the herbicide diquat, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a)(1) resulting from the application of the dibromide salt of diquat. Compliance with the tolerance levels specified in Table 1 to this paragraph (a)(1) is to be determined by measuring only diquat (6,7-dihydrodipyrido[1,2-a:2′,1′-c]pyrazinediium):

Commodity Parts per million
Alfalfa, seed 3.0
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Canola, meal 6.0
Canola, seed 2.0
Egg 0.05
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Milk 0.02
Pea and bean, dry and shelled, except soybean, subgroup 6C 1 0.9
Potato 0.1
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05
1 There are no U.S. registrations for these commodities as of October 22, 2020.

(2)

(i) Tolerances are established for residues of the herbicide diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) (calculated as the cation) derived from the application of the dibromide salt to ponds, lakes, reservoirs, marshes, drainage ditches, canals, streams, and rivers which are slow-moving or quiescent in programs of the Corp of Engineers or other Federal or State public agencies and to ponds, lakes and drainage ditches only where there is little or no outflow of water and which are totally under the control of the user, in or on the following food commodities:

Commodity Parts per million
Avocado 0.2
Berry group 13 0.05
Cotton, undelinted seed 0.2
Cranberry 0.05
Fish 2.0
Fruit, citrus, group 10 0.05
Fruit, pome, group 11 0.02
Fruit, stone, group 12 0.02
Grain, cereal, forage, fodder and straw, group 16 0.02
Grain, cereal, group 15 0.02
Grape 0.05
Grass, forage, fodder and hay, group 17 0.2
Hop, dried cones 0.2
Nut, tree, group 14 0.02
Shellfish 20.0
Strawberry 0.05
Sugarcane, cane 0.2
Vegetable, brassica, leafy, group 5 0.05
Vegetable, cucurbit, group 9 0.02
Vegetable, foliage of legume, group 7 0.2
Vegetable, fruiting, group 8 0.05
Vegetable, leafy, except brassica, group 4 0.05
Vegetable, root and tuber, group 1 0.02
Vegetable, seed and pod 0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the higher tolerances applies also to residues of the aquatic uses cited in this paragraph.

(3) Tolerances are established for the plant growth regulator diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) derived from application of the dibromide salt and calculated as the cation in or on the following food commodites:

Commodity Parts per million
Banana1 0.05
Coffee, bean, green1 0.05
Soybean, hulls 0.6
1 There are no U.S. registrations as of May 26, 2010.

(4) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and potato, chips.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29, 2010; 85 FR 67290, Oct. 22, 2020]

§ 180.227 Dicamba; tolerances for residues.

(a) General.

(1) Tolerances are established for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the sum of the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-5-hydroxy-o-anisic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million
Barley, grain 6.0
Barley, hay 2.0
Barley, straw 15.0
Corn, field, forage 3.0
Corn, field, grain 0.1
Corn, field, stover 3.0
Corn, pop, grain 0.1
Corn, pop, stover 3.0
Corn, sweet, forage 0.50
Corn, sweet, kernel plus cob with husks removed 0.04
Corn, sweet, stover 0.50
Grass, forage, fodder and hay, group 17, forage 125.0
Grass, forage, fodder and hay, group 17, hay 200.0
Millet, proso, forage 90.0
Millet, proso, grain 2.0
Millet, proso, hay 40.0
Millet, proso, straw 30.0
Oat, forage 90.0
Oat, grain 2.0
Oat, hay 40.0
Oat, straw 30.0
Rye, forage 90.0
Rye, grain 2.0
Rye, straw 30.0
Sorghum, grain, forage 3.0
Sorghum, grain, grain 4.0
Sorghum, grain, stover 10.0
Sugarcane, cane 0.3
Sugarcane, molasses 5.0
Teff, forage 90.0
Teff, grain 6.0
Teff, hay 40.0
Teff, straw 30.0
Wheat, forage 90.0
Wheat, grain 2.0
Wheat, hay 40.0
Wheat, straw 30.0

(2) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million
Asparagus 4.0
Cattle, fat 0.3
Cattle, kidney 25.0
Cattle, meat 0.25
Cattle, meat byproducts, except kidney 3.0
Goat, fat 0.3
Goat, kidney 25.0
Goat, meat 0.25
Goat, meat byproducts, except kidney 3.0
Hog, fat 0.3
Hog, kidney 25.0
Hog, meat 0.25
Hog, meat byproducts, except kidney 3.0
Horse, fat 0.3
Horse, kidney 25.0
Horse, meat 0.25
Horse, meat byproducts, except kidney 3.0
Milk 0.2
Sheep, fat 0.3
Sheep, kidney 25.0
Sheep, meat 0.25
Sheep, meat byproducts, except kidney 3.0

(3) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba, 3,6-dichloro-o-anisic acid, and its metabolites, 3,6-dichloro-5-hydroxy-o-anisic acid, and 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million
Cotton, gin byproducts 70
Cotton, undelinted seed 3.0
Grain, aspirated fractions 1000
Soybean, forage 60
Soybean, hay 100
Soybean, hulls 30.0
Soybean, seed 10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011; 81 FR 88634, Dec. 8, 2016]

§ 180.229 Fluometuron; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities:

Commodity Parts per million
Cotton, gin byproducts 3.5
Cotton, undelinted seed 1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N,N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites: CGA-236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea; and CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or on the following food commodities:

Commodity Parts per million
Cattle, meat byproducts 0.1
Egg 0.1
Goat, meat byproducts 0.1
Hog, meat byproducts 0.1
Horse, meat byproducts 0.1
Milk 0.02
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Sheep, meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities.

Commodity Parts per million
Grain, cereal, forage, fodder, and straw group 16, forage 3.0
Grain, cereal, forage, fodder, and straw, group 16, stover 6.0
Grain, cereal, group 15 0.5
Peanut 0.1
Peanut, hay 4.0
Peanut, meal 0.2
Soybean, forage 3.0
Soybean, hay 3.0
Soybean, seed 2.0
Rice, hulls 1.0
Wheat, milled byproducts 1.0

[73 FR 52613, Sept. 10, 2008]

§ 180.231 Dichlobenil; tolerances for residues.

(a) General. Tolerances are established for residues of dichlobenil, including its metabolites and degradates, in or on the commodities in the table in this paragraph (a). Compliance with the tolerance levels specified in this paragraph (a) is to be determined by measuring only the sum of dichlobenil (2,6-dichlorobenzonitrile) and its BAM metabolite (2,6-dichlorobenzamide), calculated as the stoichiometric equivalent of dichlobenil, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Apple 0.5
Bushberry subgroup 13-07B 0.15
Caneberry subgroup 13-07A 0.10
Cherry 0.15
Cranberry 0.1
Fruit, stone, group 12 1 0.15
Grape 0.15
Hazelnut 0.1
Pear 0.5
Rhubarb 0.06
1 This tolerance expires on January 19, 2024.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73 FR 50570, Aug. 27, 2008; 88 FR 46083, July 19, 2023]

§ 180.235 Dichlorvos; tolerances for residues.

(a) General.

(1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as follows:

Commodity Parts per million
Cattle, fat 0.02(N)
Cattle, meat 0.02(N)
Cattle, meat byproducts 0.02(N)
Egg 0.05(N)
Goat, fat 0.02(N)
Goat, meat 0.02(N)
Goat, meat byproducts 0.02(N)
Horse, fat 0.02(N)
Horse, meat 0.02(N)
Horse, meat byproducts 0.02(N)
Milk 0.02(N)
Mushroom (residues expressed as naled) 0.5
Poultry, fat 0.05(N)
Poultry, meat 0.05(N)
Poultry, meat byproducts 0.05(N)
Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, postharvest 0.5
Raw agricultural commodities nonperishable, packaged or bagged, containing 6 percent fat or less, postharvest 0.5
Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest 2
Sheep, fat 0.02(N)
Sheep, meat 0.02(N)
Sheep, meat byproducts 0.02(N)

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2-dichlorovinyl dimethyl phosphate in hog, fat; hog, meat; hog, meat byproducts; and hog, skin covers both its use as an anthelmintic in swine feed and as an insecticide applied directly to swine.

(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged nonperishable processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). To assure safe use of the insecticide, its label and labeling shall conform to the label and labeling registered by the U.S. Environmental Protection Agency, and the usage employed shall conform with such label or labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR 59125, Sept. 26, 2012]

§ 180.236 Triphenyltin hydroxide; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide (TPTH) and its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites, expressed in terms of parent TPTH, in or on the following raw agricultural commodities:

Commodity Parts per million
Beet, sugar, roots 0.05
Beet, sugar, tops 10.0
Cattle, fat 0.2
Cattle, kidney 2.0
Cattle, liver 4.0
Cattle, meat 0.5
Goat, fat 0.2
Goat, kidney 2.0
Goat, liver 4.0
Goat, meat 0.5
Hog, fat 0.3
Hog, meat 0.06
Hog, meat byproducts 0.3
Horse, fat 0.2
Horse, kidney 2.0
Horse, liver 4.0
Horse, meat 0.5
Milk 0.06
Pecan 0.05
Potato 0.05
Sheep, fat 0.2
Sheep, kidney 2.0
Sheep, liver 4.0
Sheep, meat 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 41929, Aug. 1, 2007]

§ 180.241 Bensulide; tolerances for residues.

(a) General. Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity Parts per million
Onion, bulb 0.10
Vegetable, brassica, leafy group 5 0.15
Vegetable, cucurbits group 9 0.15
Vegetable, fruiting group 8 0.10
Vegetable, leafy except brassica group 4 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity Parts per million
Carrot, roots 0.10

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

§ 180.242 Thiabendazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in table 1 to paragraph (a)(1). Compliance with the tolerance levels specified to table 1 to paragraph (a)(1) is to be determined by measuring only thiabendazole in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Alfalfa, forage 2 0.02
Alfalfa, hay 2 0.02
Animal feed, nongrass, group 18 0.01
Apple, wet pomace 12.0
Avocado 1 10.0
Banana, postharvest 3.0
Barley, grain 0.05
Barley, hay 0.30
Barley, straw 0.30
Beet, garden, leaves 0.01
Brassica, head and stem, subgroup 5A 2 0.02
Brassica, leafy greens, subgroup 4-16B 0.01
Burdock, edible, leaves 0.01
Cantaloupe 1 15.0
Carrot, leaves 0.01
Carrot, roots 10
Celeriac, leaves 0.01
Chervil, turnip rooted, leaves 0.01
Chicory, leaves 0.01
Citrus, oil 15.0
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, forage 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernels plus cop with husks removed 0.01
Corn, sweet, stover 0.01
Fruit, citrus, group 10-10 10
Fruit, pome, group 11-10 10
Kohlrabi 0.01
Mango 10.0
Mushroom 40.0
Oats, forage 0.30
Oats, grain 0.05
Oats, hay 0.30
Oats, straw 0.30
Onion, bulb, subgroup 3-07A 0.02
Papaya, postharvest 5.0
Radish, oriental, leaves 0.01
Rutabaga, leaves 0.01
Rye, forage 0.30
Rye, grain 0.05
Rye, straw 0.30
Salsify, black, leaves 0.01
Spinach 0.02
Strawberry 1 5.0
Sweet potato, tuber 3
Triticale, forage 0.30
Triticale, grain 0.05
Triticale, hay 0.30
Triticale, straw 0.30
Vegetable, Brassica, head and stem, group 5-16 0.01
Vegetable, cucurbit, group 9 0.02
Vegetable, foliage of legume, group 7 0.20
Vegetable, legume, group 6 0.02
Vegetable, root, except sugar beet, subgroup 1B 0.01
Vegetable, root (except sugar beet), subgroup 1B 2 0.02
Vegetable, tuberous and corm, subgroup 1C, except sweet potato 10
Wheat, forage 0.30
Wheat, grain 0.05
Wheat, hay 0.30
Wheat, straw 0.30
1 There are no U.S. registrations on the indicated commodity.
2 This tolerance expires on July 26, 2022.

(2) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in table 2 to paragraph (a)(2). Compliance with the tolerance levels specified to table 2 to paragraph (a)(2) is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite 5-hydroxythiabendazole (free and conjugated) calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, meat 0.1
Cattle, meat byproducts 0.4
Goat, meat byproducts 0.4
Hog, meat byproducts 0.3
Horse, meat byproducts 0.4
Milk 0.1
Sheep, meat byproducts 0.4

(b) Section 18 emergency exemptions. Time-limited tolerances specified in table 3 to this paragraph (b) are established for residues of the thiabendazole, including its metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in table 3 to this paragraph (b) is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole. The tolerances expire on the date specified in table 3 to this paragraph (b).

Commodity Parts per
million
Expiration/
revocation
date
Sweet potato 10 12/31/22

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 32783, June 28, 1977]

§ 180.243 Propazine; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, and its two chlorinated degradates, 2-amino-4-chloro-6-isopropylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine, calculated as the stoichiometric equivalent of propazine, in or on the commodity.

Commodity Parts per million
Sorghum, grain, forage 0.25
Sorghum, grain, grain 0.25
Sorghum, grain, stover 0.25

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60242, Sept. 29, 2010]

§ 180.245 Streptomycin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide streptomycin, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only streptomycin (O-2-Deoxy-2-(methylamino)-a-Lglucopyranosyl-(1-2)-O-5-deoxy-3-Cformyl-a-L-lyxofuranosyl-(1-4)-N,N′-bis(aminoiminomethyl)-D-streptamine) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Bean, dry, seed 0.5
Bean, succulent 0.5
Celery 0.25
Fruit, citrus, group 10-10 0.8
Fruit, citrus, group 10-10, dried pulp 3
Fruit, pome, group 11 0.25
Pepper 0.25
Potato 0.25
Tomato 0.25

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of streptomycin, in or on the agricultural commodities, as specified in Table 2 to this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels listed in Table 2 to this paragraph (b) is to be determined by measuring the levels of streptomycin only, in or on the commodities listed in this Table 2 paragraph (b). The tolerances expire on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration
date
Fruit, citrus, group 10-10 2.0 12/31/22
Fruit, citrus, group 10-10, dried pulp 6.0 12/31/22

(c)-(d) [Reserved]

[86 FR 8710, Feb. 9, 2021]

§ 180.249 Alachlor; tolerances for residues.

(a) General. Tolerances are established for combined residues of alachlor (2-chloro-2′,6″-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the following raw agricultural commodities.

Commodity Parts per million
Beans, dry 0.1
Beans, succulent lima 0.1
Cattle, fat 0.02
Cattle, meat byproducts 0.02
Cattle, meat 0.02
Corn, field, forage 2.0
Corn, field, grain 0.2
Corn, field, pop 0.2
Corn, field, stover 2.0
Corn, pop, stover 2.0
Corn, sweet (K + CWHR) 0.05
Corn, sweet, stover 2.0
Cotton, gin byproducts 0.7
Cotton, undelinted seed 0.03
Cowpea, forage 5.0
Cowpea, hay 5.0
Egg 0.02
Goat, fat 0.02
Goat, meat byproducts 0.02
Goat, meat 0.02
Hog, fat 0.02
Hog meat byproducts 0.02
Hog, meat 0.02
Horse, fat 0.02
Horse, meat byproducts 0.02
Horse, meat 0.02
Milk 0.02
Peanut 0.5
Poultry, fat 0.02
Poultry, meat byproducts 0.02
Poultry, meat 0.02
Sheep, fat 0.02
Sheep, meat byproducts 0.02
Sheep, meat 0.02
Sorghum grain, forage 2.0
Sorghum, grain, grain 0.1
Sorghum, grain, stover 1.0
Soybeans, seed 1.0
Sunflower, meal 3.4
Sunflower, seed 2.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of alachlor (2-chloro-2′,6′-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor, in or on the following raw agricultural commodities when present therein as a result of the application of alachlor to the growing crops in paragraph (a) of this section:

Commodity Parts per million
Animal feed, nongrass, group 18, forage 1.4
Animal feed, nongrass, group 18, hay 1.2
Grain, cereal, forage, and straw, group 16 except corn, sorghum, rice, straw 0.8
Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage 0.6
Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay 0.8
Grain, cereal, group 15 except corn, sorghum, rice 0.05

[72 FR 54584, Sept. 26, 2007]

§ 180.252 Tetrachlorvinphos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tetrachlorvinphos [(Z)-2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate], including its metabolites, 1-(2,4,5-trichlorophenyl)-ethanol (free and conjugated forms), 2,4,5-trichloroacetophenone, and 1-(2,4,5-trichlorophenyl)-ethanediol, in or on the following commodities:

Commodity Parts per
million
Cattle, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se) 0.2
Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) 1.0
Cattle, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.5
Cattle, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se) 2.0
Cattle, meat byproducts, except kidney and liver 1.0
Egg (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.2
Hog, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se) 0.2
Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) 1.0
Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.5
Hog, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se) 2.0
Hog, meat byproducts, except kidney and liver 1.0
Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.05
Poultry, fat (of which no more than 7.0 ppm is tetrachlorvinphos per se) 7.0
Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 2.0
Poultry, meat (of which no more than 3.0 ppm is tetrachlorvinphos per se) 3.0
Poultry, meat byproducts, except liver 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 57659, Sept. 16, 2011, as amended at 78 FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, 2013]

§ 180.253 Methomyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

Commodity Parts per million Expiration/revocation date
Alfalfa, forage 10 None
Alfalfa, hay 10 None
Apple 1 None
Asparagus 2 None
Avocado 2 None
Barley, grain 1 None
Barley, hay 10 None
Barley, straw 10 None
Bean, dry, seed 0.1 None
Bean, forage 10 None
Bean, succulent 2 None
Beet, garden, tops 6 None
Bermudagrass, forage 10 None
Bermudagrass, hay 40 None
Blueberry 6 None
Broccoli 3 None
Brussels sprouts 2 None
Cabbage 5 None
Cabbage, Chinese, bok choy 5 None
Cabbage, Chinese, napa 5 None
Cauliflower 2 None
Celery 3 None
Collards 6 None
Corn, field, forage 10 None
Corn, field, grain 0.1 None
Corn, field, stover 10 None
Corn, pop, grain 0.1 None
Corn, pop, stover 10 None
Corn, sweet, forage 10 None
Corn, sweet, kernel plus cob with husks removed 0.1 None
Corn, sweet, stover 10 None
Cotton, undelinted seed 0.1 None
Dandelion, leaves 6 None
Endive 5 None
Grape 5 12/31/16
Grapefruit 2 None
Hop, dried cones 1 12 None
Kale 6 None
Lemon 2 None
Lentil, seed 0.1 None
Lettuce 5 None
Mustard greens 6 None
Nectarine 5 None
Oat, forage 10 None
Oat, grain 1 None
Oat, hay 10 None
Oat, straw 10 None
Onion, dry bulb 0.2 None
Onion, green 3 None
Orange 2 None
Parsley, leaves 6 None
Pea 5 None
Pea, field, vines 10 None
Peach 5 None
Peanut 0.1 None
Pecan 0.1 None
Pepper, bell 2 None
Pepper, nonbell 2 None
Peppermint, tops 2 None
Pomegranate 0.2 None
Rye, forage 10 None
Rye, grain 1 None
Rye, straw 10 None
Sorghum, grain, forage 1 None
Sorghum, grain, grain 0.2 None
Soybean, forage 10 None
Soybean, seed 0.2 None
Spearmint, tops 2 None
Spinach 6 None
Swiss chard 6 None
Tangerine 2 None
Tomato 1 None
Turnip, greens 6 None
Vegetable, brassica, leafy, group 5 6.0 None
Vegetable, cucurbit, group 9 0.2 None
Vegetable, fruiting, group 8 0.2 None
Vegetables, leafy 2 0.2 None
Vegetable, root and tuber, group 1 0.2 None
Wheat, forage 10 None
Wheat, grain 1 None
Wheat, hay 10 None
Wheat, straw 10 None
1 There are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.
2 Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards, dandelions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and watercress.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(l), is established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

Commodity Parts
per million
Pear 4

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR 72598, Nov. 20, 2015]

§ 180.254 Carbofuran; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide carbofuran (2,3-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benzofuranyl-N-methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on the following raw agricultural commodities:

Commodity Parts per million
Banana 1 0.1
Coffee, bean, green 1 0.1
Rice, grain 1 0.2
Sugarcane, cane 1 0.1
1 There are no U.S. registrations for use of carbofuran on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[39 FR 20597, June 12, 1974]

§ 180.258 Ametryn; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4-(isopropylamino)-6-(methylthio)-s-triazine in or on the following raw agricultural commodities:

Commodity Parts per million Expiration/Revocation Date
Banana 0.25 6/16/10
Corn, field, forage 0.1 None
Corn, field, grain 0.05 None
Corn, field, stover 0.05 None
Corn, pop, grain 0.05 None
Corn, pop, stover 0.05 None
Corn, sweet, forage 0.5 6/16/10
Corn, sweet, kernel plus cob with husks removed 0.25 6/16/10
Corn, sweet, stover 0.5 6/16/10
Pineapple 0.05 None
Sugarcane, cane 0.05 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009]

§ 180.259 Propargite; tolerances for residues.

(a) General. Tolerances are established for residues of the pesticide propargite (2-(p-tert-butylphenoxy) cyclohexyl 2-propynyl sulfite) in or on the following food commodities.

Commodity Parts per million
Almond 0.1
Almond, hulls 55.0
Bean, dry, seed 0.2
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Citrus, oil 30.0
Corn, field, forage 10.0
Corn, field, grain 0.1
Corn, field, stover 10.0
Corn, pop, grain 0.1
Corn, pop, stover 10.0
Corn, sweet, forage 10.0
Corn, sweet, stover 10.0
Cotton, undelinted seed 0.1
Egg 0.1
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Grain, aspirated fractions 0.4
Grape 10.0
Grapefruit 5.0
Hog, fat 0.1
Hog, meat 0.1
Hog, meat byproducts 0.1
Hop, dried cones 100.0
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Lemon 5.0
Milk, fat (0.08 ppm in milk) 2.0
Nectarine 4.0
Orange 10.0
Peanut 0.1
Peppermint, tops 50.0
Poultry, fat 0.1
Potato 0.1
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Sorghum, grain, forage 10.0
Sorghum, grain, grain 5.0
Sorghum, grain, stover 10.0
Spearmint, tops 50.0
Tea, dried 10.0
Walnut 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of propargite in or on the following raw agricultural commodities:

Commodity Parts per million
Corn, sweet, kernel plus cob with husks removed 0.1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

§ 180.261 Phosmet; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

Commodity Parts per million
Alfalfa, forage 20
Alfalfa, hay 40
Almond, hulls 10
Apple 10
Apricot 5
Blueberry 10
Cattle, fat 0.2
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Cherry 10
Cranberry 10
Fruit, citrus, group 10 5
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Grape 10
Hog, fat 0.2
Hog, meat 0.04
Hog, meat byproducts 0.04
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Kiwifruit 25
Milk 0.1
Nectarine 5
Nut, tree, group 14 0.1
Pea, dry, seed 0.5
Pea, field, hay 20
Pea, field, vines 10
Pea, succulent 1
Peach 10
Pear 10
Plum, prune, fresh 5
Potato 0.1
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Sweet potato, roots 12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

Commodity Parts per million
Crabapple 20
Pistachio 0.1

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, 2010]

§ 180.262 Ethoprop; tolerances for residues.

(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, in or on the commodity.

Commodity Parts per million
Banana 0.02
Bean, lima 0.02
Bean, snap, succulent 0.02
Cabbage 0.02
Corn, field, forage 0.02
Corn, field, grain 0.02
Corn, field, stover 0.02
Corn, sweet, forage 0.02
Corn, sweet, kernel plus cob with husks removed 0.02
Corn, sweet, stover 0.02
Cucumber 0.02
Hop, dried cones 0.02
Peppermint, tops 0.02
Pineapple1 0.02
Potato 0.02
Spearmint, tops 0.02
Sugarcane, cane 0.02
Sweet potato, roots 0.02
1 There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, distribution, and use is allowed, provided it is consistent with the terms of the cancellation order of July 9, 2009; i.e., the EPA will allow the technical registrant to continue to sell and distribute existing stocks of the amended registered product bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided that such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified product.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010]

§ 180.269 Aldicarb; tolerances for residues.

(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-methyl-2-(methylthio)propionaldehyde O-(methylcarbamoyl) oxime and its cholinesterase-inhibiting metabolites 2-methyl 2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl) oxime in or on the following food commodities:

Commodity Parts per million
Bean, dry, seed 0.1
Beet, sugar, roots 0.05
Beet, sugar, tops 1
Citrus, dried pulp 0.6
Coffee, bean, green 0.1
Cotton, undelinted seed 0.1
Cotton, hulls 0.3
Grapefruit 0.3
Lemon 0.3
Lime 0.3
Orange, sweet 0.3
Peanut 0.05
Pecan 0.5
Potato 1
Soybean 0.02
Sugarcane, cane 0.02
Sweet potato, roots 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016]

§ 180.272 Tribuphos; tolerances for residues.

(a) General. Tolerances are established for residues of the defoliant tribuphos (S,S,S-tributyl phosphorotrithioate) in or on food commodities as follows:

Commodity Parts per million
Cattle, fat 0.15
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Cotton, gin byproducts 40.0
Cotton, undelinted seed 4.0
Goat, fat 0.15
Goat, meat 0.02
Goat, meat byproducts 0.02
Hog, fat 0.15
Hog, meat 0.02
Hog, meat byproducts 0.02
Horse, fat 0.15
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.01
Sheep, fat 0.15
Sheep, meat 0.02
Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

§ 180.274 Propanil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propanil (3′, 4′-dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.10
Cattle, meat 0.05
Cattle, meat byproducts 1.0
Crayfish 0.05
Egg 0.30
Goat, fat 0.10
Goat, meat 0.05
Goat, meat byproducts 1.0
Hog, fat 0.10
Hog, meat 0.05
Hog, meat byproducts 1.0
Horse, fat 0.10
Horse, meat 0.05
Horse, meat byproducts 1.0
Milk 0.05
Poultry, fat 0.05
Poultry, meat 0.10
Poultry, meat byproducts 0.50
Rice, bran 40
Rice, grain 10
Rice, hulls 30
Sheep, fat 0.10
Sheep, meat 0.05
Sheep, meat byproducts 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007; 80 FR 72598, Nov. 20, 2015]

§ 180.275 Chlorothalonil; tolerances for residues.

(a) General.

(1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity Parts per million
Almond 0.05
Almond, hulls 1.0
Apricot 0.5
Asparagus 0.1
Banana (NMT 0.05 ppm in edible pulp) 0.5
Bean, dry, seed 0.1
Bean, snap, succulent 5
Blueberry 1.0
Brassica, head and stem, subgroup 5A 5.0
Carrot, roots 1
Celery 15
Cherry, sweet 0.5
Cherry, tart 0.5
Cocoa bean, dried bean 0.05
Coffee, bean, green 0.20
Corn, sweet, kernel plus cob with husks removed 1
Cranberry 5.0
Ginseng 4.0
Horseradish 4.0
Lentil 0.10
Lychee 15
Mango 1.0
Mushroom 1.0
Nectarine 0.5
Okra 6.0
Onion, bulb 0.5
Onion, green 5
Papaya 15
Parsnip, roots 1
Passionfruit 3
Pea, edible podded 5
Peach 0.5
Peanut 0.3
Pistachio 0.2
Plum 0.2
Plum, prune 0.2
Potato 0.1
Rhubarb 4.0
Soybean 0.2
Starfruit 3.0
Tomato 5
Vegetable, cucurbit, group 9 5.0
Vegetable, fruiting, group 8, except tomato 6.0
Yam, true 0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity Parts per million
Cattle, fat 0.1
Cattle, kidney 0.5
Cattle, meat byproducts, except kidney 0.05
Cattle, meat 0.03
Goat, fat 0.1
Goat, kidney 0.5
Goat, meat byproducts, except kidney 0.05
Goat, meat 0.03
Hog, fat 0.1
Hog, kidney 0.5
Hog, meat byproducts, except kidney 0.05
Hog, meat 0.03
Horse, fat 0.1
Horse, kidney 0.5
Horse, meat byproducts, except kidney 0.05
Horse, meat 0.03
Milk 0.1
Sheep, fat 0.1
Sheep, kidney 0.5
Sheep, meat byproducts, except kidney 0.05
Sheep, meat 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for the combined residues of chlorothalonil and its metabolite in or on the following raw agricultural commodities:

Commodity Parts per million
Hazelnut 0.1
Peppermint, tops 2
Persimmon 1.5
Spearmint, tops 2

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 56114, Oct. 21, 1977]

§ 180.276 Formetanate hydrochloride; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide formetanate hydrochloride, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only formetanate hydrochloride, N,N-dimethyl-N'-[3-[(methylamino)carbonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity.

Commodity Parts per
million
Expiration/revocation date
Apple 0.50 12/31/13
Apple, wet pomace 1.5 12/31/13
Grapefruit 1.5 None
Lemon 0.60 None
Lime 0.03 None
Nectarine 0.40 None
Orange 1.5 None
Peach 0.40 12/31/13
Pear 0.50 12/31/13
Tangelo 0.03 None
Tangerine 0.03 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

§ 180.278 Phenmedipham; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide phenmedipham (3-methoxycarbonylaminophenyl-3′-methylcarbanilate) in or on the following food commodities:

Commodity Parts per million
Beet, garden, roots 0.2
Beet, garden, tops 0.2
Beet, sugar, dried pulp 0.5
Beet, sugar, molasses 0.2
Beet, sugar, roots 0.1
Beet, sugar, tops 0.1
Spinach 4.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007]

§ 180.284 Zinc phosphide; tolerances for residues.

(a) General. Tolerances are established for residues of the phosphine resulting from the use of the rodenticide zinc phosphide in or on the raw agricultural commodities as follows:

Commodity Parts per million
Alfalfa, forage 0.2
Alfalfa, hay 0.2
Barley, grain 0.05
Barley, hay 0.2
Barley, straw 0.2
Bean, dry, seed 0.05
Beet, sugar, roots 0.05
Beet, sugar, tops 0.2
Grape 0.01
Grass, rangeland, forage 0.1
Grass, rangeland, hay 0.1
Potato 0.05
Sugarcane, cane 0.01
Timothy, hay 0.5
Timothy, forage 0.5
Wheat, forage 0.05
Wheat, grain 0.05
Wheat, hay 0.05
Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on the following raw agricultural commodities as follows:

Commodity Parts per million
Artichoke, globe 0.01
Beet, sugar, roots 0.04
Beet, sugar, tops 0.02

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011]

§ 180.287 Amitraz; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N-[[(2,4-dimethylphenyl)imino]methyl]]-N-methylmethanimidamide), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring amitraz residues convertible to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.02
Cattle, meat byproducts 0.2
Hog, fat 0.1
Hog, kidney 0.1
Hog, liver 0.1
Hog, meat 0.05
Hog, meat byproducts 0.3
Honey 0.2
Honeycomb 9
Milk 0.03
Milk, fat 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013; 80 FR 72598, Nov. 20, 2015]

§ 180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole in or on the following food commodities:

Commodity Parts per million
Barley, grain 0.1(N)
Barley, straw 0.1(N)
Beet, sugar, roots 0.1(N)
Beet, sugar, tops 0.1(N)
Corn, field, forage 0.1(N)
Corn, field, grain 0.1
Corn, field, stover 0.1
Corn, pop, grain 0.1
Corn, pop, stover 0.1
Cotton, forage 0.1(N)
Cotton, undelinted seed 0.1(N)
Oat, forage 0.1(N)
Oat, grain 0.1(N)
Oat, hay 0.1(N)
Oat, straw 0.1(N)
Rice, grain 0.1(N)
Safflower, seed 0.1(N)
Sorghum, grain, forage 0.1(N)
Sorghum, grain, grain 0.1(N)
Sorghum, grain, stover 0.1(N)
Wheat, forage 0.1(N)
Wheat, grain 0.1(N)
Wheat, hay 0.1(N)
Wheat, straw 0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 74 FR 46374, Sept. 9, 2009; 80 FR 72598, Nov. 20, 2015]

§ 180.289 Methanearsonic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide methanearsonic acid, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methanearsonic acid, from application of the disodium and monosodium salts of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date
Cotton, undelinted seed 0.7 None
Cotton, hulls 0.9 None
Fruit, citrus 0.35 12/31/12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 77 FR 59126, Sept. 26, 2012]

§ 180.291 Pentachloronitrobenzene; tolerance for residues.

(a) General. Tolerances are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity Parts per million
Bean 0.1
Brassica, head and stem, subgroup 5A 0.1
Cotton, undelinted seed 0.1
Garlic, bulb 0.1
Peanut 1.0
Potato 0.1
Soybean, forage 0.02
Soybean, hay 0.02
Soybean, seed 0.02
Vegetable, fruiting, group 8 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(l), are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity Parts per million
Collards 0.2
Kale 0.2
Mustard, greens 0.2

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47456, Sept. 16, 2009]

§ 180.292 Picloram; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide picloram, 4-amino-3,5,6-trichloropicolinic acid, including its metabolites and degradates, in or on the commodities in the following table from its application in the acid form or in the form of its salts. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only picloram, 4-amino-3,5,6-trichloropicolinic acid, in or on the commodity.

Commodity Parts per million
Barley, grain 0.5
Barley, pearled barley 3.0
Barley, straw 1.0
Cattle, fat 0.4
Cattle, meat 0.4
Cattle, meat byproducts 15
Egg 0.05
Goat, fat 0.4
Goat, meat 0.4
Goat, meat byproducts 15
Grain, aspirated fractions 4.0
Grass, forage 400
Grass, hay 225
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.4
Horse, meat 0.4
Horse, meat byproducts 15
Milk 0.25
Oat, forage 1.0
Oat, grain 0.5
Oat, groats/rolled oats 3.0
Oat, straw 1.0
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Sheep, fat 0.4
Sheep, meat 0.4
Sheep, meat byproducts 15
Wheat, bran 3.0
Wheat, forage 1.0
Wheat, germ 3.0
Wheat, grain 0.5
Wheat, middlings 3.0
Wheat, shorts 3.0
Wheat, straw 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, 2007; 75 FR 60243, Sept. 29, 2010]

§ 180.293 Endothall; tolerances for residues.

(a) General.

(1) Tolerances are established for the residues of endothall, including its metabolites and degradates, in or on the commodities in the table, below. Compliance with the tolerance levels specified, below, is to be determined by measuring only endothall (7-oxabicylco [2.2.1] heptanes-2,3-dicarboxylic acid) and its mono-methyl ester.

Commodity Parts per million
Apple 0.05
Apple, wet pomace 0.15
Cotton, undelinted seed 0.1
Fish 0.1
Hop, dried cones 0.1
Potato 0.1
Rice, grain 0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di-N, N-dimethylalkylamine, and mono-N-N,-dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potential sources of water, potable.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent combined residues of the herbicide, endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in potable water from use of its potassium, sodium, di-N, N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potable water sources that may lead to endothall residues in or on the following commodities:

Commodity Parts per million
Almond, hulls 15.0
Animal feed, nongrass, group 18, forage 4.0
Animal feed, nongrass, group 18, hay 10
Apple, wet pomace 0.15
Beet, sugar, molasses 1.5
Brassica, head and stem subgroup 5A 0.1
Brassica, leafy, subgroup 5B 2.0
Bushberry subgroup 13-07B 0.6
Caneberry subgroup 13-07A 0.6
Cattle, fat 0.05
Cattle, kidney 0.05
Cattle, kidney 1 0.20
Cattle, liver 1 0.10
Cattle, liver 0.05
Cattle, meat 0.05
Corn, field, grain 0.07
Corn, pop, grain 0.07
Corn, sweet, kernel plus cob with husks removed 0.3
Citrus, dried pulp 0.1
Egg 0.05
Feed commodities not otherwise listed 10.0
Food commodities not otherwise listed 5.0
Fruit, citrus group 10 0.05
Fruit, pome, group 11 0.05
Fruit, stone, group 12 0.3
Goat, fat 0.05
Goat, kidney 1 0.15
Goat, kidney 0.05
Goat, liver 0.05
Goat, meat 0.05
Grain, aspirated fractions 35.0
Grain cereal, forage, fodder and straw, group 16 10.0
Grain, cereal, group 15, except corn 4.0
Grape 1.0
Grape, raisin 5.0
Grass, forage, fodder, and hay group 17, forage 3.5
Grass, forage, fodder, and hay group 17, hay 18.0
Herb and spice, group 19 5.0
Hog, fat 0.05
Hog, kidney 1 0.10
Hog, kidney 0.05
Hog, liver 0.05
Hog, meat 0.05
Milk 1 0.03
Milk 0.01
Nut, tree, group 14 0.05
Okra 0.05
Pea and bean, dried shelled, subgroup 6C 0.2
Pea and bean, succulent shelled, subgroup 6B 2.0
Peppermint, tops 5.0
Pistachio 0.05
Poultry, fat 0.05
Poultry, liver 0.05
Poultry, meat 0.05
Poultry, meat byproducts 1 0.20
Poultry, meat byproducts 0.05
Rice, hulls 8.0
Sheep, fat 0.05
Sheep, kidney 1 0.15
Sheep, kidney 0.05
Sheep, liver 0.05
Sheep, meat 0.05
Soybean, hulls 0.5
Soybean, seed 0.2
Spearmint, tops 5.0
Tomato, paste 0.1
Tomato, puree 0.1
Vegetable, bulb, group 3-07 0.5
Vegetable, cucurbit, group 9 1.5
Vegetable, foliage of legume, group 7 4.0
Vegetable, fruiting, group 8 0.05
Vegetable, leafy, except brassica, group 4 2.0
Vegetable, leaves of root and tuber, group 2 3.0
Vegetable, legume, edible, podded, subgroup 6A 2.0
Vegetable, root and tuber, group 1 1.0
Wheat, milled byproducts 5.0
1 This tolerance expires on May 22, 2017.

[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013; 80 FR 72598, Nov. 20, 2015; 81 FR 83169, Nov. 21, 2016]

§ 180.297 N-1-Naphthyl phthalamic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide N-1-naphthyl phthalamic acid from application of its sodium salt in or on the following raw agricultural commodities:

Commodity Parts per million
Cantaloupe 0.1(N)
Cucumber 0.1(N)
Muskmelon 0.1(N)
Watermelon 0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

§ 180.299 Dicrotophos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of 3-hydroxy-N,N-dimethyl-cis-crotonamide, in or on the following food commodities:

Commodity Parts per million
Cotton, gin byproducts 2.0
Cotton, undelinted seed 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52613, Sept. 10, 2008]

§ 180.300 Ethephon; tolerances for residues.

(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl) phosphonic acid] in or on food commodities as follows:

Commodity Parts per million
Apple 5.0
Apple, juice 10.0
Barley, bran 5.0
Barley, grain 2.0
Barley, straw 10.0
Blackberry 30.0
Blueberry 20.0
Cantaloupe 2.0
Cattle, fat 0.02
Cattle, kidney 1.0
Cattle, meat 0.02
Cattle, meat byproducts, except kidney 0.2
Cherry 10.0
Coffee, bean, green 0.5
Cotton, gin byproducts 180.0
Cotton, undelinted seed 6.0
Egg 0.002
Goat, fat 0.02
Goat, kidney 1.0
Goat, meat 0.02
Goat, meat byproducts, except kidney 0.2
Grape 2.0
Grape, raisin 12.0
Hazelnut 0.80
Hog, fat 0.02
Hog, kidney 1.0
Hog, meat 0.02
Hog, meat byproducts, except kidney 0.2
Horse, fat 0.02
Horse, kidney 1.0
Horse, meat 0.02
Horse, meat byproducts, except kidney 0.2
Milk 0.01
Nut, macadamia 0.5
Pepper 30.0
Pineapple 2.0
Poultry, fat 0.02
Poultry, liver 0.05
Poultry, meat 0.01
Poultry, meat byproducts, except liver 0.01
Sheep, fat 0.02
Sheep, kidney 1.0
Sheep, meat 0.02
Sheep, meat byproducts, except kidney 0.2
Sugarcane, molasses 1.5
Tomato 2.0
Walnut 0.5
Wheat, bran 5.0
Wheat, germ 5.0
Wheat, grain 2.0
Wheat, middlings 5.0
Wheat, shorts 5.0
Wheat, straw 10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(m), of 0.1 part per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic acid] in or on the food commodity sugarcane.

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010; 80 FR 72598, Nov. 20, 2015]

§ 180.301 Carboxin; tolerances for residues.

(a) General. Tolerances are established for residues of carboxin, 5,6-dihydro-2-methyl-N-phenyl-1,4-oxathiin-3-carboxamide, including its metabolites and degradates, in or on the commodities in table 1 to Paragraph (a). Compliance with the tolerance levels specified in table 1 to Paragraph (a) is to be determined by measuring only those carboxin residues convertible to aniline, expressed as the stoichiometric equivalent of carboxin, in or on the commodities.

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, grain 0.2
Barley, hay 0.2
Barley, straw 0.2
Bean, dry, seed 0.2
Bean, succulent 0.2
Cattle, fat 0.05
Cattle, meat byproducts 0.1
Cattle, meat 0.05
Corn, field, forage 0.2
Corn, field, grain 0.2
Corn, field, stover 0.2
Corn, pop, grain 0.2
Corn, pop, stover 0.2
Corn, sweet, forage 0.2
Corn, sweet, kernel plus cob with husks removed 0.2
Corn, sweet, stover 0.2
Cotton, gin byproducts 3
Cotton, undelinted seed 0.2
Egg 0.05
Goat, fat 0.05
Goat, meat byproducts 0.1
Goat, meat 0.05
Hog, fat 0.05
Hog, meat byproducts 0.1
Hog, meat 0.05
Horse, fat 0.05
Horse, meat byproducts 0.1
Horse, meat 0.05
Milk 0.05
Oat, forage 0.5
Oat, grain 0.2
Oat, hay 0.2
Oat, straw 0.2
Onion, bulb 0.2
Peanut 0.2
Peanut, hay 0.2
Poultry, fat 0.1
Poultry, meat byproducts 0.1
Poultry, meat 0.1
Rapeseed, seed 0.03
Rice, grain 0.2
Safflower, seed 0.2
Sheep, fat 0.05
Sheep, meat byproducts 0.1
Sheep, meat 0.05
Soybean, seed 0.2
Wheat, forage 0.5
Wheat, grain 0.2
Wheat, hay 0.2
Wheat, straw 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006; 80 FR 72598, Nov. 20, 2015; 91 FR 21388, Apr. 22, 2026]

§ 180.303 Oxamyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide oxamyl, methyl N,N-dimethyl-N-[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N-dimethyl-N-hydroxy-1-thiooxamimidate calculated as oxamyl in or on the following food commodities:

Commodity Parts per million
Apple 2
Banana 0.3
Cantaloupe 2.0
Carrot 0.1
Celery 10.0
Cotton, undelinted seed 0.2
Cucumber 2.0
Eggplant 2.0
Fruit, citrus, group 10 3
Garlic, bulb 0.2
Melon, honeydew 2.0
Onion, bulb 0.2
Peanut 0.05
Peanut, hay 2.0
Pear 2.0
Peppermint, tops 10.0
Pepper, bell 2.0
Pepper, nonbell 5.0
Pineapple 1
Pineapple, process residue 2.0
Pumpkin 2.0
Spearmint, tops 10.0
Squash, summer 2.0
Squash, winter 2.0
Tomato 2
Vegetable, tuberous and corm, subgroup 1C 0.1
Watermelon 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 72598, Nov. 20, 2015]

§ 180.304 Oryzalin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

Commodity Parts per million
Almond, hulls 0.05
Avocado 0.05
Berry group 13 0.05
Cranberry 0.05
Fig 0.05
Fruit, citrus, group 10 0.05
Fruit, pome, group 11 0.05
Fruit, stone, group 12 0.05
Grape 0.05
Kiwifruit 0.05
Nut, tree, group 14 0.05
Olive 0.05
Pistachio 0.05
Pomegranate 0.05
Strawberry 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

Commodity Parts per million
Guava 0.05
Papaya 0.05

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011]

§ 180.314 Triallate; tolerances for residues.

(a) General. Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl diisopropylthiocarbamate and its metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodity:

Commodity Parts per million
Bermudagrass, hay 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in 180.1(l),are established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its metabolite 2, 3, 3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:

Commodity Parts per million
Barley, grain 0.05
Barley, hay 1.0
Barley, straw 0.3
Beet, sugar, dried pulp 0.2
Beet, sugar, roots 0.1
Beet, sugar, tops 0.5
Pea, dry 0.2
Pea, field, hay 1.0
Pea, field, vines 0.5
Pea, succulent 0.2
Wheat, forage 0.5
Wheat, grain 0.05
Wheat, hay 1.0
Wheat, straw 1.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24, 2009]

§ 180.316 Pyrazon; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the commodities in Table 1 to paragraph (a).

Table 1 to Paragraph (a)

Commodity Parts per
million
Beet, garden, roots 1 0.9
Beet, garden, tops 1 7
Beet, sugar, molasses 1 1.5
Beet, sugar, roots 1 0.2
Beet, sugar, tops 1 3
Cattle, fat 1 0.1
Cattle, liver 1 0.15
Cattle, meat 1 0.1
Cattle, meat byproducts, except liver 1 0.1
Goat, fat 1 0.1
Goat, liver 1 0.15
Goat, meat 1 0.1
Goat, meat byproducts, except liver 1 0.1
Horse, fat 1 0.1
Horse, liver 1 0.15
Horse, meat 1 0.1
Horse, meat byproducts, except liver 1 0.1
Milk 1 0.02
Sheep, fat 1 0.1
Sheep, liver 1 0.15
Sheep, meat 1 0.1
Sheep, meat byproducts, except liver 1 0.1
1 There are no U.S. registrations. This tolerance expires on August 26, 2026.

(b)-(c) [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for combined residues of the herbicide pyrazon, 5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone, and its metabolites (calculated as pyrazon), in or on the commodities in Table 2 to paragraph (d).

Table 2 to Paragraph (d)

Commodity Parts per
million
Corn, field, forage 1 0.5
Corn, field, stover 1 0.5
Soybean, forage 1 0.5
Soybean, hay 1 0.5
Wheat, forage 1 0.3
Wheat, hay 1 0.2
Wheat, straw 1 0.1
1 There are no U.S. registrations. This tolerance expires on August 26, 2026.

[91 FR 9726, Feb. 27, 2026]

§ 180.317 Propyzamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity Parts per million
Alfalfa, seed 10.0
Animal feed, nongrass, group 18 10.0
Apple 0.1
Artichoke, globe 0.01
Blackberry 0.05
Blueberry 0.05
Boysenberry 0.05
Cattle, fat 0.2
Cattle, kidney 0.4
Cattle, liver 0.4
Cattle, meat 0.02
Cattle, meat byproducts, except kidney and liver 0.02
Egg 0.02
Endive 1.0
Fruit, stone, group 12 0.1
Goat, fat 0.2
Goat, kidney 0.4
Goat, liver 0.4
Goat, meat 0.02
Goat, meat byproducts, except kidney and liver 0.02
Grape 0.1
Hog, fat 0.2
Hog, kidney 0.4
Hog, liver 0.4
Hog, meat 0.02
Hog, meat byproducts, except kidney and liver 0.02
Horse, fat 0.2
Horse, kidney 0.4
Horse, liver 0.4
Horse, meat 0.02
Horse, meat byproducts, except kidney and liver 0.02
Lettuce, head 1.0
Lettuce, leaf 1.0
Milk 0.02
Pear 0.1
Poultry, fat 0.02
Poultry, liver 0.2
Poultry, meat 0.02
Poultry, meat byproducts, except liver 0.02
Radicchio 2.0
Raspberry 0.05
Sheep, fat 0.2
Sheep, kidney 0.4
Sheep, liver 0.4
Sheep, meat 0.02
Sheep, meat byproducts, except kidney and liver 0.02

(b) Section 18 emergency exemptions. The time-limited tolerance specified in the table in this paragraph (b) is established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the specified agricultural commodity in the table in this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance level specified in the table in this paragraph (b) is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide in or on the commodity. The time-limited tolerance expires on the date specified in the table in this paragraph (b).

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation
date
Cranberry 1 12/31/2028

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity Parts per million
Pea, field, seed 0.05
Rhubarb 0.1

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity Parts per million
Grain, cereal, forage, group 16 0.6
Grain, cereal, hay, group 16 0.2
Grain, cereal, straw, group 16 0.3

[72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011; 81 FR 1531, Jan. 13, 2016; 84 FR 60943, Nov. 12, 2019; 87 FR 76946, Dec. 16, 2022; 90 FR 54242, Nov. 26, 2025]

§ 180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.

(a) General.

(1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or on the following food commodity:

Commodity Parts per million
Pea 0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4-(4-chloro-2-methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic acid, in or on the following food commodities:

Commodity Parts per million
Peppermint, tops 0.20
Spearmint, tops 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

§ 180.319 Interim tolerances.

(a) General. While petitions for tolerances for negligible residues are pending and until action is completed on these petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the following raw agricultural commodities:

Substances Uses Tolerance in parts per million Raw
agricultural
commodity
Expiration/
revocation
date
Endothall (7-oxabicyclo-(2,2,1)heptane 2,3-dicarboxylic acid Herbicide 0.2 Beet, sugar None
Methyl parathion Herbicide 0.5 Rye 12/31/13

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014]

§ 180.324 Bromoxynil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide bromoxynil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

Commodity Parts per million
Alfalfa, forage 0.1
Alfalfa, hay 0.5
Barley, grain 0.05
Barley, hay 9.0
Barley, straw 4.0
Corn, field, forage 0.3
Corn, field, grain 0.05
Corn, field, stover 0.2
Corn, pop, grain 0.05
Corn, pop, stover 0.2
Flax, seed 0.1
Garlic 0.1
Grain, aspirated fractions 1.2
Grass, forage 18
Grass, hay 5.0
Oat, forage 0.3
Oat, grain 0.05
Oat, hay 9.0
Oat, straw 4.0
Onion, bulb 0.1
Peppermint, hay 0.1
Rye, forage 1.0
Rye, grain 0.05
Rye, straw 2.0
Sorghum, grain, forage 0.8
Sorghum, grain, grain 0.2
Sorghum, grain, stover 0.2
Spearmint, hay 0.1
Wheat, forage 1.0
Wheat, grain 0.05
Wheat, hay 4.0
Wheat, straw 2.0

(2) Tolerances are established for residues of the herbicide bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil and its metabolite, 3,5-dibromo-4-hydroxybenzoic acid (DBHA), resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

Commodity Parts per million
Cattle, fat 1
Cattle, meat byproducts 3.5
Cattle, meat 0.5
Cotton, gin byproducts 7.0
Cotton, hulls 5.0
Cotton, undelinted seed 1.5
Egg 0.05
Goat, fat 1
Goat, meat byproducts 3.5
Goat, meat 0.5
Hog, fat 1
Hog, meat byproducts 3.5
Hog, meat 0.5
Horse, fat 1
Horse, meat byproducts 3.5
Horse, meat 0.5
Milk 0.4
Poultry, fat 0.05
Poultry, meat byproducts 0.3
Poultry, meat 0.05
Sheep, fat 1
Sheep, meat byproducts 3.5
Sheep, meat 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR 31491, June 1, 2011]

§ 180.328 Napropamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide napropamide, N,N-diethyl-2-(1-napthalenyloxy) propionamide, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date
Almond, hulls 0.1 None
Asparagus 0.1 None
Basil 0.1 None
Berry group 13 0.1 None
Coffee, green bean 0.1 None
Cranberry 0.1 None
Grape 0.1 None
Kiwifruit 0.1 None
Marjoram 0.1 None
Nut, tree, group 14 0.1 None
Peppermint, tops 0.1 None
Persimmon 0.1 None
Rhubarb 0.1 None
Rosemary 0.1 None
Savory, summer 0.1 None
Savory, winter 0.1 None
Spearmint, tops 0.1 None
Strawberry 0.1 None
Sweet potato, roots 0.1 None
Vegetable, brassica, leafy, group 5 0.1 None
Vegetable, fruiting, group 8 0.1 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52614, Sept. 10, 2008, as amended at 76 FR 34885, June 15, 2011]

§ 180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.

(a) General. The tolerances in this section expire on January 19, 2024.

(1) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage 5.0
Alfalfa, hay 11.0
Bean, lima 0.2
Beet, sugar, roots 0.3
Beet, sugar, tops 0.5
Broccoli 1.0
Brussels sprouts 1.0
Cabbage 2.0
Cauliflower 1.0
Clover, forage 5.0
Clover, hay 10.0
Corn, sweet, forage 1.0
Corn, sweet, kernel plus cob with husks removed 0.5
Corn, sweet, stover 3.0
Cotton, undelinted seed 0.02
Cucumber 1.0
Eggplant 1.0
Grapefruit 1.0
Hazelnut 0.05
Lemon 1.0
Lettuce, head 2.0
Melon 0.2
Onion, bulb 0.05
Orange 1.0
Pepper 0.75
Peppermint, tops 12.5
Pumpkin 0.2
Safflower, seed 1.0
Sorghum, forage, forage 2.0
Sorghum, grain, forage 2.0
Sorghum, grain, grain 0.75
Spearmint, tops 12.5
Squash, summer 1.0
Squash, winter 0.3
Strawberry 2.0
Walnut 0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Egg 0.01
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Milk 0.01
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. The tolerances in this section expire on January 19, 2024. Tolerances with regional registrations, as defined in § 180.1(l), are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

Commodity Parts per million
Broccoli raab 2.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007, as amended at 88 FR 46083, July 19, 2023]

§ 180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid (2,4-DB), both free and conjugated, determined as the acid, in or on food commodities, as follows:

Commodity Parts per million
Alfalfa, forage 0.7
Alfalfa, hay 2.0
Cattle, meat byproducts 0.05
Clover, forage 0.2
Clover, hay 0.2
Goat, meat byproducts 0.05
Hog, meat byproducts 0.05
Horse, meat byproducts 0.05
Peanut 0.2
Peppermint, tops 0.2
Sheep, meat byproducts 0.05
Soybean, forage 0.7
Soybean, hay 2.0
Soybean, seed 0.5
Spearmint, tops 0.2
Trefoil, forage 0.7
Trefoil, hay 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 74 FR 46374, Sept. 9, 2009]

§ 180.332 Metribuzin; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1-dimethyl- ethyl)-3-(methylthio)-;1,2,4-triazin-5(4H)-one) and its triazinone metabolites in or on food commodities:

Commodity Parts per million
Alfalfa, forage 2.0
Alfalfa, hay 7.0
Asparagus 0.1
Barley, grain 0.75
Barley, hay 7.0
Barley, pearled barley 3.0
Barley, straw 1.0
Carrot, roots 0.3
Cattle, fat 0.7
Cattle, meat 0.7
Cattle, meat byproducts 0.7
Corn, field, forage 0.1
Corn, field, grain 0.05
Corn, field, stover 0.1
Corn, pop, grain 0.05
Corn, sweet, forage 0.1
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.1
Egg 0.01
Goat, fat 0.7
Goat, meat 0.7
Goat, meat byproducts 0.7
Grass, forage 2.0
Grass, hay 7.0
Hog, fat 0.7
Hog, meat 0.7
Hog, meat byproducts 0.7
Horse, fat 0.7
Horse, meat 0.7
Horse, meat byproducts 0.7
Lentil 0.05
Milk 0.05
Pea, dry, seed 0.05
Pea, field, hay 4.0
Pea, field, vines 0.5
Pea, succulent 0.1
Potato 0.6
Potato, chips 3.0
Potato, processed potato waste 3.0
Poultry, fat 0.7
Poultry, meat 0.7
Poultry, meat byproducts 0.7
Sainfoin, forage 2.0
Sainfoin, hay 7.0
Sheep, fat 0.7
Sheep, meat 0.7
Sheep, meat byproducts 0.7
Soybean, seed 0.3
Soybean, forage 4.0
Soybean, hay 4.0
Sugarcane, cane 0.1
Sugarcane, molasses 2.0
Tomato 0.1
Wheat, bran 3.0
Wheat, forage 2.0
Wheat, germ 3.0
Wheat, grain 0.75
Wheat, hay 7.0
Wheat, middlings 3.0
Wheat, shorts 3.0
Wheat, straw 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, July 31, 2002]

§ 180.337 Oxytetracycline; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the commodity.

Commodity Parts per million
Apple 0.35
Fruit, citrus, group 10-10 0.01
Peach 0.35
Pear 0.35

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire on the dates specified in the table.

Commodity Parts per
million
Expiration/
revocation date
Fruit, citrus, group 10-10 0.40 12/31/19

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23493, Apr. 27, 2011, as amended at 82 FR 13251, Mar. 10, 2017; 83 FR 62493, Dec. 4, 2018]

§ 180.339 MCPA; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide MCPA, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only MCPA, 2-(4-chloro-2-methylphenoxy)acetic acid, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Alfalfa, forage 0.5
Alfalfa, hay 2.0
Barley, grain 1.0
Barley, hay 40
Barley, straw 25
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Clover, forage 0.05
Clover, hay 0.05
Flax, seed 0.1
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Grain, aspirated fractions 3.0
Grass, forage 300
Grass, hay 20
Hog, fat 0.1
Hog, meat 0.1
Hog, meat byproducts 0.1
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Lespedeza, forage 0.5
Lespedeza, hay 2.0
Milk 0.1
Oat, forage 20
Oat, grain 1.0
Oat, hay 115
Oat, straw 25
Pea, dry 0.1
Pea, field, hay 0.1
Pea, field, vines 0.1
Pea, succulent 0.1
Rye, forage 20
Rye, grain 1.0
Rye, straw 25
Sheep meat 0.1
Sheep meat byproducts 0.1
Sheep, fat 0.1
Tea, dried 0.3
Trefoil, forage 0.5
Trefoil, hay 2.0
Vetch, forage 0.5
Vetch, hay 2.0
Wheat, forage 20
Wheat, grain 1.0
Wheat, hay 115
Wheat, straw 25
Wheatgrass, intermediate, forage 50
Wheatgrass, intermediate, grain 0.2
Wheatgrass, intermediate, hay 50
Wheatgrass, intermediate, straw 50

(b)-(d) [Reserved]

[86 FR 71154, Dec. 15, 2021]

§ 180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.

(a) General. Tolerances are established for combined negligible residues of a fungicide and insecticide that is a mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw agricultural commodities as follows:

Commodity Parts per million
Apple 1 0.1
Grape 1 0.1
1 There are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

§ 180.342 Chlorpyrifos; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage 3.0
Alfalfa, hay 13
Almond 0.2
Almond, hulls 12
Apple 0.01
Apple, wet pomace 0.02
Banana 0.1
Beet, sugar, dried pulp 5.0
Beet, sugar, molasses 15
Beet, sugar, roots 1.0
Beet, sugar, tops 8.0
Cattle, fat 0.3
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Cherry, sweet 1.0
Cherry, tart 1.0
Citrus, dried pulp 5.0
Citrus, oil 20
Corn, field, forage 8.0
Corn, field, grain 0.05
Corn, field, refined oil 0.25
Corn, field, stover 8.0
Corn, sweet, forage 8.0
Corn, sweet, kernel plus cob with husk removed 0.05
Corn, sweet, stover 8.0
Cotton, undelinted seed 0.2
Cranberry 1.0
Cucumber 0.05
Egg 0.01
Fig 0.01
Fruit, citrus, group 10 1.0
Goat, fat 0.2
Goat, meat 0.05
Goat, meat byproducts 0.05
Hazelnut 0.2
Hog, fat 0.2
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.25
Horse, meat 0.25
Horse, meat byproducts 0.25
Kiwifruit 2.0
Milk, fat (Reflecting 0.01 ppm in whole milk) 0.25
Nectarine 0.05
Onion, bulb 0.5
Peach 0.05
Peanut 0.2
Peanut, refined oil 0.2
Pear 0.05
Pecan 0.2
Pepper 1.0
Peppermint, tops 0.8
Peppermint, oil 8.0
Plum, prune, fresh 0.05
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Pumpkin 0.05
Radish 2.0
Rutabaga 0.5
Sheep, fat 0.2
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Spearmint, tops 0.8
Spearmint, oil 8.0
Sorghum, grain, forage 0.5
Sorghum, grain, grain 0.5
Sorghum, grain, stover 2.0
Soybean, seed 0.3
Strawberry 0.2
Sunflower, seed 0.1
Sweet potato, roots 0.05
Turnip, roots 1.0
Turnip, tops 0.3
Vegetable, brassica, leafy, group 5 1.0
Vegetable, legume, group 6. except soybean 0.05
Walnut 0.2
Wheat, forage 3.0
Wheat, grain 0.5
Wheat, straw 6.0

(2) Chlorpyrifos [O,O-diethyl O-(3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in accordance with the following prescribed conditions.

(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are held, processed, prepared or served. Contamination of food or food contact surfaces shall be avoided. Food must be removed or covered during treatment.

(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active ingredient by weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the spray.

(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active ingredient by weight.

(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by weight. Equipment capable of delivering a pin-stream of insecticide shall be used.

(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release product in food-handling establishments where food and food products are held, processed, prepared, or served. A maximum of 36 strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor space. The strips are not to be placed in exposed areas where direct contact with food, utensils, and food-contact surfaces would be likely to occur.

(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food commodities (other than those already covered by a higher tolerance as a result of use on growing crops) in food service establishments where food and food products are prepared and served, as a result of the application of chlorpyrifos in microencapsulated form.

(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are prepared and served. All treatments shall be applied in such a manner as to avoid contamination of food or food contact surfaces.

(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight.

(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into cracks and crevices or capable of applying small amounts of insecticide into cracks and crevices shall be used.

(iv) For spot treatment, an individual spot shall not exceed 2 square feet.

(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in 180.1(l), are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl- O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity Parts per million
Asparagus 5.0
Grape 0.01

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, Sept. 14, 2011; 86 FR 48336, Aug. 30, 2021; 89 FR 7627, Feb. 5, 2024]

§ 180.345 Ethofumesate; tolerances for residues.

(a) General. Tolerance are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the following food commodities.

Table 1 to Paragraph (a)

Commodity Parts per million
Beet, garden, leaves 5
Beet, garden, roots 0.5
Beet, sugar, molasses 2
Beet, sugar, roots 1.5
Beet, sugar, tops 1 4
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Garlic, bulb 0.25
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Grass, forage, fodder and hay, group 17, straw 1
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Onion, bulb 0.25
Shallot, bulb 0.25
Shallot, fresh leaves 0.25
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05
1 This tolerance expires on October 19, 2026.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in § 180.1(l) are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the raw agricultural commodities.

Table 2 to Paragraph (c)

Commodity Parts per
million
Carrot, roots 7

(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in Table 3 to this paragraph (d). Compliance with the tolerance levels specified in Table 3 to this paragraph (d) is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the commodity.

Table 3 to Paragraph (d)

Commodity Parts per
million
Animal feed, nongrass, group 18 1.5
Grain, cereal, forage, hay, stover, and straw, group 16-22 1.5
Vegetable, legume, forage and hay, group 7-22 0.5

[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007; 82 FR 57158, Dec. 4, 2017; 91 FR 21388, Apr. 22, 2026]

§ 180.349 Fenamiphos; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide/insecticide fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, and its cholinesterase inhibiting metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl 1-(methylethyl)phosphoramidate and ethyl 3-methyl-4-(methylsulfonyl)phenyl 1-(methylethyl)phosphoramidate, calculated as the stoichiometric equivalent of fenamiphos, in or on the commodity.

Commodity Parts per million
Banana1 0.1
Grape1 0.1
Grape, raisin1 0.3
Pineapple1 0.3
1 There are no U.S. registrations as of May 31, 2007.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, 2010]

§ 180.350 Nitrapyrin; tolerances for residues.

(a) General. Tolerances are established for residues of the nitrification inhibitor nitrapyrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of nitrapyrin (2-chloro-6-(trichloromethyl) pyridine) and its 6-CPA metabolite (6-chloro-picolinic acid), calculated as the stoichiometric equivalent of nitrapyrin, in or on the commodity:

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 0.06
Beet, sugar, molasses 0.5
Beet, sugar, roots 0.3
Beet, sugar, tops 0.7
Corn, field, forage 1.0
Corn, field, grain 0.1
Corn, field, milled byproducts 0.2
Corn, field, stover 1.0
Corn, pop, grain 0.1
Corn, pop, stover 1.0
Corn, sweet, forage 1.0
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 1.0
Cottonseed subgroup 20C 4
Cotton, gin byproduct 0.6
Cotton, meal 6
Fruit, citrus, group 10-10 0.06
Fruit, citrus, group 10-10, dried pulp 0.5
Fruit, citrus, group 10-10, oil 2
Leaf petiole vegetable subgroup 22B 0.5
Nut, tree, group 14-12 0.02
Rapeseed, seed 0.3
Rice, grain 0.03
Sorghum, forage, forage 0.5
Sorghum, grain, forage 0.5
Sorghum, grain, grain 0.1
Sorghum, grain, stover 0.5
Vegetable, Brassica, head and stem, group 5-16 0.1
Vegetable, bulb, group 3-07 0.3
Vegetable, leafy, group 4-16 0.4
Vegetable, tuberous and corm, crop subgroup 1C 0.6
Wheat, bran 3.0
Wheat, forage 2.0
Wheat, grain 0.5
Wheat, milled byproducts, except flour 2.0
Wheat, straw 6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007; 82 FR 56744, Nov. 30, 2017; 84 FR 44712, Aug. 27, 2019; 85 FR 48654, Aug. 12, 2020; 87 FR 3449, Jan. 24, 2022]

§ 180.352 Terbufos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide terbufos (phosphorodithioic acid, S-(t-butylthio)methyl O,O-diethyl ester) and its phosphorylated (cholinesterase-inhibiting) metabolites (phosphorothioic acid, S-(t-butylthio)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester; phosphorodithioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; and phosphorodithioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester) in or on food commodities:

Commodity Parts per million
Banana 0.025
Beet, sugar, roots 0.05
Beet, sugar, tops 0.1
Coffee, green bean 1 0.05
Corn, field, forage 0.5
Corn, field, grain 0.5
Corn, field, stover 0.5
Corn, pop, grain 0.5
Corn, pop, stover 0.5
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, forage 0.5
Corn, sweet, stover 0.5
Sorghum, grain, forage 0.5
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.5
1 There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 53740, Sept. 17, 2008]

§ 180.353 Desmedipham; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide desmedipham, (ethyl-m-hydroxycarbanilate carbanilate) in or on the following raw agricultural commodities in the table that follows:

Commodity Parts per million
Beet, garden, roots 0.05
Beet, garden, tops 1.0
Beet, sugar, roots 0.1
Beet, sugar, tops 5.0
Spinach 6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

§ 180.355 Bentazon; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of bentazon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring for only the sum of bentazon (3-(1-methylethyl)-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide), 6-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide, and 8-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide calculated as the stoichiometric equivalent of bentazon.

Commodity Parts per million
Bean, dry, seed 0.05
Bean, succulent 0.5
Corn, field, forage 3.0
Corn, field, grain 0.05
Corn, field, stover 3.0
Corn, pop, grain 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Cowpea, forage 10.0
Cowpea, hay 3.0
Flax, seed 1.0
Pea, dry, seed 3
Pea, field, hay 8.0
Pea, field, vines 3.0
Pea, succulent 3.0
Peanut 0.05
Peanut, hay 3.0
Pepper, nonbell 0.05
Peppermint, tops 1.0
Rice, grain 0.05
Rice, hulls 0.25
Sorghum, forage 0.20
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.05
Soybean, forage 8.0
Soybean, hay 8.0
Soybean, seed 0.05
Spearmint, tops 1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl benzamide (AIBA) in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat byproducts 0.05
Cattle, meat 0.05
Egg 0.05
Goat, fat 0.05
Goat, meat byproducts 0.05
Goat, meat 0.05
Hog, fat 0.05
Hog, meat byproducts 0.05
Hog, meat 0.05
Milk 0.02
Poultry, fat 0.05
Poultry, meat byproducts 0.05
Poultry, meat 0.05
Sheep, fat 0.05
Sheep, meat byproducts 0.05
Sheep, meat 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in § 180.1(m), are established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

Commodity Parts per million
Clover, forage 1.0
Clover, hay 2.0

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 26979, May 26, 1977]

§ 180.356 Norflurazon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro-5-(methylamino)-2-(alpha, alpha, alpha-trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its desmethyl metabolite 4-chloro-5-(amino)-2-alpha, alpha, alpha-trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural commodities:

Commodity Parts per million
Alfalfa, forage 3.0
Alfalfa, hay 5.0
Alfalfa, seed 0.1
Almond, hulls 1.0
Almond 0.1
Apple 0.1
Apricot 0.1
Asparagus 0.05
Avocado 0.20
Blackberry 0.1
Blueberry 0.2
Cattle, fat 0.1
Cattle, liver 0.50
Cattle, meat 0.1
Cattle, meat byproducts, except liver 0.1
Cherry 0.1
Citrus, dried pulp 0.4
Citrus, molasses 1.0
Cotton, undelinted seed 0.1
Cranberry 0.1
Fruit, citrus 0.2
Goat, fat 0.1
Goat, liver 0.50
Goat, meat 0.1
Goat, meat byproducts, except liver 0.1
Grape 0.1
Hazelnut 0.1
Hog, fat 0.1
Hog, liver 0.50
Hog, meat 0.1
Hog, meat byproducts, except liver 0.1
Hop, dried cones 3.0
Hop, vines 1.0
Horse, fat 0.1
Horse, liver 0.50
Horse, meat 0.1
Horse, meat byproducts, except liver 0.1
Milk 0.1
Nectarine 0.1
Peach 0.1
Peanut 0.05
Peanut, hay 5.50
Peanut, hay 1.5
Pear 0.1
Pecan 0.1
Plum, prune, fresh 0.1
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Raspberry 0.2
Sheep, fat 0.1
Sheep, liver 0.50
Sheep, meat 0.1
Sheep, meat byproducts, except liver 0.1
Soybean 0.1
Soybean, forage 1.0
Soybean, hay 1.0
Walnut 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 14909, Apr. 7, 1982]

§ 180.360 Asulam; tolerance for residues.

(a) General. Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate) and its sulfanilamide containing metabolites in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.2
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.2
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.2
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.2
Milk 0.05
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.2
Sugarcane, cane 1.0
Sugarcane, molasses 30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

§ 180.361 Pendimethalin; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on the commodities. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine] and its metabolite, 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 80
Alfalfa, hay 150
Alfalfa, seed 0.10
Almond, hulls 6.0
Apple, wet pomace 0.20
Artichoke, globe 0.1
Asparagus 0.15
Beans 0.10
Beans, forage 0.10
Beans, hay 0.10
Berry, low growing subgroup 13-07G 0.1
Brassica head and stem, subgroup 5-A 0.1
Brassica, leafy greens, subgroup 5B 0.20
Bushberry subgroup 13-07B 0.10
Caneberry subgroup 13-07A 0.10
Carrot 0.5
Citrus, oil 0.5
Corn, field, forage 0.1
Corn, field, grain 0.1
Corn, field, stover 0.1
Corn, pop, grain 0.1
Corn, sweet, forage 0.1
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 0.1
Cotton, gin byproducts 3.0
Cotton, undelinted seed 0.1
Crayfish 0.05
Fig 0.1
Fig, dried 3
Fruit, citrus, group 10-10 0.1
Fruit, pome, group 11-10 0.1
Fruit, small vine climbing, except grape, subgroup 13-07E 0.10
Fruit, stone, group 12-12 0.1
Grape 0.1
Grass, forage, fodder, and hay crop group 17, forage 1,000
Grass, forage, fodder, and hay crop group 17, hay 2,000
Hop, dried cones 0.1
Leaf petiole vegetable subgroup 22B 0.2
Lettuce, leaf 4.0
Melon subgroup 9A 0.10
Monarda, fresh leaves 0.2
Monarda, oil 1
Nut, tree, group 14-12 0.10
Olive 0.1
Onion, bulb subgroup 3-07A 0.1
Onion, green subgroup 3-07B 0.2
Peanut 0.1
Peanut, hay 0.1
Peas (except field peas) 0.10
Peppermint, oil 1.0
Peppermint, tops 0.2
Pomegranate 0.10
Potato 0.1
Rice, grain 0.1
Rosemary, fresh leaves 0.2
Rosemary, oil 1
Sorghum, forage 0.1
Sorghum, grain, grain 0.1
Sorghum, grain, stover 0.1
Soybean, forage 0.1
Soybean, hay 0.1
Soybean, seed 0.1
Spearmint, oil 1.0
Spearmint, tops 0.2
Sugarcane, cane 0.1
Sunflower subgroup 20B 0.1
Turnip greens 0.20
Vegetable, fruiting, group 8-10 0.1
Vegetable, soybean, succulent 0.10
Wheat, grain 0.10
Wheat, forage 3.0
Wheat, hay 0.60
Wheat, straw 0.30

(2) Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on commodities listed in the following table. Compliance with the tolerance levels is to be determined by measuring only the sum of pendimethalin (N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine)) and its metabolite, 1-(1-ethylpropyl)-5, 6-dimethyl-7-nitro-1H-benzimidazole (metabolite 6), calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts
per
million
Cattle, fat 0.30
Cattle, meat 0.10
Cattle, meat byproduct 3.0
Goats, fat 0.30
Goats, meat 0.10
Goats, meat byproduct 3.0
Horse, fat 0.30
Horse, meat 0.10
Horse, byproduct 3.0
Milk 0.04
Sheep, fat 0.30
Sheep, meat 0.10
Sheep, meat byproduct 3.0

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 15293, Apr. 18, 1984]

§ 180.362 Fenbutatin-oxide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity Parts per million
Almond, hulls 80.0
Apple 15.0
Apple, wet pomace 100.0
Cherry, sweet 6.0
Cherry, tart 6.0
Citrus, dried pulp 100.0
Citrus, oil 140.0
Cucumber 4.0
Eggplant 6.0
Fruit, citrus, group 10 20.0
Grape 5.0
Grape, raisin 20.0
Nut, tree, group 14 0.5
Papaya 2.0
Peach 10.0
Pear 15.0
Pistachio 0.5
Plum, prune, fresh 4.0
Plum, prune, dried 20.0
Strawberry 10.0

(2) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the animal commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, and its organotin metabolites, dihydroxybis(2-methyl-2-phenylpropyl) stannane and 2-methyl-2-phenylpropylstannoic acid, calculated as the stoichiometric equivalent of fenbutatin-oxide, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.5
Cattle, meat 0.5
Cattle, meat byproducts 0.5
Egg 0.1
Goat, fat 0.5
Goat, meat 0.5
Goat, meat byproducts 0.5
Hog, fat 0.5
Hog, meat 0.5
Hog, meat byproducts 0.5
Horse, fat 0.5
Horse, meat 0.5
Horse, meat byproducts 0.5
Milk, fat 0.1
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Sheep, fat 0.5
Sheep, meat 0.5
Sheep, meat byproducts 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(l), is established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity Parts per million
Raspberry 10.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011]

§ 180.364 Glyphosate; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine).

Commodity Parts per million
Acerola 0.2
Alfalfa, seed 0.5
Almond, hulls 25
Aloe vera 0.5
Ambarella 0.2
Animal feed, nongrass, group 18 400
Artichoke, globe 0.2
Asparagus 0.5
Atemoya 0.2
Avocado 0.2
Bamboo, shoots 0.2
Banana 0.2
Barley, bran 30
Beet, sugar, dried pulp 25
Beet, sugar, roots 10
Beet, sugar, tops 10
Berry and small fruit, group 13-07 0.20
Betelnut 1.0
Biriba 0.2
Blimbe 0.2
Breadfruit 0.2
Cacao bean, bean 0.2
Cactus, fruit 0.5
Cactus, pads 0.5
Canistel 0.2
Carrot 5.0
Chaya 1.0
Cherimoya 0.2
Citrus, dried pulp 1.5
Coconut 0.1
Coffee, bean, green 1.0
Corn, pop, grain 0.1
Corn, sweet, kernel plus cob with husk removed 3.5
Cotton, gin byproducts 210
Custard apple 0.2
Date, dried fruit 0.2
Dokudami 2.0
Durian 0.2
Epazote 1.3
Feijoa 0.2
Fig 0.2
Fish 0.25
Fruit, citrus, group 10-10 0.50
Fruit, pome, group 11-10 0.20
Fruit, stone, group 12 0.2
Galangal, roots 0.2
Ginger, white, flower 0.2
Gourd, buffalo, seed 0.1
Governor's plum 0.2
Gow kee, leaves 0.2
Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover 100
Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice 30
Grass, forage, fodder and hay, group 17 300
Guava 0.2
Herbs subgroup 19A 0.2
Hop, dried cones 7.0
Ilama 0.2
Imbe 0.2
Imbu 0.2
Jaboticaba 0.2
Jackfruit 0.2
Kava, roots 0.2
Kenaf, forage 200
Leucaena, forage 200
Longan 0.2
Lychee 0.2
Mamey apple 0.2
Mango 0.2
Mangosteen 0.2
Marmaladebox 0.2
Mioga, flower 0.2
Noni 0.20
Nut, pine 1.0
Nut, tree, group 14 1.0
Oilseeds, group 20, except canola 40
Okra 0.5
Olive 0.2
Oregano, Mexican, leaves 2.0
Palm heart 0.2
Palm heart, leaves 0.2
Palm, oil 0.1
Papaya 0.2
Papaya, mountain 0.2
Passionfruit 0.2
Pawpaw 0.2
Pea, dry 8.0
Peanut 0.1
Peanut, hay 0.5
Pepper leaf, fresh leaves 0.2
Peppermint, tops 200
Perilla, tops 1.8
Persimmon 0.2
Pineapple 0.1
Pistachio 1.0
Pomegranate 0.2
Pulasan 0.2
Quinoa, grain 5.0
Rambutan 0.2
Rice, grain 0.1
Rice, wild, grain 0.1
Rose apple 0.2
Sapodilla 0.2
Sapote, black 0.2
Sapote, mamey 0.2
Sapote, white 0.2
Shellfish 3.0
Soursop 0.2
Spanish lime 0.2
Spearmint, tops 200
Spice subgroup 19B 7.0
Star apple 0.2
Starfruit 0.2
Stevia, dried leaves 1.0
Sugar apple 0.2
Sugarcane, cane 2.0
Sugarcane, molasses 30
Surinam cherry 0.2
Sweet potato 3.0
Tamarind 0.2
Tea, dried 1.0
Tea, instant 7.0
Teff, forage 100
Teff, grain 5.0
Teff, hay 100
Ti, leaves 0.2
Ti, roots 0.2
Ugli fruit 0.5
Vegetable, bulb, group 3-07 0.20
Vegetable, cucurbit, group 9 0.5
Vegetable, foliage of legume, subgroup 7A, except soybean 0.2
Vegetable, fruiting, group 8-10 (except okra) 0.10
Vegetable, leafy, brassica, group 5 0.2
Vegetable, leafy, except brassica, group 4 0.2
Vegetable, leaves of root and tuber, group 2, except sugar beet tops 0.2
Vegetable, legume, group 6 except soybean and dry pea 5.0
Vegetables, root and tuber, group 1, except carrot, sweet potato, and sugar beet 0.20
Wasabi, roots 0.2
Water spinach, tops 0.2
Watercress, upland 0.2
Wax jambu 0.2
Yacon, tuber 0.2

(2) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine) and its metabolite N-acetyl-glyphosate (N-acetyl-N-(phosphonomethyl)glycine; calculated as the stoichiometric equivalent of glyphosate).

Commodity Parts per Million
Canola, seed 20
Cattle, meat byproducts 5.0
Corn, field, forage 13
Corn, field, grain 5.0
Corn, field, stover 100
Egg 0.05
Goat, meat byproducts 5.0
Grain aspirated fractions 310.0
Hog, meat byproducts 5.0
Horse, meat byproducts 5.0
Poultry, meat 0.10
Poultry, meat byproducts 1.0
Sheep, meat byproducts 5.0
Soybean, forage 100.0
Soybean, hay 200.0
Soybean, hulls 120.0
Soybean, seed 20.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 64911, Oct. 1, 1980]

§ 180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.

(a) General. A tolerance of 5 parts per million is established for residues of the insecticide synergist N-octyl bicycloheptene dicarboximide, including its metabolites and degradates, in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served, provided that the food is removed or covered prior to such use, except for bagged food in warehouse storage which need not be removed or covered prior to applications of formulations containing N-octyl bicycloheptene dicarboximide. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only N-octyl bicycloheptene dicarboximide, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 75 FR 60243, Sept. 29, 2010]

§ 180.368 Metolachlor and S-metolachlor; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2- ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 0.3
Animal feed, nongrass, group 18 1
Cattle, fat 0.02
Cattle, kidney 0.2
Cattle, liver 0.05
Cattle, meat 0.02
Cattle, meat byproducts, except kidney and liver 0.04
Corn, field, forage 6
Corn, field, grain 0.1
Corn, field, stover 6
Corn, pop, grain 0.1
Corn, pop, stover 6
Corn, sweet, forage 6
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 6
Cotton, gin byproducts 4
Cotton, undelinted seed 0.1
Dillweed 0.5
Egg 0.02
Goat, fat 0.02
Goat, kidney 0.2
Goat, liver 0.05
Goat, meat 0.02
Goat, meat byproducts, except kidney and liver 0.04
Grass, forage, fodder and hay, group 17, forage 10
Grass, forage, fodder and hay, group 17, hay 0.2
Horse, fat 0.02
Horse, kidney 0.2
Horse, liver 0.05
Horse, meat 0.02
Horse, meat byproducts, except kidney and liver 0.04
Milk 0.02
Nut, tree, group 14 0.1
Okra 0.5
Peanut 0.2
Peanut, hay 20
Peanut, meal 0.4
Potato 0.2
Poultry, fat 0.02
Poultry, meat 0.02
Poultry, meat byproducts 0.05
Safflower, seed 0.1
Sheep, fat 0.02
Sheep, kidney 0.2
Sheep, liver 0.05
Sheep, meat 0.02
Sheep, meat byproducts, except kidney and liver 0.04
Sorghum, grain, forage 1
Sorghum, grain, grain 0.3
Sorghum, grain, stover 4
Soybean, forage 5
Soybean, hay 8
Soybean, seed 0.2
Tomato 0.1
Vegetable, foliage of legume, except soybean, subgroup 7A 15
Vegetable, legume, group 6 0.3

(2) Tolerances are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodity(s), as defined. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Beet, sugar, leaves 15
Beet, sugar, molasses 2
Beet, sugar, roots 0.5
Berry, low growing, subgroup 13-07G, except cranberry 0.4
Brassica, leafy greens, subgroup 4-16B 1.8
Bushberry subgroup 13-07B 0.15
Caneberry subgroup 13-07A 0.1
Carrot, roots 0.4
Cattle, fat 0.02
Cattle, kidney 0.2
Cattle, liver 0.05
Cattle, meat 0.02
Cattle, meat byproducts, except kidney and liver 0.04
Cilantro, fresh leaves 8
Coriander, seed 0.13
Corn, field, forage 40
Corn, field, grain 0.1
Corn, field, stover 40
Corn, pop, grain 0.1
Corn, pop, stover 40
Corn, sweet, forage 6
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 40
Cotton, gin byproducts 4
Cottonseed subgroup 20C 0.1
Dill, seed 15
Dillweed 5
Dillweed, dried leaves 9
Egg 0.02
Goat, fat 0.02
Goat, kidney 0.2
Goat, liver 0.05
Goat, meat 0.02
Goat, meat byproducts, except kidney and liver 0.04
Grain, aspirated fractions 4
Grass, forage, fodder and hay, group 17, forage 10
Grass, forage, fodder and hay, group 17, hay 0.2
Horse, fat 0.02
Horse, kidney 0.2
Horse, liver 0.05
Horse, meat 0.02
Horse, meat byproducts, except kidney and liver 0.04
Kohlrabi 0.6
Leaf petiole vegetable subgroup 22B 0.1
Lettuce 1.5
Milk 0.02
Onion, bulb, subgroup 3-07A 0.1
Onion, green, subgroup 3-07B 2
Peanut 0.2
Peanut, hay 20
Peanut, meal 0.4
Poultry, fat 0.02
Poultry, meat 0.02
Poultry, meat byproducts 0.05
Rosemary, dried leaves 2
Rosemary, fresh leaves 1.5
Safflower, seed 0.1
Sesame, seed 0.13
Sheep, fat 0.02
Sheep, kidney 0.2
Sheep, liver 0.05
Sheep, meat 0.02
Sheep, meat byproducts, except kidney and liver 0.04
Sorghum, grain, forage 1
Sorghum, grain, grain 0.3
Sorghum, grain, stover 4
Sorghum, sweet, stalk 4
Soybean, forage 5
Soybean, hay 8
Soybean, meal 1.5
Soybean, seed 0.9
Spinach 0.5
Stalk and stem vegetable subgroup 22A, except kohlrabi 0.1
Stevia, dried leaves 15
Sugarcane, cane 0.2
Sugarcane, molasses 1.5
Sunflower, meal 1
Sunflower subgroup 20B 1
Swiss chard 0.15
Tomato, paste 0.3
Vegetable, brassica, head and stem, group 5-16 0.6
Vegetable, cucurbit, group 9 0.5
Vegetable, foliage of legume, except soybean, subgroup 7A 15
Vegetable, fruiting, group 8-10, except tabasco pepper 0.1
Vegetable, leaves of root and tuber, group 2, except sugar beet 2
Vegetable, legume, group 6 0.3
Vegetable, root, except sugar beet, subgroup 1B, except carrot 0.3
Vegetable, tuberous and corm, subgroup 1C 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations.

(1) Tolerances with regional registration as defined in 180.1(l) are established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound, in or on the following raw agricultural commodities:

Commodity Parts per million
Pepper, nonbell 0.50

(2) Tolerances with regional registration are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity Parts per million
Pepper, tabasco 0.50

(d) Indirect or inadvertent residues.

(1) Tolerances are established for the indirect or inadvertent combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2-ethyl-6- methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

Commodity Parts per million
Animal feed, nongrass, group 18 1.0
Barley, grain 0.10
Barley, hay 0.80
Barley, straw 0.80
Buckwheat, grain 0.10
Millet, forage 0.50
Millet, grain 0.10
Millet, hay 0.80
Millet, straw 0.80
Oat, forage 0.50
Oat, grain 0.10
Oat, hay 0.80
Oat, straw 0.80
Rice, grain 0.10
Rye, forage 0.50
Rye, grain 0.10
Rye, straw 0.80
Wheat, forage 0.50
Wheat, grain 0.10
Wheat, hay 0.80
Wheat, straw 0.80

(2) Tolerances for are established for the indirect or inadvertent residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity Parts per million
Animal feed, nongrass, group 18 1.0
Barley, grain 0.10
Barley, hay 0.50
Barley, straw 0.50
Buckwheat, grain 0.10
Millet, forage 0.50
Millet, grain 0.10
Millet, hay 0.50
Millet, straw 0.50
Oat, forage 0.50
Oat, grain 0.10
Oat, hay 0.50
Oat, straw 0.50
Rice, grain 0.10
Rye, forage 0.50
Rye, grain 0.10
Rye, straw 0.50
Wheat, forage 0.50
Wheat, grain 0.10
Wheat, hay 0.50
Wheat, straw 0.50

[73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015; 83 FR 12274, Mar. 21, 2018; 84 FR 8617, Mar. 11, 2019; 85 FR 40131, July 6, 2020; 91 FR 8104, Feb. 20, 2026]

§ 180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide etridiazole, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels is to be determined by measuring only the residues of etridiazole, (5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole), and its metabolite etridiazole acid, (3-carboxy-5-ethoxy-1,2,4-thiadiazole), calculated as the stoichiometric equivalent of etridiazole, in or on the commodity:

Table 1 to Paragraph (a)

Commodity Parts per million
Cotton, gin byproducts 0.1
Cotton, undelinted seed 0.1
Tomato1 0.15
Tomato 0.1
1 This tolerance expires on August 19, 2026.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016; 91 FR 8107, Feb. 20, 2026]

§ 180.371 Thiophanate-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

Commodity Parts per million
Almond 0.1
Almond, hulls 0.5
Apple 2.0
Apricot 15.0
Banana 2.0
Bean, dry, seed 0.2
Bean, snap, succulent 2.0
Beet, sugar, roots 0.2
Cherry, sweet 20.0
Cherry, tart 20.0
Grain, aspirated fractions 12
Grape 5.0
Onion, bulb 0.5
Onion, green 3.0
Peach 3.0
Peanut 0.1
Peanut, hay 5.0
Pear 3.0
Pecan 0.1
Pistachio 0.1
Plum 0.5
Potato 0.1
Soybean, hulls 1.5
Soybean, seed 0.2
Strawberry 7.0
Vegetable, cucurbit, group 9 1.0
Wheat, forage 1.1
Wheat, grain 0.1
Wheat, hay 0.1
Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis(iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

Commodity Parts per million
Canola, seed 0.1

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60244, Sept. 29, 2010]

§ 180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.

(a) General. A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in or on the following food commodity:

Commodity Parts per million
Banana 1 1.0
1 There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008]

§ 180.373 [Reserved]

§ 180.377 Diflubenzuron; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of diflubenzuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Artichoke, globe 6
Cattle, fat 0.1
Cattle, meat 0.1
Cotton, gin byproducts 30
Cottonseed subgroup 20C 0.2
Egg 0.07
Goat, fat 0.1
Goat, meat 0.1
Hog, fat 0.1
Hog, meat 0.1
Horse, fat 0.1
Horse, meat 0.1
Milk 0.05
Mushroom 8
Poultry, fat 0.1
Poultry, meat byproducts 0.08
Poultry, meat 0.05
Sheep, fat 0.1
Sheep, meat 0.1
Soybean, seed 0.05
Soybean, hulls 0.5

(2) Tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Almond, hulls 6
Barley, grain 0.06
Barley, hay 3
Barley, straw 1.8
Brassica, leafy greens, subgroup 4-16B 10
Carrot, roots 0.2
Cattle, meat byproducts 0.15
Fruit, citrus, group 10-10, oil 32
Fruit, citrus, group 10-10 3
Goat, meat byproducts 0.15
Grain, aspirated fractions 11
Grass, forage, fodder and hay, group 17 6
Hog, meat byproducts 0.15
Horse, meat byproducts 0.15
Oat, forage 7
Oat, grain 0.06
Oat, hay 6
Oat, straw 3.5
Peanut 0.1
Peanut, hay 55
Peanut, refined oil 0.2
Peach subgroup 12-12B 0.5
Pear 0.5
Pepper/eggplant subgroup 8-10B 1
Plum subgroup 12-12C 0.5
Nut, tree, group 14-12 0.2
Rice, grain 0.02
Sheep, meat byproducts 0.15
Turnip greens 9
Wheat, forage 7
Wheat, grain 0.06
Wheat, hay 6
Wheat, straw 3.5

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

Table 3 to Paragraph (c)

Commodity Parts per million
Alfalfa, forage 6
Alfalfa, hay 20
Alfalfa, seed 0.9

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33699, May 24, 2000]

§ 180.378 Permethrin; tolerances for residues.

(a) General. Tolerances are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 20
Alfalfa, hay 45
Almond 0.05
Almond, hulls 20
Artichoke, globe 5.0
Arugula 50
Asparagus 2.0
Avocado 1.0
Broccoli 2.0
Brussels sprouts 1.0
Cabbage 6.0
Cattle, fat 1.5
Cattle, meat 0.10
Cattle, meat byproducts 0.10
Cauliflower 0.5
Celtuce 5
Cherry subgroup 12-12A 4
Corn, field, forage 50
Corn, field, stover 30
Corn, pop, stover 30
Corn, sweet, forage 50
Corn, sweet, stover 30
Cress, garden 50
Cress, upland 50
Dragon fruit 3
Egg 0.10
Eggplant 0.50
Fennel, Florence, fresh leaves and stalks 5
Field corn subgroup 15-22C 0.05
Fruit, pome, group 11 0.05
Garlic, bulb 0.10
Grain, aspirated fractions 0.50
Goat, fat 1.5
Goat, meat 0.10
Goat, meat byproducts 0.10
Hazelnut 0.05
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 1.5
Horse, meat 0.10
Horse, meat byproducts 0.10
Horseradish 0.50
Kiwifruit 2.0
Leaf petiole vegetable subgroup 22B 5
Leafy greens subgroup 4-16A 50
Milk, fat (reflecting 0.88 ppm in whole milk) 3.0
Mushroom 5.0
Onion, bulb 0.10
Peach subgroup 12-12B 2
Pepper, bell 0.50
Pepper, black 2 0.1
Pistachio 0.10
Poultry, fat 0.15
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Sheep, fat 1.5
Sheep, meat 0.10
Sheep, meat byproducts 0.10
Soybean, seed 0.05
Sweet corn subgroup 15-22D 0.1
Swiss chard 5
Tea, plucked leaves 1 20
Tomato 2.0
Vegetable, cucurbit, group 9 1.5
Vegetable, tuberous and corm, subgroup 1C 0.05
Walnut 0.05
Watercress 5.0
1 There are no United States registrations for use of permethrin on tea, plucked leaves as of July 28, 2020.
2 There are no United States registrations for use of permethrin on pepper, black as of August 3, 2026.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(l), are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

Commodity Parts per million
Collards 15
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2
Grass, forage 15
Grass, hay 15
Papaya 1.0
Turnip, tops 10
Turnip, roots 0.20

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52019, Sept. 12, 2007, as amended at 85 FR 45335, July 28, 2020; 91 FR 1400, Jan. 14, 2026; 91 FR 48775, Aug. 3, 2026]

§ 180.380 Vinclozolin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5-dichloroaniline moiety in or on the food commodities in the table below. There are no U.S. registrations for grape (wine) as of July 30, 1997.

Commodity Parts per million Expiration/Revocation Date
Bean, succulent 2.0 11/30/05
Canola, seed 1.0 11/30/08
Cattle, fat 0.05 11/30/08
Cattle, meat 0.05 11/30/08
Cattle, meat byproducts 0.05 11/30/08
Egg 0.05 11/30/08
Goat, fat 0.05 11/30/08
Goat, meat 0.05 11/30/08
Goat, meat byproducts 0.05 11/30/08
Grape, wine 6. 0 None
Hog, fat 0.05 11/30/08
Hog, meat 0.05 11/30/08
Hog, meat byproducts 0.05 11/30/08
Horse, fat 0.05 11/30/08
Horse, meat 0.05 11/30/08
Horse, meat byproducts 0.05 11/30/08
Lettuce, head 10.0 11/30/05
Lettuce, leaf 10.0 11/30/05
Milk 0.05 11/30/08
Poultry, fat 0.1 11/30/08
Poultry, meat 0.1 11/30/08
Poultry, meat byproducts 0.1 11/30/08
Sheep, fat 0.05 11/30/08
Sheep, meat 0.05 11/30/08
Sheep, meat byproducts 0.05 11/30/08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities with residues of vinclozolin resulting from lawful use are subject to the channels of trade provisions of section 408(l)(5) of the FFDCA:

Commodity Parts per million
Cucumber 1.0
Fruit, stone, except plum, prune, fresh 25.0
Pepper, bell 3.0
Strawberry 10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005]

§ 180.381 Oxyfluorfen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity Parts per million
Almond, hulls 0.1
Artichoke, globe 0.05
Avocado 0.05
Banana 0.05
Broccoli 0.05
Cabbage 0.05
Cacao bean, dried bean 0.05
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Cauliflower 0.05
Coffee, bean, green 0.05
Corn, field, grain 0.05
Cotton, undelinted seed 0.05
Date, dried fruit 0.05
Egg 0.03
Feijoa 0.05
Fig 0.05
Fruit, pome, group 11 0.05
Fruit, stone, group 12 0.05
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Grape 0.05
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Horseradish 0.05
Kiwifruit 0.05
Milk 0.01
Nut, tree, group 14 0.05
Olive 0.05
Onion, bulb 0.05
Peppermint, tops 0.05
Persimmon 0.05
Pistachio 0.05
Pomegranate 0.05
Poultry, fat 0.2
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01
Soybean 0.05
Spearmint, tops 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity Parts per million
Blackberry 0.05
Chickpea, seed 0.05
Grass, forage 0.05
Grass, hay 0.05
Grass, seed screenings 0.05
Guava 0.05
Papaya 0.05
Raspberry 0.05
Taro, corm 0.05
Taro, leaves 0.05

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 85022, Dec. 24, 1980]

§ 180.383 Sodium salt of acifluorfen; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen, sodium 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding acid, methyl ester, and amino analogues) in or on the following raw agricultural commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Berry, low growing, subgroup 13-07G 0.1
Peanut 0.1
Rice, grain 0.1
Soybean, seed 0.1
Soybean, vegetable, edible podded 0.09
Soybean, vegetable, succulent shelled 0.09

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide sodium salt of acifluorfen, including its metabolites and degradates, in or on the specified agricultural commodities in the following table, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of acifluorfen acid, (5-[2-chloro-4-(trifluoromethyl) phenoxy]-2-nitrobenzoate), acifluorfen amine methyl ester (methyl 5-[2-chloro-4(trifluoromethyl)phenoxy]-2-aminobenzoate), calculated as the stoichiometric equivalent of acifluorfen acid in or on the commodities. The tolerances expire on the date specified in the table.

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration
date
Beet, sugar, roots 0.1 12/31/2027
Beet, sugar, leaves 0.1 12/31/2027

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006; 80 FR 72598, Nov. 20, 2015; 87 FR 18722, Mar. 31, 2022; 88 FR 48388, July 27, 2023; 89 FR 85069, Oct. 25, 2024]

§ 180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator mepiquat, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only mepiquat, N,N-dimethylpiperidinium, in or on the commodity.

Commodity Parts
per million
Cattle, meat byproducts 0.1
Cotton, gin byproducts 6.0
Cotton, undelinted seed 2.0
Goat, meat byproducts 0.1
Grape 1.0
Grape, raisin 5.0
Hog, meat byproducts 0.1
Horse, meat byproducts 0.1
Sheep, meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 3118, Jan. 23, 2002, as amended at 80 FR 72598, Nov. 20, 2015]

§ 180.385 Diclofop-methyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoic acid and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agricultural commodities:

Commodity Parts per million
Barley, grain 0.1
Barley, straw 0.1
Wheat, grain 0.1
Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

§§ 180.388-180.389 [Reserved]

§ 180.390 Tebuthiuron; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity Parts per million
Grass, forage 10.0
Grass, hay 10.0

(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino-1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, fat 1.0
Cattle, meat 1.0
Cattle, meat byproducts 5.0
Goat, fat 1.0
Goat, meat 1.0
Goat, meat byproducts 5.0
Horse, fat 1.0
Horse, meat 1.0
Horse, meat byproducts 5.0
Sheep, fat 1.0
Sheep, meat 1.0
Sheep, meat byproducts 5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity Parts per million
Milk 0.8

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 53461, Sept. 19, 2007]

§ 180.395 Hydramethylnon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)hydrazone in or on the following raw agricultural commodities:

Commodity Parts per million
Grass, forage 2.0
Grass, hay 2.0
Pineapple 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug. 1, 2007]

§ 180.396 Hexazinone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant metabolites: metabolite A, 3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite D, 3-cyclohexyl-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity Parts per million
Alfalfa, forage 2.0
Alfalfa, hay 4.0
Alfalfa, seed 2.0
Blueberry 0.6
Grass, forage 250
Grass, hay 230
Pineapple 0.6
Sugarcane, cane 0.6
Sugarcane, molasses 4.0

(2) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its animal tissue metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.5
Cattle, meat byproducts 4.0
Goat, fat 0.1
Goat, meat 0.5
Goat, meat byproducts 4.0
Hog, fat 0.1
Hog, meat 0.5
Hog, meat byproducts 4.0
Horse, fat 0.1
Horse, meat 0.5
Horse, meat byproducts 4.0
Sheep, fat 0.1
Sheep, meat 0.5
Sheep, meat byproducts 4.0

(3) A tolerance is established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C-2, 3-(3-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity Parts per million
Milk 11

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, 2010]

§ 180.399 Iprodione; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide in or on the following food commodities:

Commodity Parts per million
Almond, hulls 2.0
Almond 0.3
Apricot 20.0
Bean, dry, seed 2.0
Bean, forage 90.0
Bean, succulent 2.0
Blueberry 15.0
Boysenberry 15.0
Broccoli 25.0
Caneberry subgroup 13A 25.0
Carrot, roots 5.0
Cherry, sweet, postharvest 20.0
Cherry, tart 20.0
Cotton, undelinted seed 0.10
Cowpea, hay 90.0
Currant 15.0
Garlic 0.1
Ginseng 2.0
Ginseng, dried root 4.0
Grape 60.0
Grape, raisin 300
Kiwifruit 10.0
Lettuce 25.0
Nectarine, postharvest 20.0
Onion, bulb 0.5
Peach, postharvest 20.0
Peanut 0.5
Peanut, hay 150.0
Plum, postharvest 20.0
Plum, prune 20.0
Potato 0.5
Raspberry 15.0
Rice, bran 30.0
Rice, grain 10.0
Rice, hulls 50.0
Strawberry 15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide] and [N-(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as iprodione equivalents in or on the following food commodities of animal origin:

Commodity Parts per million
Cattle, fat 0.5
Cattle, kidney 3.0
Cattle, liver 3.0
Cattle, meat 0.5
Cattle, meat byproducts, except kidney and liver 0.5
Egg 1.5
Goat, fat 0.5
Goat, kidney 3.0
Goat, liver 3.0
Goat, meat 0.5
Goat, meat byproducts, except kidney and liver 0.5
Hog, fat 0.5
Hog, kidney 3.0
Hog, liver 3.0
Hog, meat 0.5
Hog, meat byproducts, except kidney and liver 0.5
Horse, fat 0.5
Horse, kidney 3.0
Horse, liver 3.0
Horse, meat 0.5
Horse, meat byproducts, except kidney and liver 0.5
Milk 0.5
Poultry, fat 3.5
Poultry, liver 5.0
Poultry, meat 1.0
Poultry, meat byproducts, except liver 1.0
Sheep, fat 0.5
Sheep, kidney 3.0
Sheep, liver 3.0
Sheep, meat 0.5
Sheep, meat byproducts, except kidney and liver 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide], and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide] in or on the following food commodity:

Commodity Parts per million
Mustard greens 15.0

(d) Indirect or inadvertent residues. [Reserved]

[48 FR 40385, Sept. 7, 1983]

§ 180.401 Thiobencarb; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide thiobencarb, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only the sum of thiobencarb and its metabolites containing the chlorobenzyl or chlorophenyl moieties, calculated as the stoichiometric equivalent of thiobencarb, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Part per million
Cattle, fat 0.2
Cattle, meat byproducts 0.2
Cattle, meat 0.2
Celery 1 0.2
Egg 0.2
Endive 1 0.2
Goat, fat 0.2
Goat, meat byproducts 0.2
Goat, meat 0.2
Hog, fat 0.2
Hog, meat byproducts 0.2
Hog, meat 0.2
Horse, fat 0.2
Horse, meat byproducts 0.2
Horse, meat 0.2
Lettuce, head 1 0.2
Lettuce, leaf 1 0.2
Milk 0.05
Poultry, fat 0.2
Poultry, meat byproducts 0.2
Poultry, meat 0.2
Rice, grain 0.2
Sheep, fat 0.2
Sheep, meat byproducts 0.2
Sheep, meat 0.2
1 There are no U.S. registrations for this commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015; 91 FR 21389, Apr. 22, 2026]

§ 180.403 Thidiazuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenyl-N-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.4
Cattle, meat 0.4
Cattle, meat byproducts 0.4
Cotton, gin byproducts 24.0
Cotton, undelinted seed 0.3
Goat, fat 0.4
Goat, meat 0.4
Goat, meat byproducts 0.4
Hog, fat 0.4
Hog, meat 0.4
Hog, meat byproducts 0.4
Horse, fat 0.4
Horse, meat 0.4
Horse, meat byproducts 0.4
Milk 0.05
Sheep, fat 0.4
Sheep, meat 0.4
Sheep, meat byproducts 0.4

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

§ 180.404 Profenofos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2-chlorophenyl)-O-ethyl-S-propyl phosphorothioate) in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Cotton, gin byproducts 55.0
Cotton, undelinted seed 2.0
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Milk 0.01
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007]

§ 180.405 Chlorsulfuron; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5-hydroxy-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the following raw agricultural commodities:

Commodity Parts per million
Barley, grain 0.1
Barley, straw 0.5
Oat, forage 20.0
Oat, grain 0.1
Oat, straw 0.5
Wheat, forage 20.0
Wheat, grain 0.1
Wheat, straw 0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2- yl)aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities.

Commodity Parts per million
Cattle, fat 0.3
Cattle, meat 0.3
Cattle, meat byproducts 0.3
Goat, fat 0.3
Goat, meat 0.3
Goat, meat byproducts 0.3
Grass, forage 11.0
Grass, hay 19.0
Hog, fat 0.3
Hog, meat 0.3
Hog, meat byproducts 0.3
Horse, fat 0.3
Horse, meat 0.3
Horse, meat byproducts 0.3
Milk 0.1
Sheep, fat 0.3
Sheep, meat 0.3
Sheep, meat byproducts 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 52873, Aug. 14, 2002]

§ 180.407 Thiodicarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl N,N′-[thiobis[[(methylimino)carbonyloxy]] bis[ethanimidothioate]) and its metabolite methomyl (S-methyl N-[(methylcarbamoyl) oxy]thioacetimidate) in or on the following food commodities or groups. The time-limited tolerances expire and are revoked on the dates listed in the following table:

Table 1 to Paragraph (a)

Commodity Parts per million Expiration/revocation date
Broccoli 7.0 January 19, 2024.
Cabbage 7.0 January 19, 2024.
Cauliflower 7.0 January 19, 2024.
Corn, sweet, kernel plus cob with husks removed 2.0 January 19, 2024.
Cotton, undelinted seed 0.4 None
Soybean, hulls 0.8 None
Soybean 0.2 None
Vegetable, leafy, except brassica, group 4 35 January 19, 2024.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 44595, Aug. 22, 1997, as amended at 75 FR 60245, Sept. 29, 2010; 88 FR 46083, July 19, 2023]

§ 180.408 Metalaxyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [N-(2,6-dmethylphyenyl)-N-(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methylphenyl)-N-(methoxyacetyl)-alanine methyl ester, each expressed as metalaxyl equivalents, in or on the following food commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 6.0
Alfalfa, hay 20.0
Almond 0.5
Almond, hulls 10.0
Apple 0.2
Apple, wet pomace 0.4
Apricot, dried 4.0
Asparagus 7.0
Avocado 4.0
Beet, garden, roots 0.1
Beet, garden, tops 0.1
Beet, sugar 0.1
Beet, sugar, molasses 1.0
Beet, sugar, roots 0.5
Beet, sugar, tops 10.0
Blueberry 2.0
Broccoli 2.0
Brussels sprouts 2.0
Cabbage 1.0
Cattle, fat 0.4
Cattle, kidney 0.4
Cattle, liver 0.4
Cattle, meat 0.05
Cattle, meat byproducts, except kidney and liver 0.05
Cauliflower 1.0
Citrus, oil 7.0
Citrus, dried pulp 7.0
Clover, forage 1.0
Clover, hay 2.5
Cotton, undelinted seed 0.1
Cranberry 4.0
Egg 0.05
Fruit, citrus 1.0
Fruit, stone, group 12 1.0
Ginseng 3.0
Goat, fat 0.4
Goat, kidney 0.4
Goat, liver 0.4
Goat, meat 0.05
Goat, meat byproducts, except kidney and liver 0.05
Grain, cereal, group 15, except barley, oat and wheat 0.1
Grain, crop 0.1
Grape 2.0
Grape, raisin 6.0
Grass, forage 10.0
Grass, hay 25.0
Hog, fat 0.4
Hog, kidney 0.4
Hog, liver 0.4
Hog, meat 0.05
Hog, meat byproducts, except kidney and liver 0.05
Hop, dried cones 20
Hop, vines 2.0
Horse, fat 0.4
Horse, kidney 0.4
Horse, liver 0.4
Horse, meat 0.05
Horse, meat byproducts, except kidney and liver 0.05
Lettuce, head 5.0
Milk 0.02
Mustard greens 5.0
Onion, bulb 3.0
Onion, green 10.0
Peanut 0.2
Peanut, hay 20.0
Peanut, meal 1.0
Peanut, hulls 2.0
Pepper, black 1 0.3
Pineapple 0.1
Pineapple, fodder 0.1
Pineapple, forage 0.1
Plum, prune, dried 4.0
Potato, chips 4.0
Potato, granules, flakes 4.0
Potato, processed potato waste 4.0
Potato, wet peel 4.0
Poultry, fat 0.4
Poultry, kidney 0.4
Poultry, liver 0.4
Poultry, meat 0.05
Poultry, meat byproducts, except kidney and liver 0.05
Potato 0.5
Raspberry 0.5
Sheep, fat 0.4
Sheep, kidney 0.4
Sheep, liver 0.4
Sheep, meat 0.05
Sheep, meat byproducts, except kidney and liver 0.05
Soybean, hulls 2.0
Soybean, meal 2.0
Soybean, seed 1.0
Spinach 10.0
Strawberry 10.0
Sunflower, seed 0.1
Sunflower, forage 0.1
Tomato, paste 3.0
Tomato, puree 3.0
Vegetable, brassica, leafy, group 5, except broccoli, cabbage, cauliflower, brussels sprouts, and mustard greens 0.1
Vegetable, cucurbit, group 9 1.0
Vegetable, foilage of legume, group 7 8.0
Vegetable, fruiting, group 8 1.0
Vegetable, leafy, except brassica, group 4, except spinach 5.0
Vegetable, leaves of root and tuber, group 2 15.0
Vegetable, legume, cannery waste 5.0
Vegetable, legume, group 6 0.2
Vegetable, root and tuber, group 1 0.5
Walnut 0.5
1 There are no U.S. registrations for use of this pesticide on this commodity as of September 24, 2021.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration (refer to § 180.1(m)) are established for the combined residues of the fungicide metalaxyl [N-(2,6-dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N-(methoxyacetyl)-alanine methylester, each expressed as metalaxyl, in or on the following raw agricultural commodity:

Commodity Parts per million
Papaya 0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of metalaxyl in or on the food commodities when present therein as a result of the application of metalaxyl to growing crops listed in paragraph (a) of this section and other non-food crops to read as follows:

Commodity Part per million
Barley, bran 1.0
Barley, flour 1.0
Barley, grain 0.2
Barley, pearled barley 1.0
Barley, straw 2.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage 1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; stover 1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; straw 1.0
Oat, flour 1.0
Oat, forage 2.0
Oat, grain 0.2
Oat, groats, rolled oats 1.0
Oat, straw 2.0
Wheat, bran 1.0
Wheat, flour 1.0
Wheat, forage 2.0
Wheat, germ 1.0
Wheat, grain 0.2
Wheat, middlings 1.0
Wheat, shorts 1.0
Wheat, straw 2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, 2009; 75 FR 56015, Sept. 15, 2010; 86 FR 53009, Sept. 24, 2021]

§ 180.409 Pirimiphos-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2-diethylamino-6-methyl-4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, fat 0.02
Cattle, meat byproducts 0.02
Corn, field, grain 8.0
Corn, pop, grain 8.0
Goat, fat 0.02
Goat, meat byproducts 0.02
Grain, aspirated fractions 20.0
Hog, fat 0.02
Hog, meat byproducts 0.02
Horse, fat 0.02
Horse, meat byproducts 0.02
Poultry, fat 0.02
Sheep, fat 0.02
Sheep, meat byproducts 0.02
Sorghum, grain, grain 8.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Sept. 19, 2007]

§ 180.410 Triadimefon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date
Pineapple 2.0 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 76 FR 34885, June 15, 2011]

§ 180.411 Fluazifop-P-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fluazifop-P-butyl, butyl (2R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 is to be determined by measuring only those fluazifop-P-butyl residues convertible to fluazifop, 2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, expressed as fluazifop, in or on the commodity”.

Table 1 to Paragraph (a)

Commodity Parts per
million
Banana 0.01
Beans, dry, seed 50
Beet, sugar, dried pulp 1.0
Beet, sugar, molasses 3.5
Beet, sugar, roots 0.25
Berry, low growing, subgroup 13-07G 3
Brassica, leafy greens, subgroup 4-16B 15
Bushberry subgroup 13-07B 0.30
Caneberry subgroup 13-07A 0.08
Carrot, roots 2.0
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Chives, dried leaves 40
Chives, fresh leaves 4
Citrus, dried pulp 0.40
Citrus, juice 0.06
Citrus, oil 30.0
Cotton, gin byproducts 1.5
Cotton, refined oil 1.3
Cotton, undelinted seed 1.0
Egg 0.05
Endive 6.0
Fruit, citrus, group 10 2 0.03
Fruit, citrus, group 10-10 0.01
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.03
Fruit, stone 2 0.05
Fruit, stone, group 12-12 0.01
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Leaf petiole vegetable subgroup 22B 3
Lettuce, head 3.0
Lettuce, leaf 5.0
Milk 0.05
Nut, macadamia 0.1
Onion, bulb, subgroup 3-07A 0.50
Onion, green, subgroup 3-07B 1.5
Papaya 0.01
Peanut 1.5
Peanut, meal 2.2
Pecans 0.05
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Potato 1 1.0
Potato, chips 1 2.0
Potato, granules/flakes 1 4.0
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Soybean, seed 2.5
Vegetable, Brassica, head and stem, group 5-16 30
Vegetable, tuberous and corm, except potato, subgroup 1D 1.5
1 No U.S. registrations.
2 This tolerance expires on June 26, 2023.

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of the herbicide fluazifop-P-butyl, butyl (2R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (c). Compliance with the tolerance levels specified in table 2 is to be determined by measuring only those fluazifop-P-butyl residues convertible to fluazifop, 2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, expressed as fluazifop, in or on the commodity”.

Table 2 to Paragraph (c)

Commodity Parts per
million
Asparagus 3.0
Coffee, bean 0.1
Fescue, forage 4.0
Fescue, hay 15
Pepper, tabasco 1.0

(d) Indirect or inadvertent residues. Tolerances are established for residues of the herbicide fluazifop-P-butyl, butyl (2R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, including its metabolites and degradates, in or on the commodities in table 3 to this paragraph (d). Compliance with the tolerance levels specified in table 3 is to be determined by measuring only those fluazifop-P-butyl residues convertible to 5-trifluoromethyl-2-pyridinone (TFP), expressed as TFP, in or on the commodity.

Table 3 to Paragraph (d)

Commodity Parts per
million
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.015

[88 FR 25506, Apr. 27, 2023]

§ 180.412 Sethoxydim; tolerances for residues.

(a) Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No. 74051-80-2) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Alfalfa, forage 40
Alfalfa, hay 40
Almond, hulls 2.0
Apricot 0.2
Apple, wet pomace 0.8
Asparagus 4.0
Basil, dried leaves 20
Basil, fresh leaves 8
Bean, succulent 15
Beet, sugar, molasses 10
Beet, sugar, tops 3.0
Berry, low growing, subgroup 13-07H, except strawberry 2.5
Borage, meal 40
Buckwheat, flour 25
Buckwheat, grain 19
Bushberry subgroup 13-07B 4.0
Calendula, meal 20
Caneberry subgroup 13-07A 5.0
Canola, meal 40
Castor oil plant, meal 20
Cattle, fat 0.2
Cattle, meat 0.2
Cattle, meat byproducts 1.0
Cherry, sweet 0.2
Cherry, tart 0.2
Chinese tallowtree, meal 20
Citrus, dried pulp 1.5
Clover, forage 35
Clover, hay 55
Coriander, leaves 4.0
Corn, field, forage 2.0
Corn, field, grain 0.5
Corn, field, stover 2.5
Corn, sweet, forage 3.0
Corn, sweet, kernel plus cob with husk removed 0.4
Corn, sweet, stover 3.5
Cottonseed subgroup 20C 5.0
Cowpea, forage 15
Cowpea, hay 50
Crambe, meal 40
Cuphea, meal 40
Dillweed, fresh leaves 10
Echium, meal 40
Egg 2.0
Euphorbia, meal 20
Evening primrose, meal 20
Flax seed, meal 40
Fruit, citrus, group 10-10 0.5
Fruit, pome, group 11-10 0.2
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0
Goat, fat 0.2
Goat, meat 0.2
Goat, meat byproducts 1.0
Gold of pleasure, meal 40
Grape, raisin 2.0
Hare's ear mustard, meal 40
Hog, fat 0.2
Hog, meat 0.2
Hog, meat byproducts 1.0
Horse, fat 0.2
Horse, meat 0.2
Horse, meat byproducts 1.0
Jojoba, meal 20
Juneberry 1 5.0
Lesquerella, meal 40
Lingonberry 1 5.0
Lunaria, meal 40
Meadowfoam, meal 40
Milk 0.5
Milkweed, meal 40
Mustard, meal 40
Nectarine 0.2
Niger seed, meal 20
Nut, tree, group 14 0.2
Oil radish, meal 40
Pea and bean, dried shelled, except soybean, subgroup 6C 25
Pea, field, hay 40
Pea, field, vines 20
Pea, succulent 10
Peach 0.2
Peanut 25
Peppermint, tops 30
Pistachio 0.2
Poppy seed, meal 40
Potato granules/flakes 8.0
Potato waste, processed 8.0
Poultry, fat 0.2
Poultry, meat 0.2
Poultry, meat byproducts 2.0
Radish, tops 4.5
Rapeseed, meal 40
Rapeseed subgroup 20A 35
Rose hip, meal 20
Safflower, seed 15
Salal 1 5.0
Sesame, meal 40
Sheep, fat 0.2
Sheep, meat 0.2
Sheep, meat byproducts 1.0
Soybean, hay 10
Soybean, seed 16
Spearmint, tops 30
Strawberry 10
Stokes aster, meal 20
Sunflower, meal 20
Sunflower subgroup 20B, except safflower 7.0
Sweet rocket, meal 40
Tallowwood, meal 20
Tea oil plant, meal 20
Turnip, tops 5.0
Vegetable, brassica, leafy, group 5 5.0
Vegetable, bulb, group 3-07 1.0
Vegetable, cucurbit, group 9 4.0
Vegetable, fruiting, group 8-10 4.0
Vegetable, leafy, except brassica, group 4 4.0
Vegetable, root and tuber, group 1 4.0
Vernonia, meal 20
1 The individual tolerances for Juneberry, Lingonberry, and Salal expire on December 15, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

Commodity Parts per
million
Artichoke, globe 5.0
Fescue, forage 7.0
Fescue, hay 4.0
Rhubarb 0.3

(d) Indirect and inadvertent residues. [Reserved]

[80 FR 34077, June 15, 2015, as amended at 85 FR 78002, Dec. 3, 2020]

§ 180.413 Imazalil; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1H-imidazole-1-yl)-1-ethanol, in or on the following food commodities:

Commodity Parts per million
Banana 3.0
Barley, grain 0.1
Barley, hay 0.5
Barley, straw 0.5
Citrus, dried pulp 25.0
Citrus, oil 200.0
Fruit, citrus, postharvest 10.0
Wheat, forage 0.5
Wheat, grain 0.1
Wheat, hay 0.5
Wheat, straw 0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2-(2,3-dihydroxypropoxy)ethyl]-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]-2,4-imidazolidinedione (FK284), in or on the following food commodities:

Commodity Parts per million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.2
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.2
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.2
Milk 0.02
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

§ 180.414 Cyromazine; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Bean, dry, except cowpea 3
Bean, lima 1
Bean, succulent 2
Brassica, leafy greens, subgroup 4-16B 35
Broccoli 1
Cattle, fat 0.05
Cattle, meat 0.3
Cattle, meat byproducts 0.3
Celtuce 10
Chickpea, edible podded 0.4
Chickpea, succulent shelled 0.3
Dwarf pea, edible podded 0.4
Edible podded pea, edible podded 0.4
Egg 0.3
English pea, succulent shelled 0.3
Fennel, Florence, fresh leaves and stalk 10
Garden pea, succulent shelled 0.3
Goat, fat 0.05
Goat, meat 0.3
Goat, meat byproducts 0.3
Grass-pea, edible podded 0.4
Green pea, edible podded 0.4
Green pea, succulent shelled 0.3
Hog, fat 0.05
Hog, meat 0.3
Hog, meat byproducts 0.3
Horse, fat 0.05
Horse, meat 0.3
Horse, meat byproducts 0.3
Kohlrabi 35
Leaf petiole vegetable subgroup 22B 10
Leafy greens subgroup 4-16A 10
Lentil, edible podded 0.4
Lentil, succulent shelled 0.3
Mango 1 0.5
Milk 0.1
Mushroom 8
Onion, bulb, subgroup 3-07A 0.3
Onion, green, subgroup 3-07B 3
Pepper/eggplant subgroup 8-10B 3
Pigeon pea, edible podded 0.4
Pigeon pea, succulent shelled 0.3
Poultry, fat (from chicken layer hens and chicken breeder hens only) 0.05
Poultry, meat (from chicken layer hens and chicken breeder hens only) 0.1
Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) 0.2
Sheep, fat 0.05
Sheep, meat 0.3
Sheep, meat byproducts 0.3
Snap pea, edible podded 0.4
Snow pea, edible podded 0.4
Sugar snap pea, edible podded 0.4
Tomato subgroup 8-10A 1
Vegetable, brassica, head and stem, group 5-16, except broccoli 35
Vegetable, cucurbit, group 9 2
Vegetable, tuberous and corm, subgroup 1C 0.8
1 There are no U.S. registrations on mango as of May 4, 2000.
2 This tolerance expires on April 7, 2020.

(2) A tolerance of 5.0 parts per million is established for residues of the insecticide cyromazine, including its metabolites and degradates, in or on poultry feed when used as a feed additive only in feed for chicken layer hens and chicken breeder hens at the rate of not more than 0.01 pound of cyromazine per ton of poultry feed for control of flies in manure of treated chicken layer hens and chicken breeder hens, provided the feeding of cyromazine-treated feed must stop at least 3 days (72 hours) before slaughter. If the feed is formulated by any person other than the end user, the formulator must inform the end user, in writing, of the 3-day (72 hours) pre-slaughter interval. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues.

(1) Tolerances are established for indirect or inadvertent residues of the insecticide cyromazine, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (d)(1) when present therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of this section. Compliance with the tolerance levels specified in this paragraph (d)(1) is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

Table 2 to Paragraph (d)(1)

Commodity Parts per million
Cotton, undelinted seed 0.1
Corn, sweet, kernel plus cob with husks removed 0.5
Corn, sweet, forage 0.5
Corn, sweet, stover 0.5
Radish, roots 0.5
Radish, tops 0.5

(2) Tolerances are established for indirect or inadvertent residues of the insecticide cyromazine, including its metabolites and degradates, in or on the commodities in the table 3 to this paragraph (d)(2) when present therein as a result of the application of poultry manure-based fertilizer containing cyromazine to soil in which the crops identified in this section are grown. Compliance with the tolerance levels specified in this paragraph (d)(2) is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

Table 3 to Paragraph (d)(2)

Commodity Parts per million
Grain, cereal, forage, fodder and straw, group 16 0.6
Grain, cereal, group 15 0.6
Herbs and spices, group 19 0.6
Oilseed, group 20 0.6
Onion, bulb, subgroup 3-07A 0.6
Strawberry 0.6
Vegetable, foliage of legume, group 7 0.6
Vegetable, fruiting, group 8-10 0.6
Vegetable, leaves of root and tuber, group 2 0.6
Vegetable, legume, group 6 0.6
Vegetable, root and tuber, group 1 0.6

[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Apr. 27, 2011; 84 FR 53322, Oct. 7, 2019; 88 FR 46084, July 19, 2023; 88 FR 56772, Aug. 21, 2023]

§ 180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Avocado 25
Banana 3.0
Bushberry subgroup 13-07B 40
Caneberry subgroup 13-07A 0.1
Cranberry 0.5
Fruit, citrus, group 10-10 9.0
Fruit, pome, group 11-10 10
Ginseng 0.05
Ginseng 2 0.1
Hop, dried cones 45
Juneberry 40
Lingonberry 40
Nut, macadamia 0.20
Onion, bulb 0.5
Onion, green 10.0
Pea, succulent 0.3
Pepper/eggplant, subgroup 8-10B1 0.01
Pineapple 0.1
Salal 40
Strawberry 75
Tomato 3
Turnip, greens 40
Turnip, roots 15
Vegetable, brassica, leafy, group 5 60
Vegetable, cucurbit, group 9 15
Vegetable, leafy, except brassica, group 4 100
1 There are no US registrations as of December 23, 2014.
2 This tolerance expires on January 19, 2024.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Commodity Parts per million
Asparagus 0.1
Grape 10

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015; 83 FR 12265, Mar. 21, 2018; 88 FR 46085, July 19, 2023; 88 FR 56773, Aug. 21, 2023]

§ 180.416 Ethalfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide ethalfluralin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the residues of ethalfluralin, N-ethyl-N-(2-methyl-2-propenyl)-2,6-dinitro-4-(trifluoromethyl)benzenamine.

Table 1 to Paragraph (a)

Commodity Parts per
million
Dill, dried leaves 0.05
Dill, fresh leaves 0.05
Hemp, seed 0.05
Onion, bulb, subgroup 3-07A 0.01
Peanut 0.05
Rapeseed subgroup 20A 0.05
Soybean 0.05
Stevia, dried leaves 0.05
Stevia, fresh leaves 0.05
Sunflower subgroup 20B 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.05
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.05
Vegetable, tuberous and corm, subgroup 1C 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, 2013; 85 FR 45341, July 28, 2020; 88 FR 21111, Apr. 10, 2023]

§ 180.417 Triclopyr; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide triclopyr, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1) resulting from the application of the butoxyethyl ester of triclopyr, triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified in table 1 to this paragraph (a)(1) is to be determined by measuring only triclopyr, 2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Egg 0.05
Grass, forage, fodder and hay, group 17, forage 700
Grass, forage, fodder and hay, group 17, hay 200
Milk 0.6
Orange subgroup 10-10A 1 0.1
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts, except kidney 0.1
Rice, grain 0.3
Sugarcane, cane 0.04
1 There are no U.S. registrations.

(2) Tolerances are established for residues of the herbicide triclopyr, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (a)(2) resulting from the application of the butoxyethyl ester of triclopyr, triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified in table 2 to this paragraph (a)(2) is to be determined by measuring the combined residues of triclopyr, 2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid, and its metabolite 3,5,6-trichloro-2-pyridinol (TCP), calculated as the stoichiometric equivalent of triclopyr in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.5
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.5
Hog, fat 0.1
Hog, meat 0.1
Hog, meat byproducts 0.5
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.5
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.5

(3) Tolerances are established for residues of the herbicide triclopyr, including its metabolites and degradates, in or on the commodities in table 3 to this paragraph (a)(3) resulting from the application of the butoxyethyl ester of triclopyr, triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified in table 3 to this paragraph (a)(3) is to be determined by measuring the combined residues of triclopyr (2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid) and its metabolites 3,5,6-trichloro-2-pyridinol (TCP) and 2-methoxy-3,5,6-trichloropyridine (TMP), calculated as the stoichiometric equivalent of triclopyr in or on the commodity.

Table 3 to Paragraph (a)(3)

Commodity Parts per million
Fish, freshwater, finfish 3
Fish, shellfish, crustacean 3.5
Fish, shellfish, mollusc 3.5

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the triclopyr (2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid), including its metabolites and degradates in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire on the date specified in the table.

Table 3 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation date
Sugarcane, cane 40 12/31/26

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[50 FR 18486, May 1, 1985, as amended at 55 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, 1995; 62 FR 46894, Sept. 5, 1997; 63 FR 45406, Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007; 80 FR 72599, Nov. 20, 2015; 81 FR 9359, Feb. 25, 2016; 82 FR 26603, June 8, 2017; 86 FR 8703, Feb. 9, 2021; 88 FR 75506, Nov. 3, 2023; 89 FR 14594, Feb. 28, 2024; 90 FR 31893, July 16, 2025; 91 FR 8107, Feb. 20, 2026]

§ 180.418 Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of cypermethrin, (±)alpha cyano-(3-phenoxyphenyl)methyl (±)cis,trans-3(2,2-dichloroethenyl-2,2-dimethylcyclopropanecarboxylate, including its metabolites and degradates, in or on the commodities in table 1 to paragraph (a). Compliance with the tolerance levels specified in the following table is to be determined by measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts
per million
Allspice 1 0.5
Angelica, seed 1 0.2
Anise pepper 1 0.5
Asafoetida 1 0.2
Ashwagandha fruit 1 0.5
Batavia-casia, fruit 1 0.5
Belleric myrobalan 1 0.5
Brassica, head and stem, subgroup 5A 2.0
Brassica, leafy greens, subgroup 5B 14.0
Calamus-root 1 0.2
Caper buds 1 0.5
Cardamom, black 1 0.5
Cardamom, Ethiopian 1 0.5
Cardamom, green 1 0.5
Cardamom, Nepal 1 0.5
Cardamom-amomum 1 0.5
Cassia, fruit 1 0.5
Cassia, Chinese, fruit 1 0.5
Cattle, fat 1.0
Cattle, meat 0.2
Cattle, meat byproducts 0.05
Chaste tree, Chinese, roots 1 0.2
Chinese hawthorne 1 0.5
Chinese-pepper 1 0.5
Cinnamon, fruit 1 0.5
Cinnamon, Saigon, fruit 1 0.5
Coptis 1 0.2
Coriander, fruit 1 0.5
Coriander, seed 1 0.2
Cotton, gin byproducts 11.0
Cotton, undelinted seed 0.5
Cumin, black 1 0.5
Dorrigo pepper, berry 1 0.5
Dorrigo pepper, leaf 1 0.5
Durian1 1
Egg 0.05
Eucalyptus 1 0.5
Fingerroot 1 0.2
Gamboge 1 0.5
Grains of Selim 1 0.5
Goat, fat 1.0
Goat, meat 0.2
Goat, meat byproducts 0.05
Hog, fat 0.1
Hog, meat 0.05
Horse, fat 1.0
Horse, meat 0.2
Horse, meat byproducts 0.05
Jalap 1 0.2
Juniper, berry 1 0.5
Lettuce, head 4.0
Lovage, root 1 0.2
Lovage, seed 1 0.2
Milk, fat (reflecting 0.10 in whole milk) 2.5
Miracle fruit 1 0.5
Onion, bulb 0.1
Onion, green 6.0
Pecan 0.05
Pepper, black 1 0.5
Pepper, Indian long 1 0.5
Pepper, Javanese, long 1 0.5
Pepper, pink 1 0.5
Pepper, Sichuan 1 0.5
Pepper, white 1 0.5
Pepperbush berry 1 0.5
Pepperbush leaf 1 0.5
Peppercorn, green 1 0.5
Peppertree 1 0.5
Peppertree, Peruvian 1 0.5
Poultry, fat 0.05
Poultry, meat 0.05
Saunders, red 1 0.5
Sheep, fat 1.0
Sheep, meat 0.2
Sheep, meat byproducts 0.05
Sumac, fragrant 1 0.5
Sumac, smooth, leaf 1 0.5
Tamarind, seed 1 0.5
Tasmanian, pepper, berry 1 0.5
Tea, dried 1 15
Tsaoko 1 0.5
Vanilla 1 0.5
Yellow gentian, roots 1 0.2
1 There are no U.S. registrations as of July 17, 2025.

(2) Tolerances are established for residues of zeta-cypermethrin, (S-cyano(3-phenoxyphenyl) methyl (±))(cis-trans 3-(2,2-dichloroethenyl)-2,2 dimethylcyclopropanecarboxylate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Alfalfa, forage 15
Alfalfa, hay 30
Alfalfa, seed 0.50
Almond, hulls 6
Animal feed, nongrass, group 18, forage 8
Animal feed, nongrass, group 18, hay 40
Artichoke, globe 0.60
Avocado 0.50
Barley, grain 3.0
Barley, hay 6.0
Barley, straw 20.0
Basil, dried leaves 40
Basil, fresh leaves 7
Bean, adzuki, dry seed 0.05
Bean, American potato, dry seed 0.05
Bean, asparagus, dry seed 0.05
Bean, asparagus, edible podded 0.7
Bean, black, dry seed 0.05
Bean, broad, dry seed 0.05
Bean, broad, succulent shelled 0.1
Bean, catjang, dry seed 0.05
Bean, catjang, edible podded 0.7
Bean, catjang, succulent shelled 0.1
Bean, cranberry, dry seed 0.05
Bean, dry, dry seed 0.05
Bean, field, dry seed 0.05
Bean, French, dry seed 0.05
Bean, French, edible podded 0.7
Bean, garden, dry seed 0.05
Bean, garden, edible podded 0.7
Bean, goa, dry seed 0.05
Bean, goa, edible podded 0.7
Bean, goa, succulent shelled 0.1
Bean, great northern, dry seed 0.05
Bean, green, dry seed 0.05
Bean, green, edible podded 0.7
Bean, guar, dry seed 0.05
Bean, guar, edible podded 0.7
Bean, kidney, dry seed 0.05
Bean, kidney, edible podded 0.7
Bean, lablab, dry seed 0.05
Bean, lablab, edible podded 0.7
Bean, lablab, succulent shelled 0.1
Bean, lima, dry seed 0.05
Bean, lima, succulent shelled 0.1
Bean, morama, dry seed 0.05
Bean, moth, dry seed 0.05
Bean, moth, edible podded 0.7
Bean, moth, succulent shelled 0.1
Bean, mung, dry seed 0.05
Bean, mung, edible podded 0.7
Bean, navy, dry seed 0.05
Bean, navy, edible podded 0.7
Bean, pink, dry seed 0.05
Bean, pinto, dry seed 0.05
Bean, red, dry seed 0.05
Bean, rice, dry seed 0.05
Bean, rice, edible podded 0.7
Bean, scarlet runner, dry seed 0.05
Bean, scarlet runner, edible podded 0.7
Bean, scarlet runner, succulent shelled 0.1
Bean, snap, edible podded 0.7
Bean, sword, dry seed 0.05
Bean, sword, edible podded 0.7
Bean, tepary, dry seed 0.05
Bean, urd, dry seed 0.05
Bean, urd, edible podded 0.7
Bean, wax, edible podded 0.7
Bean, wax, succulent shelled 0.1
Bean, yardlong, dry seed 0.05
Bean, yardlong, edible podded 0.7
Bean, yellow, dry seed 0.05
Beet, sugar, roots 0.05
Beet, sugar, tops 0.20
Brassica, leafy greens, subgroup 4-16B 14
Buckwheat, grain 3.0
Buckwheat, hay 6.0
Buckwheat, straw 20.0
Bushberry subgroup 13-07B 0.8
Caneberry subgroup 13-07A 0.8
Canistel 0.50
Castor oil plant, refined oil 0.4
Cattle, fat 1.00
Cattle, meat 0.2
Cattle, meat byproducts 0.05
Celtuce 10
Chickpea, dry seed 0.05
Chickpea, edible podded 0.7
Chickpea, succulent shelled 0.1
Chinese tallowtree, refined oil 0.4
Citrus, dried pulp 1.8
Citrus, oil 4.0
Corn, field, forage 9.0
Corn, field, grain 0.05
Corn, field, stover 30
Corn, pop, grain 0.05
Corn, pop, stover 30
Corn, sweet, forage 15.00
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 15.00
Cottonseed subgroup 20C 0.5
Cowpea, dry seed 0.05
Cowpea, edible podded 0.7
Cowpea, succulent shelled 0.1
Egg 0.05
Euphorbia, refined oil 0.4
Evening primrose, refined oil 0.4
Fennel, Florence, fresh leaves and stalk 10
Food commodities/feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling establishments 0.05
Fruit, citrus, group 10 1 0.35
Fruit, pome, group 11-10 2
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2
Fruit, stone, group 12-12 2
Goat, fat 1.00
Goat, meat 0.2
Goat, meat byproducts 0.05
Grain, aspirated fractions 10.0
Gram, horse, dry seed 0.05
Grapefruit subgroup 10-10C 0.5
Grass, forage, fodder, and hay, group 17, forage 10
Grass, forage, fodder and hay, group 17, hay 35
Grass pea, dry seed 0.05
Grass pea, edible podded 0.7
Hog, fat 0.1
Hog, meat 0.05
Horse, fat 1.00
Horse, meat 0.2
Horse, meat byproducts 0.05
Jackbean, dry seed 0.05
Jackbean, edible podded 0.7
Jackbean, succulent shelled 0.1
Jojoba, refined oil 0.4
Kohlrabi 2
Leaf petiole vegetable subgroup 22B 10
Leafy greens subgroup 4-16A 10
Lemon/Lime subgroup 10-10B 0.3
Lentil, dry seed 0.05
Lentil, edible podded 0.7
Lentil, succulent shelled 0.1
Longbean, Chinese, dry seed 0.05
Longbean, Chinese, edible podded 0.7
Lupin, Andean, dry seed 0.05
Lupin, Andean, succulent shelled 0.1
Lupin, blue, dry seed 0.05
Lupin, blue, succulent shelled 0.1
Lupin, grain, dry seed 0.05
Lupin, grain, succulent shelled 0.1
Lupin, sweet white, dry seed 0.05
Lupin, sweet white, succulent shelled 0.1
Lupin, sweet, dry seed 0.05
Lupin, sweet, succulent shelled 0.1
Lupin, white, dry seed 0.05
Lupin, white, succulent shelled 0.1
Lupin, yellow, dry seed 0.05
Lupin, yellow, succulent shelled 0.1
Mango 0.70
Milk, fat (reflecting 0.10 in whole milk) 2.50
Niger seed, refined oil 0.4
Nut, tree, group 14-12 0.05
Oat, grain 3.0
Oat, hay 6.0
Oat, straw 20.0
Onion, bulb, subgroup 3-07A 0.1
Onion, green, subgroup 3-07B 3
Orange subgroup 10-10A 0.3
Papaya 0.50
Pea, blackeyed, dry seed 0.05
Pea, blackeyed, succulent shelled 0.1
Pea, crowder, dry seed 0.05
Pea, crowder, succulent shelled 0.1
Pea, dry, dry seed 0.05
Pea, dwarf, edible podded 0.7
Pea, English, succulent shelled 0.1
Pea, field, dry seed 0.05
Pea, garden, dry seed 0.05
Pea, garden, succulent shelled 0.1
Pea, green, dry seed 0.05
Pea, green, edible podded 0.7
Pea, green, succulent shelled 0.1
Pea, pigeon, dry seed 0.05
Pea, pigeon, edible podded 0.7
Pea, pigeon, succulent shelled 0.1
Pea, snap, edible podded 0.7
Pea, snow, edible podded 0.7
Pea, southern, dry seed 0.05
Pea, southern, succulent shelled 0.1
Pea, sugar snap, edible podded 0.7
Pea, winged, dry seed 0.05
Pea, winged, edible podded 0.7
Peanut 0.05
Poultry, fat 0.05
Poultry, meat 0.05
Quinoa, grain 3
Quinoa, hay 6
Quinoa, straw 20
Rapeseed subgroup 20A 0.2
Rice, grain 1.50
Rice, hulls 6.00
Rice, wild, grain 1.5
Rose hip, refined oil 0.4
Rye, grain 3.0
Rye, hay 6.0
Rye, straw 20.0
Sapodilla 0.50
Sapote, black 0.50
Sapote, mamey 0.50
Sheep, fat 1.00
Sheep, meat 0.2
Sheep, meat byproducts 0.05
Sorghum, grain, forage 0.1
Sorghum, grain, grain 0.5
Sorghum, grain, stover 5.0
Soybean, seed 0.05
Soybean, vegetable, dry seed 0.05
Soybean, vegetable, edible podded 0.7
Soybean, vegetable, succulent shelled 0.1
Star apple 0.50
Stokes aster, refined oil 0.4
Sugarcane, cane 0.60
Sunflower subgroup 20B 0.2
Sunflower, refined oil 0.5
Tallowwood, refined oil 0.4
Tea oil plant, refined oil 0.4
Teff, forage 3
Teff, grain 0.3
Teff, hay 6
Teff, straw 7
Vegetable, brassica, head and stem, group 5-16 2
Vegetable, cucurbit, group 9 0.2
Vegetable, fruiting, group 8-10 0.2
Vegetable, root and tuber, group 1, except sugar beet 0.1
Velvetbean, dry seed 0.05
Velvetbean, edible podded 0.7
Velvetbean, succulent shelled 0.1
Vernonia, refined oil 0.4
Wheat, forage 3.0
Wheat, grain 0.2
Wheat, hay 6.0
Wheat, straw 7.0
Yam bean, African, dry seed 0.05
1 This tolerance expires on February 4, 2022.

(3) Tolerances are established for residues of the insecticide, alpha-cypermethrin, (R)-cyano(3-phenoxyphenyl)methyl (1S,3S)-rel-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, in or on the commodity.

Table 3 to Paragraph (a)(3)

Commodity Parts per million
Alfalfa, hay 15
Beet, sugar, roots 0.05
Beet, sugar, tops 0.20
Brassica, head and stem, subgroup 5A 2.0
Cattle, fat 1.0
Cattle, meat 0.20
Cattle, meat byproducts 0.05
Citrus, dried pulp 1.8
Citrus, oil 4.0
Corn, field, grain 0.05
Corn, pop, grain 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, undelinted seed 0.50
Egg 0.05
Food commodities/feed commodities (other than those covered by a higher tolerance as a results of use on growing crops) in food/feed handling establishments 0.05
Fruit, citrus, group 10-10 0.35
Goat, fat 1.0
Goat, meat 0.20
Goat, meat byproducts 0.05
Hog, fat 0.10
Hog, meat 0.05
Horse, fat 1.0
Horse, meat 0.20
Horse, meat byproducts 0.05
Milk, fat, reflecting 0.10 ppm in whole milk 2.5
Nut, tree, group 14-12 0.05
Pea and bean, dried shelled, except soybean, subgroup 6C 0.05
Pea and bean, succulent shelled, subgroup 6B 0.10
Poultry, fat 0.05
Poultry, meat 0.05
Rice, grain 1.5
Sheep, fat 1.0
Sheep, meat 0.20
Sheep, meat byproducts 0.05
Sorghum, grain, grain 0.50
Soybean, seed 0.05
Vegetable, cucurbit, group 9 0.20
Vegetable, fruiting, group 8-10 0.20
Vegetable, leafy, group 4 10
Vegetable, legume, edible podded, subgroup 6A 0.50
Vegetable, root and tuber, group 1, except sugar beet 0.10
Wheat, grain 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63235, 63243, Nov. 26, 1997, as amended at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Sept. 17, 2001; 67 FR 6430, Feb. 12, 2002; 67 FR 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. 19, 2007; 72 FR 71801, Dec. 19, 2007; 73 FR 1525, Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10, 2014; 79 FR 77394, Dec. 24, 2014; 80 FR 45438, July 30, 2015; 80 FR 72599, Nov. 20, 2015; 83 FR 25943, June 5, 2018; 86 FR 41903, Aug. 4, 2021; 88 FR 68481, Oct. 4, 2023; 90 FR 33282, July 17, 2025]

§ 180.419 Chlorpyrifos-methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl [O,-O,-dimethyl O-(3,5,6-trichloro-2-pyridyl)] phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the following food commodities:

Commodity Parts per million
Barley, grain 6.0
Cattle, fat 0.5
Cattle, meat 0.5
Cattle, meat byproducts 0.5
Egg 0.1
Goat, fat 0.5
Goat, meat 0.5
Goat, meat byproducts 0.5
Hog, fat 0.5
Hog, meat 0.5
Hog, meat byproducts 0.5
Horse, fat 0.5
Horse, meat 0.5
Horse, meat byproducts 0.5
Milk, fat (0.05 ppm (N) in whole milk 1.25
Oat, grain 6.0
Poultry, fat 0.5
Poultry, meat .5
Poultry, meat byproducts .5
Rice, grain 6.0
Sheep, fat 0.5
Sheep, meat 0.5
Sheep, meat byproducts 0.5
Sorghum, grain 6.0
Wheat, grain 6.0

(2) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl (O,-O- dimethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the following food commodities when present therein as a result of application to stored grains:

Commodity Parts per million
Barley, bran 90
Barley, pearled barley 90
Rice, bran 30
Rice, hulls 30
Rice, polished rice 30
Sorghum, grain, bran 90
Wheat, bran 30
Wheat, germ 30
Wheat, middlings 30
Wheat, shorts 30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33715, May 24, 2000, as amended at 74 FR 46374, Sept. 9, 2009]

§ 180.420 Fluridone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide fluridone, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, and its bound residues, calculated as the stoichiometric equivalent of fluridone, in or on the commodity.

Commodity Parts per million
Crayfish 0.5
Fish 0.5

(2) Tolerances are established for residues of the herbicide fluridone, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the commodity.

Commodity Parts per million
Animal feed, nongrass, group 18 0.15
Berry and small fruit, group 13-07 0.1
Cattle, fat 0.05
Cattle, kidney 0.1
Cattle, liver 0.1
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Cotton, gin byproducts 0.1
Cotton, undelinted seed 0.1
Egg 0.05
Fruit, citrus, group 10-10 0.1
Fruit, pome, group 11-10 0.1
Fruit, stone, group 12-12 0.1
Goat, fat 0.05
Goat, kidney 0.1
Goat, liver 0.1
Goat, meat 0.05
Goat, meat byproducts 0.05
Grass, forage, fodder and hay, group 17 0.15
Hog, fat 0.05
Hog, kidney 0.1
Hog, liver 0.1
Hog, meat 0.05
Hog, meat byproducts 0.05
Hop, dried cones 0.1
Horse, fat 0.05
Horse, kidney 0.1
Horse, liver 0.1
Horse, meat 0.05
Horse, meat byproducts 0.05
Milk 0.05
Nut, tree, group 14-12 0.1
Peanut 0.1
Peanut, hay 0.15
Poultry, fat 0.05
Poultry, kidney 0.01
Poultry, liver 0.01
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Rice, grain 0.1
Sheep, fat 0.05
Sheep, kidney 0.1
Sheep, liver 0.1
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Tropical and subtropical, small fruit, edible peel, subgroup 23A 0.1
Tropical and subtropical, medium to large fruit, smooth, inedible peel, subgroup 24B 0.1

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide fluridone, including its metabolites and degradates, in or on the irrigated crop commodities and crop groupings in the table in this paragraph, resulting from use of irrigation water containing residues of 0.15 parts per million following applications of fluridone on or around aquatic sites. Where tolerances are established at higher levels from other uses of fluridone on the crops in the table in this paragraph, the higher tolerance also applies to residues in or on the irrigated commodity. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the commodity.

Commodity Parts per million
Cranberry 0.1
Grain, cereal, forage, fodder and straw, group 16 0.1
Grain, cereal, group 15 0.1
Grape 0.1
Okra 0.1
Strawberry 0.1
Vegetable, brassica, leafy, group 5 0.1
Vegetable, cucurbit, group 9 0.1
Vegetable, fruiting, group 8 0.1
Vegetable, leafy, except brassica, group 4 0.1
Vegetable, leaves of root and tuber, group 2 0.1
Vegetable, legume, group 6 0.1
Vegetable, root and tuber, group 1 0.1

[76 FR 23495, Apr. 27, 2011, as amended at 77 FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, 2015; 81 FR 7987, Feb. 17, 2016; 81 FR 72539, Oct. 20, 2016; 85 FR 29637, May 18, 2020; 87 FR 10982, Feb. 28, 2022; 88 FR 3667, Jan. 20, 2023]

§ 180.421 Fenarimol; tolerances for residues.

(a) General. Tolerances are established for residues of fenarimol, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only fenarimol alpha-(2 chlorophenyl)-alpha-(4-chlorophenyl)-5-pyrimidinemethanol.

Commodity Parts per
million
Expiration/
revocation
date
Apple 0.3 7/31/16
Apple, wet pomace 0.3 7/31/16
Banana 1 0.25 None
Cattle, fat 0.01 7/31/16
Cattle, kidney 0.01 7/31/16
Cattle, meat 0.01 7/31/16
Cattle, meat byproducts, except kidney 0.05 7/31/16
Cherry, sweet 1.0 7/31/16
Cherry, tart 1.0 7/31/16
Goat, fat 0.01 7/31/16
Goat, kidney 0.01 7/31/16
Goat, meat 0.01 7/31/16
Goat, meat byproducts, except kidney 0.05 7/31/16
Grape 0.1 7/31/16
Hazelnut 0.02 7/31/16
Hop, dried cones 5.0 7/31/16
Horse, fat 0.01 7/31/16
Horse, kidney 0.01 7/31/16
Horse, meat 0.01 7/31/16
Horse, meat byproducts, except kidney 0.05 7/31/16
Pear 0.1 7/31/16
Pecan 0.02 7/31/16
Sheep, fat 0.01 7/31/16
Sheep, kidney 0.01 7/31/16
Sheep, meat 0.01 7/31/16
Sheep, meat byproducts, except kidney 0.05 7/31/16
Vegetable, cucurbit, group 9 2 0.20 None
1 There are no U.S. registrations for bananas as of April 26, 1995.
2 There are no U.S. registrations for cucurbit vegetable group 9 as of August 27, 2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[51 FR 39662, Oct. 30, 1986, as amended at 53 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989; 60 FR 33354, June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; 67 FR 41807, June 19, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, Sept. 15, 2006; 74 FR 68173, Dec. 23, 2009; 75 FR 56897, Sept. 17, 2010; 81 FR 34905, June 1, 2016]

§ 180.425 Clomazone; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide clomazone, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only clomazone, 2-[(2-chlorophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone, in or on the commodity.

Commodity Parts per million
Bean, asparagus, dry seed 0.05
Bean, broad, dry seed 0.05
Bean, broad, succulent seed 0.05
Bean, kidney, dry seed 0.05
Bean, lima, dry seed 0.05
Bean, lima, succulent seed 0.05
Bean, mung, dry seed 0.05
Bean, navy, dry seed 0.05
Bean, pinto, dry seed 0.05
Bean, snap, succulent 0.05
Bean, wax, succulent seed 0.05
Broccoli, Chinese 0.10
Chickpea, dry seed 0.05
Cilantro, dried leaves 0.30
Cilantro, fresh leaves 0.05
Coriander, seed 0.05
Cottonseed subgroup 20C 0.05
Cowpea, forage 0.05
Cowpea, hay 0.05
Cucumber * 0.1
Dill, dried leaves 0.40
Dill, fresh leaves 0.08
Dill, oil 0.07
Dill, seed 0.05
Grain lupin, dry seed 0.05
Kohlrabi 0.10
Pea, southern, dry seed 0.05
Pea, southern, succulent seed 0.05
Pea, succulent 0.05
Pepper 0.05
Peppermint, tops 0.05
Pumpkin * 0.1
Rapeseed subgroup 20A 0.05
Rhubarb 0.30
Rice, grain 0.02
Soybean 0.05
Soybean, vegetable, succulent 0.05
Spearmint, tops 0.05
Squash, summer * 0.1
Squash, winter * 0.1
Stalk and stem vegetable subgroup 22A, except kohlrabi 0.05
Sugarcane, cane 0.05
Sweet lupin, dry seed 0.05
Vegetable, Brassica, head and stem, group 5-16 0.10
Vegetable, cucurbit, group 9 0.05
Vegetable, tuberous and corm, except potato, subgroup 1D 0.05
White lupin, dry seed 0.05
White sweet lupin, dry seed 0.05
* This tolerance expires on June 5, 2019.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[51 FR 9446, Mar. 19, 1986]

§ 180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance for residues.

A tolerance is established for residues of the herbicide 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid, in or on the raw agricultural commodity soybean at 0.05 part per million.

[51 FR 13309, Apr. 2, 1986]

§ 180.427 Tau-Fluvalinate; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tau-fluvalinate, including its metabolites and degradates, in or on commodities in the table below. Compliance with the specified tolerance level is to be determined by measuring only tau-fluvalinate, (cyano-(3-phenoxyphenyl)methylN-[2-chloro-4-(trifluoromethyl)phenyl]-D-valinate), in or on the commodity.

Commodity Parts per million
Grape, wine 1 1.0
Honey 0.02
1 There is no U.S. registration for use of tau-fluvalinate on wine grapes.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertent residues. [Reserved]

[65 FR 33701, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, 2008; 81 FR 87462, Dec. 5, 2016]

§ 180.428 Metsulfuron methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the herbicide metsulfuron methyl (methyl 2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl] benzoate) and its metabolite methyl 2-[[[[(4-methoxy-6-methyl-1-,3,5- triazin-2-yl)amino]carbonyl]amino] sulfonyl]-4-hydroxybenzoate in or on the following raw material agricultural commodities:

Commodity Parts per million
Barley, grain 0.1
Barley, hay 20.0
Barley, straw 0.3
Grass, forage 15.0
Grass, hay 15.0
Grass, straw 15.0
Sorghum, grain, forage 0.2
Sorghum, grain, grain 0.1
Sorghum, grain, stover 0.2
Sugarcane, cane 0.05
Wheat, forage 5.0
Wheat, grain 0.1
Wheat, hay 20.0
Wheat, straw 0.3

(2) Tolerances are established for residues of metsulfuron methyl (methyl-2[[[[(4-methoxy- 6-methyl-1,3,5-triazin-2- yl)amino]carbonyl]amino] sulfonyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, fat 0.1
Cattle, kidney 0.5
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Goat, fat 0.1
Goat, kidney 0.5
Goat, meat 0.1
Goat, meat byproducts 0.1
Hog, fat 0.1
Hog, kidney 0.5
Hog, meat 0.1
Hog, meat byproducts 0.1
Horse, fat 0.1
Horse, kidney 0.5
Horse, meat 0.1
Horse, meat byproducts 0.1
Milk 0.05
Sheep, fat 0.1
Sheep, kidney 0.5
Sheep, meat 0.1
Sheep, meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 70191, Dec. 16, 1999, as amended at 66 FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, 2002]

§ 180.429 Chlorimuron ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide chlorimuron ethyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following table is to be determined by measuring only chlorimuron ethyl, ethyl 2-[[[[(4-chloro-6-methoxypyrimidin-2yl)amino]carbonyl]sulfonyl]benzoate] in or on the following commodities:

Commodity Parts per million
Berry, low growing, except strawberry, subgroup 13-07H 0.02
Corn, field, forage 0.5
Corn, field, grain 0.01
Corn, field, stover 2.0
Grain, aspirated fractions 3.0
Peanut 0.02
Soybean, forage 0.45
Soybean, hay 1.8
Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 10494, Mar. 11, 2009, as amended at 74 FR 67087, Dec. 18, 2009]

§ 180.430 Fenoxaprop-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, grain 0.05
Barley, straw 0.1
Cattle, fat 0.05
Cattle, meat byproducts 0.05
Cattle, meat 0.05
Cotton, undelinted seed 0.05
Goat, fat 0.05
Goat, meat byproducts 0.05
Goat, meat 0.05
Hog, fat 0.05
Hog, meat byproducts 0.05
Hog, meat 0.05
Horse, fat 0.05
Horse, meat byproducts 0.05
Horse, meat 0.05
Milk 0.02
Peanut 0.05
Peanut, hulls 1 0.05
Rice, grain 0.05
Sheep, fat 0.05
Sheep, meat byproducts 0.05
Sheep, meat 0.05
Soybean, seed 0.05
Wheat, grain 0.05
Wheat, straw 0.50
1 This tolerance expires on August 26, 2026.

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph when fenoxaprop-ethyl is used in the states of Oregon, Washington, and Utah. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl, in or on the commodity

Table 2 to Paragraph (c)

Commodity Parts per
million
Grass, hay 0.09

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 1377, Jan. 9, 1998, as amended at 63 FR 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; 75 FR 80346, Dec. 22, 2010; 76 FR 23495, Apr. 27, 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, May 7, 2014; 91 FR 9727, Feb. 27, 2026]

§ 180.431 Clopyralid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide clopyralid, including its metabolites and degradates, in or on the commodities in the table below from its application in the acid form or in the form of its salts. Compliance with the tolerance levels specified below is to be determined by measuring only clopyralid, (3,6-dichloro-2-pyridinecarboxylic acid), in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, bran 12
Barley, grain 3.0
Barley, hay 9.0
Barley, pearled barley 12
Barley, straw 9.0
Beet, garden, roots 4.0
Beet, sugar, molasses 10
Beet, sugar, roots 2.0
Berry, low growing, subgroup 13-07G 4.0
Brassica, leafy greens, subgroup 4-16B 5.0
Broccoli, Chinese 2.0
Bushberry subgroup 13-07B 0.50
Caneberry subgroup 13-07A 0.1
Canola, meal 6.0
Cattle, fat 1.0
Cattle, liver 3.0
Cattle, meat 1.0
Cattle, meat byproducts, except liver 36.0
Corn, field, forage 3.0
Corn, field, grain 1.0
Corn, field, milled byproducts 1.5
Corn, field, stover 10.0
Corn, pop, grain 1.0
Corn, pop, stover 10.0
Corn, sweet, forage 7.0
Corn, sweet, kernel plus cob with husks removed 1.0
Corn, sweet, stover 10.0
Egg 0.1
Flax, meal 6.0
Fruit, pome, group 11-10 0.05
Fruit, stone, group 12-12 0.50
Goat, fat 1.0
Goat, liver 3.0
Goat, meat 1.0
Goat, meat byproducts, except liver 36.0
Grass, forage 500.0
Grass, hay 500.0
Hog, fat 0.2
Hog, meat 0.2
Hog, meat byproducts 0.2
Hop, dried cones 5.0
Horse, fat 1.0
Horse, liver 3.0
Horse, meat 1.0
Horse, meat byproducts, except liver 36.0
Kohlrabi 2.0
Milk 0.2
Oat, forage 9.0
Oat, grain 3.0
Oat, groats/rolled oats 12
Oat, straw 9.0
Onion, bulb, subgroup 3-07A 0.4
Peppermint, tops 3.0
Plum, prune, dried 1.5
Poultry, fat 0.2
Poultry, meat 0.2
Poultry, meat byproducts 0.2
Radish, roots 0.30
Rapeseed, forage 3.0
Rapeseed, meal 6.0
Rapeseed, subgroup 20A, except gold of pleasure 3.0
Sheep, fat 1.0
Sheep, liver 3.0
Sheep, meat 1.0
Sheep, meat byproducts, except liver 36.0
Spearmint, tops 3.0
Spinach 5.0
Stalk and stem vegetable subgroup 22A 1.0
Swiss chard 3.0
Teff, forage 9.0
Teff, grain 3.0
Teff, hay 9.0
Teff, straw 9.0
Turnip, roots 1.0
Vegetable, Brassica, head and stem, group 5-16 2.0
Vegetable, leaves of root and tuber, group 2 5.0
Wheat, bran 12
Wheat, forage 9.0
Wheat, germ 12
Wheat, grain 3.0
Wheat, middling 12
Wheat, shorts 12
Wheat, straw 9.0
Wheatgrass, intermediate, bran 12
Wheatgrass, intermediate, forage 9
Wheatgrass, intermediate, germ 12
Wheatgrass, intermediate, grain 3
Wheatgrass, intermediate, middling 12
Wheatgrass, intermediate, shorts 12
Wheatgrass, intermediate, straw 9

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[52 FR 10566, Apr. 2, 1987]

§ 180.432 Lactofen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide lactofen, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, in or on the commodity.

Commodity Parts per million
Beans, snap, succulent, except lima bean 0.01
Cotton, gin byproducts 0.02
Cotton, undelinted seed 0.01
Peanut 0.01
Soybean, seed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of the herbicide lactofen, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, in or on the commodity.

Commodity Parts per million
Okra 0.02
Vegetables, fruiting, group 08 0.02

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 57216, Sept. 24, 2004, as amended at 72 FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, 2011]

§ 180.433 Fomesafen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fomesafen, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table 1 to this paragraph (a) is to be determined by measuring only fomesafen, 5-[2-chloro-4-(trifluoromethyl)phenoxy]-N-(methylsulfonyl)-2-nitrobenzamide, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Berry, low growing, subgroup 13-07G, except cranberry 0.02
Cotton, gin byproducts 0.025
Cotton, undelinted seed 0.025
Vegetable, bulb, group 3-07 0.02
Vegetable, cucurbit, group 9 0.03
Vegetable, fruiting, group 8-10 0.03
Vegetable, legume, forage and hay, except soybean, subgroup 7-22A 0.05
Vegetable, legume, group 6 0.05
Vegetable, tuberous and corm, subgroup 1C 0.025

(b)-(d) [Reserved]

[88 FR 29839, May 9, 2023]

§ 180.434 Propiconazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of propiconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those propiconazole residues convertible to 2,4-dichlorobenzoic acid (2,4-DCBA), expressed as the stoichiometric equivalent of propiconazole, in or on the commodity in the table below:

Commodity Parts per million
Almond, hulls 7.0
Avocado 0.2
Banana 0.2
Barley, bran 6.0
Barley, grain 3.0
Barley, hay 30
Barley, straw 20
Bean, dry seed 0.40
Bean, snap 0.70
Bean, succulent shelled 0.10
Beet, garden, tops 5.5
Beet, sugar, dried pulp 1.0
Beet, sugar, molasses 1.5
Beet, sugar, roots 0.3
Beet, sugar, tops 10
Brassica, leafy greens, subgroup 4-16B, except watercress 20
Bushberry, subgroup 13-07B 1.0
Caneberry, subgroup 13-07A 1.0
Cattle, fat 0.05
Cattle, kidney 2.0
Cattle, liver 2.0
Cattle, meat 0.05
Cattle, meat byproducts, except liver and kidney 0.05
Celtuce 5
Cilantro, leaves 13
Citrus, oil 1000
Corn, field, forage 12
Corn, field, grain 0.2
Corn, field, stover 30
Corn, pop, grain 0.2
Corn, pop, stover 30
Corn, sweet, forage 6.0
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 30
Dill, seed 15
Dillweed, dried leaves 80
Dillweed, fresh leaves 30
Fennel, Florence, fresh leaves and stalk 5
Fruit, citrus, group 10-10 8.0
Fruit, stone, group 12-12, except plum 4.0
Goat, fat 0.05
Goat, kidney 2.0
Goat, liver 2.0
Goat, meat 0.05
Goat, meat byproducts, except liver and kidney 0.05
Grain, aspirated fractions 110
Grass, forage 0.5
Grass, hay 0.5
Grass, straw 40
Hog, kidney 0.2
Hog, liver 0.2
Horse, fat 0.05
Horse, kidney 2.0
Horse, liver 2.0
Horse, meat 0.05
Horse, meat byproducts, except liver and kidney 0.05
Leaf petiole vegetable subgroup 22B 5
Low growing berry subgroup 13-07G, except cranberry 1.3
Milk 0.05
Mushroom 0.1
Nut, tree, group 14-12 0.10
Oat, forage 4.0
Oat, grain 3.0
Oat, hay 15
Oat, straw 10
Onion, bulb subgroup 3-07A 0.2
Onion, green, subgroup 3-07B 9.0
Parsley, fresh leaves 13
Parsley, dried leaves 35
Peanut 0.2
Peanut, hay 20
Peppermint, tops 10.0
Pineapple 4.5
Pineapple, process residue 7.0
Plum 0.60
Rapeseed subgroup 20A 0.30
Quinoa, grain 3.0
Radish, tops 0.20
Rice, bran 15
Rice, grain 7.0
Rice, hulls 20
Rye, bran 0.6
Rye, forage 9.0
Rye, grain 0.3
Rye, straw 10
Sheep, fat 0.05
Sheep, kidney 2.0
Sheep, liver 2.0
Sheep, meat 0.05
Sheep, meat byproducts, except liver and kidney 0.05
Sorghum, grain, forage 12
Sorghum, grain, grain 3.5
Sorghum, grain, stover 15
Soybean, forage 11
Soybean, hay 30
Soybean, seed 2.0
Spearmint, tops 10.0
Sugarcane, cane 0.4
Swiss chard 5
Ti palm, leaves 10
Ti palm, roots 0.30
Tomato 3.0
Vegetable, foliage of legume, group 7 30
Vegetable, root, except sugar beet, subgroup 1B 0.3
Watercress 6.0
Wheat, bran 0.6
Wheat, forage 15
Wheat, grain 0.3
Wheat, hay 30
Wheat, straw 20

(2) Tolerances are established for propiconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only propiconazole, 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole, in or on the commodity.

Commodity Parts per
million
Tea 1 4.0
1 There are no United States registrations for use of propiconazole on tea as of December 24, 2015.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of propiconazole (1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole) and its metabolites determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in connection with use of the pesticide under section 18 emergency exemptions granted by EPA. The tolerances will expire and are revoked on the dates specified in the following table:

Commodity Parts per million Expiration/revocation date
Nectarine 2.0 12/31/13
Peach 2.0 12/31/13

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(l), is established for residues of 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole and its metabolites determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in or on the following commodities:

Commodity Parts per million
Cranberry 1.0
Rice, wild, grain 0.5

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the fungicide 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole and its metabolites determined as 2,4-dichlorobenzoic acid and expressed as parent compound in or on the following commodities when present therein as a result of application of propiconazole to growing crops in paragraphs (a) and (c) of this section:

Commodity Parts per million
Alfalfa, forage 0.1
Alfalfa, hay 0.1

[71 FR 55306, Sept. 22, 2006, as amended at 72 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, 2009; 75 FR 80346, Dec. 22, 2010; 76 FR 27268, May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; 78 FR 78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, 2014; 80 FR 72599, Nov. 20, 2015; 80 FR 79718, Dec. 23, 2015; 80 FR 80275, Dec. 24, 2015; 82 FR 1210, Jan. 5, 2017; 84 FR 39774, Aug. 12, 2019]

§ 180.435 Deltamethrin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of deltamethrin, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3-phenoxybenzyl ester, and its major metabolites, trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, and alpha-R-deltamethrin, (R)-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 2.5
Apple, wet pomace 1
Artichoke, globe 0.5
Barley, bran 5
Cattle, fat 0.05
Cattle, meat 0.02
Cattle, meat byproducts 0.05
Citrus, dried pulp 1 3
Citrus, oil 1 50
Corn, field, forage 0.7
Corn, field, refined oil 2.5
Corn, field, stover 5
Corn, pop, stover 5
Corn, sweet, forage 10
Corn, sweet, kernel plus cob with husks removed 0.03
Corn, sweet, stover 15
Cotton, refined oil 0.2
Cotton, undelinted seed 0.04
Egg 0.02
Fish—freshwater finfish 0.01
Fish—freshwater finfish, farm raised 0.01
Fish—freshwater finfish, other 0.01
Fish—freshwater finfish, tuna 0.01
Fruit, pome, group 11 0.2
Goat, fat 0.05
Goat, meat 0.02
Goat, meat byproducts 0.05
Grain, aspirated fractions 65
Grain, cereal, group 15, except sweet corn 2
Hog, fat 0.05
Horse, fat 0.05
Horse, meat 0.02
Horse, meat byproducts 0.05
Lychee 1 0.2
Milk, fat (reflecting 0.02 ppm in whole milk) 0.1
Nut, tree, group 14 0.1
Onion, bulb 0.1
Onion, green 1.5
Orange 1 0.3
Poultry, fat 0.05
Poultry, meat 0.02
Poultry, meat byproducts 0.02
Radish, tops 4
Rapeseed 0.2
Rice, hulls 2.5
Rye, bran 5
Sheep, fat 0.05
Sheep, meat 0.02
Sheep, meat byproducts 0.05
Sorghum, grain, forage 0.5
Sorghum, grain, stover 1
Soybean, seed 0.1
Soybean, hulls 0.2
Starfruit 1 0.2
Sunflower, seed 0.1
Tomato 0.3
Tomato, paste 1
Tomato, puree 1
Vegetable, cucurbit, group 9 0.2
Vegetable, fruiting, group 8 0.3
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 1 0.07
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 1 0.07
Vegetable, root, except sugar beet, subgroup 1B 0.2
Vegetable, tuberous and corm, subgroup 1C 0.04
Wheat, bran 5
1 There are no U.S. registrations.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide deltamethrin, including its metabolites and degradates, in or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing crops) when deltamethrin is used in food/feed handling establishments or as a wide-area mosquito adulticide. Compliance with the tolerance levels specified is to be determined by measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3-phenoxybenzyl ester, and its major metabolites, trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, and alpha-R-deltamethrin, (R)-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63001, Nov. 26, 1997, as amended at 63 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, 2004; 74 FR 46375, Sept. 9, 2009; 76 FR34885, June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR 16302, Mar. 27, 2015; 82 FR 18580, Apr. 20, 2017; 88 FR 19879, Apr. 4, 2023; 91 FR 8108, Feb. 20, 2026]

§ 180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of cyfluthrin, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in table 1 to this paragraph (a)(1) is to be determined by measuring only cyfluthrin, (cyano(4-fluoro-3-phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2dimethyl-cyclopropane-carboxylate, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa 5
Alfalfa, forage 5
Alfalfa, hay 13
Almond, hulls 0.5
Barley, bran 0.5
Barley, grain 0.15
Beet, sugar, dried pulp 1
Beet, sugar, roots 0.1
Brassica, leafy greens, subgroup 4-16B 7
Buckwheat, grain 0.15
Carrot, roots 0.2
Cattle, fat 2
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Celtuce 6
Citrus, dried pulp 0.3
Citrus, oil 0.3
Corn, field, grain 0.05
Corn, pop, grain 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, hulls 2
Cotton, refined oil 2
Cotton, undelinted seed 1
Egg 0.01
Fennel, florence, fresh leaves and stalk 6
Fruit, citrus, group 10-10 0.3
Fruit, pome, group 11-10 0.5
Fruit, stone, group 12-12 0.3
Goat, fat 2
Goat, meat 0.05
Goat, meat byproducts 0.05
Grain, aspirated fractions 150
Grain, cereal, forage, fodder and hay, group 16, forage, except rice 25
Grain, cereal, forage, fodder and hay, group 16, hay, except rice 6
Grain, cereal, forage, fodder and hay, group 16, stover, except rice 30
Grain, cereal, forage, fodder and hay, group 16, straw, except rice 7
Grape 1
Grape, raisin 3.5
Grass, forage, fodder and hay, group 17, forage 12
Grass, forage, fodder and hay, group 17, hay 50
Hog, fat 0.5
Hog, meat 0.01
Hog, meat byproducts 0.02
Hop, dried cones 20
Hop, vines 4
Horse, fat 2
Horse, meat 0.05
Horse, meat byproducts 0.05
Kohlrabi 2.5
Leaf petiole vegetable subgroup 22B 6
Leafy greens subgroup 4-16A 6
Milk 0.2
Milk, fat 5
Millet, grain 0.15
Nut, tree, group 14-12 0.01
Oat, bran 0.5
Oat, grain 0.15
Pea and bean, dried shelled, except soybean, subgroup 6C 0.15
Pea, dry, seed 0.15
Pea, southern, succulent 0.25
Peanut 0.01
Peanut, hay 6
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Radish, roots 1
Rye, bran 0.5
Rye, grain 0.15
Sheep, fat 2
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Sorghum, grain, grain 3.5
Soybean, forage 8
Soybean, hay 4
Soybean, seed 0.03
Sugarcane, cane 0.05
Sugarcane, molasses 0.2
Sunflower, forage 5
Sunflower, seed 0.02
Teosinte, grain 0.05
Tomato, dry pomace 5
Tomato, paste 0.5
Tomato, wet pomace 5
Triticale, grain 0.15
Vegetable, brassica, head and stem, group 5-16 2.5
Vegetable, cucurbit, group 9 0.1
Vegetable, fruiting, group 8-10 0.5
Vegetable, tuberous and corm, subgroup 1C 0.01
Wheat, bran 0.5
Wheat, grain 0.15
Wheat, shorts 0.5

(2) A tolerance of 0.05 parts per million is established for residues of cyfluthrin, including its metabolites and degradates, in or on all food and feed items when cyfluthrin is used in food or feed handling establishments. Compliance with the tolerance level specified is to be determined by measuring only cyfluthrin, (cyano(4-fluoro-3-phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2dimethyl-cyclopropane-carboxylate, in or on the commodity.

(3) Tolerances are established for residues of beta-cyfluthrin, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (a)(3). Compliance with the tolerance levels specified in table 2 to this paragraph (a)(3) is to be determined by measuring only the sum of beta-cyfluthrin, cyano(4-fluoro-3-phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2-dimethyl-cyclopropanecarboxylate [mixture comprising the enantiomeric pair (R)-α-cyano-4-fluoro-3-phenoxybenzyl (1S,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3-phenoxybenzyl (1R,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate with the enantiomeric pair (R)-α-cyano-4-fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3-phenoxybenzyl (1R,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate], in or on the commodity.

Table 2 to Paragraph (a)(3)

Commodity Parts per million
Alfalfa 5
Alfalfa, forage 5
Alfalfa, hay 13
Almond, hulls 0.5
Barley, bran 0.5
Barley, grain 0.15
Beet, sugar, dried pulp 1
Beet, sugar, roots 0.1
Brassica, leafy greens, subgroup 4-16B 7
Buckwheat, grain 0.15
Carrot, roots 0.2
Cattle, fat 2
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Celtuce 6
Citrus, dried pulp 0.3
Citrus, oil 0.3
Corn, field, grain 0.05
Corn, pop, grain 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, hulls 2
Cotton, refined oil 2
Cotton, undelinted seed 1
Egg 0.01
Fennel, florence, fresh leaves and stalk 6
Fruit, citrus, group 10-10 0.3
Fruit, pome, group 11-10 0.5
Fruit, stone, group 12-12 0.3
Goat, fat 2
Goat, meat 0.05
Goat, meat byproducts 0.05
Grain, aspirated fractions 150
Grain, cereal, forage, fodder and hay, group 16, forage, except rice 25
Grain, cereal, forage, fodder and hay, group 16, hay, except rice 6
Grain, cereal, forage, fodder and hay, group 16, stover, except rice 30
Grain, cereal, forage, fodder and hay, group 16, straw, except rice 7
Grape 1
Grape, raisin 3.5
Grass, forage, fodder and hay, group 17, forage 12
Grass, forage, fodder and hay, group 17, hay 50
Hog, fat 0.5
Hog, meat 0.01
Hog, meat byproducts 0.02
Hop, dried cones 20
Hop, vines 4
Horse, fat 2
Horse, meat 0.05
Horse, meat byproducts 0.05
Kohlrabi 2.5
Leaf petiole vegetable subgroup 22B 6
Leafy greens subgroup 4-16A 6
Milk 0.2
Milk, fat 5
Millet, grain 0.15
Nut, tree, group 14-12 0.01
Oat, bran 0.5
Oat, grain 0.15
Pea and bean, dried shelled, except soybean, subgroup 6C 0.15
Pea, dry, seed 0.15
Pea, southern, succulent 0.25
Peanut 0.01
Peanut, hay 6
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Radish, roots 1
Rye, bran 0.5
Rye, grain 0.15
Sheep, fat 2
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Sorghum, grain, grain 3.5
Soybean, forage 8
Soybean, hay 4
Soybean, seed 0.03
Sugarcane, cane 0.05
Sugarcane, molasses 0.2
Sunflower, forage 5
Sunflower, seed 0.02
Teosinte, grain 0.05
Tomato, paste 0.5
Tomato, pomace 5
Triticale, grain 0.15
Vegetable, brassica, head and stem, group 5-16 2.5
Vegetable, cucurbit, group 9 0.1
Vegetable, fruiting, group 8-10 0.5
Vegetable, tuberous and corm, subgroup 1C 0.01
Wheat, bran 0.5
Wheat, grain 0.15
Wheat, shorts 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[53 FR 1924, Jan. 25, 1988]

§ 180.437 Imazamethabenz-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide imazamethabenz-methyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only imazamethabenz-methyl (methyl 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-4-methylbenzoate) or (methyl 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methylbenzoate), as the sum of its para- and meta-isomers in or on the commodity.

Commodity Parts per
million
Expiration/
revocation
date
Barley, grain 0.10 12/31/16
Barley, straw 2.00 12/31/16
Sunflower, seed 0.10 12/31/16
Wheat, grain 0.10 12/31/16
Wheat, straw 2.00 12/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[81 FR 34906, June 1, 2016]

§ 180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the pyrethroid lambda-cyhalothrin, 1:1 mixture of (S)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and (R)-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and its epimer expressed as epimer of lambda-cyhalothrin, a 1:1 mixture of (S)-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and (R)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate, on plants and livestocks, as indicated in the following table.

Commodity Parts per million
Alfalfa, forage 5.0
Alfalfa, hay 6.0
Almond, hulls 1.5
Apple, wet pomace 2.50
Avocado, imported 0.20
Barley, bran 0.2
Barley, grain 0.05
Barley, hay 2.0
Barley, straw 2.0
Brassica, head and stem, subgroup 5A 0.4
Buckwheat, grain 0.05
Canola, refined oil 2.0
Canola, seed 1.0
Cattle, fat 3.0
Cattle, meat 0.2
Cattle, meat byproducts 0.2
Corn, field, flour 0.15
Corn, field, forage 6.0
Corn, field, grain 0.05
Corn, field, stover 1.0
Corn, pop, grain 0.05
Corn, pop, grain, flour 0.05
Corn, pop, stover 1.0
Corn, sweet, forage 6.0
Corn, sweet, stover 1.0
Corn, sweet, kernel plus cob with husks removed 0.05
Cotton, undelinted seed 0.05
Egg 0.01
Fruit, pome, group 11 0.30
Fruit, stone, group 12 0.50
Garlic 0.1
Goat, fat 3.0
Goat, meat 0.2
Goat, meat byproducts 0.2
Grain, aspirated fractions 2.0
Grass, forage, fodder and hay, group 17 7.0
Hog, fat 0.2
Hog, meat 0.01
Hog, meat byproducts 0.02
Hop, dried cones 10.0
Horse, fat 3.0
Horse, meat 0.2
Horse, meat byproducts 0.2
Lettuce, head 2.0
Lettuce, leaf 2.0
Milk, fat (reflecting 0.4 ppm in whole milk) 10.0
Nut, tree, group 14 0.05
Oat, grain 0.05
Oat, forage 2.0
Oat, hay 2.0
Oat, straw 2.0
Onion, bulb 0.1
Pea and bean, dried shelled, except soybean, subgroup 6C 0.10
Pea and bean, succulent shelled, subgroup 6B 0.01
Peanut 0.05
Peanut, hay 3.0
Pistachio 0.05
Poultry, fat 0.03
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Rice, grain 1.0
Rice, hulls 5.0
Rice, wild, grain 1.0
Rye, bran 0.2
Rye, grain 0.05
Rye, forage 2.0
Rye, straw 2.0
Sheep, fat 3.0
Sheep, meat 0.2
Sheep, meat byproducts 0.2
Soybean 0.01
Sorghum, grain, grain 0.2
Sorghum, grain, forage 0.30
Sorghum, grain, stover 0.50
Sugarcane, cane 0.05
Sunflower, forage 0.2
Sunflower, seed, hulls 0.50
Sunflower, refined oil 0.30
Sunflower, seed 0.2
Tomato 0.1
Tomato, dry pomace 6.0
Tomato, wet pomace 6.0
Vegetable, cucurbit, group 9 0.05
Vegetable, fruiting, group 8 0.20
Vegetable, legume, edible podded, subgroup 6A 0.20
Vegetable, tuberous and corm, subgroup 1C 0.02
Wheat, grain 0.05
Wheat, forage 2.0
Wheat, hay 2.0
Wheat, straw 2.0
Wheat, bran 0.2

(2) Tolerances1 are established for the combined residues of the pyrethroid [gamma-cyhalothrin (the isolated active isomer of lambda-cyhalothrin) (S)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate)) and its epimer (R)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate in/on the following commodities:

Commodity Parts per million
Alfalfa, forage 5
Alfalfa, hay 6
Almond, hulls 1.5
Apple, pomace, wet 2.50
Avocado, imported 0.20
Brassica, head and stem, subgroup 5A 0.4
Canola, seed 0.15
Cattle, fat 3
Cattle, meat 0.2
Cattle, meat byproducts 0.2
Corn, field, flour 0.15
Corn, field, forage 6.0
Corn, field, grain 0.05
Corn, field, stover 1.0
Corn, pop, grain 0.05
Corn, pop, stover 1.0
Corn, sweet, forage 6.0
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 1.0
Cotton, undelinted seed 0.05
Egg 0.01
Fruit, pome, group 11 0.30
Fruit, stone, group 12 0.50
Garlic 0.10
Goat, fat 3.0
Goat, meat 0.2
Goat, meat byproducts 0.2
Grain, aspirated fractions 2.0
Hog, fat 3.0
Hog, meat 0.2
Hog, meat byproducts 0.2
Horse, fat 3.0
Horse, meat 0.2
Horse, meat byproducts 0.2
Lettuce, head 2.0
Lettuce, leaf 2.0
Milk, fat (reflecting 0.20 ppm in whole milk) 5.0
Nut, tree, group 14 0.05
Okra 0.20
Onion, bulb 0.1
Pea and bean, dried shelled, except soybean, subgroup 6C 0.10
Pea and bean, succulent shelled, subgroup 6B 0.01
Peanut 0.05
Peanut, hay 3.0
Pistachio 0.05
Poultry, fat 0.03
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Rice, grain 1.0
Rice, hulls 5.0
Sheep, fat 3.0
Sheep, meat 0.2
Sheep, meat byproducts 0.2
Sorghum, grain, forage 0.30
Sorghum, grain, grain 0.20
Sorghum, grain, stover 0.50
Soybean 0.01
Sugarcane 0.05
Sunflower, forage 0.20
Sunflower, refined oil 0.30
Sunflower, seed 0.20
Sunflower, seed, hulls 0.50
Tomato 0.10
Tomato, dry pomace 6.0
Tomato, wet pomace 6.0
Vegetables, fruiting, group 8 0.20
Vegetable, legume, edible podded, subgroup 6A 0.20
Wheat, bran 2.0
Wheat, forage 2.0
Wheat, grain 0.05
Wheat, hay 2.0
Wheat, straw 2.0
1 The analytical enforcement methods for lambda-cyhalothrin are applicable for determination of gamma-cyhalothrin residues in plant and animal commodities.

(3) A tolerance of 0.01 part per million is established for residues of the insecticide lamba-cyhalothrin and an isomer gamma-cyhalothrin in or on all food commodities (other than those already covered by a higher tolerance as a result of use on growing crops) in food-handling establishments where food products are held, processed, or prepared.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74817, Dec. 13, 2006, as amended at 72 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, 2008; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015]

§ 180.439 Thifensulfuron methyl; tolerances for residues.

(a) General. Tolerances are established for residues of thifensulfuron methyl, including its metabolites and degradates, in or on the commodities listed in the following table [below]. Compliance with the tolerance levels specified in the following table [below] is to be determined by measuring only thifensulfuron methyl (methyl 3-[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).

Commodity Parts per million
Barley, grain 0.05
Barley, hay 0.8
Barley, straw 0.10
Canola, seed 0.02
Chicory, roots 0.01
Chicory, tops 0.01
Corn, field, forage 0.10
Corn, field, grain 0.05
Corn, field, stover 0.10
Cotton, gin byproducts 0.02
Cotton, undelinted seed 0.02
Flax, seed 0.02
Oat, forage 0.2
Oat, grain 0.05
Oat, hay 0.05
Oat, straw 0.10
Rice, grain 0.05
Sorghum, grain, forage 0.05
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.05
Soybean 0.10
Wheat, forage 2.5
Wheat, grain 0.05
Wheat, hay 0.7
Wheat, straw 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of thifensulfuron methyl, including its metabolites and degradates, in or on the commodities listed in the following table [below]. Compliance with the tolerance levels specified in the following table [below] is to be determined by measuring only thifensulfuron methyl (methyl 3-[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).

Commodity Parts per million
Safflower, seed 0.05

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 55982, Sept. 17, 2004, as amended at 69 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, 2007; 73 FR 47075, Aug. 13, 2008; 75 FR 19277, Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012; 80 FR 72599, Nov. 20, 2015]

§ 180.440 Tefluthrin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tefluthrin (2,3,5,6 tetrafluroro-4-methylphenyl)methyl-(1 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-diemthylcyclopropanecarboxylate) and its metabolite (Z)-3-(2-chloro-3,3,3-trifluroro-1-propenyl)-2,2-dimethylcyclopropanecarboxylic acid in or on the following commodities:

Commodity Parts per million
Corn, field, forage 0.06
Corn, field, grain 0.06
Corn, field, stover 0.06
Corn, pop, grain 0.06
Corn, pop, stover 0.06
Corn, sweet, forage 0.06
Corn, sweet, kernel plus cob with husks removed 0.06
Corn, sweet, stover 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 62961, Nov. 26, 1997, as amended at 74 FR 46375, Sept. 9, 2009]

§ 180.441 Quizalofop ethyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only those quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, expressed as the stoichiometric equivalent of quizalofop ethyl, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Barley, grain 0.05
Barley, hay 0.05
Barley, straw 0.05
Bean, dry, seed 0.4
Bean, succulent 0.25
Beet, sugar, molasses 0.2
Beet, sugar, roots 0.1
Beet, sugar, tops 0.5
Brassica carinata, meal 2
Brassica carinata, seed 1.5
Corn, field, forage 0.02
Corn, field, grain 0.02
Corn, field, stover 0.03
Cottonseed subgroup 20C 0.1
Cowpea, forage 3.0
Cowpea, hay 3.0
Crambe, meal 2.0
Flax, seed 0.05
Fruit, pome, group 11-10 0.1
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.1
Fruit, stone, group 12-12 0.1
Gold of pleasure, meal 2.0
Lentil, seed 0.05
Pea, dry 0.25
Pea, field, hay 3.0
Pea, field, vines 3.0
Pea, succulent 0.3
Pennycress, seed 1.5
Peppermint, tops 2.0
Rapeseed, meal 2.0
Rapeseed subgroup 20A, except flax, seed 1.5
Rice, grain 0.05
Sorghum, grain, aspirated grain fractions 1.0
Sorghum, grain, forage 0.20
Sorghum, grain, grain 0.20
Sorghum, grain, stover 0.30
Soybean, flour 0.5
Soybean, hulls 0.02
Soybean, meal 0.5
Soybean, seed 0.05
Spearmint, tops 2.0
Sunflower subgroup 20B 3
Wheat, forage 2.0
Wheat, germ 0.40
Wheat, grain 0.05
Wheat, hay 2.0
Wheat, milled byproducts 0.40
Wheat, straw 0.80

(2) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only those quizalofop ethyl residues convertible to quizalofop (2-[4-(6-chloroquinoxalin-2-yl-oxy)phenoxy]propanoic acid), expressed as quizalofop, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.02
Cattle, meat byproducts 0.05
Egg 0.02
Goat, fat 0.05
Goat, meat 0.02
Goat, meat byproducts 0.05
Hog, fat 0.05
Hog, meat 0.02
Hog, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.02
Horse, meat byproducts 0.05
Milk 0.01
Milk, fat 0.25
Poultry, fat 0.05
Poultry, meat 0.02
Poultry, meat byproducts 0.05
Sheep, fat 0.05
Sheep, meat 0.02
Sheep, meat byproducts 0.05

(3) Tolerances are established for residues of the herbicide quizalofop-P-ethyl, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring quizalofop ethyl and quizalofop acid, expressed as the stoichiometric equivalent of quizalofop ethyl, in or on the commodity.

Commodity Parts per
million
Fish-shellfish, crustacean 0.04

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the herbicide quizalofop ethyl, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only those quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, expressed as the stoichiometric equivalent of quizalofop ethyl, in or on the commodity.

Commodity Parts per million
Pineapple 0.1

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 32759, June 16, 1998, as amended at 70 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, 2006; 76 FR 56045, Sept. 15, 2010; 77 FR 23630, Apr. 20, 2012; 80 FR 72599, Nov. 20, 2015; 81 FR 86586, Dec. 1, 2016; 83 FR 7115, Feb. 20, 2018; 83 FR 8011, Feb. 23, 2018; 86 FR 13199, Mar. 8, 2021]

§ 180.442 Bifenthrin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide bifenthrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 2.0
Apple, wet pomace 1.5
Artichoke, globe 1.0
Avocado 0.5
Banana 1 0.1
Beet, garden, roots 0.45
Beet, garden, tops 15
Berry, low growing, subgroup 13-07G 3
Brassica, leafy greens, subgroup 4-16B 4
Bushberry subgroup 13-07B 1.8
Cabbage 4.0
Caneberry subgroup 13-07A 1
Cattle, fat 3
Cattle, meat byproducts 0.2
Cattle, meat 0.5
Celtuce 3
Coffee, green bean 0.05
Coriander, dried leaves 25
Coriander, leaves 6.0
Coriander, seed 5.0
Corn, field, forage 3.0
Corn, field, grain 0.05
Corn, field, stover 5.0
Corn, pop, grain 0.05
Corn, pop, stover 5.0
Corn, sweet, forage 3.0
Corn, sweet, kernel plus cob with husk removed 0.05
Corn, sweet, stover 5.0
Cottonseed subgroup 20C 0.5
Egg 0.05
Fennel, florence, fresh leaves and stalk 3
Fruit, citrus, group 10-10 0.05
Fruit, citrus, group 10-10, oil 0.8
Fruit, pome, group 11-10, except mayhaw 0.9
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.3
Goat, fat 3
Goat, meat byproducts 0.2
Goat, meat 0.5
Grain, aspirated fractions 70
Herb subgroup 19A 0.05
Hog, fat 1.0
Hog, meat byproducts 0.10
Hog, meat 0.5
Hop, dried cones 10.0
Horse, fat 3
Horse, meat byproducts 0.2
Horse, meat 0.5
Kiwifruit, fuzzy 1.5
Kohlrabi 0.9
Leaf petiole vegetable subgroup 22B 3
Lettuce, head 3.0
Mayhaw 1.4
Milk 0.2
Milk, fat 3
Nut, tree, group 14-12 0.05
Peach subgroup 12-12B 0.7
Peanut 0.05
Pepper/eggplant subgroup 8-10B 0.5
Pomegranate 0.5
Poultry, fat 0.05
Poultry, meat byproducts 0.05
Poultry, meat 0.05
Radish, tops 4.5
Rapeseed subgroup 20A 0.05
Safflower, seed 0.2
Sheep, fat 3
Sheep, meat byproducts 0.2
Sheep, meat 0.5
Soybean, hulls 0.50
Soybean, refined oil 0.30
Soybean, seed 0.2
Spinach 0.2
Sunflower subgroup 20B 0.05
Swiss chard 3
Tea, dried 1 30
Tomato subgroup 8-10A 0.3
Tropical and subtropical, palm fruit, edible peel, subgroup 23C 4
Vegetable, brassica, head and stem, group 5-16, except cabbage 0.9
Vegetable, cucurbit, group 9 0.4
Vegetable, legume, bean, edible podded, subgroup 6-22A 0.8
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.05
Vegetable, legume, pea, edible podded, subgroup 6-22B 0.8
Vegetable, legume, pea, succulent shelled, subgroup 6-22D 0.05
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.3
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.3
Vegetable, root, subgroup 1B except sugar beet and garden beet 0.10
Vegetable, tuberous and corm, subgroup 1C 0.05
1 There are no U.S. registrations.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide bifenthrin, (2-methyl[1,1′-biphenyl]-3-yl)methyl-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropane-carboxylate, as follows:

(i) In or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling establishments.

(ii) The insecticide may be present as a residue from application of bifenthrin in food handling establishments, including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, feed handling establishments including feed manufacturing and processing establishments, in accordance with the following prescribed conditions:

(A) Application shall be limited to general surface and spot and/or crack and crevice treatment in food/feed handling establishments where food/feed and food/feed products are held, processed, prepared and served. General surface application may be used only when the facility is not in operation provided exposed food/feed has been covered or removed from the area being treated. Spot and/or crack and crevice application may be used while the facility is in operation provided exposed food/feed is covered or removed from the area being treated prior to application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of food/feed or food/feed contact surfaces shall be avoided.

(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency and shall be used in accordance with such label and labeling.

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the insecticide bifenthrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate.

Table 2 to Paragraph (c)

Commodity Parts per
million
Clover, forage 7
Clover, hay 30
Grass, forage 4.0
Grass, hay 15

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 31002, June 6, 1997]

§ 180.443 Myclobutanil; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide myclobutanil alpha-butyl-alpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile and its alcohol metabolite (alpha-(3-hydroxybutyl)-alpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile (free and bound), in or on the following food commodities:

Commodity Parts per million
Almond 0.1
Almond, hulls 2.0
Apple 0.5
Apple, dry pomace 5.0
Apple, wet pomace 5.0
Artichoke, globe 0.90
Asparagus 0.02
Banana, postharvest 4.0
Bean, snap, succulent 1.0
Caneberry subgroup 13A 2.0
Canistel 3.0
Cattle, fat 0.05
Cattle, liver 1.0
Cattle, meat 0.1
Cattle, meat byproducts, except liver 0.2
Cherry, sweet 5.0
Cherry, tart 5.0
Cilantro, leaves 9.0
Cotton, undelinted seed 0.02
Currant 3.0
Egg 0.02
Fruit, stone, except cherry 2.0
Goat, fat 0.05
Goat, liver 1.0
Goat, meat 0.1
Goat, meat byproducts, except liver 0.2
Gooseberry 2.0
Grain, aspirated fractions 35
Grape 1.0
Grape, dried pomace 10.0
Grape, raisin 10.0
Grape, raisin, waste 25.0
Grape, wet pomace 10.0
Hog, fat 0.05
Hog, liver 1.0
Hog, meat 0.1
Hog, meat byproducts, except liver 0.2
Hop, dried cones 10
Horse, fat 0.05
Horse, liver 1.0
Horse, meat 0.1
Horse, meat byproducts, except liver 0.2
Leafy greens, subgroup 4A, except spinach 9.0
Mango 3.0
Mayhaw 0.70
Milk 0.2
Okra 4.0
Papaya 3.0
Peppermint, tops 3.0
Plum, prune, dried 8.0
Poultry, fat 0.02
Poultry, meat 0.02
Poultry, meat byproducts 0.02
Sapodilla 3.0
Sapote, black 3.0
Sapote, mamey 3.0
Sheep, fat 0.05
Sheep, liver 1.0
Sheep, meat 0.1
Sheep, meat byproducts, except liver 0.2
Soybean, forage 3.5
Soybean, hay 15
Soybean, refined oil 0.40
Soybean, seed 0.25
Spearmint, tops 3.0
Star apple 3.0
Strawberry 0.50
Tomato 0.30
Tomato, puree 0.50
Tomato, paste 1.0
Vegetable, cucurbit, group 9 0.20
Vegetable, fruiting, group 8, except tomato 4.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide myclobutanil alpha-butyl-alpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile in or on the following food commodities:

Commodity Parts per million
Animal feed, nongrass, group 18 0.03
Grain, cereal, forage, fodder and straw, group 16 0.03
Grain, cereal, group 15 0.03
Vegetable, brassica, leafy, group 5 0.03
Vegetable, foliage of legume, group 7 0.03
Vegetable, fruiting, group 8 0.03
Vegetable, leafy, except brassica, group 4 0.03
Vegetable, leaves of root and tuber, group 2 0.03
Vegetable, legume, group 6 0.03
Vegetable, root and tuber, group 1 0.03

[54 FR 6131, Feb. 8, 1989]

§ 180.444 Sulfur dioxide; tolerances for residues.

(a) General. A tolerance is established as follows for sulfite residues of the fungicide sulfur dioxide (determined as (SO2)) in or on the following raw agricultural commodity(ies):

Table 1 to Paragraph (a)

Commodity Parts per million
Blueberry 9
Grape, postharvest 10.0

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[54 FR 20126, May 10, 1989, as amended at 76 FR 56648, Sept. 14, 2011; 87 FR 68911, Nov. 17, 2022]

§ 180.445 Bensulfuron methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide bensulfuron methyl (methyl-2[[[[[(4,6-dimethoxy-pyrimidin-2-yl) amino] carbonyl] amino] sulfonyl] methyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million
Crayfish 0.05
Rice, grain 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 9435, Feb. 25, 1998, as amended at 80 FR 72599, Nov. 20, 2015]

§ 180.446 Clofentezine; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, in or on the commodity.

Commodity Parts per million
Almond, hulls 5.0
Almond 0.5
Apple, dry pomace 3.0
Apple, wet pomace 3.0
Apricot 1.0
Avocado 0.30
Cherry, subgroup 12-12A 1.0
Fruit, pome, group 11-10 0.50
Fruit, small, vine climbing, except fuzzy kiwifruit, Subgroup 13-07F 1.0
Guava 3
Hop, dried cones 7
Persimmon 0.05
Papaya 0.30
Peach, subgroup 12-12B 1.0
Walnut 0.02

(2) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, and its metabolite, 3-(2-chloro-4-hydroxyphenyl)-6-(2-chlorophenyl)-1,2,4,5-tetrazine, calculated as the stoichiometric equivalent of clofentezine, in or on commodity.

Commodity Parts per million
Cattle, fat 0.05
Cattle, liver 0.4
Cattle, meat 0.05
Cattle, meat byproducts, except liver 0.05
Goat, fat 0.05
Goat, liver 0.4
Goat, meat 0.05
Goat, meat byproducts, except liver 0.05
Hog, fat 0.05
Hog, liver 0.4
Hog, meat 0.05
Hog, meat byproducts, except liver 0.05
Horse, fat 0.05
Horse, liver 0.4
Horse, meat 0.05
Horse, meat byproducts, except liver 0.05
Milk 0.01
Sheep, fat 0.05
Sheep, liver 0.4
Sheep, meat 0.05
Sheep, meat byproducts, except liver 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[56 FR 15503, Apr. 17, 1991, as amended at 56 FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60 FR 12709, Mar. 8, 1995; 64 FR 19050, Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011; 81 FR 38609, June 14, 2016; 84 FR 24726, May 29, 2019; 85 FR 67287, Oct. 22, 2020]

§ 180.447 Imazethapyr; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, applied as its acid or ammonium salt, in or on the following raw agricultural commodities:

Commodity Parts per million
Canola, seed 1 0.10
Soybean 0.1
Vegetable, legume, group 6 0.1
1 There are no U.S. registrations for canola as of March 21, 2003.

(2) Tolerances are established for the sum of the residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid; its metabolite CL 288511, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid; and its metabolite CL 182704, 5-[1-(beta-D-glucopyranosyloxy)ethyl]-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-pyridinecarboxylic acid, applied as its acid or ammonium salt, in or on the following commodities:

Commodity Parts per million
Alfalfa, seed 0.15
Alfalfa, seed screenings 0.15
Animal feed, nongrass, group 18, forage 3.0
Animal feed, nongrass, group 18, hay 5.5
Peanut 0.1
Rice, bran 1.2
Rice, grain 0.3

(3) A tolerance is established for the sum of residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, and its metabolite CL 288511, 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid, applied as its acid or ammonium salt, in or on the following commodities:

Commodity Parts per million
Cattle, meat byproducts 0.10
Corn, field, forage 0.1
Corn, field, grain 0.1
Corn, field, stover 0.1
Crayfish 0.15
Goat, meat byproducts 0.10
Hog, meat byproducts 0.10
Horse, meat byproducts 0.10
Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l) of this chapter, are established for the sum of residues of the herbicide imazethapyr, 2- [4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-ethyl- 3-pyridine carboxylic acid, as its ammonium salt, and its metabolite, 2- [4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1- hydroxyethyl)-3-pyridine carboxylic acid, both free and conjugated, applied as its acid or ammonium salt, in or on the following raw agricultural commodities:

Commodity Parts per million
Endive 0.1
Lettuce, head 0.1
Lettuce, leaf 0.1

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 55331, Aug. 29, 2002, as amended at 68 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, 2006; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015]

§ 180.448 Hexythiazox; tolerance for residues.

(a) General. Tolerances are established for residues of hexythiazox, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, calculated as the stoichiometric equivalent of hexythiazox.

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 10
Apple, wet pomace 0.40
Beet, sugar, dried pulp 0.30
Beet, sugar, root 0.15
Berry, low growing, subgroup 13-07G 6
Caneberry, Subgroup 13-07A 3
Cattle, fat 0.05
Cattle, meat byproducts 0.5
Citrus, oil 25
Corn, field, forage 3.0
Corn, field, grain 0.02
Corn, field, stover 7.0
Cotton, gin byproducts 15
Cotton, undelinted seed 0.4
Date, dried 3
Egg 0.05
Fruit, pome, group 11-10 0.4
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 1
Fruit, stone, group 12 1.0
Goat, fat 0.05
Goat, meat byproducts 0.5
Grain, aspirated fractions 5
Hog, fat 0.02
Hog, meat byproducts 0.05
Hop, dried cones 20
Horse, fat 0.05
Horse, meat byproducts 0.5
Lemon/Lime, subgroup 10-10B 0.6
Milk 0.05
Nut, tree, group 14 0.30
Pepper/eggplant subgroup 8-10B 1.5
Peppermint, tops 2.0
Pistachio 0.30
Plum, prune, dried 1.3
Poultry, fat 0.05
Poultry, meat byproducts 0.05
Sheep, fat 0.05
Sheep, meat byproducts 0.5
Spearmint, tops 2.0
Tea, dried 1 15
Tomato 0.50
1 There are no U.S. registrations for this commodity as of July 20, 2020.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined by § 180.1(l), are established for residues of hexythiazox, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, calculated as the stoichiometric equivalent of hexythiazox.

Table 2 to Paragraph (c)

Commodity Parts per million
Alfalfa, forage (EPA Regions 7-11 only) 20
Alfalfa, hay (EPA Regions 7-11 only) 60
Bean, dried, seed (EPA Regions 7-12 only) 0.4
Bean, succulent (EPA Regions 7-12 only) 0.3
Bermuda grass, forage (EPA Regions 9-10 only) 40
Bermuda grass, hay (EPA Regions 9-10 only) 70
Corn, field, forage 6.0
Corn, field, grain 0.02
Corn, field, stover 2.5
Corn, sweet, forage (EPA Regions 7-12 only) 4.0
Corn, sweet, kernel plus cob with husks removed (EPA Regions 7-12 only) 0.1
Grapefruit, subgroup 10-10C (CA, AZ, TX only) 0.5
Orange, subgroup 10-10A (CA, AZ, TX only) 0.5
Potato 0.02
Sorghum, grain, forage (EPA Regions 6-8 only) 5
Sorghum, grain, grain (EPA Regions 6-8 only) 3
Sorghum, grain, stover (EPA Regions 6-8 only) 6
Timothy, forage (EPA Regions 9-11 only) 40
Timothy, hay (EPA Regions 9-11 only) 40
Wheat, forage (EPA Regions 9-12 only) 6.0
Wheat, grain (EPA Regions 9-12 only) 0.02
Wheat, hay (EPA Regions 9-12 only) 30
Wheat, straw (EPA Regions 9-12 only) 8.0

(d) Indirect or inadvertent residues. [Reserved]

[54 FR 17948, Apr. 26, 1989]

§ 180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.

(a) General. Tolerances are established for residues of abamectin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only avermectin B1 a mixture of avermectins containing greater than or equal to 80% avermectin B1 a (5-O-demethyl avermectin A1) and less than or equal to 20% avermectin B1b (5-O-demethyl-25-de(1-methylpropyl)-25-(1-methylethyl) avermectin A1) and its delta-8,9-isomer in or on the following commodities:

Commodity Parts per
million
Acerola 0.015
Almond, hulls 0.10
Apple, wet pomace 0.10
Arugula 0.1
Avocado 0.020
Banana 1 0.006
Bean 0.015
Berry, low growing, subgroup 13-07G 0.05
Black sapote 0.40
Caneberry subgroup 13-07A 0.20
Canistel 0.40
Carrot, roots 0.03
Cattle, fat 0.05
Cattle, meat 0.02
Cattle, meat byproducts 0.09
Celeriac, roots 0.05
Celeriac, tops 0.05
Celtuce 0.1
Chive, dried leaves 0.02
Chive, fresh leaves 0.01
Citrus, dried pulp 0.10
Citrus, oil 0.10
Corn, sweet, forage 0.20
Corn, sweet, kernel plus cob with husk removed 0.01
Corn, sweet, stover 0.50
Cotton, gin byproducts 1.0
Cotton, undelinted seed 0.02
Feijoa 0.015
Fennel, Florence, fresh leaves and stalk 0.1
Food products in food handling establishments (other than those already covered by higher tolerances as a result of use on growing crops, and other than those already covered by tolerances on milk, meat, and meat byproducts) 0.01
Fruit, citrus, group 10-10 0.02
Fruit, pome, group 11-10 0.02
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.02
Fruit, stone, group 12-12 0.09
Garden cress 0.1
Goat, fat 0.03
Goat, meat 0.02
Goat, meat byproducts 0.04
Grain, aspirated grain fractions 0.40
Guava 0.015
Herb subgroup 19A, except chive 0.030
Hog, fat 0.01
Hog, meat 0.02
Hog, meat byproducts 0.02
Hop, dried cones 0.20
Horse, fat 0.03
Horse, meat 0.02
Horse, meat byproducts 0.04
Jaboticaba 0.015
Leaf petiole vegetable subgroup 22B 0.1
Leafy greens subgroup 4-16A 0.1
Longan 0.01
Mamey sapote 0.40
Milk 0.015
Nut, tree, group 14-12 0.01
Onion, bulb, subgroup 3-07A 0.01
Onion, green, subgroup 3-07B 0.08
Papaya 0.40
Passionfruit 0.015
Peppermint, tops 0.010
Pineapple 0.015
Plum, prune, dried 0.025
Poultry, meat 0.02
Poultry, meat byproducts 0.02
Pulasan 0.01
Rambutan 0.01
Sapodilla 0.40
Sheep, fat 0.03
Sheep, meat 0.02
Sheep, meat byproducts 0.04
Soybean, forage 0.30
Soybean, hay 1.0
Soybean, seed 0.01
Spanish lime 0.01
Spearmint, tops 0.010
Star apple 0.40
Starfruit 0.015
Tea, dried 1 1.0
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 0.01
Upland cress 0.1
Vegetable, cucurbit, group 9 0.005
Vegetable, fruiting, group 8-10 0.07
Vegetable, legume, dried shelled, except soybean, subgroup 6C 0.01
Vegetable, legume, edible podded, subgroup 6A 0.08
Vegetable, legume, succulent shelled, subgroup 6B 0.08
Vegetable, tuberous and corm, subgroup 01C 0.01
Wax jambu 0.015
1 There are no U.S. registrations for use of abamectin on banana or tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 44095, Aug. 19, 1997]

§ 180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol (triadimenol) and its butanediol metabolite, 4-(4-chlorophenoxy)-2,2-dimethyl-4-(1H-1,2,4-triazol-l-yl)-1,3-butanediol, calculated as triadimenol, in or on the following commodities:

Commodity Parts per million Expiration/Revocation Date
Banana 1 0.2 None
Barley, grain 0.05 None
Barley, straw 0.2 None
Corn, field, forage 0.05 None
Corn, field, grain 0.05 None
Corn, field, stover 0.05 None
Corn, pop, grain 0.05 None
Corn, pop, stover 0.05 None
Corn, sweet, forage 0.05 None
Corn, sweet, kernel plus cob with husks removed 0.05 None
Corn, sweet, stover 0.05 None
Cotton, undelinted seed 0.02 None
Oat, forage 2.5 None
Oat, grain 0.05 None
Oat, straw 0.2 None
Rye, forage 2.5 None
Rye, grain 0.05 None
Rye, straw 0.1 None
Wheat, forage 2.5 None
Wheat, grain 0.05 None
Wheat, straw 0.2 None
1 There are no U.S. registrations for banana (whole) as of September 22, 1993.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 74 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, 2011]

§ 180.451 Tribenuron methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide tribenuron methyl and its metabolites and degradates in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only tribenuron methyl, methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] carbonyl] amino] sulfonyl] benzoate, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Amaranth, grain, forage 0.3
Amaranth, grain, grain 0.05
Amaranth, grain, hay 0.5
Amaranth, grain, straw 0.1
Amaranth, purple, forage 0.3
Amaranth, purple, grain 0.05
Amaranth, purple, hay 0.5
Amaranth, purple, straw 0.1
Barley, grain 0.05
Barley, hay 0.4
Barley, straw 0.10
Bean, adzuki, dry seed 0.01
Bean, American potato, dry seed 0.01
Bean, asparagus, dry seed 0.01
Bean, black, dry seed 0.01
Bean, broad, dry seed 0.01
Bean, catjang, dry seed 0.01
Bean, cranberry, dry seed 0.01
Bean, dry, dry seed 0.01
Bean, field, dry seed 0.01
Bean, French, dry seed 0.01
Bean, garden, dry seed 0.01
Bean, goa, dry seed 0.01
Bean, great northern, dry seed 0.01
Bean, green, dry seed 0.01
Bean, guar, dry seed 0.01
Bean, kidney, dry seed 0.01
Bean, lablab, dry seed 0.01
Bean, lima, dry seed 0.01
Bean, morama, dry seed 0.01
Bean, moth, dry seed 0.01
Bean, mung, dry seed 0.01
Bean, navy, dry seed 0.01
Bean, pink, dry seed 0.01
Bean, pinto, dry seed 0.01
Bean, red, dry seed 0.01
Bean, rice, dry seed 0.01
Bean, scarlet runner, dry seed 0.01
Bean, sword, dry seed 0.01
Bean, tepary, dry seed 0.01
Bean, urd, dry seed 0.01
Bean, yardlong, dry seed 0.01
Bean, yellow, dry seed 0.01
Buckwheat, grain 0.05
Buckwheat, hay 0.4
Buckwheat, straw 0.1
Buckwheat, tartary, grain 0.05
Buckwheat, tartary, hay 0.4
Buckwheat, tartary, straw 0.1
Canarygrass, annual, grain 0.05
Canarygrass, annual, hay 0.4
Canarygrass, annual, straw 0.1
Cañihua, forage 0.3
Cañihua, grain 0.05
Cañihua, hay 0.5
Cañihua, straw 0.1
Chia, forage 0.3
Chia, grain 0.05
Chia, hay 0.5
Chia, straw 0.1
Chickpea, dry seed 0.01
Corn, field, forage 0.15
Corn, field, grain 0.01
Corn, field, stover 1.1
Cottonseed subgroup 20C 0.02
Cowpea, dry seed 0.01
Cram-cram, forage 0.3
Cram-cram, grain 0.05
Cram-cram, hay 0.5
Cram-cram, straw 0.1
Fonio, black, forage 0.05
Fonio, black, grain 0.05
Fonio, black, stover 0.05
Fonio, white, forage 0.05
Fonio, white, grain 0.05
Fonio, white, stover 0.05
Grain, aspirated fractions 1.5
Gram, horse, dry seed 0.01
Huauzontle, grain, forage 0.3
Huauzontle, grain, grain 0.05
Huauzontle, grain, hay 0.5
Huauzontle, grain, straw 0.1
Inca wheat, forage 0.3
Inca wheat, grain 0.05
Inca wheat, hay 0.5
Inca wheat, straw 0.1
Jackbean, dry seed 0.01
Job's tears, forage 0.05
Job's tears, grain 0.05
Job's tears, stover 0.05
Lentil, dry seed 0.01
Longbean, Chinese, dry seed 0.01
Lupin, Andean, dry seed 0.01
Lupin, blue, dry seed 0.01
Lupin, grain, dry seed 0.01
Lupin, sweet, dry seed 0.01
Lupin, white, dry seed 0.01
Lupin, white sweet, dry seed 0.01
Lupin, yellow, dry seed 0.01
Millet, barnyard, forage 0.05
Millet, barnyard, grain 0.05
Millet, barnyard, stover 0.05
Millet, finger, forage 0.05
Millet, finger, grain 0.05
Millet, finger, stover 0.05
Millet, foxtail, forage 0.05
Millet, foxtail, grain 0.05
Millet, foxtail, stover 0.05
Millet, little, forage 0.05
Millet, little, grain 0.05
Millet, little, stover 0.05
Millet, pearl, forage 0.05
Millet, pearl, grain 0.05
Millet, pearl, stover 0.05
Millet, proso, forage 0.05
Millet, proso, grain 0.05
Millet, proso, stover 0.05
Oat, Abyssinian, grain 0.05
Oat, Abyssinian, hay 0.4
Oat, Abyssinian, straw 0.1
Oat, common, grain 0.05
Oat, common, hay 0.4
Oat, common, straw 0.1
Oat, forage 0.05
Oat, grain 0.05
Oat, hay 0.4
Oat, naked, grain 0.05
Oat, naked, hay 0.4
Oat, naked, straw 0.1
Oat, sand, grain 0.05
Oat, sand, hay 0.4
Oat, sand, straw 0.1
Oat, straw 0.10
Pea, blackeyed, dry seed 0.01
Pea, crowder, dry seed 0.01
Pea, dry, dry seed 0.01
Pea, field, dry seed 0.01
Pea, field, hay 0.01
Pea, field, vines 0.01
Pea, garden, dry seed 0.01
Pea, grass, dry seed 0.01
Pea, green, dry seed 0.01
Pea, pigeon, dry seed 0.01
Pea, southern, dry seed 0.01
Pea, winged, dry seed 0.01
Popcorn, forage 0.15
Popcorn, grain 0.01
Popcorn, stover 1.1
Princess-feather, forage 0.3
Princess-feather, grain 0.05
Princess-feather, hay 0.5
Princess-feather, straw 0.1
Psyllium, forage 0.3
Psyllium, grain 0.05
Psyllium, hay 0.5
Psyllium, straw 0.1
Psyllium, blond, forage 0.3
Psyllium, blond, grain 0.05
Psyllium, blond, hay 0.5
Psyllium, blond, straw 0.1
Quinoa, forage 0.3
Quinoa, grain 0.05
Quinoa, hay 0.5
Quinoa, straw 0.1
Rapeseed subgroup 20A 0.02
Rice, grain 0.05
Rice, African, grain 0.05
Rye, forage 0.3
Rye, grain 0.05
Rye, hay 0.5
Rye, straw 0.1
Sorghum, grain, forage 0.05
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.05
Soybean, forage 0.07
Soybean, hay 0.35
Soybean, hulls 0.04
Soybean, seed 0.01
Soybean, vegetable, dry seed 0.01
Sunflower, seed 0.05
Teff, forage 0.05
Teff, grain 0.05
Teff, stover 0.05
Teosinte, forage 0.15
Teosinte, grain 0.01
Teosinte, stover 1.1
Triticale, forage 0.3
Triticale, grain 0.05
Triticale, hay 0.5
Triticale, straw 0.1
Velvetbean, dry seed 0.01
Wheat, forage 0.3
Wheat, grain 0.05
Wheat, hay 0.5
Wheat, straw 0.10
Wheat, club, forage 0.3
Wheat, club, grain 0.05
Wheat, club, hay 0.5
Wheat, club, straw 0.1
Wheat, common, forage 0.3
Wheat, common, grain 0.05
Wheat, common, hay 0.5
Wheat, common, straw 0.1
Wheat, durum, forage 0.3
Wheat, durum, grain 0.05
Wheat, durum, hay 0.5
Wheat, durum, straw 0.1
Wheat, einkorn, forage 0.3
Wheat, einkorn, grain 0.05
Wheat, einkorn, hay 0.5
Wheat, einkorn, straw 0.1
Wheat, emmer, forage 0.3
Wheat, emmer, grain 0.05
Wheat, emmer, hay 0.5
Wheat, emmer, straw 0.1
Wheat, macha, forage 0.3
Wheat, macha, grain 0.05
Wheat, macha, hay 0.5
Wheat, macha, straw 0.1
Wheat, oriental, forage 0.3
Wheat, oriental, grain 0.05
Wheat, oriental, hay 0.5
Wheat, oriental, straw 0.1
Wheat, Persian, forage 0.3
Wheat, Persian, grain 0.05
Wheat, Persian, hay 0.5
Wheat, Persian, straw 0.1
Wheat, Polish, forage 0.3
Wheat, Polish, grain 0.05
Wheat, Polish, hay 0.5
Wheat, Polish, straw 0.1
Wheat, poulard, forage 0.3
Wheat, poulard, grain 0.05
Wheat, poulard, hay 0.5
Wheat, poulard, straw 0.1
Wheat, shot, forage 0.3
Wheat, shot, grain 0.05
Wheat, shot, hay 0.5
Wheat, shot, straw 0.1
Wheat, spelt, forage 0.3
Wheat, spelt, grain 0.05
Wheat, spelt, hay 0.5
Wheat, spelt, straw 0.1
Wheat, timopheevi, forage 0.3
Wheat, timopheevi, grain 0.05
Wheat, timopheevi, hay 0.5
Wheat, timopheevi, straw 0.1
Wheat, vavilovi, forage 0.3
Wheat, vavilovi, grain 0.05
Wheat, vavilovi, hay 0.5
Wheat, vavilovi, straw 0.1
Wheat, wild einkorn, forage 0.3
Wheat, wild einkorn, grain 0.05
Wheat, wild einkorn, hay 0.5
Wheat, wild einkorn, straw 0.1
Wheat, wild emmer, forage 0.3
Wheat, wild emmer, grain 0.05
Wheat, wild emmer, hay 0.5
Wheat, wild emmer, straw 0.1
Wheatgrass, intermediate, forage 0.3
Wheatgrass, intermediate, grain 0.05
Wheatgrass, intermediate, hay 0.5
Wheatgrass, intermediate, straw 0.1
Wild rice, grain 0.05
Wild rice, eastern, grain 0.05
Yam bean, African, dry seed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l) are established for residues of the herbicide tribenuron methyl (methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] carbonyl]amino]sulfonyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million
Grass, forage, fodder and hay, group 17, except bermudagrass; forage 0.10
Grass, forage, fodder and hay, group 17, except bermudagrass; hay 0.10

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 56718, Sept. 22, 2004, as amended at 72 FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, 2008; 74 FR 67128, Dec. 18, 2009; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015; 87 FR 42337, July 15, 2022]

§ 180.452 Primisulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of primisulfuron-methyl (3-[4,6-bis-(difluoromethoxy)-pyrimidin-2-yl]-1-(2-methoxycarbonylphenylsulfonyl) urea) in or on the following raw agricultural commodities.

Commodity Parts per million
Cattle, fat 0.10
Cattle, meat 0.10
Cattle, meat byproducts 0.10
Corn, field, forage 0.10
Corn, field, grain 0.02
Corn, field, stover 0.10
Corn, pop, grain 0.02
Corn, pop, stover 0.10
Egg 0.10
Goat, fat 0.10
Goat, meat 0.10
Goat, meat byproducts 0.10
Hog, fat 0.10
Hog, meat 0.10
Hog, meat byproducts 0.10
Horse, fat 0.10
Horse, meat 0.10
Horse, meat byproducts 0.10
Milk 0.02
Poultry, fat 0.10
Poultry, meat 0.10
Poultry, meat byproducts 0.10
Sheep, fat 0.10
Sheep, meat 0.10
Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[55 FR 21548, May 25, 1990, as amended at 62 FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, 1998; 67 FR 35049, May 17, 2002; 74 FR 46375, Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR 59128, Sept. 26, 2012]

§ 180.454 Nicosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide nicosulfuron, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only nicosulfuron, 2-[[[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]amino]sulfonyl]-N,N-dimethyl-3-pyridinecarboxamide.

Commodity Parts per million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.05
Corn, field, forage 0.1
Corn, field, grain 0.1
Corn, field, stover 0.1
Corn, pop, grain 0.1
Corn, pop, stover 0.1
Corn, sweet, forage 0.1
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 0.1
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.05
Grass, forage 9.0
Grass, hay 25.0
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.05
Milk 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.05
Sorghum, grain, forage 0.3
Sorghum, grain, grain 0.8
Sorghum, grain, stover 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 17578, Apr. 7, 2010, as amended at 80 FR 68265, Nov. 4, 2015]

§ 180.455 Procymidone; tolerances for residues.

A tolerance is established for the residues of the fungicide procymidone, N-(3,5-dichlorophenyl)-1,2-dimethylcyclopropane-1,2 dicarboximide, in or on the following raw agricultural commodity:

Commodity Parts per million
Grape, wine 5.0

[59 FR 42514, Aug. 18, 1994]

§ 180.457 Bitertanol; tolerances for residues.

(a) General. A tolerance is established for the residues of the fungicide bitertanol, β-([1,1′-biphenyl]-4-yloxy)-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the following raw agricultural commodity:

Commodity Parts per million
Banana 1 0.5
1 There are no U.S. registrations as of April 1, 1992.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47457, Sept. 16, 2009]

§ 180.458 Clethodim; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide clethodim, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2-propenyl]oxy]imino]propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one, and its metabolites containing the 5-(2-ethylthiopropyl)cyclohexene-3-one and 5-(2-ethylthiopropyl)-5-hydroxycyclohexene-3-one moieties and their sulphoxides and sulphones, calculated as the stoichiometric equivalent of clethodim, in or on the commodity.

Commodity Parts per million
Alfalfa, forage 6.0
Alfalfa, hay 10
Almond, hulls 0.20
Artichoke, globe 1.2
Berry, low growing, subgroup 13-07G, except cranberry 3.0
Beet, sugar, molasses 1.0
Beet, sugar, roots 0.20
Beet, sugar, tops 1.0
Brassica, leafy, greens, subgroup 4-16B 3.0
Bushberry subgroup 13-07B 0.20
Caneberry subgroup 13-07A 0.30
Canola, meal 1.0
Cattle, fat 0.2
Cattle, meat 0.2
Cattle, meat byproducts 0.2
Clover, forage 10.0
Clover, hay 20.0
Corn, field, forage 0.2
Corn, field, grain 0.2
Corn, field, stover 0.2
Cotton, meal 2.0
Cottonseed subgroup 20C 1.0
Cranberry 0.50
Egg 0.2
Flax, meal 1.0
Flax, seed 0.6
Fruit, pome, group 11-10 0.20
Fruit, stone, group 12-12 0.20
Goat, fat 0.2
Goat, meat 0.2
Goat, meat byproducts 0.2
Herb subgroup 19A 12.0
Hog, fat 0.2
Hog, meat 0.2
Hog, meat byproducts 0.2
Hop, dried cones 0.5
Horse, fat 0.2
Horse, meat 0.2
Horse, meat byproducts 0.2
Kohlrabi 1 3.0
Leaf petiole vegetable subgroup 22B 0.60
Leafy greens subgroup 4-16A 2.0
Melon subgroup 9A 2.0
Milk 0.05
Nut, tree, group 14-12 0.20
Okra 1.5
Onion, bulb, subgroup 3-07A 0.50
Onion, green, subgroup 3-07B 2.0
Peanut 3.0
Peanut, hay 3.0
Peanut, meal 5.0
Peppermint, tops 5.0
Potato, granules/flakes 2.0
Poultry, fat 0.2
Poultry, meat 0.2
Poultry, meat byproducts 0.2
Radish, tops 0.70
Rapeseed subgroup 20A, except flax seed 0.50
Safflower, meal 10.0
Sheep, fat 0.2
Sheep, meat 0.2
Sheep, meat byproducts 0.2
Soybean 10.0
Spearmint, tops 5.0
Squash/cucumber subgroup 9B 0.50
Stalk and stem vegetable subgroup 22A 1.7
Stevia, dried leaves 12
Sunflower, meal 10.0
Sunflower subgroup 20B 5.0
Vegetable, brassica, head and stem, group 5-16 3.0
Vegetable, fruiting, group 8-10, except okra 1.0
Vegetable, legume, group 6, except soybean 3.5
Vegetable, root, except sugar beet, subgroup 1B 1.0
Vegetable, tuberous and corm, subgroup 1C 1.0
1 This tolerance expires on October 12, 2018.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23496, Apr. 27, 2011, as amended at 77 FR 59128, Sept. 26, 2012; 81 FR 27342, May 6, 2016; 83 FR 15753, Apr. 12, 2018]

§ 180.459 Triasulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide triasulfuron [3-(6-methoxy-4-methyl-1,3,5-triazin-2-yl)-1-(2-(2-chloroethoxy)phenylsulfonyl)urea] in or on the following raw agricultural commodities:

Commodity Parts per million
Barley, grain 0.02
Barley, straw 2.0
Cattle, fat 0.1
Cattle, kidney 0.5
Cattle, meat byproducts, except kidney 0.1
Cattle, meat 0.1
Goat, fat 0.1
Goat, kidney 0.5
Goat, meat byproducts, except kidney 0.1
Goat, meat 0.1
Grass, forage 7.0
Grass, hay 2.0
Hog, fat 0.1
Hog, kidney 0.5
Hog, meat byproducts 0.1
Hog, meat 0.1
Horse, fat 0.1
Horse, kidney 0.5
Horse, meat byproducts, except kidney 0.1
Horse, meat 0.1
Milk 0.02
Sheep, fat 0.1
Sheep, kidney 0.5
Sheep, meat byproducts, except kidney 0.1
Sheep, meat 0.1
Wheat, forage 5.0
Wheat, grain 0.02
Wheat, straw 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, 1998]

§ 180.460 Benoxacor; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the inert ingredient (safener) benoxacor (4-(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1, 4-benzoxazine) at 0.01 parts per million (ppm) when used in pesticide formulations containing metolachlor or S-metolachlor in or on raw agricultural commodities for which tolerances have been established for metolachlor orS-metolachlor.

(2) Tolerances are established for residues of benoxacor, including its metabolites and degradates, in or on the commodities in the following table, when used as an inert ingredient (herbicide safener) in pesticide formulations. Compliance with the tolerance levels specified in the following table is to be determined by measuring only benoxacor (4-(dichloroacetyl)-3,4-dihydro-3-methyl-2H-1,4-benzoxazine).

Table 1 to Paragraph (a)

Commodity Parts per
million
Corn, field forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01

(b) Section 18 energency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 7305, Feb. 13, 1998, as amended at 70 FR 21631, Apr. 27, 2005; 87 FR 42331, July 15, 2022]

§ 180.461 Cadusafos; tolerances for residues.

A tolerance is established for the residues of the nematicide/insecticide cadusafos, O-ethyl S,S-di-sec-butyl phosphorodithioate, in or on the following raw agricultural commodity:

Commodity Parts per million
Banana 0.01

There are no U.S. registrations as of May 10, 1994, for the nematicide/insecticid cadusafos.

[59 FR 39467, Aug. 3, 1994]

§ 180.462 Pyridate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pyridate, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of pyridate, O-(6-chloro-3-phenyl-4-pyridazinyl)-S-octyl-carbonothioate, and its metabolites, 6-chloro-3-phenyl-pyridazine-4-ol and conjugates of 6-chloro-3-phenyl-pyridazine-4-ol, calculated as the stoichiometric equivalent of pyridate, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Chickpea, seed 0.1
Collards 0.03
Corn, field, forage 0.03
Corn, field, stover 0.03
Corn, pop, stover 0.03
Field corn subgroup 15-22C 0.03
Kohlrabi 0.03
Lentil, dry, seed 0.4
Mint, dried leaves 30
Mint, fresh leaves 6
Pea, field, forage 2
Pea, field, hay 5
Peanut 0.03
Rapeseed subgroup 20A 0.05
Soybean, forage 0.4
Soybean, hay 0.8
Soybean, seed 0.05
Vegetable, brassica, head and stem, group 5-16 0.03
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[57 FR 54303, Nov. 18, 1992, as amended at 62 FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64 FR 46298, Aug. 25, 1999; 65 FR 25652, May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011; 87 FR 31742, May 25, 2022; 90 FR 13293, Mar. 21, 2025; 91 FR 9721, Feb. 27, 2026]

§ 180.463 Quinclorac; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of the herbicide quinclorac, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Asparagus 0.08
Barley, grain 1 2
Berry, low growing, except strawberry, subgroup 13-07H 1.5
Bushberry subgroup 13-07B 0.08
Caneberry subgroup 13-07A 0.08
Cattle, fat 0.7
Cattle, meat 0.05
Cattle, meat byproducts 1.5
Egg 0.05
Goat, fat 0.7
Goat, meat 0.05
Goat, meat byproducts 1.5
Grain, aspirated fractions 2 1200
Grass, forage 150
Grass, hay 130
Hog, fat 2 0.7
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 2 1.5
Hog, meat byproducts 0.05
Horse, fat 0.7
Horse, meat 0.05
Horse, meat byproducts 1.5
Milk 0.05
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 2 0.1
Poultry, meat byproducts 0.05
Rhubarb 0.5
Rice, bran 30
Rice, grain 10
Sheep, fat 0.7
Sheep, meat 0.05
Sheep, meat byproducts 1.5
Sorghum, grain, forage 3
Sorghum, grain, grain 6
Sorghum, grain, stover 1
Wheat, forage 1
Wheat, germ 0.75
Wheat, grain 0.5
Wheat, hay 0.5
Wheat, straw 0.1
1 There are no U.S. registrations.
2 This tolerance expires on August 26, 2026.

(2) Tolerances are established for residues of the herbicide quinclorac, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, and its methyl ester, methyl-3,7-dichloro-8-quinolinecarboxylate, calculated as the stoichiometric equivalent of quinclorac, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Rapeseed, subgroup 20A 1 1.5
1 There are no U.S. Registrations.

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[57 FR 47996, Oct. 21, 1992, as amended at 64 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. 26, 1999; 65 FR 33701, May 24, 2000; 67 FR 35049, May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; 76 FR 23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, 2012; 78 FR 71528, Nov. 29, 2013; 80 FR 72599, Nov. 20, 2015; 82 FR 57149, Dec. 4, 2017; 85 FR 43702, July 20, 2020; 91 FR 9727, Feb. 27, 2026]

§ 180.464 Dimethenamid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide dimethenamid, 1(R,S)-2-chloro-N-[(1-methyl-2-methoxy)ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide, applied as either the 90:10 or 50:50 S:R isomers, in or on the following food commodities:

Commodity Parts per million
Bean, dry, seed 0.01
Beet, garden, roots 0.01
Beet, garden, tops 0.01
Beet, sugar, dried pulp 0.01
Beet, sugar, molasses 0.01
Beet, sugar, roots 0.01
Beet, sugar, tops 0.01
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, forage 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01
Cotton, gin byproducts 1.5
Cottonseed subgroup 20C 0.01
Garlic 0.01
Grass, forage 0.15
Grass, hay 2.5
Grass, seed screenings 0.01
Grass, straw 0.01
Hop, dried cones 0.05
Horseradish 0.01
Leek 0.01
Onion, bulb 0.01
Onion, green 0.01
Onion, Welsh 0.01
Peanut 0.01
Peanut, hay 0.01
Radish, roots 0.01
Radish, tops 0.01
Rutabaga, roots 0.01
Rutabaga, tops 0.1
Shallot, bulb 0.01
Shallot, fresh leaves 0.01
Sorghum, grain, forage 0.01
Sorghum, grain, grain 0.01
Sorghum, grain, stover 0.01
Soybean, seed 0.01
Turnip, greens 0.1
Turnip, roots 0.01
Turnip, tops 0.1
Vegetable, tuberous and corm, subgroup 1C 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of dimethenamid, 1 (R,S)-2-chloro-N-[(1-methyl-2-methoxy) ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide) in or on the following raw agricultural commodities:

Commodity Parts per million
Pumpkin 0.01
Squash, winter 0.01

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 51551, Aug. 24, 2000, as amended at 67 FR 46884, July 17, 2002; 69 FR 29459, May 24, 2004; 69 FR 57207, Sept. 24, 2004; 70 FR 24712, May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; 72 FR 73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, 2015]

§ 180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.

(a) General. Tolerances are established for the residues of 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane, (CAS No. 71526-07-3) when used as an inert ingredient (safener) in or on the following raw agricultural commodities:

Commodity 1 Parts per million
Corn, field, forage 0.005
Corn, field, grain 0.005
Corn, field, stover 0.005
Corn, pop, grain 0.005
Corn, pop, stover 0.005
1 There are no U.S. registered products containing 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 4392, Jan. 29, 2003]

§ 180.466 Fenpropathrin; tolerances for residues.

(a) General. Tolerances are established for residues of fenpropathrin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only fenpropathrin (alpha-cyano-3-phenoxy-benzyl 2,2,3,3 tetramethylcyclopropanecarboxylate).

Commodity Parts per million
Acerola 3.0
Almond, hulls 4.5
Atemoya 1.5
Avocado 1.0
Barley, grain 0.04
Barley, hay 3.0
Barley, straw 2.0
Berry, low growing, subgroup 13-07G 2.0
Biriba 1.5
Brassica, head and stem, subgroup 5A 3.0
Bushberry subgroup 13-07B 3.0
Caneberry subgroup 13-07A 12
Canistel 1.0
Cattle, fat 1.0
Cattle, meat byproducts 0.1
Cattle, meat 0.1
Cherimoya 1.5
Cherry, sweet 5.0
Cherry, tart 5.0
Citrus, dried pulp 4.0
Citrus, oil 75
Cotton, refined oil 3.0
Cotton, undelinted seed 1.0
Custard apple 1.5
Egg 0.05
Feijoa 3.0
Fruit, citrus, group 10-10 2.0
Fruit, pome, group 11-10 5.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0
Fruit, stone, crop group 12, except cherry 1.4
Goat, fat 1.0
Goat, meat byproducts 0.1
Goat, meat 0.1
Grape, raisin 10.0
Guava 3.0
Hog, fat 1.0
Hog, meat byproducts 0.1
Hog, meat 0.1
Horse, fat 1.0
Horse, meat byproducts 0.1
Horse, meat 0.1
Ilama 1.5
Jaboticaba 3.0
Longan 7.0
Lychee 7.0
Mango 1.0
Melon subgroup 9A 0.5
Milk, fat (reflecting 0.08 ppm in whole milk) 2.0
Nut, tree, crop group 14 0.10
Olive 5.0
Papaya 1.0
Passionfruit 3.0
Pea, succulent 0.02
Peanut, hay 20.0
Peanut 0.01
Pistachio 0.10
Poultry, fat 0.05
Poultry, meat byproducts 0.05
Poultry, meat 0.05
Pulasan 7.0
Rambutan 7.0
Sapodilla 1.0
Sapote, black 1.0
Sapote, mamey 1.0
Sheep, fat 1.0
Sheep, meat byproducts 0.1
Sheep, meat 0.1
Soursop 1.5
Spanish lime 7.0
Squash/Cucumber subgroup 9B 0.5
Star apple 1.0
Starfruit 3.0
Sugar apple 1.5
Tea, dried 1 2.0
Vegetable, fruiting, group 8-10 1.0
Wax jambu 3.0
1 There are no U.S. registrations as of November 28, 2012, for the use of fenpropathrin on tea, dried.

(b) Section 18 emergency exemptions. Time-limited tolerances specified in Table 2 to this paragraph (b) are established for residues of fenpropathrin, (alpha-cyano-3-phenoxy-benzyl 2,2,3,3 tetramethylcyclopropane carboxylate) in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerance expires on the date specified in Table 2.

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration
date
Kiwifruit, fuzzy 5 12/31/2022

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63034, Nov. 26, 1997, as amended at 63 FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, 1999; 65 FR 11242, Mar. 2, 2000; 65 FR 24397, Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; 70 FR 38789, July 6, 2005; 70 FR 55747, Sept. 23, 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013; 84 FR 70434, Dec. 23, 2019]

§ 180.467 Carbon disulfide; tolerances for residues.

Tolerances are established for the nematicide, insecticide, and fungicide carbon disulfide, from the application of sodium tetrathiocarbonate, in or on the following raw agricultural commodities. These tolerances expire on January 19, 2024.

Commodity Parts per million
Almond 0.1
Almond, hulls 0.1
Grape 0.1
Grapefruit 0.1
Lemon 0.1
Orange, sweet 0.1
Peach 0.1
Plum, prune, fresh 0.1

[58 FR 33771, June 21, 1993, as amended at 62 FR 26949, May 16, 1997; 88 FR 46086, July 19, 2023]

§ 180.468 Flumetsulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide flumetsulam, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only flumetsulam, N-(2,6-difluorophenyl)-5-methyl-(1,2,4)-triazolo-(1,5a)-pyrimidine-2-sulfonamide, in or on the commodity.

Commodity Parts per million
Bean, dry, seed 0.05
Corn, field, forage 0.05
Corn, field, grain 0.05
Corn, field, stover 0.05
Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23497, Apr. 27, 2011]

§ 180.469 Dichlormid; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of dichlormid, including its metabolites and degradates, when used as an inert ingredient (herbicide safener) in pesticide formulations, in or on the commodities in the following table. Compliance with the tolerances is to be determined by measuring only dichlormid (2,2-dichloro-N,N-di-2-propenylacetamide).

Commodity Parts per million
Corn, field, forage 0.05
Corn, field, grain 0.05
Corn, field, stover 0.05
Corn, pop, grain 0.05
Corn, pop, stover 0.05
Corn, sweet, forage 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.05

(2) Tolerances are established for residues of dichlormid, including its metabolites and degradates, at 0.05 parts per million (ppm) when used as an inert ingredient (herbicide safener) in pesticide formulations containing metolachlor or S-metolachlor in or on raw agricultural commodities for which tolerances have been established for metolachlor or S-metolachlor. Compliance with the tolerances is to be determined by measuring only dichlormid (2,2-dichloro-N,N-di-2-propenylacetamide).

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 16149, Mar. 27, 2000, as amended at 67 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, 2004; 70 FR 76699, Dec. 28, 2005; 74 FR 37623, July 29, 2009; 76 FR 16310, Mar. 23, 2011; 81 FR 69406, Oct. 6, 2016]

§ 180.470 Acetochlor; tolerances for residues.

(a) General. Tolerances are established for residues of acetochlor, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only acetochlor, 2-chloro-2'-methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites shall be determined as ethyl methyl aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the stoichiometric equivalents of acetochlor, in or on the following commodities:

Commodity Parts per million
Alfalfa, forage 8.0
Alfalfa, hay 20
Beet, sugar, dried pulp 0.50
Beet, sugar, molasses 0.80
Beet, sugar, roots 0.30
Beet, sugar, tops 0.70
Cattle, fat 0.02
Cattle, kidney 0.03
Cattle, meat 0.02
Cattle, meat byproducts, except kidney 0.02
Corn, field, forage 4.5
Corn, field, grain 0.05
Corn, field, stover 2.5
Corn, pop, grain 0.05
Corn, pop, stover 2.5
Corn, sweet, forage 1.5
Corn, sweet, kernels plus cob with husks removed 0.05
Corn, sweet, stover 1.0
Cotton, gin byproducts 4.0
Cotton, undelinted seed 0.6
Goat, fat 0.02
Goat, kidney 0.03
Goat, meat 0.02
Goat, meat byproducts, except kidney 0.02
Hog, kidney 0.02
Horse, fat 0.02
Horse, kidney 0.03
Horse, meat 0.02
Horse, meat byproducts, except kidney 0.02
Milk 0.02
Peanut 0.20
Peanut, hay 7.0
Peanut, meal 0.25
Sheep, fat 0.02
Sheep, kidney 0.03
Sheep, meat 0.02
Sheep, meat byproducts, except kidney 0.02
Sorghum, grain, forage 1.6
Sorghum, grain, grain 0.05
Sorghum, grain, stover 1.7
Soybean, meal 1.2
Soybean, seed 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of acetochlor, including its metabolites and degradates, in or on the raw agricultural commodities in the table to this paragraph when present therein as a result of application of acetochlor to the growing crops in the table to paragraph (a) of this section. Compliance with the tolerance levels specified below is to be determined by measuring only acetochlor, 2-chloro-2'-methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites shall be determined as ethyl methyl aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the stoichiometric equivalents of acetochlor, in or on the following commodities.

Commodity Parts per million
Animal feed, nongrass, group 18, except alfalfa, forage 1.3
Animal feed, nongrass, group 18, except alfalfa, hay 3.5
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, forage 0.5
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, hay 2.0
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, stover 0.1
Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, and wheat, straw 0.3
Grain, cereal, group 15, except corn, grain sorghum, and wheat, grain 0.05
Pea and bean, dried shelled, except soybean, subgroup 6C 0.05
Potato 0.05
Soybean, forage 0.7
Soybean, hay 1.0
Sunflower, seed 0.05
Wheat, forage 0.5
Wheat, grain 0.02
Wheat, hay 2.0
Wheat, straw 0.1

[72 FR 27468, May 16, 2007, as amended at 74 FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, 2009; 78 FR 13268, Feb. 27, 2013; 79 FR 3517, Jan. 22, 2014; 83 FR 29028, June 22, 2018]

§ 180.471 Furilazole; tolerances for residues.

(a) General. Tolerances are established for residues of furilazole, including its metabolites and degradates, when used as an inert ingredient (safener) in pesticide formulations applied to the following raw agricultural commodities. Compliance with the tolerance levels specified in the table in this paragraph (a) is to be determined by measuring only furilazole, 3-dichloroacetyl-5-(2-furanyl)-2, 2-dimethyloxazolidine (CAS Reg. No. 121776-33-8) in or on the commodity.

Commodity Parts per million
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01
Sorghum, forage 0.01
Sorghum, grain 0.01
Sorghum, stover 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 8867, Feb. 23, 2000, as amended at 67 FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007; 84 FR 52774, Oct. 3, 2019]

§ 180.472 Imidacloprid; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide imidacloprid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl) methyl]-N-nitro-2-imidazolidinimine) and its metabolites containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Acerola 1.0
Almond, hulls 4.0
Apple 0.5
Apple, wet pomace 3.0
Artichoke, globe 2.5
Aspirated grain fractions 240
Atemoya 0.30
Avocado 1.0
Banana 0.50
Beet, sugar, molasses 0.30
Beet, sugar, roots 0.05
Beet, sugar, tops 0.50
Biriba 0.30
Blueberry 3.5
Borage, seed 0.05
Caneberry, subgroup 13-A 2.5
Canistel 1.0
Canola, seed 0.05
Cattle, fat 0.30
Cattle, meat 0.30
Cattle, meat byproducts 0.30
Cherimoya 0.30
Citrus, dried pulp 5.0
Coffee, bean, green 0.80
Cotton, gin byproducts 4.0
Cotton, meal 8.0
Cotton, undelinted seed 6.0
Crambe, seed 0.05
Cranberry 0.05
Currant 3.5
Custard apple 0.30
Egg 0.02
Elderberry 3.5
Feijoa 1.0
Fish 0.05
Fish-shellfish, mollusc 0.05
Flax, seed 0.05
Fruit, citrus, group 10 0.70
Fruit, pome, group 11 0.6
Fruit, stone, group 12 3.0
Goat, fat 0.30
Goat, meat 0.30
Goat, meat byproducts 0.30
Gooseberry 3.5
Grain, cereal, forage, fodder and straw, group 16, forage, except rice 7.0
Grain, cereal, forage, fodder and straw, group 16, hay, except rice 6.0
Grain, cereal, forage, fodder and straw, group 16, stover, except rice 0.30
Grain, cereal, forage, fodder and straw, group 16, straw, except rice 3.0
Grain, cereal, group 15, except rice 0.05
Grape 1.0
Grape, juice 1.5
Grape, raisin 1.5
Guava 1.0
Herbs subgroup 19A, dried herbs 48
Herbs subgroup 19-A, fresh herbs 8.0
Hog, fat 0.30
Hog, meat 0.30
Hog, meat byproducts 0.30
Hop, dried cones 6.0
Horse, fat 0.30
Horse, meat 0.30
Horse, meat byproducts 0.30
Huckleberry 3.5
Ilama 0.30
Jaboticaba 1.0
Juneberry 3.5
Kava, leaves 4.0
Kava, roots 0.40
Leaf petioles subgroup 4B 6.0
Leafy greens subgroup 4A 3.5
Lettuce, head 3.5
Lettuce, leaf 3.5
Lingonberry 3.5
Longan 3.0
Lychee 3.0
Mango 1.0
Milk 0.10
Mustard, black, seed 0.05
Mustard, field, seed 0.05
Mustard, Indian, seed 0.05
Mustard, rapeseed, seed 0.05
Mustard, seed 0.05
Nut, tree, group 14 0.05
Okra 1.0
Onion, dry bulbs, subgroup 3-07A 0.15
Onion, green, subgroup 3-07B 2.5
Papaya 1.0
Passionfruit 1.0
Peanut 0.45
Peanut, hay 35
Peanut, meal 0.75
Pecan 0.05
Pepper, Black 1 0.05
Persimmon 3.0
Pistachio 0.05
Pomegranate 0.90
Potato, chip 0.40
Potato, processed potato waste 0.90
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Pulasan 3.0
Rambutan 3.0
Rapeseed, seed 0.05
Raspberry, wild 2.5
Safflower, seed 0.05
Salal 3.5
Sapodilla 1.0
Sapote, black 1.0
Sapote, mamey 1.0
Sheep, fat 0.30
Sheep, meat 0.30
Sheep, meat byproducts 0.30
Soursop 0.30
Soybean, forage 8.0
Soybean, hay 35
Soybean, meal 4.0
Soybean, seed 3.5
Spanish lime 3.0
Star apple 1.0
Starfruit 1.0
Strawberry 0.50
Sugar apple 0.30
Sunflower, seed 0.05
Tomato, paste 6.0
Tomato, puree 3.0
Vegetable, brassica leafy, group 5 3.5
Vegetable, cucurbit, group 9 0.5
Vegetable, fruiting, group 8 1.0
Vegetable, leaves of root and tuber, group 2 4.0
Vegetable, legume, group 6, except soybean 4.0
Vegetable, root and tuber, group 1, except sugar beet 0.40
Watercress 3.5
Watercress, upland 3.5
Wax jambu 1.0
1 There are no U.S. registrations for this commodity as of February 20, 2026.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide imidacloprid, including its metabolites and degradates in connection with use of the pesticide under a Section 18 emergency exemption granted by EPA. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl)methyl]-N-nitro-2-imidazolidinimine) and its metabolites containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid. These tolerances will expire and are revoked on the dates specified in the following table:

Commodity Parts per million Expiration/revocation date
Sugarcane, cane 6.0 12/31/18
Sugarcane, molasses 50 12/31/18

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide imidacloprid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl) methyl]-N-nitro-2-imidazolidinimine) and its metabolites containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid, in or on the following commodities, when present therein as a result of the application of the pesticide to growing crops listed in this section and other non-food crops as follows:

Commodity Parts per million
Rice, grain 0.05
Vegetable, foliage of legume, group 7 2.5
Vegetable, legume, group 6 0.3

[75 FR 22251, Apr. 28, 2010, as amended at 78 FR 33743, June 5, 2013; 80 FR 78145, Dec. 16, 2015; 91 FR 8100, Feb. 20, 2026]

§ 180.473 Glufosinate; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of glufosinate, including its metabolites and degradates, in or on the commodities in table 1 to paragraph (a)(1). Compliance with the tolerance levels specified in table 1 to paragraph (a)(1) is to be determined by measuring the sum of glufosinate (2-amino-4-(hydroxymethylphosphinyl)butanoic acid) and its metabolites, 2-(acetylamino)-4-(hydroxymethyl phosphinyl) butanoic acid, and 3-(hydroxymethylphosphinyl) propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 0.50
Beet, sugar, molasses 5.0
Beet, sugar, roots 0.9
Beet, sugar, tops (leaves) 1.5
Bushberry subgroup 13-07B 0.15
Canola, meal 1.1
Cattle, fat 0.40
Cattle, meat 0.15
Cattle, meat byproducts 6.0
Corn, field forage 4.0
Corn, field, grain 0.20
Corn, field, stover 6.0
Corn, sweet, forage 1.5
Corn, sweet, kernels plus cob with husks removed 0.30
Corn, sweet, stover 6.0
Cotton, gin byproducts 30
Cottonseed subgroup 20C 15
Egg 0.15
Fig, dried 0.15
Fruit, citrus, group 10-10 0.15
Fruit, pome, group 11-10 0.25
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.05
Fruit, stone, group 12-12 0.30
Goat, fat 0.40
Goat, meat 0.15
Goat, meat byproducts 6.0
Grain aspirated fractions 25
Hog, fat 0.40
Hog, meat 0.15
Hog, meat byproducts 6.0
Hop, dried cones 0.9
Horse, fat 0.40
Horse, meat 0.15
Horse, meat byproducts 6.0
Melon subgroup 9A 0.08
Milk 0.15
Nut, tree, group 14-12 0.50
Pepper/eggplant subgroup 8-10B 0.15
Potato, chips 1.6
Potato granules/flakes 2.0
Poultry, fat 0.15
Poultry, meat 0.15
Poultry, meat byproducts 0.60
Rapeseed subgroup 20A 0.4
Rice, grain 1 0.9
Rice, grain 2 1.0
Rice, hull 2 2.0
Sheep, fat 0.40
Sheep, meat 0.15
Sheep, meat byproducts 6.0
Soybean 2.0
Soybean, hulls 10
Squash/cucumber subgroup 9B 0.15
Tea, dried 1 0.5
Tea, instant 1 0.09
Tea, plucked leaves 1 0.05
Tomato, paste 0.15
Tomato subgroup 8-10A 0.1
Tropical and subtropical, medium to large fruit, edible peel, subgroup 23B 0.1
Tropical and subtropical, medium to large fruit, smooth, inedible peel, subgroup 24B 0.2
Tropical and subtropical, small fruit, edible peel, subgroup 23A 0.5
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 0.1
Vegetable, tuberous and corm, subgroup 1C 0.8
1 There are no U.S. registrations as of November 20, 2025.
2 This tolerance expires on May 20, 2026.

(2) Tolerances are established for residues of glufosinate-P, including its metabolites and degradates, in or on the commodities in table 2 to paragraph (a)(2), as a result of applications of glufosinate-P or glufosinate-P-ammonium to those commodities. Compliance with the tolerance levels specified in table 2 to paragraph (a)(2) is to be determined by measuring the sum of glufosinate (2-amino-4-(hydroxymethylphosphinyl) butanoic acid) and its metabolites, 2-(acetylamino)-4-(hydroxymethyl phosphinyl) butanoic acid, and 3-(hydroxymethylphosphinyl) propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Canola, meal 1.1
Cattle, fat 0.4
Cattle, meat 0.15
Cattle, meat byproducts 6
Corn, field, forage 4
Corn, field, grain 0.2
Corn, field, stover 6
Corn, sweet, forage 1.5
Corn, sweet, kernels plus cob with husks removed 0.3
Corn, sweet, stover 6
Cotton, gin byproducts 30
Cottonseed, subgroup 20C 15
Egg 0.15
Goat, fat 0.4
Goat, meat 0.15
Goat, meat byproducts 6
Grain, aspirated fractions 25
Hog, fat 0.4
Hog, meat 0.15
Hog, meat byproducts 6
Horse, fat 0.4
Horse, meat 0.15
Horse, meat byproducts 6
Milk 0.15
Poultry, fat 0.15
Poultry, meat 0.15
Poultry, meat byproducts 0.6
Rapeseed, subgroup 20A 0.4
Sheep, fat 0.4
Sheep, meat 0.15
Sheep, meat byproducts 6
Soybean 2
Soybean, hulls 10

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of glufosinate, including its metabolites and degradates, in or on the commodities in table 3 to paragraph (c). Compliance with the tolerance levels specified in table 3 to paragraph (c) is to be determined by measuring the sum of glufosinate, (2-amino-4-(hydroxymethylphosphinyl)butanoic acid) and its metabolites, 2-(acetylamino)-4-(hydroxymethyl phosphinyl) butanoic acid, and 3-(hydroxymethylphosphinyl) propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.

Table 3 to Paragraph (c)

Commodity Parts per
million
Grass, forage 0.15
Grass, hay 0.2

(d) Indirect or inadvertent residues.

(1) Tolerances are established for indirect or inadvertent residues of glufosinate, including its metabolites and degradates, in or on the commodities in table 4 to paragraph (d)(1), as a result of the application of glufosinate to crops listed in paragraph (a) of this section. Compliance with the tolerance levels specified in table 4 to paragraph (d)(1) is to be determined by measuring the sum of glufosinate (2-amino-4-(hydroxymethylphosphinyl) butanoic acid) and its metabolite, 3-(hydroxymethylphosphinyl) propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.

Table 4 to Paragraph (d)(1)

Commodity Parts per
million
Barley, hay 0.40
Barley, straw 0.40
Buckwheat, fodder 0.40
Buckwheat, forage 0.40
Oat, forage 0.40
Oat, hay 0.40
Oat, straw 0.40
Rye, forage 0.40
Rye, straw 0.40
Teosinte 0.40
Triticale 0.40
Wheat, forage 0.40
Wheat, hay 0.40
Wheat, straw 0.40

(2) Tolerances are established for indirect or inadvertent residues of glufosinate-P, including its metabolites and degradates, in or on the commodities in table 5 to paragraph (d)(2), as a result of the application of glufosinate-P or glufosinate-P-ammonium to crops listed in paragraph (a)(2) of this section. Compliance with the tolerance levels specified in table 5 to paragraph (d)(2) is to be determined by measuring the sum of glufosinate (2-amino-4-(hydroxymethylphosphinyl) butanoic acid) and its metabolite, 3-(hydroxymethylphosphinyl) propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.”

Table 5 to Paragraph (d)(2)

Commodity Parts per
million
Barley, hay 0.4
Barley, straw 0.4
Buckwheat, fodder 0.4
Buckwheat, forage 0.4
Oat, forage 0.4
Oat, hay 0.4
Oat, straw 0.4
Rye, forage 0.4
Rye, straw 0.4
Teosinte 0.4
Triticale 0.4
Wheat, forage 0.4
Wheat, hay 0.4
Wheat, straw 0.4

[68 FR 55849, Sept. 29, 2003, as amended at 71 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, 2007; 76 FR 23497, Apr. 27, 2011; 77 FR 59113, Sept. 26, 2012; 80 FR 72599, Nov. 20, 2015; 84 FR 21708, May 15, 2019; 87 FR 57626, Sept. 21, 2022; 88 FR 39780, June 20, 2023; 89 FR 85865, Oct. 29, 2024; 90 FR 52256, Nov. 20, 2025; 91 FR 7121, Feb. 17, 2026]

§ 180.474 Tebuconazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only tebuconazole [α-[2-(4-chlorophenyl) ethyl]-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol], in or on the commodity.

Commodity Parts per million
Almond, hulls 6.0
Apple, wet pomace 0.1
Asparagus 0.05
Banana 0.05
Barley, grain 0.3
Barley, hay 7.0
Barley, straw 3.5
Bean, dry seed 0.1
Bean, succulent 0.1
Beet, garden, roots 0.70
Beet, garden, tops 7.0
Brassica, leafy greens, subgroup 4-16B, except watercress 2.5
Cherry, sweet, pre- and post-harvest 5.0
Cherry, tart, pre- and post-harvest 5.0
Coffee, green bean 1 0.15
Coffee, roasted bean 1 0.3
Corn, field, forage 4.0
Corn, field, grain 0.05
Corn, field, stover 3.5
Corn, pop, grain 0.05
Corn, pop, stover 3.5
Corn, sweet, forage 7.0
Corn, sweet, kernel plus cob with husks removed 0.5
Corn, sweet, stover 6.0
Cotton, gin byproducts 25.0
Cottonseed, subgroup 20C 2
Fruit, pome, group 11-10 1
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 6
Ginseng, dried 1 0.40
Ginseng, fresh 1 0.15
Grain, aspirated fractions 16.0
Grass, forage 8.0
Grass, hay 25.0
Grass, seed screenings 55.0
Grass, straw 30.0
Hop, dried cones 35.0
Mango, postharvest 0.15
Nut, tree, group 14-12 0.05
Oat, forage 0.10
Oat, grain 0.15
Oat, hay 0.10
Oat, straw 0.10
Onion, bulb, subgroup 3-07A 0.2
Onion, green, subgroup 3-07B 1.3
Orange 1 1.0
Orange, oil 1 10
Peach subgroup 12-12B 2
Peanut 0.1
Plum subgroup 12-12C 1
Soybean, forage 25
Soybean, hay 50
Soybean, seed 0.08
Sunflower, subgroup 20B 0.1
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 1.6
Sunflower, meal 0.2
Sunflower, refined oil 0.2
Vegetable, cucurbit, group 9 0.4
Vegetable, fruiting, group 8-10 1.3
Watercress 9
Wheat, forage 3.0
Wheat, germ 0.20
Wheat, grain 0.15
Wheat, hay 7.0
Wheat, shorts 0.20
Wheat, straw 1.5
1 There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide tebuconazole, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of tebuconazole (alpha-[2-(4-chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol) and its diol metabolite (1-(4-chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4-triazole-1-yl-methyl)-pentane-3,5-diol), calculated as the stoichiometric equivalent of tebuconzole, in or on the commodity.

Commodity Parts per million
Cattle, meat byproducts 0.2
Goat, meat byproducts 0.2
Horse, meat byproducts 0.2
Milk 0.1
Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of the fungicide tebuconazole, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the commodity.

Commodity Parts per million
Turnip, roots 0.5
Turnip, tops 7.0

(d) Indirect or inadvertent residues. [Reserved]

[59 FR 39464, Aug. 3, 1994]

§ 180.475 Difenoconazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of difenoconazole, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1H-1,2,4-triazole, in or on the following raw agricultural commodities:

Commodity Parts per million
Almond, hulls 7.0
Apple, wet pomace 25
Artichoke, globe 1.5
Aspirated grain fractions 95
Banana1 0.2
Barley, grain 0.1
Barley, hay 0.05
Barley, straw 0.05
Beet, sugar, dried pulp 1.9
Berry, low growing, subgroup 13-07G, except cranberry 2.5
Brassica, leafy greens, subgroup 4-16B 35
Bushberry subgroup 13-07B 4.0
Citrus, dried pulp 2.0
Citrus, oil 25
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01
Cotton, gin byproducts 15
Cottonseed subgroup 20C 0.40
Cranberry 0.60
Dragonfruit1 1.5
Fruit, citrus, group 10-10 0.60
Fruit, pome, group 11-10 5.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0
Fruit, stone, group 12-12 2.5
Ginseng 2 1.0
Ginseng 0.8
Grape, raisin 6.0
Guava 3.0
Kohlrabi 2.0
Mango 1 0.07
Nut, tree, group 14-12 0.03
Oat, forage 0.15
Oat, grain 0.01
Oat, hay 0.05
Oat, straw 0.05
Olive 1 3
Olive, with pit 1 2
Onion, bulb, subgroup 3-07A 0.20
Onion, green, subgroup 3-07B 6.0
Papaya 0.60
Pea and bean, dried shelled, except soybean, subgroup 6C 0.20
Pea, field, hay 40
Pea, field, vines 10
Pepper, black 1 0.1
Persimmon, Japanese 1 0.7
Potato, wet peel 7.3
Rapeseed subgroup 20A 0.10
Rice, grain 7.0
Rice, wild, grain 7.0
Rye, forage 0.15
Rye, grain 0.01
Rye, straw 0.05
Soybean, hulls 0.20
Soybean, seed 0.15
Tea, dried 1 15
Vegetable, Brassica, head and stem, group 5-16 2.0
Vegetable, cucurbit, group 9 0.70
Vegetable, fruiting, group 8-10 0.60
Vegetable, leaves of root and tuber, group 2 8
Vegetable, root, subgroup 1A, except ginseng 0.6
Vegetable, tuberous and corm, subgroup 1C 4.0
Wax jambu 1 1.5
Wheat, forage 0.1
Wheat, grain 0.1
Wheat, hay 0.05
Wheat, straw 0.1
1 There are no U.S. registrations for these commodities.
2 This tolerance expires on August 14, 2020.

(2) Tolerances are established for residues of difenoconazole, including its metabolites and degradates, in the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring the sum of difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1H-1,2,4-triazole, and its metabolite, CGA-205375, 1-[2-chloro-4-(4-chloro-phenoxy)phenyl]-2-[1,2,4]triazol-1-yl-ethanol, calculated as the stoichiometric equivalent of difenoconazole, in the following commodities:

Commodity Parts per million
Cattle, fat 0.10
Cattle, liver 0.7
Cattle, meat 0.05
Cattle, meat byproduct (except liver) 0.10
Egg 0.02
Goat, fat 0.10
Goat, liver 0.7
Goat, meat 0.05
Goat, meat byproduct (except liver) 0.10
Hog, fat 0.10
Hog, liver 0.40
Hog, meat 0.05
Hog, meat byproduct (except liver) 0.10
Horse, fat 0.10
Horse, liver 0.7
Horse, meat 0.05
Horse, meat byproduct (except liver) 0.10
Milk 0.02
Sheep, fat 0.10
Sheep, liver 0.7
Sheep, meat 0.05
Sheep, meat byproduct (except liver) 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36254, July 6, 1999]

§ 180.476 Triflumizole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-propoxyethyl)-1 H -imidazole, and its metabolites containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as stoichiometric equivalent of the parent compound.

Table 1 to Paragraph (a)(1)

Commodity Parts
per million
Berry, low growing, subgroup 13-07G, except cranberry 2.0
Brassica, head and stem, subgroup 5A 8.0
Brassica, leafy greens, subgroup 5B 40
Canistel 2.5
Cherry, sweet 1.5
Cherry, tart 1.5
Cilantro, fresh leaves 35
Fruit, pome, group 11-10 0.50
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.5
Hazelnut 0.05
Hop, dried cones 50
Leafy greens subgroup 4A, except spinach 35
Mango 2.5
Papaya 2.5
Pineapple 4.0
Sapodilla 2.5
Sapote, black 2.5
Sapote, mamey 2.5
Star apple 2.5
Swiss chard 18
Tomato 1.5
Turnip, greens 40
Vegetable, cucurbit, group 9 0.5

(2) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and degradates, in or on the commodities of animal origin listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-propoxyethyl)-1 H -imidazole, the metabolite 4-chloro-2-hydroxy-6-trifluoromethylaniline sulfate, and other metabolites containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as the parent compound.

Table 2 to Paragraph (a)(2)

Commodity Parts
per million
Cattle, fat 0.10
Cattle, meat byproducts 0.20
Goat, fat 0.10
Goat, meat byproducts 0.20
Horse, fat 0.10
Horse, meat byproducts 0.20
Sheep, fat 0.10
Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33702, May 24, 2000, as amended at 67 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, 2002; 70 FR 7047, Feb. 10, 2005; 70 FR 17915, Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; 74 FR 46376, Sept. 9, 2009; 76 FR 34885, June 15, 2011; 79 FR 12408, Mar. 5, 2014; 80 FR 72599, Nov. 20, 2015; 91 FR 9727, Feb. 27, 2026]

§ 180.477 Flumiclorac pentyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide flumiclorac pentyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only flumiclorac pentyl, pentyl(2-chloro-4-fluoro-5-(1,3,4,5,6,7-hexahydro-1,3-dioxo-2H-isoindol-2-yl)phenoxy)acetate, in or on the commodity.

Commodity Parts per million
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Cotton, gin byproducts 3.0
Cotton, undelinted seed 0.2
Soybean, hulls 0.02
Soybean, seed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33702, May 24, 2000, as amended at 71 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, 2011]

§ 180.478 Rimsulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide rimsulfuron, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only rimsulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)amino] carbonyl]-3-(ethylsulfonyl)-2-pyridinesulfonamide.

Commodity Parts per million
Almond, hulls 0.09
Berry, low growing, except strawberry, subgroup 13-07H 0.02
Bushberry, subgroup 13-07B 0.01
Caneberry, subgroup 13-07A 0.01
Chicory, roots 0.01
Chicory, tops 0.01
Corn, field, forage 0.4
Corn, field, grain 0.1
Corn, field, stover 2.5
Fruit, citrus, group 10-10 0.01
Fruit, pome, group 11-10 0.01
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.01
Fruit, stone, group 12-12 0.01
Grain, aspirated fractions 4.5
Nut, tree, group 14-12 0.01
Pomegranate 0.01
Sorghum, grain, forage 0.01
Sorghum, grain, grain 0.01
Sorghum, grain, stover 0.01
Soybean, forage 0.25
Soybean, hay 1.2
Soybean, hulls 0.04
Soybean, seed 0.01
Tomato 0.05
Tropical and subtropical, small fruit, edible peel, subgroup 23A 0.01
Vegetable, tuberous and corm, subgroup 1C 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1(1), are established for residues of the herbicide rimsulfuron, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specific in the following table is to be determined by measuring only rimsulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)amino] carbonyl]-3-(ethylsulfonyl)-2-pyridinesulfonamide.

Commodity Parts per
million
Fescue, forage 0.01
Fescue, hay 0.01
Ryegrass, perennial, forage 0.01
Ryegrass, perennial, hay 0.01

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 16696, Apr. 6, 1998, as amended at 72 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, 2009; 77 FR 3625, Jan. 25, 2012; 77 FR 46306, Aug. 3, 2012; 80 FR 66805, Oct. 30, 2015; 83 FR 5947, Feb. 12, 2018; 88 FR 4735, Jan. 25, 2023]

§ 180.479 Halosulfuron-methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidiny)amino] carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only those halosulfuron-methyl residues containing the 3-chlorosulfonamide (3-CSA) moiety, expressed as the stoichiometric equivalent of halosulfuron-methyl, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 1.0
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 1.0
Hog, meat byproducts 0.1
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 1.0
Milk 0.05
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 1.0

(2) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only halosulfuron-methyl.

Commodity Parts per million
Alfalfa, forage 1.0
Alfalfa, hay 2.0
Almond, hulls 0.2
Artichoke 0.05
Asparagus 0.8
Bean, dry, seed 0.05
Bushberry, subgroup 13-07B 0.05
Caneberry subgroup 13-07A 0.05
Corn, field, forage 0.2
Corn, field, grain 0.05
Corn, field, stover 0.8
Corn, pop, grain 0.05
Corn, pop, stover 0.8
Corn, sweet, forage 0.2
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.8
Cotton, gin byproducts 0.05
Cotton, undelinted seed 0.05
Fruit, pome, group 11-10 0.05
Grass, forage, fodder, and hay, group 17, forage 20
Grass, forage, fodder, and hay, group 17, hay 0.5
Melon subgroup 9A 0.1
Millet, proso, forage 10
Millet, proso, grain 0.01
Millet, proso, hay 0.01
Millet, proso, straw 0.01
Nut, tree, group 14 0.05
Okra 0.05
Pea and bean, succulent shelled, subgroup 6 0.05
Pea and bean, succulent shelled, subgroup 6B 0.05
Pistachio 0.05
Rhubarb 0.05
Rice, grain 0.05
Sorghum, grain, forage 0.05
Sorghum, grain, grain 0.05
Sorghum, grain, stover 0.1
Soybean, seed 0.05
Squash/Cucumber subgroup 9B 0.5
Sugarcane, cane 0.05
Vegetable, fruiting, group 8 0.05
Vegetable, tuberous and corm, subgroup 1C 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only halosulfuron-methyl.

Commodity Parts per million
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.05

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25448, May 12, 1999, as amended at 65 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, 2001; 66 FR 66786, Dec. 27, 2001; 67 FR 45649, July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; 74 FR 48401, Sept. 23, 2009; 75 FR 46853, Aug. 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, Dec. 3, 2012; 78 FR 53051, Aug. 28, 2013; 80 FR 55773, Sept. 17, 2015; 80 FR 72599, Nov. 20, 2015]

§ 180.480 Fenbuconazole; tolerances for residues.

(a) Tolerances are established for residues of the fungicide fenbuconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of fenbuconazole, alpha-[2-(4-chlorophenyl)-ethyl]-alpha-phenyl-3-(1H-1,2,4-triazole)-1-propanenitrile, and its metabolites RH-9129, cis-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3 H-furanone, and RH-9130, trans-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3 H-furanone, calculated as the stoichiometric equivalent of fenbuconazole, in or on the following agricultural commodities.

Commodity Parts per million
Almond 0.05
Almond, hulls 1.0
Apple 0.4
Apple, wet pomace 1.0
Banana 0.3
Beet, sugar, dried pulp 1.0
Beet, sugar, molasses 0.4
Beet, sugar, roots 0.3
Beet, sugar, tops 9.0
Bushberry subgroup 13B 0.3
Cattle, meat byproducts 0.05
Citrus, dried pulp 5.0
Citrus, oil 40.0
Cranberry 0.5
Fruit, citrus, group 10 1.0
Fruit, stone, group 12 1.0
Goat, meat byproducts 0.05
Grain, aspirated fractions 6.0
Grape 1 1.0
Horse, meat byproducts 0.05
Peanut 0.1
Pecan 0.05
Pepper 1.0
Sheep, meat byproducts 0.05
Tea, dried 2 30
Tea, instant 2 30
Wheat, forage 4.0
Wheat, grain 0.1
Wheat, hay 8.0
Wheat, straw 8.0
1 There are no United States registrations for grape as of August 2006.
2 There are no U.S. registrations for use of fenbuconazole on tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[60 FR 11032, Mar. 1, 1995]

§ 180.481 Prosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of prosulfuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only prosulfuron (N-[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]-2-(3,3,3-trifluoropropyl)benzenesulfonamide) in or on the commodity.

Commodity Parts per
million
Grain, cereal, forage, fodder, and straw, group 16, forage 0.10
Grain, cereal, forage, fodder, and straw, group 16, hay 0.20
Grain, cereal, forage, fodder, and straw, group 16, stover 0.01
Grain, cereal, forage, fodder, and straw, group 16, straw 0.02
Grain, cereal, group 15 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 67118, Dec. 18, 2009, as amended at 82 FR 31475, July 7, 2017]

§ 180.482 Tebufenozide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, in or on the commodity.

Commodity Parts per million
Almond, hulls 30
Apple, dry pomace 3.0
Apple, wet pomace 3.0
Bushberrry subgroup 13-07B 3.0
Brassica, head and stem, subgroup 5A 5.0
Brassica, leafy greens, subgroup 5B 10.0
Canola, refined oil 4.0
Canola, seed 2.0
Caneberry subgroup 13-07A 3.0
Citrus, oil 15.0
Cotton 1.5
Cotton, gin byproducts 30
Cranberry 1.0
Fruit, citrus, group 10-10 2.0
Fruit, pome 1 1.5
Fruit, pome, group 11-10 1.0
Grape 3.0
Kiwifruit 2 0.5
Leaf petioles subgroup 4B 2.0
Leafy greens subgroup 4A 10.0
Nut, tree, group 14-12 0.1
Peppermint, tops 10.0
Spearmint, tops 10.0
Sugarcane, cane 1.0
Sugarcane, molasses 3.0
Turnip, greens 9.0
Turnip, roots 0.3
Vegetable, fruiting, group 8-10 1.0
Vegetable, tuberous and corm, except potato, subgroup 1D 0.015
1 This tolerance expires on May 16, 2018.
2 There are no U.S. registrations on kiwifruit.

(2) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and its metabolites, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-((4-carboxymethyl)benzoyl)hydrazide, 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, stearic acid conjugate of 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the stoichiometric equivalent of tebufenozide, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.08
Cattle, meat byproducts 0.08
Goat, fat 0.1
Goat, meat 0.08
Goat, meat byproducts 0.08
Hog, fat 0.1
Hog, meat 0.08
Hog, meat byproducts 0.08
Horse, fat 0.1
Horse, meat 0.08
Horse, meat byproducts 0.08
Milk 0.04
Sheep, fat 0.1
Sheep, meat 0.08
Sheep, meat byproducts 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide tebufenozide, including its metabolites and degradates, in or on the commodities in the table in this paragraph when present therein as a result of the application of tebufenozide to growing crops listed in the table to paragraph (a)(1) of this section. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and its metabolite, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the stoichiometric equivalent of tebufenozide, in or on the commodity.

Commodity Parts per million
Animal feed, nongrass, group 18 1.0
Grain, cereal, forage, fodder and straw, group 16 1.0
Grass, forage, fodder and hay, group 17 1.0
Vegetable, foliage of legume, group 7 0.20

[60 FR 29347, May 31, 1995]

§ 180.484 Flutolanil; tolerances for residues.

(a) General. Tolerances are established for residues of flutolanil, N-(3-(1-methylethoxy) phenyl)-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only flutolanil and its metabolites converted to 2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Cattle, fat 0.1
Cattle, kidney 1
Cattle, liver 2
Cattle, meat byproducts 0.05
Cattle, meat 0.05
Cotton, gin byproducts 0.2
Cotton, undelinted seed 0.2
Egg 0.05
Goat, fat 0.1
Goat, kidney 1
Goat, liver 2
Goat, meat byproducts 0.05
Goat, meat 0.05
Hog, fat 0.1
Hog, kidney 1
Hog, liver 2
Hog, meat byproducts 0.05
Hog, meat 0.05
Horse, fat 0.1
Horse, kidney 1
Horse, liver 2
Horse, meat byproducts 0.05
Horse, meat 0.05
Milk 0.05
Peanut 0.5
Peanut, hay 20
Peanut, meal 1
Potato 0.2
Potato, wet peel 0.3
Poultry, fat 0.05
Poultry, meat 0.05
Poultry, meat byproducts 0.05
Rice, bran 10
Rice, grain 7
Sheep, fat 0.1
Sheep, kidney 1
Sheep, liver 2
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Soybean, forage 8
Soybean, hay 2.5
Soybean, seed 0.2
Turnip greens 0.2
Vegetable, brassica, leafy, group 5 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of flutolanil, N-(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only flutolanil and its metabolites converted to 2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the following commodities.

Table 2 to Paragraph (d)

Commodity Parts per million
Wheat, bran 0.2
Wheat, forage 2.5
Wheat, grain 0.05
Wheat, hay 1.2
Wheat, straw 0.2

[60 FR 42458, Aug. 16, 1995, as amended at 61 FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7, 1998; 66 FR 10825, Feb. 20, 2001; 71 FR 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, 2010; 75 FR 80350, Dec. 22, 2010; 80 FR 72599, Nov. 20, 2015; 91 FR 8087, Feb. 20, 2026]

§ 180.485 Cyproconazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the free and conjugated forms of the fungicide cyproconazole, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1). Compliance with the proposed tolerance levels specified in table 1 to this paragraph (a)(1) is to be determined by measuring only cyproconazole (α-(4-chlorophenyl)-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Cattle, fat 0.01
Cattle, meat byproducts, except liver 0.01
Coffee, green bean 1 0.1
Corn, field, forage 0.6
Corn, field, grain 0.01
Corn, field, stover 1.2
Goat, fat 0.01
Goat, meat byproducts, except liver 0.01
Grain, aspirated fractions 2.5
Horse, fat 0.01
Horse, meat byproducts, except liver 0.01
Peanut 0.01
Peanut, hay 6
Sheep, fat 0.01
Sheep, meat byproducts, except liver 0.01
Soybean, forage 1
Soybean, hay 3
Soybean, oil 0.1
Soybean, seed 0.05
Wheat, forage 0.8
Wheat, grain 0.08
Wheat, hay 1.3
Wheat, milled byproducts 0.1
Wheat, straw 0.9
1 There are no U.S. registrations.

(2) A tolerance is established for the combined residues of the free and conjugated forms of the fungicide cyproconazole, including its metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) and its metabolite δ-(4-chlorophenyl)-β,δ-dihydroxy-γ-methyl-1H-1,2,4-triazole-1-hexenoic acid, calculated as the stoichiometric equivalent of cyproconazole, in or on the following commodity:

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Milk 0.02

(3) Tolerances are established for the combined residues of the free and conjugated forms of the fungicide cyproconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) and its metabolite 2-(4-chlorophenyl)-3-cyclopropyl-1-[1,2,4]triazol-1-yl-butane-2,3-diol, calculated as the stoichiometric equivalent of cyproconazole, in or on the following commodities:

Table 3 to Paragraph (a)(3)

Commodity Parts per million
Cattle, liver 0.5
Goat, liver 0.5
Hog, liver 0.01
Horse, liver 0.5
Sheep, liver 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 53835, Oct. 7, 1998, as amended at 71 FR 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; 78 FR 37473, June 21, 2013; 91 FR 8112, Feb. 20, 2026]

§ 180.486 Chlorethoxyfos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide chlorethoxyfos, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only chlorethoxyfos, O,O-diethyl O-(1,2,2,2-tetrachloroethyl) phosphorothioate, in or on the commodity.

Commodity Parts per million
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23498, Apr. 27, 2011]

§ 180.487 Pyrithiobac sodium; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, pyrithiobac sodium, (sodium 2-chloro-6-[(4,6-dimethoxypyrimidin-2-yl)thio]benzoate), resulting from the application of the pesticide chemical in or on the following foods/feeds:

Commodity Parts per million
Cotton, gin byproducts 0.15
Cotton, undelinted seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 54783, Oct. 22, 1997, as amended at 64 FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 2002]

§ 180.490 Imazapic; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide imazapic, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid) and its metabolites (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-hydroxymethyl-3-pyridinecarboxylic acid and (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(β-D-glucopyranosyloxy)methyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.

Commodity Parts per million
Grass, forage 15
Grass, hay 30
Peanut 0.1
Soybean, seed 1 0.40
Sugarcane, cane 2 0.03
1 There are no US registrations as of April 4, 2014.
2 There are no U.S. registrations as of June 4, 2014.

(2) Tolerances are established for residues of the herbicide imazapic, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid) and its metabolite (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-hydroxymethyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.

Commodity Parts per million
Cattle, fat 0.10
Cattle, kidney 1.0
Cattle, meat byproducts, except kidney 0.1
Cattle, meat 0.1
Goat, fat 0.1
Goat, kidney 1.0
Goat, meat byproducts, except kidney 0.1
Goat, meat 0.1
Horse, fat 0.1
Horse, kidney 1.0
Horse, meat byproducts, except kidney 0.1
Horse, meat 0.1
Milk 0.1
Sheep, fat 0.1
Sheep, kidney 1.0
Sheep, meat byproducts, except kidney 0.1
Sheep, meat 0.1

(3) Tolerances are established for residues of the herbicide imazapic, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by measuring only imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3-pyridinecarboxylic acid).

Table 3 to Paragraph (a)(3)

Commodity Parts per million
Rice, bran 0.2
Rice, grain 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 54224, Oct. 6, 1999, as amended at 66 FR 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013; 79 FR 18818, Apr. 4, 2014; 79 FR 32170, June 4, 2014; 88 FR 52042, Aug. 7, 2023]

§ 180.491 Propylene oxide; tolerances for residues.

(a) General. Tolerances are established for residues of the fumigant propylene oxide, including its metabolites and its degradates, including the reaction products propylene chlorohydrin and propylene bromohydrin, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only propylene oxide in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Cacao bean, cocoa powder 200
Cacao bean, dried bean 200
Fig, dried 3
Garlic, dried 300
Ginger, dried 300
Grape, raisin 1
Herbs and spices, group 19, dried 300
Nut, tree, group 14-12 300
Onion, dried 300
Pepper, bell, dried 300
Pepper, nonbell, dried 300
Plum, prune, dried 2
Sesame, seed 300
Turmeric, roots, dried 300

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33702, May 24, 2000, as amended at 68 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, 2007; 73 FR 54963, Sept. 24, 2008; 76 FR 38037, June 29, 2011; 77 FR 28495, May 15, 2012; 91 FR 21389, Apr. 22, 2026; 91 FR 31962, May 29, 2026]

§ 180.492 Triflusulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of triflusulfuron-methyl, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only triflusulfuron-methyl (methyl 2-[[[[[4-(dimethylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-yl]amino]carbonyl]amino]sulfonyl]-3-methylbenzoate) in or on the following commodities:

Commodity Parts per million
Beet, garden, roots 0.01
Beet, garden, tops 0.02
Beet, sugar, roots 0.05
Beet, sugar, tops 0.05
Chicory, roots 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 40196, June 12, 2002, as amended at 76 FR 22625, Apr. 22, 2011]

§ 180.493 Dimethomorph; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only dimethomorph in or on the commodities.

Commodity Parts per million
Brassica, head and stem, subgroup 5A 6.0
Brassica, leafy greens, subgroup 5B 30.0
Ginseng 0.90
Grape 3.0
Grape, raisin 7.0
Hop, dried cones 60
Onion, bulb, subgroup 3-07A 0.6
Onion, green, subgroup 3-07B 15.0
Papaya 1 1.5
Potato 0.05
Potato, wet peel 0.20
Strawberry 0.90
Taro, corm 0.5
Taro, leaves 6.0
Turnip, greens 20.0
Vegetable, cucurbit, group 9 0.5
Vegetable, fruiting, group 8 1.5
Vegetable, leafy (except Brassica) group 4 30.0
1 There are no U.S. registrations as of January 20, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the fungicide dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only dimethomorph in or on the commodity.

Commodity Parts per million
Bean, lima, succulent 0.60

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only dimethomorph in or on the commodity.

Commodity Parts per million
Wheat, forage 0.15
Wheat, hay 0.15
Wheat, straw 0.4

[62 FR 26416, May 14, 1997]

§ 180.494 Pyridaben; tolerance for residues.

(a) General. Tolerances are established for residues of the insecticide pyridaben, including its metabolites and degradates, in or on the commodities as indicated in the following table. Compliance with the tolerance levels specified below for plant commodities is to be determined by measuring the insecticide pyridaben [2-tert-butyl-5-(4-tert-butylbenzylthio)-4-chloropyridazin-3(2H)-one] on the plant commodity. Compliance with the tolerance levels specified below for animal commodities is to be determined by measuring the insecticide pyridaben and its metabolites, [2-tert-butyl-5-(4-(1-carboxy-1-methylethy 1) benzylthio)-4-chloropyridazin-3 (2H)one] and [2-tert-butyl-5-[4(-1, l-dimethyl-2-hydroxyethyl)benzylthio-4-chloropyridazin-3(2H)one] on the animal commodity.

Commodity Parts per
million
Almond, hulls 4.0
Apple, wet pomace 0.75
Berry, low growing, subgroup 13-07G, except cranberry 2.5
Canistel 0.10
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Citrus, dried pulp 1.5
Citrus, oil 10.0
Cucumber 0.50
Fruit, citrus group 10-10 0.9
Fruit, pome group 11-10 0.75
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 3.0
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Hop, dried cones 10.0
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Mango 0.10
Milk 0.01
Nut, tree, group 14-12 0.05
Papaya 0.10
Sapodilla 0.10
Sapote, black 0.10
Sapote, mamey 0.10
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Star apple 0.10
Tomato 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(m) are established for residues of the insecticide pyridaben, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring the insecticide pyridaben [2-tert-butyl-5-(4-tert-butylbenzylthio)-4-chloropyridazin-3(2H)-one] on the following plant commodity.

Commodity Parts per
million
Cranberry 0.5

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 43712, July 14, 2000, as amended at 66 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, 2005; 76 FR 56015, Sept. 15, 2010; 81 FR 70979, Oct. 14, 2016]

§ 180.495 Spinosad; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide spinosad, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spinosyn A (Factor A: CAS #131929-60-7; (2R,3aS,5aR,5bS,9S,13S,14R,16aS,16bR)-2-[(6-deoxy-2,3,4-tri-O-methyl-α-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5-(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-14-methyl-1H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione); and Spinosyn D (Factor D; CAS #131929-63-0) or (2S,3aR,5aS,5bS,9S,13S,14R,16aS,16bS)-2-[(6-deoxy-2,3,4-tri-O-methyl-α-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5-(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-4,14-dimethyl-1H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione), calculated as the stoichiometric equivalent of spinosad.

Table 1 to Paragraph (a)

Commodity Parts per million
Acerola 1.5
Alfalfa, seed 0.15
Alfalfa, seed screenings 2.0
Almond, hulls 19
Amaranth, grain, grain 1.0
Amaranth, grain, stover 10
Animal feed, nongrass, group, 18 0.02
Animal feed, nongrass, group, 18, forage 35.0
Animal feed, nongrass, group, 18, hay 30.0
Apple, dry pomace 0.5
Apple, wet pomace 0.5
Artichoke, globe 0.3
Atemoya 0.3
Avocado 0.3
Banana 0.25
Beet, sugar, molasses 0.75
Berry, low growing, except strawberry, subgroup 13-07H 0.04
Berry, low growing, subgroup 13-07G, except cranberry 0.90
Biriba 0.3
Bushberry subgroup 13-07B 0.40
Caneberry subgroup 13-07A 1.0
Canistel 0.3
Cattle, fat 50
Cattle, liver 10
Cattle, meat 2.0
Cattle, meat byproducts, except liver 5.0
Celtuce 8
Cherimoya 0.3
Citrus, oil 3.0
Citrus, dried pulp 0.5
Coffee, green bean 0.04
Corn, sweet, kernel plus cob with husks removed 0.02
Cotton, gin byproducts 1.5
Cottonseed subgroup 20C 0.02
Custard apple 0.3
Date 0.10
Dragon fruit 1.5
Egg 0.30
Feijoa .05
Fennel, Florence, fresh leaves and stalk 8
Fig 0.10
Fish 4.0
Fish-shellfish, crustacean 4.0
Fish-shellfish, mollusc 4.0
Food commodities 0.02
Fruit, citrus, group 10-10 0.30
Fruit, pome, group 11-10 0.20
Fruit, small, vine climbing, subgroup13-07F, except fuzzy kiwifruit 0.50
Fruit, stone 12-12 0.20
Goat, fat 50
Goat, liver 10
Goat, meat 2.0
Goat, meat byproducts, except liver 5.0
Grain, aspirated fractions 200
Grain, cereal, group 15 1.5
Grain, cereal, group 16, forage, except rice 2.5
Grain, cereal, group 16, hay, except rice 10.0
Grain, cereal, group, 16, stover, except rice 10.0
Grain, cereal, group, 16, straw, except rice 1.0
Grape, raisin 1.0
Grass, forage, fodder and hay, group 17, forage 10.0
Grass, forage, fodder and hay, group 17, hay 5.0
Guava 0.3
Herb subgroup 19A, dried 22
Herb subgroup 19A, fresh 3.0
Hog, fat 5.0
Hog, meat 0.50
Hog, meat byproducts 2.0
Hop, dried cones 22
Horse, fat 50
Horse, liver 10
Horse, meat 2.0
Horse, meat byproducts, except liver 5.0
Ilama 0.3
Jaboticaba 0.3
Kohlrabi 2
Leaf petiole vegetable subgroup 22B 8
Longan 0.3
Lychee 0.3
Mango 0.3
Milk 7.0
Milk, fat 85
Nut, tree, group 14-12 0.10
Onion, bulb, subgroup 3-07A 0.10
Onion, green, subgroup 3-07B 4.0
Papaya 0.3
Passionfruit 0.3
Pea and bean, dried shelled, except soybean, subgroup 6C 0.02
Pea and bean, succulent shelled, subgroup 6B 0.02
Peanut 0.02
Peanut, hay 11.0
Peppermint, tops 3.5
Pineapple 0.02
Pineapple, process residue 0.08
Pomegranate 0.30
Poultry, fat 1.3
Poultry, meat 0.10
Poultry, meat byproducts 0.20
Pulasan 0.3
Quinoa, grain 0.02
Rambutan 0.3
Rice, hulls 4.0
Sapodilla 0.3
Sapote, black 0.3
Sapote, mamey 0.3
Sapote, white 0.3
Sheep, fat 50
Sheep, liver 10
Sheep, meat 2.0
Sheep, meat byproducts, except liver 5.0
Soursop 0.3
Soybean 0.02
Spanish lime 0.3
Spearmint, tops 3.5
Spice group 26 1.7
Stalk and stem vegetable subgroup 22A 0.4
Star apple 0.3
Starfruit 0.3
Sugar apple 0.3
Tea, dried 1 2
Tea, instant 1 2
Ti, leaves 10.0
Vegetable, Brassica, head and stem, group 5-16 2
Vegetable, cucurbit, group 9 0.3
Vegetable, foliage of legume, group 7 8.0
Vegetable, fruiting, group 8-10 0.40
Vegetable, leafy, group 4-16 10
Vegetable, leaves of root and tuber, group 2 10.0
Vegetable, legume, edible podded, subgroup 6A 0.30
Vegetable, root and tuber, group 1 0.10
Watercress 8.0
Wax jambu 0.3
1 There are no U.S. registrations for use on tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[72 FR 68540, Dec. 5, 2007, as amended at 74 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, 2009; 75 FR 60327, Sept. 30, 2010; 80 FR 72599, Nov. 20, 2015; 80 FR 80672, Dec. 28, 2015; 84 FR 49201, Sept. 19, 2019; 86 FR 17913, Apr. 7, 2021; 88 FR 58505, Aug. 28, 2023]

§ 180.498 Sulfentrazone; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolite HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Soybean, seed 0.05

(2) Tolerances are established for the combined residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Apple 0.15
Berry and small fruit, group 13-07 0.15
Brassica, leafy greens, subgroup 4-16B 0.60
Chia, seed 0.15
Corn, field, forage 0.20
Corn, field, grain 0.15
Corn, field, stover 0.30
Corn, pop, grain 0.15
Corn, pop, stover 0.3
Flax, seed 0.15
Fruit, citrus, group 10-10 0.15
Horseradish 0.20
Melon, subgroup 9A 0.15
Nut, tree, group 14-12 0.15
Pea and bean, dried shelled, except soybean, subgroup 6C 0.15
Pea, succulent 0.15
Peanut 0.20
Peanut, meal 0.40
Peppermint, tops 0.30
Rhubarb 0.15
Spearmint, tops 0.30
Stalk and stem vegetable subgroup 22A 0.15
Sugarcane, cane 0.15
Sugarcane, molasses 0.20
Sunflower subgroup 20B 0.20
Teff, forage 0.50
Teff, grain 0.15
Teff, hay 0.30
Teff, straw 1.5
Turnip, roots 0.15
Vegetable, Brassica, head and stem, group 5-16 0.20
Vegetable, fruiting, group 8-10 0.15
Vegetable, soybean, succulent 0.15
Vegetable, tuberous and corm, subgroup 1C 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities.

Commodity Parts per
million
Bean, lima, succulent 0.15
Cowpea, succulent 0.15
Wheat, forage 0.50
Wheat, grain 0.15
Wheat, hay 0.30
Wheat, straw 1.5

(d) Indirect or inadvertent residues. Tolerances are established for inadvertent and indirect combined residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities when present therein as a result of the application of sulfentrazone to growing crops.

Commodity Parts per million
Grain, cereal (excluding sweet corn), Hulls 0.30
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage 0.2
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; hay 0.2
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; stover 0.1
Grain, cereal, forage, fodder and straw, group 16, except sweet corn; straw 0.6
Grain, cereal, group 15, except sweet corn 0.1
Grain, cereal, group 15, except sweet corn; bran 0.15

[62 FR 10708, Mar. 10, 1997]

§ 180.499 Propamocarb; tolerances for residues.

(a) General. Tolerances are established for the residues of propamocarb, including its metabolites and degradates, in or on the commodities specified in table 1 to this paragraph (a) resulting from the application of the hydrochloride salt of propamocarb. Compliance with the tolerance levels in table 1 to this paragraph (a) is to be determined by measuring only propamocarb (propyl N-[3-(dimethylamino)propyl]carbamate):

Table 1 to Paragraph (a)

Commodity Parts per
million
Guava 0.05
Kale 1 20
Leafy greens subgroup 4-16A 150
Leek 1 30
Onion, bulb, crop subgroup 3-07A 1 2
Starfruit 0.05
Tomato, paste 5.0
Vegetable, Brassica, Head and Stem, Group 5-16 15
Vegetable, cucurbit, group 9 1.5
Vegetable, fruiting, group 8-10 4
Vegetable, tuberous and corm, subgroup 1C 0.3
1 There are no U.S. registrations for these commodities as of September 30, 2022.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerance with regional registrations. Tolerances with regional registrations are established for the residues of propamocarb, including its metabolites and degradates, in or on the commodities specified in the following table resulting from the application of the hydrochloride salt of propamocarb. Compliance with the following tolerance levels is to be determined by measuring only propamocarb (propyl N-[3-(dimethylamino)propyl]carbamate):

Commodity Parts per
million
Bean, lima, succulent 2.0

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 15620, Apr. 2, 1997, as amended at 62 FR 26966, May 16, 1997; 63 FR 32136, June 12, 1998; 64 FR 16843, Apr. 7, 1999; 65 FR 58399, Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; 69 FR 47022, Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005; 78 FR 33736, June 5, 2013; 82 FR 9523, Feb. 7, 2017; 84 FR 66620, Dec. 5, 2019; 86 FR 57756, Oct. 19, 2021; 87 FR 59327, Sept. 30, 2022]

§ 180.500 Imazapyr; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, imazapyr, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the residues of imazapyr [2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-pyridinecarboxylic acid].

Table 1 to Paragraph (a)

Commodity Parts per million
Cattle, fat 0.05
Cattle, kidney 0.3
Cattle, meat 0.05
Cattle, meat byproducts, except kidney 0.05
Corn, field, forage 0.05
Corn, field, grain 0.05
Corn, field, stover 0.05
Fish 1.0
Goat, fat 0.05
Goat, kidney 0.3
Goat, meat 0.05
Goats, meat byproducts, except kidney 0.05
Grass, forage 100
Grass, hay 30
Horse, fat 0.05
Horse, kidney 0.3
Horse, meat 0.05
Horse, meat byproducts, except kidney 0.05
Lentil 1 0.2
Milk 0.01
Rapeseed subgroup 20A 1 0.05
Rice, bran 1 0.15
Rice, grain 1 0.06
Sheep, fat 0.05
Sheep, kidney 0.3
Sheep, meat 0.05
Sheep, meat byproducts, except kidney 0.05
Shellfish 0.10
Soybean, meal 1 4.5
Soybean, seed 1 4.0
Sunflower subgroup 20B 1 0.05
1 There are no U.S. registrations as of August 24, 2023.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55484, Sept. 26, 2003, as amended at 78 FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, 2014; 88 FR 57894, Aug. 24, 2023; 91 FR 9727, Feb. 27, 2026]

§ 180.501 Hydroprene; tolerances for residues.

(a) General. A tolerance of 0.2 part per million is established for residues of hydroprene [(S)-(Ethyl (2E,4E,7S)-3,7,11-trimrthyl-2,4-dodecadienoate)], (CAS Reg. No. 65733-18-8) on food commodities in food-handling establishments in accordance with the following prescribed conditions:

(1) Application shall be limited to spot, crack and crevice, perimeter and ultra low volume (ULV) fogging treatment in food storage or food-handling establishments, including warehouses, food service, manufacturing, and processing establishments such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries where food and food products are held, processed, and served: Provided that the food is removed or covered prior to such use, and food-processing surfaces are covered during treatment or thoroughly cleaned before using, or in the case of point-source device treatments, devices must not come into direct contact with food preparation surfaces and must be in a minimum distance of 3 feet from exposed foods.

(2) To assure safe use of the insect growth regulator, the label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 61647, Nov. 19, 1997, as amended at 71 FR 74818, Dec. 13, 2006]

§ 180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.

(a) General. Tolerances are established for residues of aminoethoxyvinylglycine hydrochloride (aviglycine HCl) in or on the following food commodities:

Commodity Parts per million
Apple 0.08
Fruit, stone, group 12, except cherry 0.170
Pear 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 24838, May 7, 1997, as amended at 64 FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12, 2001; 69 FR 7606, Feb. 18, 2004]

§ 180.503 Cymoxanil, tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide, cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]-2-(methoxyimino) acetamide, in or on the following food commodities:

Commodity Parts per million
Caneberry, subgroup 13A-07 4.0
Cilantro, leaves 19
Hop, dried cones 7.0
Leafy greens, subgroup 4A 19
Leaf petioles, subgroup 4B 6.0
Lychee 1 1.0
Onion, bulb, subgroup 3-07A 0.05
Onion, green, subgroup 3-07B 1.1
Potato 0.05
Vegetable, cucurbit, group 9 0.05
Vegetable, fruiting, group 8 0.2
1 There is no U.S. registration for lychee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with a regional registration. Tolerances with a regional registration as defined in § 180.1(l) are established for the residues of the fungicide cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]-2-(methoxyimino) acetamide) in or on the raw agricultural commodities:

Commodity Parts per million
Grape 0.10

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 26411, May 14, 1997, as amended at 62 FR 39956, July 25, 1997; 63 FR 24949, May 6, 1998; 63 FR 66464, Dec. 2, 1998; 64 FR 6539, Feb. 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR 41936, July 16, 2003; 70 FR 7047, Feb. 10, 2005; 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, 2008; 76 FR 34885, June 15, 2011]

§ 180.504 [Reserved]

§ 180.505 Emamectin; tolerances for residues.

(a) General.

(1) Tolerances are established for emamectin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of emamectin (a mixture of a minimum of 90% 4′-epi-methylamino-4′-deoxyavermectin B1a and maximum of 10% 4′-epi-methylamino-4′-deoxyavermectin B1b) and its metabolites 8,9-isomer of the B1a and B1b component of the parent (8,9-ZMA), or 4′-deoxy-4′-epi-amino-avermectin B1a and 4'-deoxy-4′-epi-amino-avermectin B1b; 4′-deoxy-4′-epi-amino avermectin B1a (AB1a); 4′-deoxy-4′-epi-(N-formyl-N-methyl)amino-avermectin (MFB1a); and 4′-deoxy-4′-epi-(N-formyl)amino-avermectin B1a (FAB1a), calculated as the stoichiometric equivalent of emamectin.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 0.20
Apple, wet pomace 0.075
Artichoke, globe 0.05
Brassica, leafy greens, subgroup 4-16B 0.2
Celtuce 0.1
Cherry subgroup 12-12A 0.09
Cotton, gin byproducts 0.050
Cotton, undelinted seed 0.025
Fennel, florence, fresh leaves and stalk 0.1
Fruit, pome, group 11-10 0.02
Grape, wine 1 0.03
Herb subgroup 19A 0.4
Kohlrabi 0.05
Leaf petiole vegetable subgroup 22B 0.1
Leafy greens subgroup 4-16A 1
Nut, tree, group 14-12 0.02
Soybean, seed 0.01
Tea, dried 2 0.5
Tea, instant 2 0.5
Tomato, paste 0.150
Vegetable, brassica, head and stem, group 5-16 0.05
Vegetable, cucurbit, group 9 0.02
Vegetable, fruiting, group 8-10 0.02
1 There are no U.S. registrations for use of emamectin on grape, wine.
2 Emamectin benzoate has not been registered for use in the United States as of February 17, 2021.

(2) Tolerances are established for emamectin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of emamectin (MAB1a + MAB1b isomers) and the associated 8,9-Z isomers (8,9-ZB1a and 8,9-ZB1b).

Commodity Parts per million
Cattle, fat 0.010
Cattle, liver 0.050
Cattle, meat 0.003
Cattle, meat byproducts, except liver 0.020
Goat, fat 0.010
Goat, liver 0.050
Goat, meat 0.003
Goat, meat byproducts, except liver 0.020
Hog, fat 0.003
Hog, liver 0.020
Hog, meat 0.002
Hog, meat byproducts (except liver) 0.005
Horse, fat 0.010
Horse, liver 0.050
Horse, meat 0.003
Horse, meat byproducts, except liver 0.020
Milk 0.003
Sheep, fat 0.010
Sheep, liver 0.050
Sheep, meat 0.003
Sheep, meat byproducts, except liver 0.020

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[71 FR 18649, Apr. 12, 2006, as amended at 74 FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 2013; 78 FR 49939, Aug. 16, 2013; 84 FR 44725, Aug. 27, 2019; 86 FR 9868, Feb. 17, 2021; 86 FR 44620, Aug. 13, 2021]

§ 180.506 Cyclanilide; tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator, cyclanilide, [1-(2,4-dichlorophenylaminocarbonyl)-cyclopropane carboxylic acid] determined as 2,4-dichloroaniline (calculated as cyclanilide) in or on the following food commodities and processed feed:

Commodity Parts Per Million
Cattle, fat 0.10
Cattle, meat 0.02
Cattle, meat byproducts, except kidney 0.2
Cattle, kidney 2.0
Cotton, undelinted seed 0.60
Cotton, gin byproducts 25.0
Goat, fat 0.10
Goat, meat 0.02
Goat, meat byproducts, except kidney 0.20
Goat, kidney 2.0
Horse, fat 0.10
Horse, meat 0.02
Horse, meat byproducts, except kidney 0.20
Horse, kidney 2.0
Hog, fat 0.10
Hog, meat 0.02
Hog, meat byproducts, except kidney 0.20
Hog, kidney 2.0
Milk 0.04
Sheep, fat 0.10
Sheep, meat 0.20
Sheep, meat byproducts, except kidney 0.20
Sheep, kidney 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 28355, May 23, 1997; 62 FR 34182, June 25, 1997]

§ 180.507 Azoxystrobin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to be determined by measuring only the sum of azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate], and the Z-isomer of azoxystrobin [methyl(Z)-2-(2-(6-(2-cyanophenoxy)pyrimidin-4-yloxy)phenyl)-3 methoxyacrylate] in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Acerola 2.0
Almond, hulls 4.0
Animal feed, nongrass, group 18, forage 45
Animal feed, nongrass, group 18, hay 120
Artichoke, globe 4.0
Asparagus 0.04
Atemoya 2.0
Avocado 2.0
Banana *
Barley, bran 6.0
Barley, forage 25
Barley, grain 3.0
Barley, hay 10.0
Barley, straw 15.0
Beet, sugar, roots 5.0
Berry, low growing, subgroup 13-07G, except cranberry 10.0
Biriba 2.0
Brassica, head and stem, subgroup 5A 3.0
Brassica, leafy greens, subgroup 5B 25
Bushberry subgroup 13-07B 5.0
Caneberry subgroup 13-07A 5.0
Canistel 2.0
Cherimoya 2.0
Cilantro, leaves 30.0
Citrus, dried pulp 20.0
Citrus, oil 40.0
Coffee, green bean 1 0.03
Corn, field, forage 12.0
Corn, field, grain 0.05
Corn, field, refined oil 0.3
Corn, field, stover 25.0
Corn, pop, grain 0.05
Corn, pop, stover 25.0
Corn, sweet, forage 12.0
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 25.0
Cotton, gin byproducts 45
Cottonseed subgroup 20C 0.7
Cranberry 0.50
Custard apple 2.0
Dragon fruit 2.0
Feijoa 2.0
Fruit, citrus, group 10-10 15.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 2.0
Ginseng 1 0.5
Grain, aspirated fractions 420
Grass, forage 15
Grass, hay 20
Guava 2.0
Herb Subgroup 19A, dried leaves 260
Herb Subgroup 19A, fresh leaves 50
Hop, dried cones 20.0
Ilama 2.0
Jaboticaba 2.0
Jackfruit 2.0
Longan 2.0
Loquat 2.0
Lychee 2.0
Mango 4
Nut, tree, group 14-12, except pistachio 0.02
Oats, forage 5.0
Oats, grain 1.5
Oats, hay 10.0
Oats, straw 3.0
Onion, bulb, subgroup 3-07A 1.0
Onion, green, subgroup 3-07B 7.5
Palm, oil 2 0.06
Papaya 6
Passionfruit 2.0
Pawpaw 2.0
Pea and bean, dried shelled, except soybean, subgroup 6C 0.5
Pea and bean, succulent shelled, subgroup 6B 0.5
Peanut 0.2
Peanut, hay 15.0
Peanut, refined oil 0.6
Pear, Asian 1 0.07
Pepper, black 3 1
Pepper/eggplant subgroup 8-10B 3.0
Peppermint, tops 30
Persimmon 2.0
Pistachio 0.50
Pulasan 2.0
Quinoa, grain 3.0
Rambutan 2.0
Rapeseed subgroup 20A 1.0
Rice, grain 5.0
Rice, hulls 20
Rice, wild, grain 5.0
Rye, forage 7.0
Rye, grain 0.2
Rye, straw 1.5
Sapodilla 2.0
Sapote, black 2.0
Sapote, mamey 2.0
Sapote, white 2.0
Sorghum, grain, forage 25
Sorghum, grain, grain 11
Sorghum, grain, stover 40
Soursop 2.0
Soybean, hay 55.0
Soybean, hulls 1.0
Soybean, seed 0.5
Spanish lime 2.0
Spearmint, tops 30
Spice Subgroup 19B, except black pepper 38
Star apple 2.0
Starfruit 2.0
Sugar apple 2.0
Sugarcane, cane 0.2
Sunflower subgroup 20B 0.5
Tamarind 2.0
Tea, dried 1 20.0
Ti, leaves 50.0
Ti, roots 0.5
Tomato, paste 0.6
Tomato subgroup 8-10A 0.2
Turnip, greens 25
Vegetable, cucurbit, group 9 0.3
Vegetable, foliage of legume, group 7 30.0
Vegetable, leafy, except brassica, group 4 30.0
Vegetable, leaves of root and tuber, group 2 50.0
Vegetable, legume, edible podded, subgroup 6A, except soybean 3.0
Vegetable, root, except sugar beet, subgroup 1B 1.0
Vegetable, tuberous and corm, subgroup 1C 8.0
Wasabi, dry 260
Wasabi, fresh 50
Watercress 3.0
Wax jambu 2.0
Wheat, forage 15.0
Wheat, grain 0.2
Wheat, hay 30.0
Wheat, straw 10.0
* 2.0 (of which not more than 0.1 is contained in the pulp)
1 There are no United States registrations for use of azoxystrobin on coffee, green bean; ginseng; pear, Asian and tea, dried.
2 There are no U.S. registrations on palm, oil as of March 20, 2023.
3 There are no U.S. registrations for use of azoxystrobin on pepper, black as of December 8, 2025.

(2) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to be determined by measuring only azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate] in or on the commodity.

Commodity Parts per million
Cattle, fat 0.03
Cattle, meat 0.01
Cattle, meat byproducts 0.07
Goat, fat 0.03
Goat, meat 0.01
Goat, meat byproducts 0.07
Hog, fat 0.010
Hog, meat 0.01
Hog, meat byproducts 0.010
Horse, fat 0.03
Horse, meat 0.01
Horse, meat byproducts 0.07
Milk 0.006
Sheep, fat 0.03
Sheep, meat 0.01
Sheep, meat byproducts 0.07

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 32235, June 13, 1997]

§ 180.509 Mefenpyr-diethyl; tolerance for residues.

(a) General. Tolerances are established for residues of the safener, mefenpyr-diethyl, including its metabolites and degradates, when applied at a rate no greater than 0.053 pound safener per acre per growing season in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl-1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the stoichiometric equivalent of mefenpyr-diethyl, in or on the commodity.

Commodity Parts per
million
Barley, grain 0.05
Barley, hay 0.2
Barley, straw 0.5
Cattle, meat byproducts 0.1
Goat, meat byproducts 0.1
Grass, forage 1.6
Grass, hay 0.2
Hog, meat byproducts 0.1
Horse, meat byproducts 0.1
Sheep, meat byproducts 0.1
Sorghum, grain, forage 0.4
Sorghum, grain, grain 0.04
Sorghum, grain, stover 0.2
Wheat, forage 0.2
Wheat, grain 0.05
Wheat, hay 0.2
Wheat, straw 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of mefenpyr-diethyl, including its metabolites and degradates, when applied at a rate no greater than 0.053 pound safener per acre per growing season in or on the commodities identified in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl-1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the stoichiometric equivalent of mefenpyr-diethyl, in or on the commodity.

Commodity Parts per
million
Canola, seed 0.02
Soybean, forage 0.1
Soybean, hay 0.1
Soybean, seed 0.02

[73 FR 74977, Dec. 10, 2008, as amended at 76 FR 23903, Apr. 29, 2011]

§ 180.510 Pyriproxyfen; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of pyriproxyfen, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified is determined by measuring only pyriproxyfen, 2-[1-methyl-2-(4-phenoxyphenoxy) ethoxy]pyridine, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Acerola 0.10
Almond, hulls 2.0
Animal feed, nongrass, group 18, forage 0.70
Animal feed, nongrass, group 18, hay 1.1
Animal feed, nongrass, group 18, seed 2.0
Apple, wet pomace 0.8
Artichoke, globe 2.0
Asparagus 2.0
Atemoya 0.20
Avocado 1.0
Banana 0.20
Beet, sugar, dried pulp 3.0
Berry, low growing, except strawberry, subgroup 13-07H 1.0
Biriba 0.20
Brassica, head and stem, subgroup 5A 0.70
Brassica, leafy greens, subgroup 5B 2.0
Bushberry subgroup 13-07B 1.0
Cacao bean, dried 0.02
Caneberry subgroup 13-07A 1.0
Canistel 1.0
Canola, seed 0.20
Cherimoya 0.20
Citrus, oil 20
Citrus, dried pulp 2.0
Coffee, instant 0.10
Coffee, green bean 0.02
Cotton, gin byproducts 2.0
Cotton, undelinted seed 0.05
Custard apple 0.20
Date 0.30
Egg 0.1
Feijoa 0.10
Fig 0.30
Fig, dried fruit 1.0
Fruit, citrus, group 10-10 0.50
Fruit, pome, group 11-10 0.20
Fruit, small, vine climbing, except grape, subgroup 13-07E 0.35
Fruit, stone, group 12 1.0
Grain, cereal, group 15 1.1
Grain, cereal, forage, fodder and straw, group 16 1.1
Grape 2.5
Grass, forage, fodder, and hay, group 17, forage 0.70
Grass, forage, fodder, and hay, group 17, hay 1.1
Guava 0.10
Herb subgroup 19A 100
Ilama 0.20
Jaboticaba 0.10
Lychee 0.30
Mango 1.0
Nut, tree, group 14 0.02
Olive 1.0
Olive, oil 2.0
Papaya 1.0
Passionfruit 0.10
Pawpaw 1.0
Peanut 0.20
Pineapple 0.30
Pineapple, process residue 1.1
Pistachio 0.02
Pomegranate 0.20
Potato, chips 0.75
Potato, granules/flakes 0.75
Potato, wet peel 0.75
Poultry, fat 0.1
Poultry, meat 0.1
Poultry, meat byproducts 0.1
Pulasan 0.30
Rambutan 0.30
Rice, hulls 5.5
Safflower, seed 0.20
Sapodilla 1.0
Sapote, black 1.0
Sapote, mamey 1.0
Sapote, white 0.30
Sesame, seed 0.02
Soursop 0.20
Spanish lime 0.30
Star apple 1.0
Starfruit 0.10
Strawberry 0.30
Sugar apple 0.20
Sugarcane 1.1
Tea 15
Vegetable, bulb, group 3-07 0.70
Vegetable, cucurbit, group 9 0.10
Vegetable, foliage of legume, group 7 2.0
Vegetable, fruiting, group 8-10 0.80
Vegetable, leafy, except Brassica, group 4 3.0
Vegetable, leaves of root and tuber, group 2 2.0
Vegetable, legume, group 6 0.20
Vegetable, root and tuber, group 1 0.15
Walnut 0.02
Watercress 2.0
Wax jambu 0.10

(2) A tolerance of 0.10 parts per million is established for all food commodities as a result of the proposed use of NYLAR in food handling establishments where food and food products are held, prepared, processed or served. Application is limited to space, general surface, spot, and/or crack and crevice treatment in food handling establishments where food and food products are held, processed, prepared and served. Space and general surface application may be used only when the facility is not in operation provided exposed food is covered or removed from the area being treated prior to application. Spot, and/or crack and crevice treatment may be used while the facility is in operation provided exposed food is covered or removed from the area being treated prior to application. Food contact surfaces should be thoroughly washed with an effective cleaning compound and rinced with potable water after use of the product. To assure safe use of this additive, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency, and shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 10233, Mar. 3, 1999]

§ 180.511 Buprofezin; tolerances for residues.

(a) General. Tolerances are established for residues of buprofezin, including its metabolites and degradates in or on the commodities in the table in this paragraph (a). Compliance with the tolerance levels specified in the table in this paragraph (a) is to be determined by measuring only the buprofezin, 2-[(1,1-dimethylethyl)imino]tetrahydro-3-(1-methylethyl)-5-phenyl-4H-1,3,5-thiadiazin-4-one, in the commodity.

Commodity Parts per million
Almond, hulls 2.0
Apricot 3 9.0
Atemoya 0.30
Avocado 0.30
Banana 0.20
Bean, asparagus, edible podded 0.02
Bean, catjang, edible podded 0.02
Bean, french, edible podded 0.02
Bean, garden, edible podded 0.02
Bean, goa, edible podded 0.02
Bean, green, edible podded 0.02
Bean, guar, edible podded 0.02
Bean, kidney, edible podded 0.02
Bean, lablab, edible podded 0.02
Bean, moth, edible podded 0.02
Bean, mung, edible podded 0.02
Bean, navy, edible podded 0.02
Bean, rice, edible podded 0.02
Bean, scarlet runner, edible podded 0.02
Bean, snap, edible podded 0.02
Bean, succulent 0.02
Bean, sword, edible podded 0.02
Bean, urd, edible podded 0.02
Bean, wax, edible podded 0.02
Bean, yardlong, edible podded 0.02
Berry, low growing, subgroup 13-07G 2.5
Birida 0.30
Brassica, leafy greens, subgroup 4-16B 60
Bushberry subgroup 13-07B 0.08
Canistel 0.90
Cattle, fat 0.05
Cattle, kidney 0.05
Cattle, liver 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Celtuce 35
Cherimoya 0.30
Citrus, dried pulp 7.5
Citrus, oil 80
Coffee, green bean 0.35
Cotton, gin byproducts 20.0
Cottonseed subgroup 20C 0.35
Cowpea, edible podded 0.02
Custard apple 0.30
Feijoa 0.30
Fennel, Florence, fresh leaves and stalk 35
Fig 0.7
Fruit, citrus, group 10-10 4
Fruit, pome, group 11-10, except pear and pear, Asian 3.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1
Fruit, stone, group 12-12, except nectarine and peach 2
Goat, fat 0.05
Goat, kidney 0.05
Goat, liver 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Grape 3 2.5
Grape, raisin 2
Guava 0.3
Hog, fat 0.05
Hog, kidney 0.05
Hog, liver 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.05
Horse, kidney 0.05
Horse, liver 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Ilama 0.30
Jaboticaba 0.30
Jackbean, edible podded 0.02
Kohlrabi 12
Leaf petiole vegetable subgroup 22B 35
Leafy greens subgroup 4-16A 35
Longbean, chinese, edible podded 0.02
Mango 0.90
Milk 0.01
Nut, tree, group 14-12 0.05
Papaya 0.90
Passionfruit 0.30
Pea, winged, edible podded 0.02
Peach 9.0
Pear 6.0
Pear, Asian 6.0
Persimmon 1.9
Pomegranate 1.9
Pulasan 0.30
Rambutan 0.30
Rice, grain 1 1.5
Sapodilla 0.90
Sapote, black 0.90
Sapote, mamey 0.90
Sheep, fat 0.05
Sheep, kidney 0.05
Sheep, liver 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05
Soursop 0.30
Soybean, vegetable, edible podded 0.02
Star apple 0.90
Starfruit 0.30
Sugar apple 0.30
Tea2 20
Tropical and subtropical, small fruit, edible peel, subgroup 23A 5
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 0.3
Vegetable, Brassica, head and stem, group 5-16 12
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, group 8-10 2.0
Velvetbean, edible podded 0.02
1 There are no U.S. registrations as of July 10, 2017 for use on rice.
2 There are no U.S. registrations at this time.
3 This tolerance expires on March 2, 2020.

(b) Section 18 emergency exemption. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 40741, July 30, 1997]

§ 180.512 [Reserved]

§ 180.513 Chlorfenapyr; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of chlorfenapyr, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only chlorfenapyr, 4-bromo-2-(4-chlorophenyl)-1-(ethoxymethyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile, in or on the commodity.

Commodity Parts per
million
Basil, fresh leaves 80
Chive, fresh leaves 20
Cucumber 0.5
Tea, dried 1 70
Vegetable, fruiting, group 8-10 2
1 There are no U.S. registrations for Tea, dried as of January 26, 2018.

(2) A tolerance of 0.01 parts per million is established for residues of chlorfenapyr in or on all food commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling areas where food/feed products are prepared, held, processed, or served and in accordance with the following prescribed conditions:

(i) Application shall be no greater than a 0.5% active ingredient solution for spot crack and crevice use in food/feed handling establishments, where food and food products are held, processed, prepared and/or served.

(ii) Application may only be undertaken when the facility is not in operation, and provided exposed food has been covered, or removed from the area being treated prior to application.

(iii) Food contact surfaces and equipment should be throughly washed with an effective cleaning compound, and rinsed with potable water after each use of the product.

(iv) Contamination of food or food contact surfaces shall be avoided. Application excludes any direct application to any food, food packaging, or any food contact surfaces.

(v) To assure safe use, the label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55527, Sept. 26, 2003, as amended at 70 FR 3654, Jan. 26, 2005; 83 FR 3610, Jan. 26, 2018; 85 FR 8472, Feb. 14, 2020]

§ 180.514 Cloransulam-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, cloransulam-methyl, N-(2-carboxymethyl-6-chlorophenyl)-5-ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-pyrimidine-2-sulfonamide, plus its acid, cloransulam, calculated as parent ester in or on the following raw agricultural commodities:

Commodity Parts per million
Soybean, forage 0.1
Soybean, hay 0.2
Soybean, seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 49163, Sept. 19, 1997]

§ 180.515 Carfentrazone-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide carfentrazone-ethyl, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the following tolerance levels is to be determined by measuring only the sum of carfentrazone-ethyl (ethyl-alpha-2-dichloro-5-[-4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H -1,2,4-triazol-1-yl]-4-fluorobenzenepropanoate) and its metabolite carfentrazone-chloropropionic acid (alpha, 2-dichloro-5-[-4-difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]-4-fluorobenzenepropanoic acid), calculated as the stoichiometric equivalent of carfentrazone-ethyl, in or on the following commodities:

Commodity Parts per million
Acerola 0.10
Almond, hulls 0.20
Animal feed, nongrass, crop group 18, forage 2.0
Animal feed, nongrass, crop group 18, hay 5.0
Animal feed, nongrass, crop group 18, seed 15.0
Artichoke, globe 0.10
Asparagus 0.10
Atemoya 0.10
Avocado 0.10
Banana 0.10
Berry, low growing, subgroup 13-07G 0.10
Birida 0.10
Bushberry subgroup 13-07B 0.10
Cacao bean, bean 0.10
Cactus 0.10
Caneberry subgroup 13-07A 0.10
Canistel 0.10
Cattle, fat 0.10
Cattle, meat 0.10
Cattle, meat byproducts 0.10
Cherimoya 0.10
Coffee, bean, green 0.10
Cotton, gin byproducts 10
Cottonseed subgroup 20C 0.20
Custard apple 0.10
Date, dried fruit 0.10
Feijoa 0.10
Fig 0.10
Fish 0.30
Fruit, citrus, group 10-10 0.10
Fruit, pome, group 11-10 0.10
Fruit, small vine climbing, subgroup 13-07F, except Fuzzy kiwifruit 0.10
Fruit, stone, group 12-12 0.10
Goat, fat 0.10
Goat, meat 0.10
Goat, meat byproducts 0.10
Grain, aspirated grain fractions 1.8
Grain, cereal, group 15 (except rice grain and sorghum grain) 0.10
Grain, cereal, group 16, forage 1.0
Grain, cereal, group 16, hay 0.30
Grain, cereal, group 16, stover 0.80
Grain, cereal, group 16, straw 3.0
Grass, forage 5.0
Grass, hay 8.0
Guava 0.10
Herbs and spices group 19 2.0
Hog, fat 0.10
Hog, meat 0.10
Hog, meat byproducts 0.10
Hop, dried cones 0.10
Horse, fat 0.10
Horse, meat 0.10
Horse, meat byproducts 0.10
Horseradish 0.10
Ilama 0.10
Jaboticaba 0.10
Kava, roots 0.10
Kiwifruit 0.10
Longan 0.10
Lychee 0.10
Mango 0.10
Milk 0.05
Noni 0.10
Nut, tree, group 14-12 0.10
Olive 0.10
Palm heart 0.10
Palm heart, leaves 0.10
Papaya 0.10
Passionfruit 0.10
Pawpaw 0.10
Peanut 0.10
Peanut, hay 0.10
Peppermint, tops 0.10
Persimmon 0.10
Pomegranate 0.10
Poultry, meat byproducts 0.10
Psyllium, seed 0.10
Pulasan 0.10
Quinoa, grain 0.10
Rambutan 0.10
Rapeseed, forage 0.10
Rapeseed subgroup 20A 0.10
Rice, grain 1.3
Sapodilla 0.10
Sapote, black 0.10
Sapote, mamey 0.10
Sheep, fat 0.10
Sheep, meat 0.10
Sheep, meat byproducts 0.10
Shellfish 0.30
Sorghum, grain 0.25
Soursop 0.10
Soybean, seed 0.10
Spanish lime 0.10
Spearmint, tops 0.10
Star apple 0.10
Starfruit 0.10
Stevia 0.10
Strawberrypear 0.10
Sugar apple 0.10
Sugarcane 0.15
Sunflower, subgroup 20B 0.10
Tea, dried 0.10
Teff, forage 1.0
Teff, grain 0.25
Teff, hay 0.30
Teff, straw 3.0
Ti, leaves 0.10
Ti, roots 0.10
Vanilla 0.10
Vegetable, brassica, leafy, group 5 0.10
Vegetable, bulb, group 3-07 0.10
Vegetable, cucurbit, group 9 0.10
Vegetable, foliage of legume, except soybean, subgroup 7A 0.10
Vegetable, fruiting, group 8-10 0.10
Vegetable, leafy, except brassica, group 4 0.10
Vegetable, leaves of root and tuber, group 2 0.10
Vegetable, legume, group 6 0.10
Vegetable, root and tuber, group 1 0.10
Wasaba, roots 0.10
Wax jambu 0.10
1 Effective Date to be removed: May 18, 2016.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 52180, Sept. 30, 1998]

§ 180.516 Fludioxonil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile).

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Acerola 5.0
African Tree Nut 0.01
Almond 0.2
Almond, hulls 15
Animal feed, nongrass, group 18 0.01
Atemoya 20
Avocado 5.0
Banana1 3
Bean, dry 0.4
Bean, succulent 0.4
Beechnut 0.2
Beet, sugar, roots 4.0
Berry, low growing, subgroup 13-07G, except cranberry 3.0
Biriba 20
Brassica, leafy greens, subgroup 4-16B, except watercress 15
Brazil nut 0.01
Brazilian pine 0.2
Bunya 0.2
Bur oak 0.01
Bushberry subgroup 13-07B 2.0
Butternut 0.01
Cajou 0.01
Candlenut 0.2
Caneberry subgroup 13-07A 5.0
Canistel 5.0
Carrot, roots 7
Cashew 0.01
Celtuce 15
Cherimoya 20
Chestnut 0.2
Chinquapin 0.2
Citrus, oil 500
Coconut 0.01
Coquito nut 0.01
Cotton, gin byproducts 0.05
Cottonseed subgroup 20C 0.05
Cranberry 0.04
Custard apple 20
Dika nut 0.01
Dragon fruit 20
Durian 20
Feijoa 5.0
Fennel, Florence, fresh leaves and stalk 15
Flax, seed 0.05
Fruit, citrus, group 10-10 10
Fruit, pome, group 11-10 5.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 5.0
Ginkgo 0.2
Ginseng 4.0
Grain, cereal, group 15 0.02
Grain, cereal, forage, fodder, and straw, group 16 0.01
Grass, forage, fodder and hay, group 17 0.01
Guava 5.0
Guiana chestnut 0.01
Hazelnut 0.01
Heartnut 0.01
Herb subgroup 19A, dried leaves 65
Herb subgroup 19A, fresh leaves 10
Hickory nut 0.01
Ilama 20
Jaboticaba 5.0
Jackfruit 20
Japanese horse-chestnut 0.01
Kiwifruit, fuzzy 20
Kohlrabi 2
Leaf petioles subgroup 4B 15
Leaf petiole vegetable subgroup 22B 15
Leafy greens subgroup 4-16A 30
Macadamia nut 0.01
Mango 8
Mangosteen 5
Mongongo nut 0.01
Monkey puzzle 0.2
Monkey-pot 0.01
Okari nut 0.2
Onion, bulb, subgroup 3-07A 0.50
Onion, green, subgroup 3-07B 7.0
Pachira nut 0.01
Papaya 5
Passionfruit 5.0
Peach palm nut 0.2
Peanut 0.01
Peanut, hay 0.01
Pecan 0.01
Pequi 0.2
Persimmon, Japanese 5
Pili nut 0.2
Pine nut 0.2
Pineapple 20
Pistachio 0.1
Pomegranate 5.0
Pulasan 20
Rambutan 20
Rapeseed, forage 0.01
Rapeseed subgroup 20A, except flax seed 0.01
Sapodilla 5.0
Sapote, black 5.0
Sapote, mamey 5.0
Sapucaia nut 0.01
Soursop 20
Spice subgroup 19B 0.02
Star apple 5.0
Starfruit 5.0
Sugar apple 20
Sunflower subgroup 20B 0.01
Tomato 5.0
Tropical almond 0.2
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 20
Turnip, greens 10
Vegetable, Brassica, head and stem, group 5-16 2
Vegetable, cucurbit, group 9 0.45
Vegetable, foliage of legume, group 7 0.01
Vegetable, fruiting, group 8-10, except tomato 0.50
Vegetable, leaves of root and tuber, group 2 30
Vegetable, legume, group 6, except bean 0.01
Vegetable, root, except sugar beet, subgroup 1B 0.75
Vegetable, tuberous and corm, subgroup 1C 6
Walnut, black 0.01
Walnut, English 0.01
Watercress 10
Wax jambu 5.0
Yam, true, tuber 8.0
Yellowhorn 0.01
1 There are no U.S. registrations as of July 28, 2021.

(2) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile), and its metabolites converted to 2,2-difluoro-l,3-benzodioxole-4-carboxylic acid, calculated as the stoichiometric equivalent of fludioxonil.

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.01
Cattle, meat byproducts 0.05
Goat, fat 0.05
Goat, meat 0.01
Goat, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.01
Horse, meat byproducts 0.05
Milk 0.01
Sheep, fat 0.05
Sheep, meat 0.01
Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 56082, Oct. 29, 1997]

§ 180.517 Fipronil; tolerances for residues.

(a) General. Therefore, tolerances are established for combined residues of the insecticide fipronil (5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile) and its metabolites 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl) sulfonyl]-1H-pyrazole-3-carbonitrile and 5-amino-1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-4-[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile and its photodegradate 5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile in or on the following items at the levels specified:

Commodity Parts per million
Cattle, fat 0.40
Cattle, liver 0.10
Cattle, meat 0.04
Cattle, meat byproducts, except liver 0.04
Corn, field, grain 0.02
Corn, field, stover 0.30
Corn, field, forage 0.15
Egg 0.03
Goat, fat 0.40
Goat, liver 0.10
Goat, meat 0.04
Goat, meat byproducts, except liver 0.04
Hog, fat 0.04
Hog, liver 0.02
Hog, meat 0.01
Hog, meat byproducts, except liver 0.01
Horse, fat 0.40
Horse, liver 0.10
Horse, meat 0.04
Horse, meat byproducts, except liver 0.04
Milk, fat (reflecting 0.05 ppm in whole milk) 1.50
Potato 0.03
Potato, wet peel 0.10
Poultry, fat 0.05
Poultry, meat 0.02
Poultry, meat byproducts 0.02
Rice, grain 0.04
Sheep, fat 0.40
Sheep, liver 0.10
Sheep, meat 0.04
Sheep, meat byproducts, except liver 0.04

(b) Section 18 emergency exemptions.. Time-limited tolerances are established for combined residues of the insecticide, fipronil, 5-amino-1-(2,6-dichloro-4-(trifluoromethyl) phenyl)-4-((1,R,S)-trifluoromethyl)sulfinyl)-1-H-pyrazole-3-carbonitrile and its 2 metabolites MB45950 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile) and MB46136 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)sulfonyl]-1H-pyrazole-3-carbonitrile) and its photodegradate MB46513 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile), in connection with use of the pesticide under Section 18 emergency exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the table for this paragraph.

Commodity Parts per million Expiration/revocation date
Rutabaga 1.0 12/31/16
Turnip 1.0 12/31/16

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for combined indirect or inadvertent residues of the insecticide fipronil and its metabolites and photodegradate in or on food commodities when present therein as a result of the application of fipronil to growing crops listed in paragraphs (a) and (b) of this section and other nonfood crops to read as follows:

Commodity Parts per million
Wheat, forage 0.02
Wheat, grain 0.005
Wheat, hay 0.03
Wheat, straw 0.03

[62 FR 62979, Nov. 26, 1997, as amended at 63 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, 2007; 74 FR 46377, Sept. 9, 2009; 75 FR 80346, Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013; 80 FR 72599, Nov. 20, 2015]

§ 180.518 Pyrimethanil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in or on the commodities in the following table Compliance with the tolerance levels specified in the following table is to be determined by measuring only pyrimethanil (4,6-dimethyl-N-phenyl-2-pyrimidinamine).

Commodity Parts per million
Almond 0.20
Almond, hulls 12
Apple, wet pomace 40
Banana 0.10
Berry, low growing, subgroup 13-07G 3.0
Bushberry subgroup 13-07B 8.0
Caneberry subgroup 13-07A 15
Citrus, oil 150
Cucumber 1.5
Fruit, citrus, group 10-10 10
Fruit, pome, group 11-10 15
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 5.0
Fruit, stone, group 12-12 10
Ginseng 1.5
Grape, raisin 8.0
Onion, bulb, subgroup 3-07A 0.2
Onion, green, subgroup 3-07B 3.0
Pistachio 0.20
Pomegranate 5.0
Tomato subgroup 8-10A 0.50
Vegetable, tuberous and corm, subgroup 1C 0.05

(2) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of pyrimethanil and its metabolite 4-[4,6-dimethyl-2-pyrimidinyl)amino]phenol, calculated as the stoichiometric equivalent of pyrimethanil.

Commodity Parts per million
Cattle, fat 0.01
Cattle, kidney 2.5
Cattle, meat 0.01
Cattle, meat byproducts, except kidney 0.01
Goat, fat 0.01
Goat, kidney 2.5
Goat, meat 0.01
Goat, meat byproducts, except kidney 0.01
Horse, fat 0.01
Horse, kidney 2.5
Horse, meat 0.01
Horse, meat byproducts, except kidney 0.01
Sheep, fat 0.01
Sheep, kidney 2.5
Sheep, meat 0.01
Sheep, meat byproducts, except kidney 0.01

(3) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of pyrimethanil and its metabolite 4,6-dimethyl-2-(phenylamino)-5-pyrimidinol, calculated as the stoichiometric equivalent of pyrimethanil.

Commodity Parts per million
Milk 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63669, Dec. 2, 1997, as amended at 69 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, 2008; 74 FR 32448, July 8, 2009; 77 FR 45503, Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015; 80 FR 63691, Oct. 21, 2015]

§ 180.519 Bromide ion and residual bromine; tolerances for residues.

(a) General. The food additives, bromide ion and residual bromine, may be present in water, potable in accordance with the following conditions:

(1) The food additives are present as a result of treating water aboard ships with a polybrominated ion-exchange resin (as a source of bromine) under the supervision of trained personnel.

(2) Residual bromine levels are controlled to not exceed 1.0 part per million (ppm) in the final treated water. Control is effected using calibrated recirculating or proportioning bromine feeder equipment and periodic checks of residual bromine using a bromine test kit. To assure safe use of the additives, the label and labeling of the disinfectant formulation containing the food additives shall conform to the label and labeling registered by the U.S. Environmental Protection Agency.

(3) No tolerance is established for bromide ion levels.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988. Redesignated and amended at 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. 13, 2006]

§ 180.521 Fumigants for grain-mill machinery; tolerances for residues.

(a) General. Fumigants may be safely used in or on grain-mill machinery in accordance with the following prescribed conditions:

(1) The fumigants consist of methyl bromide.

(2) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the U.S. Environmental Protection Agency.

(3) Residues of inorganic bromides (calculated as Br) in milled fractions derived from cereal grain from all fumigation sources, including fumigation of grain-mill machinery, shall not exceed 125 parts per million.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, as amended at 49 FR 44459, Nov. 7, 1984. Further redesignated at 53 FR 24667, June 29, 1988, as amended at 54 FR 6130, Feb. 8, 1989. Further redesignated and amended at 63 FR 34319, June 24, 1998]

§ 180.522 Fumigants for processed grains used in production of fermented malt beverage; tolerances for residues.

(a) General. Fumigants for processed grain may be safely used, in accordance with the following conditions.

(1) Methyl bromide. Total residues of inorganic bromides (calculated as Br) from the use of this fumigant shall not exceed 125 parts per milion.

(2) Methyl bromide is used to fumigate corn grits and cracked rice in the production of fermented malt beverage.

(3) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the U.S. Environmental Protection Agency, and the usage employed should conform with such label or labeling.

(4) The total residue of inorganic bromides in fermented malt beverage, resulting from the use of corn grits and cracked rice fumigated with the fumigant described in paragraph (a)(2) of this section plus additional residues of inorganic bromides that may be present from uses in accordance with other regulations in this chapter promulgated under section 408 and/or 409 of the Act, does not exceed 25 parts per million bromide (calculated as Br).

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74818, Dec. 13, 2006]

§ 180.523 Metaldehyde; tolerances for residues.

(a) General. Tolerances are established for residues of the molluscicide metaldehyde, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the specified tolerance levels is to be determined by measuring only metaldehyde, 2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.

Commodity Parts per million
Artichoke, globe 0.07
Berry, low growing, subgroup 13-07G 6.25
Bushberry subgroup 13-07B 0.15
Cactus 0.07
Caneberry subgroup 13-07A 0.15
Corn, field, forage 0.30
Corn, field, grain 0.05
Corn, field, stover 0.10
Corn, sweet, forage 0.30
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.10
Fruit, citrus, group 10-10 0.26
Ginseng 0.05
Grass, forage 2.0
Grass, hay 2.0
Leaf petioles subgroup 4B 0.50
Lettuce 1.73
Pea and bean, succulent shelled, subgroup 6B 0.20
Peppermint, oil 12
Peppermint, tops 4.0
Spearmint, oil 12
Spearmint, tops 4.0
Taro, corm 0.15
Taro, leaves 1.0
Tomato subgroup 8-10A 0.24
Vegetable, brassica, leafy, group 5 2.5
Vegetable, foliage of legume, except soybean, subgroup 7A 1.5
Vegetable, legume, edible podded subgroup 6A 0.80
Watercress 3.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in § 180.1(l) are established for residues of the molluscicide metaldehyde, including its metabolites and degradates, in or on the following commodities. Compliance with the specified tolerance level is to be determined by measuring only metaldehyde, 2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.

Commodity Parts per million
Beet, garden, leaves 0.08
Beet, garden, roots 0.05
Clover, forage 0.60
Clover, hay 0.60
Hop, dried cones 0.10
Rutabaga, roots 0.05
Soybean, seed 0.05
Turnip greens 0.08
Turnip, roots 0.05
Wheat, forage 0.05
Wheat, grain 0.05
Wheat, hay 0.05
Wheat, straw 0.05

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54963, Sept. 24, 2008, as amended at 78 FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, 2015; 81 FR 71638, Oct. 18, 2016]

§ 180.525 Resmethrin; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide resmethrin [5-(phenylmethyl)-3-furanyl] methyl 2,2-dimethyl-3-(2-methyl-1-propenyl) cyclopropanecarboxylate in or on food commodities at 3.0 ppm resulting from use of the insecticide in food handling and storage areas as a space concentration for spot/or crack and crevice treatment and shall be limited to a maximum of 3.00 percent of the active ingredient by weight, and as a space treatment shall be limited to a maximum of 0.5 fluid ounce of 3.0 percent active ingredient by weight per 1000 cubic feet of space provided that the food is removed or covered prior to such use. To assure safe use of the additive, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency, and shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74819, Dec. 13, 2006]

§ 180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.

(a) General. Synthetic isoparaffinic petroleum hydrocarbons complying with 21 CFR 172.882 (a) and (b) may be safely used as a component of insecticide formulations for use on animal feed in an amount no greater than reasonably required to accomplish its intended effect as an adjuvant in the insecticide formulation and shall not be intended to accomplish any effect in animal feed. It is used or intended for use as a component of insecticide formulations used in compliance with regulations issued in 40 CFR part 180 and in this part.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR 24668, 24669, June 29, 1988. Redesignated and amended at 63 FR 34319, June 24, 1998]

§ 180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine moiety in or on the following commodities.

Commodity Parts per million
Cattle, kidney 0.05
Corn, field, forage 0.4
Corn, field, grain 0.05
Corn, field, stover 0.4
Corn, sweet, forage 0.45
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.30
Goat, kidney 0.05
Hog, kidney 0.05
Horse, kidney 0.05
Sheep, kidney 0.05
Soybean, seed 0.1
Wheat, bran 0.80
Wheat, forage 6.0
Wheat, grain 0.60
Wheat, hay 1.2
Wheat, straw 0.35

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for combined residues of flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide, and its metabolites containing the 4-fluoro-N-methylethyl benzenamine moiety, with regional registration.

Commodity Parts per million
Grass, forage 7.0
Grass, hay 0.4

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1,3,4-thiadiazol-2-yl]oxy]acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine moiety in or on the following raw agricultural commodities when present therein as a result of application of flufenacet to the growing crops in paragraph (a) of this section.

Commodity Parts per million
Alfalfa, forage 0.1
Alfalfa, hay 0.1
Alfalfa, seed 0.1
Clover, forage 0.1
Clover, hay 0.1
Grain, cereal, group 15, except rice 0.1
Grain, cereal, forage, fodder, and straw, group 16, except rice 0.1
Grass, forage, fodder, and hay, group 17 0.1

[63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, 1999; 65 FR 64366, Oct. 27, 2000; 68 FR 2247, Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; 72 FR 26310, May 9, 2007]

§ 180.532 Cyprodinil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine.

Table 1 to Paragraph (a)

Commodity Parts per
million
Acerola 1.5
Almond 0.02
Almond, hulls 8.0
Apple, wet pomace 4.6
Artichoke, globe 4.0
Avocado 1.2
Bean, dry 0.6
Bean, succulent 0.6
Berry, low growing, subgroup 13-07G, except cranberry 5.0
Brassica, leafy greens, subgroup 4-16B 10
Bushberry subgroup 13-07B 3.0
Caneberry subgroup 13-07A 10
Canistel 1.2
Canola, seed 1 0.03
Celtuce 30
Citrus, dried pulp 8.0
Citrus, oil 60
Cranberry 0.4
Dragon fruit 2.0
Feijoa 1.5
Fennel, Florence, fresh leaves and stalk 30
Fruit, pome, group 11-10 1.7
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0
Fruit, stone, group 12-12 2.0
Grape, raisin 5.0
Guava 1.5
Herb subgroup 19A, dried, except parsley 15.0
Herb subgroup 19A, fresh, except parsley 3.0
Jaboticaba 1.5
Kiwifruit 1.8
Kohlrabi 1
Leaf petiole vegetable subgroup 22B 30
Leafy greens subgroup 4-16A, except parsley, fresh leaves 50
Lemon/lime subgroup 10-10B 0.6
Mango 1.2
Nut, tree, group 14-12; except almond and pistachio 0.04
Onion, bulb, subgroup 3-07A 0.6
Onion, green, subgroup 3-07B 4.0
Papaya 1.2
Parsley, dried leaves 170
Parsley, leaves 35
Passionfruit 1.5
Pistachio 0.10
Pomegranate 10
Potato, wet peel 0.03
Pulasan 2.0
Rambutan 2.0
Sapodilla 1.2
Sapote, black 1.2
Sapote, mamey 1.2
Star apple 1.2
Starfruit 1.5
Sugar apple 4
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 2
Vegetable, Brassica, head and stem, group 5-16 1
Vegetable, cucurbit, group 9 0.70
Vegetable, fruiting, group 8-10 1.5
Vegetable, leaves of root and tuber, group 2 10
Vegetable, root, except sugarbeet, subgroup 1B 0.75
Vegetable, tuberous and corm, subgroup 1C 0.01
Watercress 20
Wax jambu 1.5
1 Import only.

(2) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and degradates, in the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine and free and conjugated CGA-304075 4-(4-cyclopropyl-6-methyl-pyrimidin-2-ylamino)-phenol, calculated as the stoichiometric equivalent of cyprodinil.

Commodity Parts per
million
Cattle, meat byproducts 0.02
Goat, meat byproducts 0.02
Horse, meat byproducts 0.02
Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 17706, Apr. 10, 1998]

§ 180.533 Esfenvalerate; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the insecticide esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, (R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as follows:

Commodity Parts per million
Almond 0.2
Almond, hulls 5.0
Apple 1.0
Artichoke, globe 1.0
Bean, dry, seed 0.25
Bean, snap, succulent 1.0
Beet, sugar, roots 0.05
Beet, sugar, tops 5.0
Blueberry 1.0
Broccoli 1.0
Cabbage, except Chinese cabbage 3.0
Caneberry subgroup 13A 1.0
Cantaloupe 0.5
Carrot, roots 0.5
Cattle, fat 1.5
Cattle, meat 1.5
Cattle, meat byproducts 1.5
Cauliflower 0.5
Collards 3.0
Corn, field, forage 15.0
Corn, field, grain 0.02
Corn, field, stover 15.0
Corn, pop, grain 0.02
Corn, pop, stover 15.0
Corn, sweet, forage 15.0
Corn, sweet, kernel plus cob with husks removed 0.1
Corn, sweet, stover 15.0
Cotton, undelinted seed 0.2
Cucumber 0.5
Egg 0.03
Eggplant 0.5
Elderberry 1.0
Fruit, stone, group 12 3.0
Goat, fat 1.5
Goat, meat 1.5
Goat, meat byproducts 1.5
Gooseberry 1.0
Hazelnut 0.2
Hog, fat 1.5
Hog, meat 1.5
Hog, meat byproducts 1.5
Horse, fat 1.5
Horse, meat 1.5
Horse, meat byproducts 1.5
Kiwifruit 0.5
Lentil, seed 0.25
Melon, honeydew 0.5
Milk 0.3
Milk, fat 7.0
Muskmelon 0.5
Mustard greens 5.0
Okra 0.5
Pea, dry, seed 0.25
Pea, succulent 0.5
Peanut 0.02
Pear 1.0
Pecan 0.2
Pepper 0.5
Potato 0.02
Poultry, fat 0.3
Poultry, liver 0.03
Poultry, meat 0.03
Poultry, meat byproducts, except liver 0.3
Pumpkin 0.5
Radish, roots 0.3
Radish, tops 3.0
Sheep, fat 1.5
Sheep, meat 1.5
Sheep, meat byproducts 1.5
Sorghum, grain, forage 10.0
Sorghum, grain, grain 5.0
Sorghum, grain, stover 10.0
Soybean, hulls 0.5
Soybean, seed 0.05
Squash, summer 0.5
Squash, winter 0.5
Sugarcane, cane 1.0
Sunflower, seed 0.5
Sweet potato, roots 0.05
Tomato 0.5
Turnip, greens 7.0
Turnip, roots 0.5
Walnut 0.2
Watermelon 0.5

(2) A tolerance of 0.05 ppm on raw agricultural food commodities (other than those food commodities already covered by a higher tolerance as a result of use on growing crops) is established for the combined residues of the insecticide esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, (R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate as a result of the use of esfenvalerate in food-handling establishments.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined residues of the insecticide esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, (R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as follows:

Commodity Parts per million
Cabbage, chinese, bok choy 1.0
Kohlrabi 2.0
Lettuce, head 5.0

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 23401, Apr. 29, 1998, as amended at 63 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, 2009]

§ 180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fluroxypyr 1-methylheptyl ester, including its metabolites and degradates, in or on the commodities listed in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring only the sum of the free and conjugated forms of fluroxypyr 1-methylheptyl ester [1-methylheptyl 2-[(4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy]acetate] and its metabolite fluroxypyr [2-[(4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy]acetic acid] calculated as the stoichiometric equivalent of fluroxypyr, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, forage 12
Barley, grain 0.5
Barley, hay 20
Barley, straw 12
Cattle, fat 0.1
Cattle, kidney 1.5
Cattle, meat byproducts 0.1
Corn, field, forage 1
Corn, field, grain 0.02
Corn, field, stover 0.5
Corn, sweet, forage 1
Corn, sweet, kernel plus cob with husks removed 0.02
Corn, sweet, stover 2
Fruit, pome, group 11 0.02
Garlic, bulb 0.03
Goat, fat 0.1
Goat, kidney 1.5
Goat, meat 0.1
Goat, meat byproducts 0.1
Grain, aspirated fractions 0.6
Grass, forage, fodder and hay, group 17, forage 120
Grass, forage, fodder and hay, group 17, hay 160
Hog, fat 0.1
Hog, kidney 1.5
Hog, meat 0.1
Hog, meat byproducts 0.1
Horse, fat 0.1
Horse, kidney 1.5
Horse, meat 0.1
Horse, meat byproducts 0.1
Milk 0.3
Millet, forage 12
Millet, grain 0.5
Millet, hay 20
Millet, proso, straw 12
Oat, forage 12
Oat, grain 0.5
Oat, hay 20
Oat, straw 12
Onion, bulb 0.03
Rice, bran 3
Rice, grain 1.5
Shallot, bulb 0.03
Sheep, fat 0.1
Sheep, kidney 1.5
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Sorghum, grain, forage 2
Sorghum, grain, grain 0.02
Sorghum, grain, stover 4
Teff, forage 12
Teff, grain 0.5
Teff, hay 20
Teff, straw 12
Wheat, forage 12
Wheat, grain 0.5
Wheat, hay 20
Wheat, straw 12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 52169, Sept. 30, 1998, as amended at 64 FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001; 66 FR 47971, Sept. 17, 2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; 70 FR 3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Dec. 28, 2007; 78 FR 3333, Jan. 16, 2013; 83 FR 29706, June 26, 2018; 91 FR 8113, Feb. 20, 2026]

§ 180.537 Isoxaflutole; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, isoxaflutole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of isoxaflutole ((5-cyclopropyl-4-isoxazolyl) [2-(methylsulfonyl)-4-(trifluoromethyl)phenyl] methanone) and its metabolite 1-(2-methylsulfonyl-4-trifluoromethylphenyl)-2-cyano-3-cyclopropyl propan-1,3-dione (RPA 202248), calculated as the stoichiometric equivalent of isoxaflutole, in or on the commodity:

Table 1 to Paragraph (a)

Commodity Parts per million
Corn, field, forage 0.04
Corn, field, grain 0.02
Corn, field, stover 0.02
Grain, aspirated fractions 0.3
Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 50784, Sept. 23, 1998, as amended at 73 FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, 2011; 91 FR 8088, Feb. 20, 2026]

§ 180.540 Fenitrothion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide fenitrothion, O,O-dimethyl O-(4-nitro-m-tolyl) phosphorothioate, from the postharvest application of the insecticide to stored wheat in Australia, in or on the following food commodity:

Commodity Parts per million
Wheat, gluten 1 3.0
1 There are no U.S. registrations on food commodities since 1987.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54963, Sept. 24, 2008]

§ 180.543 Diclosulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide diclosulam [N-(2,6-dichlorophenyl)-5-ethoxy-7-fluoro[1,2,4] triazolo[1,5-c]pyrimidine-2-sulfonamide] in or on the following raw agricultural commodities as follows:

Commodity Parts per
million
Peanut 0.020
Soybean, seed 0.020

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 12134, Mar. 8, 2000]

§ 180.544 Methoxyfenozide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only methoxyfenozide (3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide) in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Acerola 0.4
Achachairu 6
Almond, hulls 25
Ambarella 6
Animal feed, nongrass, group 18, forage 50.0
Animal feed, nongrass, group 18, hay 150.0
Apple, wet pomace 7.0
Araza 6
Artichoke, globe 3.0
Atemoya 0.60
Avocado 0.6
Babaco 6
Beet, sugar, roots 0.50
Berry, low growing, subgroup 13-07G, except cranberry 2.0
Bilimbi 6
Biriba 0.60
Borojo 6
Bushberry subgroup 13-07B 3.0
Cajou, fruit 6
Cambuca 6
Caneberry subgroup 13-07A 6.0
Canistel 0.6
Carob 6
ashew apple 6
Cattle, fat 0.50
Cattle, meat 0.02
Celtuce 25
Cherimoya 0.60
Chive, fresh leaves 30
Ciruela verde 6
Citrus, oil 100
Coffee bean 2 0.15
Corn, field, forage 15
Corn, field, refined oil 0.20
Corn, field, stover 125
Corn, pop, stover 125
Corn, sweet, forage 30
Corn, sweet, stover 60
Cotton, gin byproducts 35
Cottonseed subgroup 20C 7
Cranberry 0.5
Custard apple 0.60
Davidson's plum 6
Edible podded bean subgroup 6-22A 2
Edible podded pea subgroup 6-22B 2
Feijoa 6
Fennel, Florence, fresh leaves and stalk 25
Field corn subgroup 15-22C 0.05
Fig 6
Fruit, citrus, group 10-10 3.0
Fruit, pome, group 11-10 2.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0
Fruit, stone, group 12-12, except plum, prune, fresh 3.0
Goat, fat 0.50
Goat, meat 0.02
Gooseberry, Indian 6
Grain, aspirated grain fractions 120
Grain sorghum and millet subgroup 15-22E 6
Grape, raisin 1.5
Grass, forage, fodder and hay, group 17, forage 18.0
Grass, forage, fodder and hay, group 17, hay 30.0
Guava 0.4
Herb subgroup 19A, except chive, fresh leaves 400
Hog, fat 0.1
Hog, meat 0.02
Horse, fat 0.50
Horse, meat 0.02
Ilama 0.60
Imbe 6
Imbu 6
Jaboticaba 6
Jujube, Indian 6
Kohlrabi 7
Kwai muk 6
Leaf petiole vegetable subgroup 22B 25
Mangaba 6
Mango 0.6
Marian plum 6
Milk 0.10
Mombin, Malayan 6
Mombin, purple 6
Monkeyfruit 6
Nance 6
Natal plum 6
Noni 6
Nut, tree, group 14-12 0.10
Onion, green, subgroup 3-07B, except chive, fresh leaves 5.0
Papaya 0.6
Papaya, mountain 6
Passionfruit 0.4
Pea, blackeyed, seed 4.0
Pea, southern, seed 4.0
Peanut 0.02
Peanut, hay 55.0
Peanut, oil 0.04
Peppermint, tops 7.0
Persimmon, Japanese 6
Pineapple 0.70
Plum, prune, fresh 0.30
Pomegranate 0.6
Pomerac 6
Poultry, fat 0.02
Poultry, meat 0.02
Pulasan 2.0
Pulses, dried shelled bean, except soybean, subgroup 6-22E, except pea, blackeyed, seed and pea, southern, seed 0.5
Pulses, dried shelled pea subgroup 6-22F 0.5
Rambai 6
Rambutan 2.0
Rose apple 6
Sapodilla 0.6
Sapote, black 0.6
Sapote, mamey 0.6
Sentul 6
Sheep, fat 0.50
Sheep, meat 0.02
Sorghum, grain, forage 15
Sorghum, grain, stover 20
Sorghum, sweet, forage 15
Sorghum, sweet, grain 6
Sorghum, sweet, stalk 15
Sorghum, sweet, stover 20
Soursop 0.60
Soybean, aspirated grain fractions 160
Soybean, forage 30
Soybean, hay 80
Soybean, hulls 2.0
Soybean, seed 1.0
Spearmint, tops 7.0
Star apple 0.6
Starfruit 6
Succulent shelled bean subgroup 6-22C 0.3
Succulent shelled pea subgroup 6-22D 0.3
Sugar apple 0.60
Sugar cane 2 0.03
Sugar cane, molasses 2 0.1
Surinam cherry 6
Sweet corn subgroup 15-22D 0.05
Tamarind 6
Tea, dried 1 20
Tea, instant 1 20
Tropical and subtropical, palm fruit, edible peel, subgroup 23C 8
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 2
Uvalha 6
Vegetable, brassica, head and stem, group 5-16 7
Vegetable, cucurbit, group 9 0.3
Vegetable, foliage of legume, except soybean, subgroup 7A 35
Vegetable, fruiting, group 8-10 2.0
Vegetable, leafy, group 4-16 30
Vegetable, leaves of root and tuber, group 2 30
Vegetable, root, except sugar beet, Subgroup 1B 0.90
Vegetable, tuberous and corm, except potato, subgroup 1D 0.02
Wax jambu 0.4
1 There are no U.S. registrations as of March 12, 2019 for use on tea.
2 There are no U.S. registrations as of August 28, 2023.

(2) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of methoxyfenozide [3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and its glucuronide metabolite (β-D-Glucopyranuronic acid, 3-[[2-(1,1-dimethylethyl)-2-(3,5-dimethylbenzoyl)-hydrazino]carbonyl]-2-methylphenyl-), calculated as the stoichiometric equivalent of methoxyfenozide.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, liver 0.40
Cattle, meat byproducts, except liver 0.10
Egg 0.02
Goat, liver 0.40
Goat, meat byproducts, except liver 0.10
Hog, liver 0.1
Hog, meat byproducts, except liver 0.02
Horse, liver 0.40
Horse, meat byproducts, except liver 0.10
Poultry, liver 0.10
Poultry, meat byproducts, except liver 0.02
Sheep, liver 0.40
Sheep, meat byproducts, except liver 0.10

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances for regional registration are established for the insecticide methoxyfenozide, including its metabolites and degradates, in or on the raw agricultural commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only methoxyfenozide [3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide].

Table 3 to Paragraph (c)

Commodity Parts per million
Rice, hulls 55
Rice subgroup 15-22F 30

(d) Indirect or inadvertent tolerances.

(1) Tolerances are established for the indirect or inadvertent residues of the insecticide methoxyfenozide, including its metabolites and degradates, in or on the raw agricultural commodities in the following table, when present therein as a result of the application of methoxyfenozide to growing crops as listed in paragraph (a) of this section. Compliance with the tolerance levels specified in the following table is to be determined by measuring only methoxyfenozide [3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide].

Commodity Parts per
million
Onion, bulb, subgroup 3-07A 0.10
Potato 0.02

(2) Tolerances are established for the indirect or inadvertent residues of the insecticide methoxyfenozide, including its metabolites and degradates, in or on the raw agricultural commodities in the following table, when present therein as a result of the application of methoxyfenozide to growing crops as listed in paragraph (a) of this section. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of methoxyfenozide [3-methoxy-2-methylbenzoic acid, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and the following metabolites (all calculated as the stoichiometric equivalent of methoxyfenozide): free phenol of methoxyfenozide [3,5-dimethylbenzoic acid N-tert-butyl-N′-(3-hydroxy-2-methylbenzoyl) hydrazide], the glucose conjugate of the phenol [3,5-dimethyl benzoic acid N-tert-butyl-N′-[3 (β-D-glucopyranosyloxy)-2-methylbenzoyl]-hydrazide] and the malonylglycosyl conjugate of the phenol [3,5-dimethyl benzoic acid N-tert-butyl-N′-[3 (β-D-6-malonyl-glucopyranosyl-1-oxy)-2-methylbenzoyl]-hydrazide].

Commodity Parts per
million
Animal feed, nongrass, group 18, straw 8.0
Grain, cereal, forage, fodder and straw group 16, except corn 6.0
Rapeseed subgroup 20A 1.0
Spice subgroup 19B 4.5
Sunflower subgroup 20B 1.0

[67 FR 59203, Sept. 20, 2002]

§ 180.545 Prallethrin; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide prallethrin, including its metabolites and degradates, in or on all raw agricultural commodities and processed food from use of prallethrin in food handling establishments where food and food products are held, processed, prepared and/or served, or as a wide-area mosquito adulticide at 1.0 part per million (ppm). Compliance with the tolerance level specified is to be determined by measuring only prallethrin, 2-methyl-4-oxo-3-(2-propyn-1-yl)-2-cyclopenten-1-yl-2,2-dimethyl-3-(2-methyl-1-propen-1-yl)cyclopropanecarboxylate.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 64330, Oct. 29, 2014]

§ 180.546 Mefenoxam; tolerances for residues.

(a) General. Tolerances are established for residues of mefenoxam, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only metalaxyl (methyl N-(2,6-dimethylphenyl)-N-(methoxyacetyl)-DL-alaninate).

Table 1 to Paragraph (a)

Commodity Parts per million
Almond hulls 5
Artichoke, globe 0.05
Atemoya 0.20
Bean, snap, succulent 0.20
Bushberry subgroup 13-07B 2.0
Cacao, dried bean 0.20
Caneberry subgroup 13-07A 0.70
Canistel 0.40
Cottonseed, subgroup 20C 0.1
Custard apple 0.20
Fruit, small, vine climbing, except grape, subgroup 13-07E 0.10
Herbs, dried 55
Herbs, fresh 8.0
Leaf petiole, subgroup 22B 5
Leafy Vegetable, Crop Group 4-16 (except spinach) 5
Mango 0.40
Onion, bulb, subgroup 3-07A 3.0
Onion, green, subgroup 3-07B 10
Palm, oil 1 0.02
Papaya 0.40
Rapeseed subgroup 20A 0.05
Sapodilla 0.40
Sapote, black 0.40
Sapote, mamey 0.40
Spinach 10
Star apple 0.40
Starfruit 0.20
Sugar apple 0.20
Tree nut, crop group 14-12 0.3
Vegetable, Brassica, head and stem, group 5-16 2
Vegetable, fruiting, group 8-10 1
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.2
Vegetable, legume, pea, succulent shelled, subgroup 6-22D 0.2
Vegetable, stalk and stem, subgroup 22A 7
Wasabi, stem 3.0
Wasabi, tops 6.0
1 There is no U.S. registration as of November 4, 2024.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of mefenoxam in or on the food commodities when present therein as a result of the application of mefenoxam to growing crops listed in paragraph (a) of this section and other non-food crops to read as follows:

Table 2 to Paragraph (d)

Commodity Parts per
million
Sugarcane 0.1

[65 FR 57556, Sept. 25, 2000, as amended at 66 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, 2002; 76 FR 4548, Jan. 26, 2011; 81 FR 26727, May 4, 2016; 83 FR 65546, Dec. 21, 2018; 85 FR 72574, Nov. 13, 2020; 88 FR 39189, June 15, 2023; 89 FR 87512, Nov. 4, 2024]

§ 180.547 Prohexadione calcium; tolerances for residues.

(a) General. Tolerances are established for residues of the growth regulator, prohexadione calcium, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only prohexadione calcium (calcium 3-oxido-5-oxo-4-propionylcyclohex-3-enecarboxylate)” in or on the following commodities.

Commodity Parts per
million
Cattle, kidney 0.10
Cattle, meat byproducts, except kidney 0.05
Cherry, sweet 0.40
Fruit, pome, group 11 3.0
Goat, kidney 0.10
Goat, meat byproducts, except kidney 0.05
Grass, forage 1 0.10
Grass, hay 1 0.10
Grass, seed screenings 1 3.5
Grass, straw 1 1.2
Hog, kidney 0.10
Hog, meat byproducts, except kidney 0.05
Horse, kidney 0.10
Horse, meat byproducts, except kidney 0.05
Peanut 1.0
Peanut, hay 0.60
Sheep, kidney 0.10
Sheep, meat byproducts, except kidney 0.05
Strawberry 0.30
Watercress 4.0
1 Registration is limited to grass grown for seed.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the plant growth regulator, prohexadione calcium, including its metabolites and degradates, in or on the commodities in table 2 in this paragraph (c). Compliance with the tolerance levels specified in table 2 in this paragraph (c) is to be determined by measuring only prohexadione calcium (calcium 3-oxido-5-oxo-4-propionylcyclohex-3-enecarboxylate) in or on the following commodities.

Table 2 to Paragraph (c)

Commodity Parts per
million
Alfalfa, forage 0.1
Alfalfa, hay 0.1
Corn, field, forage 0.1
Corn, field, grain 0.1
Corn, field, stover 0.1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, 2011; 80 FR 38980, July 8, 2015; 85 FR 8461, Feb. 14, 2020]

§ 180.549 Diflufenzopyr; tolerances for residues.

(a) General. Tolerances are established for combined residues of diflufenzopyr, 2-(1-[([3,5-difluorophenylamino] carbonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, and its metabolites convertible to 8- methylpyrido[2,3-d]pyridazin-5(6H)-one, expressed as diflufenzopyr, in or on the following raw agricultural commodities:

Commodity Parts per million
Corn, field, forage 0.05
Corn, field, grain 0.05
Corn, field, stover 0.05
Corn, pop, grain 0.05
Corn, pop, stover 0.05
Corn, sweet, forage 0.05
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 0.05
Grass, forage 22.0
Grass, hay 7.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, 2011]

§ 180.551 Fluthiacet-methyl; tolerances for residues.

(a) General.

(1) A tolerance is established for residues of the herbicide, fluthiacet-methyl, acetic acid [[2-chloro-4-fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]-methyl ester, in or on the food commodity:

Commodity Parts per million
Corn, field, forage 0.050
Corn, field, grain 0.010
Corn, field, stover 0.050
Corn, pop, grain 0.010
Corn, pop, stover 0.050
Corn, sweet, forage 0.050
Corn, sweet, kernel plus cob with husks removed 0.010
Corn, sweet, stover 0.050
Soybean, seed 0.01

(2) A tolerance is established for the combined residues of the herbicide fluthiacet-methyland its acid metabolite: acetic acid, [[2-chloro-4-fluoro-5-[tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]-methyl ester, and its acid metabolite, acetic acid, [[2-chloro-4-fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]- , in or on the following food commodities:

Commodity Parts per million
Cotton, gin byproducts 0.20
Cotton, undelinted seed 0.020

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 18357, Apr. 14, 1999, as amended at 66 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, 2006]

§ 180.552 Sulfosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide sulfosulfuron, 1-(4,6-dimethoxypyrimidin-2-yl)-3-[(2-ethanesulfonyl-imidazo[1,2-a]pyridine-3-yl) sulfonyl]urea and its metabolites converted to 2-(ethylsulfonyl)-imidazo[1,2-a]pyridine and calculated as sulfosulfuron in or on the raw agricultural commodities.

Commodity Parts per million
Cattle, fat 0.02
Cattle, meat 0.01
Cattle, meat byproducts 0.3
Goat, fat 0.02
Goat, meat 0.01
Goat, meat byproducts 0.3
Grass, forage, fodder and hay, group 17, forage 14
Grass, forage, fodder and hay, group 17, hay 25
Hog, fat 0.005
Hog, meat 0.005
Hog, meat byproducts 0.05
Horse, fat 0.02
Horse, meat 0.01
Horse, meat byproducts 0.3
Milk 0.02
Sheep, fat 0.02
Sheep, meat 0.01
Sheep, meat byproducts 0.3
Wheat, forage 4.0
Wheat, grain 0.02
Wheat, hay 0.3
Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, 2007]

§ 180.553 Fenhexamid; tolerances for residues.

(a) General. Tolerances are established for residues of fenhexamid, including its metabolites and degradate, in or on the commodities in the table in this paragraph (a). Compliance with the tolerance levels specified in this paragraph (a) is to be determined by measuring only fenhexamid (N-2,3-dichloro-4-hydroxyphenyl)-1-methylcyclohexanecarboxamide).

Commodity Parts per million
Almond, hulls 2.0
Almond 0.02
Arugula 30
Asparagus 0.02
Berry, low growing, subgroup 13-07G 3
Bushberry subgroup 13-07B 5
Caneberry subgroup 13-07A 20
Cress, garden 30
Cress, upland 30
Cucumber 2.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 4
Fruit, stone, group 12-12, except plum, prune 10
Ginseng 0.3
Grape, raisin 6.0
Kiwifruit, fuzzy 30
Leafy greens, subgroup 4-16A, except spinach 30
Onion, bulb, subgroup 3-07A 2
Onion, green, subgroup 3-07B 30
Pear 10
Pepper, nonbell 0.02
Pistachio 0.02
Plum, prune, dried 2.5
Plum, prune, fresh 1.5
Pomegranate 2.0
Vegetable, fruiting, group 8-10, except nonbell pepper 2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 28924, May 28, 1999, as amended at 65 FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, 2000; 67 FR 19120, Apr. 18, 2002; 68 FR 2247, Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; 73 FR 19154, Apr. 9, 2008; 85 FR 2659, Jan. 16, 2020]

§ 180.554 Kresoxim-methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for the combined residues of the fungicide kresoxim-methyl (methyl (E)-2-[2-(2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetate) and its metabolites as follows: (E)-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid; (E)-2-[2-(2-hydroxymethylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid (free and glucose conjugated); and (E)-2-[2-(4-hydroxy-2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetic acid (free and glucose conjugated) in or on the following commodities:

Commodity Parts per million
Apple, dry pomace 1.0
Apple, wet pomace 1.0
Fruit, pome 0.5
Grape 1.0
Grape, raisin 1.5
Pecan 0.15
Vegetable, cucurbit, group 9 0.40

(2) Tolerances are established in or on the following commodities for the residues of the metabolite (E)-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid resulting from the use of the fungicide kresoxim-methyl:

Commodity Parts per million
Cattle, meat byproducts 0.01
Goat, meat byproducts 0.01
Sheep, meat byproducts 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 31136, June 10, 1999, as amended at 71 FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, 2009]

§ 180.555 Trifloxystrobin; tolerances for residues.

(a) General. Tolerances are established for residues of trifloxystrobin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of trifloxystrobin, benzeneacetic acid, (E,E)-α-(methoxyimino)-2-[[[[1-[3-(trifluoromethyl) phenyl]ethylidene] amino]oxy]methyl]-, methyl ester, and the free form of its acid metabolite CGA-321113, (E,E)-methoxyimino-[2-[1-(3-trifluoromethyl-phenyl)-ethylideneaminooxymethyl]-phenyl]acetic acid, calculated as the stoichiometric equivalent of trifloxystrobin, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Alfalfa, forage 0.01
Alfalfa, hay 0.01
Almond, hulls 9.0
Apple, wet pomace 5.0
Artichoke, globe 1.0
Asparagus 0.07
Banana 1 0.10
Barley, grain 0.05
Barley, hay 0.3
Barley, straw 5.0
Beet, sugar, dried pulp 0.4
Beet, sugar, molasses 0.2
Beet, sugar, roots 0.1
Beet, sugar, tops 4.0
Berry, low growing subgroup 13-07G 1.5
Brassica, leafy greens, subgroup 4-16B 30
Caneberry, subgroup 13-07A 4 2
Canistel 0.7
Cattle, fat 0.1
Cattle, meat 0.1
Cattle, meat byproducts 0.1
Celtuce 9
Citrus, dried pulp 1.0
Citrus, oil 38
Coffee, green bean 2 0.02
Corn, field, forage 8.0
Corn, field, grain 0.05
Corn, field, stover 7
Corn, field, refined oil 0.1
Corn, pop, grain 0.05
Corn, pop, stover 7
Corn, sweet, cannery waste 0.6
Corn, sweet, forage 7.0
Corn, sweet, kernel plus cob with husks removed 0.04
Corn, sweet, stover 4.0
Cotton, gin byproducts 3.0
Cottonseed subgroup 20C 0.50
Currant 4 3
Egg 0.04
Fennel, Florence, fresh leaves and stalk 9
Flax, seed 0.40
Fruit, citrus, group 10-10 0.6
Fruit, pome, group 11-10 0.7
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 3
Goat, fat 0.1
Goat, meat 0.1
Goat, meat byproducts 0.1
Grain, aspirated fractions 10
Grape, raisin 5.0
Grass, forage 12
Grass, hay 17
Herbs, subgroup 19A 200
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Hop, dried cones 11.0
Horse, fat 0.1
Horse, meat 0.1
Horse, meat byproducts 0.1
Kohlrabi 2
Leaf petiole vegetable subgroup 22B 9
Leafy greens subgroup 4-16A 30
Mango 0.7
Milk 0.02
Nut, tree, group 14-12 0.04
Oat, forage 0.3
Oat, grain 0.05
Oat, hay 0.3
Oat, straw 5.0
Onion, bulb, subgroup 3-07A 0.04
Onion, green, subgroup 3-07B 1.5
Papaya 0.7
Pea, dwarf, edible podded 4 1.5
Pea, field, hay 15
Pea, field, vines 4
Pea, green, edible podded 4 1.5
Pea, pigeon, edible podded 4 1.5
Pea, snap, edible podded 4 1.5
Pea, snow, edible podded 4 1.5
Pea, sugar snap, edible podded4 1.5
Pea and bean, succulent shelled, subgroup 6B 4 0.2
Peanut, hay 4.0
Peanut 0.05
Poultry, fat 0.04
Poultry, meat 0.04
Poultry, meat byproducts 0.04
Radish, tops 10
Rice, grain 3.5
Rice, hulls 8
Sapodilla 0.7
Sapote, black 0.7
Sapote, mamey 0.7
Sheep, fat 0.1
Sheep, meat 0.1
Sheep, meat byproducts 0.1
Soybean, forage 10.0
Soybean, hay 25.0
Soybean, seed 0.08
Spice group 26 30
Star apple 0.7
Tea, dried 3 5
Tea, instant 3 5
Tropical and subtropical, small fruit, edible peel, subgroup 23A 4 0.3
Vegetable, Brassica, head and stem, group 5-16 2
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, group 8-10 0.5
Vegetable, legume, bean, edible podded, subgroup 6-22A 1.5
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.06
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.2
Vegetable, root, except sugar beet, subgroup 1B 0.1
Vegetable, tuberous and corm, subgroup 1C 0.04
Wheat, bran 0.15
Wheat, forage 0.3
Wheat, grain 0.05
Wheat, hay 0.2
Wheat, straw 5.0
1 There are no U.S. registrations as of September 27, 1999, for use on banana.
2 There are no U.S. registrations as of January 18, 2012, for use on coffee, green bean.
3 There are no U.S. registrations as of June 24, 2019, for use on tea.
4 There are no U.S. registrations on this commodity as of January 11, 2022.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 51907, Sept. 27, 1999]

§ 180.556 Pymetrozine; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pymetrozine 1,2,4-triazin-3(2H)-one,4,5-dihydro-6-methyl-4-[(3-pyridinylmethylene) amino] in or on the following raw agricultural commodities. The tolerance level for each commodity is expressed in terms of the parent insecticide only, which serves as an indicator of the use of pymetrozine on these raw agricultural commodities.

Commodity Parts per million
Asparagus 0.04
Brassica, head and stem, subgroup 5A 0.5
Brassica, leafy greens, subgroup 5B 0.25
Cotton, gin byproducts 2.0
Cotton, undelinted seed 0.3
Hop, dried cones 6.0
Pecan 0.02
Turnip, greens 0.25
Vegetable, fruiting, group 8 0.2
Vegetable, cucurbit, group 9 0.1
Vegetable, leafy, execpt brassica, group 4 0.6
Vegetable, tuberous and corm, subgroup 1C 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 48634, Aug. 9, 2000, as amended at 66 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, 2001; 70 FR 7047, Feb. 10, 2005; 70 FR 43298, July 27, 2005]

§ 180.557 Tetraconazole; tolerances for residues.

(a) General. Tolerances are established for residues of tetraconazole, including its metabolites and degradates, in or on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only tetraconazole (1-[2-(2,4-dichlorophenyl)-3-(1,1,2,2-tetrafluoroethoxy)propyl]-1H-1,2,4-triazole), in or on the following commodities.

Commodity Parts per million
Barley, bran 1.0
Barley, flour 0.50
Barley, grain 0.30
Beet sugar, dried pulp 0.20
Beet sugar, molasses 0.25
Beet sugar, root 0.15
Cattle, fat 0.15
Cattle, liver 1.50
Cattle, meat 0.02
Cattle, meat byproducts (except liver) 0.15
Corn, field, grain 0.01
Corn, pop, grain 0.01
Eggs 0.02
Goat, fat 0.15
Goat, liver 1.50
Goat, meat 0.02
Goat, meat byproducts (except liver) 0.15
Grain, aspirated fractions 4.0
Grain, cereal, forage, fodder, and straw, group 16 7.0
Hog, fat 0.01
Hog, liver 0.05
Hog, meat 0.01
Hog, meat byproducts (except liver) 0.01
Horse, fat 0.15
Horse, liver 1.50
Horse, meat 0.02
Horse, meat byproducts (except liver) 0.15
Low growing berry subgroup 13-07G, except cranberry 0.25
Milk 0.06
Milk, fat 0.75
Pea and bean, dried shelled (except soybean) subgroup 6C 0.09
Peanut 0.03
Peanut, oil 0.10
Pecan 0.04
Poultry, fat 0.05
Poultry, meat 0.01
Poultry meat byproducts 0.05
Rapeseed subgroup 20A 0.90
Sheep, fat 0.15
Sheep, liver 1.50
Sheep, meat 0.02
Sheep, meat byproducts (except liver) 0.15
Small fruit vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.20
Soybean, refined oil 0.80
Soybean, seed 0.15
Vegetable, cucurbit, group 9 0.15
Vegetable, foliage of legume (except soybeans) subgroup 7A 8.0
Vegetable, fruiting, group 8-10 0.30
Wheat, bran 0.15
Wheat, flour 0.08
Wheat, germ 0.50
Wheat, grain 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, 2007; 73 FR 67406, Nov. 14, 2008; 76 FR 53648, Aug. 29, 2011; 82 FR 2905, Jan. 10, 2017; 83 FR 16206, Apr. 16, 2018]

§ 180.559 Clodinafop-propargyl; tolerances for residues.

(a) General. Tolerances are established for clodinafop-propargyl, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only clodinafop-propargyl [(2R)-2-[4-[(5-chloro-3-fluoro-2-pyridinyl)oxy]phenoxy]propanoic acid, 2-propynyl ester] and its metabolite clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro-2- pyridinyl)oxy]phenoxy]propanoic acid].

Commodity Parts per million
Wheat, forage 0.1
Wheat, grain 0.02
Wheat, hay 0.1
Wheat, straw 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 38774, June 22, 2000, as amended at 77 FR 72226, Dec. 5, 2012]

§ 180.560 Cloquintocet-mexyl; tolerances for residues.

(a) General. Tolerances are established for residues of the inert ingredient cloquintocet-mexyl, including its metabolites and degradates, in or on the commodities in the following table when used as a safener in herbicide formulations. Compliance with the tolerance levels specified is to be determined by measuring the combined residues of cloquintocet-mexyl, (acetic acid [(5-chloro-8-quinolinyl)oxy]-, 1-methylhexyl ester; CAS Reg. No. 99607-70-2) and its acid metabolite (5-chloro-8-quinolinoxyacetic acid), expressed as cloquintocet-mexyl, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, grain 0.1
Barley, hay 0.1
Barley, straw 0.1
Teff, forage 1 0.2
Teff, grain 1 0.1
Teff, hay 1 0.5
Teff, straw 1 0.1
Wheat, forage 0.2
Wheat, grain 0.1
Wheat, hay 0.5
Wheat, straw 0.1
1 There are no U.S. registrations for use on this commodity as of March 22, 2017.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, 2008; 75 FR 16020, Mar. 31, 2010; 76 FR 38035, June 29, 2011; 81 FR 50634, Aug. 2, 2016; 82 FR 14623, Mar. 22, 2017; 83 FR 45843, Sept. 11, 2018; 89 FR 18553, Mar. 14, 2024]

§ 180.561 Acibenzolar-S-methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of acibenzolar-S-methyl, benzo(1,2,3)thiadiazole-7-carbothioic acid-S-methyl ester, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those acibenzolar-S-methyl residues convertible to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the stoichiometric equivalent of acibenzolar-S-methyl, in or on the following raw agricultural commodities.

Commodity Parts per million
Banana 1 0.1
Berry, low growing, subgroup 13-07G 0.15
Fruit, citrus, group 10-10 0.02
Fruit, pome, group 11-10 0.03
Onion, bulb, subgroup 3-07A 0.1
Spinach 1.0
Tomato, paste 3.0
Vegetable, brassica, leafy, group 5 1.0
Vegetable, cucurbit, group 9 2.0
Vegetable, fruiting, group 8 1.0
Vegetable, leafy, group 4 0.25
1 There are no United States registrations for banana.

(2) Tolerances are established for residues of acibenzolar- S -methyl, benzo(1,2,3)thiadiazole-7-carbothioic acid- S -methyl ester, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those acibenzolar- S -methyl residues convertible to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the Stoichiometric equivalent of acibenzolar- S -methyl, in or on the following raw agricultural commodities.

Commodity Parts per million Expiration/revocation date
Apple 0.05 12/31/15
Grapefruit 0.05 12/31/15
Pear 0.05 12/31/15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 50446, Aug. 18, 2000, as amended at 70 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, 2006; 74 FR 24710, May 26, 2009; 76 FR 34886, June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR 30406, May 23, 2012; 80 FR 58620, Sept. 30, 2015]

§ 180.562 Flucarbazone-sodium; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide flucarbazone-sodium, 4,5-dihydro-3-methoxy-4-methyl-5-oxo-N-[[2(trifluoromethoxy)phenyl] sulfonyl]-1H-1,2,4-triazole 1-carboxamide, sodium salt) and its N-desmethyl metabolite; and its metabolites converted to 2-(trifluoromethoxy)benzene sulfonamide and calculated as flucarbazone-sodium in or on the following food commodities:

Commodity Parts per million
Cattle, liver 1.50
Cattle, meat 0.01
Cattle, meat byproducts, except liver 0.01
Goat, liver 1.50
Goat, meat 0.01
Goat, meat byproducts, except liver 0.01
Hog, liver 1.50
Hog, meat 0.01
Hog, meat byproducts, except liver 0.01
Horse, liver 1.50
Horse, meat 0.01
Horse, meat byproducts, except liver 0.01
Milk 0.005
Sheep, liver 1.50
Sheep, meat 0.01
Sheep, meat byproducts, except liver 0.01
Wheat, forage 0.30
Wheat, grain 0.01
Wheat, hay 0.10
Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[70 FR 67915, Nov. 9, 2005, as amended at 71 FR 76931, Dec. 22, 2006]

§ 180.563 Ethametsulfuron-methyl; tolerances for residues.

(a) General. A tolerance is established for residues of ethametsulfuron methyl (methyl 2- ((((4-ethoxy-6- (methylamino)-1,3,5- triazin-2-yl) amino) carbonyl) amino) sulfonyl) benzoate) in or on the following raw agricultural commodities.

Commodity Parts per million
Canola, seed 0.02
Crambe, seed 0.02
Rapeseed, seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect of inadvertent residues. [Reserved]

[65 FR 57972, Sept. 27, 2000, as amended at 66 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, 2002]

§ 180.564 Indoxacarb; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only indoxacarb, (S)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate, and its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Alfalfa, forage 10
Alfalfa, hay 50
Almond, hulls 8
Apple, wet pomace 3.0
Beet, garden, roots 0.30
Beet, garden, tops 6.0
Berry, low growing, except strawberry, subgroup 13-07H 1
Brassica, leafy greens, subgroup 4-16B 12
Bushberry subgroup 13-07B 1.5
Cattle, fat 1.5
Cattle, meat 0.05
Cattle, meat byproducts 0.03
Celtuce 14
Chickpea, dry seed 0.2
Coffee, green bean 0.03
Corn, field, forage 6.0
Corn, field, stover 15
Corn, pop, stover 15
Corn, sweet, forage 10
Corn, sweet, stover 15
Cotton, gin byproducts 15
Cottonseed subgroup 20C 2
Cowpea, forage 50
Cowpea, hay 100
Fennel, florence, fresh leaves and stalk 14
Field corn subgroup 15-22C 0.02
Fruit, pome, group 11-10, except pear 1
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2
Fruit, stone, group 12-12 1
Goat, fat 1.5
Goat, meat 0.05
Goat, meat byproducts 0.03
Grain, aspirated fractions 45
Grape, raisin 5.0
Hog, fat 1.5
Hog, meat 0.05
Hog, meat byproducts 0.03
Horse, fat 1.5
Horse, meat 0.05
Horse, meat byproducts 0.03
Kohlrabi 12
Leaf petiole vegetable subgroup 22B 14
Leafy greens subgroup 4-16A 14
Milk 0.15
Milk, fat 4.0
Nut, tree, group 14-12 0.08
Peanut 0.01
Peanut, hay 40
Pear 0.20
Pear, asian 0.2
Peppermint, tops 11
Sheep, fat 1.5
Sheep, meat 0.05
Sheep, meat byproducts 0.03
Soybean, hulls 4.0
Soybean, seed 0.80
Spearmint, tops 11
Strawberry 4
Sunflower subgroup 20B 1.5
Sweet corn subgroup 15-22D 0.02
Vegetable, brassica, head and stem, group 5-16 12
Vegetable, cucurbit, group 9 0.60
Vegetable, fruiting, group 8-10 0.5
Vegetable, legume, bean, edible podded, subgroup 6-22A 0.9
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.9
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.2
Vegetable, tuberous and corm, subgroup 1-C 0.01

(2) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of indoxacarb, (S)-methyl-7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)-phenyl]amino]carbonyl]indeno[1,2e] [1,3,4]oxadiazine-4a(3H)-carboxylate, its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy) phenyl]amino]carbonyl]indeno [1,2-e] [1,3,4] oxadiazine-4a(3H)-carboxylate, and the metabolites: IN-JT333, methyl 7-chloro-2,5-dihydro-2-[[[4-(trifluoromethoxy)phenyl]-amino]carbonyl]indeno[1,2-e][1,3,4]oxadiazine-4a(3H)-carboxylate; IN-KT319, (E)-methyl 5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]-carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-JU873, methyl 5-chloro-2,3-dihydro-2-hydroxy-1-[[[[4-(triflurormethoxy)-phenyl]amino]carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-KG433, methyl 5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]-hydrazono]-1H-indene-2-carboxylate; and IN-KB687, methyl [4-(trifluoromethoxy)phenyl]carbamate, calculated as the stoichiometric equivalent of indoxacarb in the commodity.

Commodity Parts per million
Egg 0.20
Poultry, fat 0.20
Poultry, meat 0.06
Poultry, meat byproducts 0.06

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the indoxacarb, including its metabolites and degradates, in or on the specified agricultural commodities in the table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in the table below is to be determined by measuring only indoxacarb, (S)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate, and its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate.

The tolerances expire on the dates specified in the table.

Commodity Parts per
million
Expiration
date
Grass, forage 10 12/31/2022
Grass, hay 50 12/31/2022

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 58424, Sept. 29, 2000]

§ 180.565 Thiamethoxam; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide thiamethoxam, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels specified below is to be determined by measuring only thiamethoxam 3-[(2-chloro-5-thiazolyl)methyl]tetrahydro-5-methyl-N-nitro-4H-1,3,5-oxadiazin-4-imine and its metabolite CGA-322704 N-[(2-chloro-thiazol-5-yl)methyl]-N′-methyl-N″-nitro-guanidine, calculated as the stoichiometric equivalent of thiamethoxam, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Alfalfa, forage 0.05
Alfalfa, hay 0.12
Almond, hulls 1.2
Artichoke, globe 0.45
Avocado 0.40
Banana 1 0.03
Barley, grain 0.4
Barley, hay 0.40
Barley, straw 0.40
Bean, succulent 0.02
Berry, low growing, subgroup 13-07G, except cranberry 0.30
Borage, seed 0.02
Brassica, head and stem, subgroup 5-A 4.5
Brassica, leafy greens, subgroup 5-B 3.0
Buckwheat, forage 0.50
Buckwheat, hay 0.02
Buckwheat, straw 0.02
Bushberry subgroup 13-07B, except lingonberry and blueberry, lowbush 0.20
Caneberry subgroup 13-07A 0.35
Canistel 0.40
Canola, seed 0.02
Cattle, meat 0.02
Cattle, meat byproducts 0.04
Citrus, dried pulp 0.60
Coffee, green, bean 1 0.20
Corn, field, forage 0.10
Corn, field, stover 0.05
Corn, pop, forage 0.10
Corn, pop, stover 0.05
Corn, sweet, forage 0.10
Corn, sweet, kernel plus cob with husks removed 0.02
Corn, sweet, stover 0.05
Cotton, gin byproducts 1.5
Cotton, undelinted seed 0.10
Crambe, seed 0.02
Cranberry 0.02
Flax, seed 0.02
Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling establishments 0.02
Fruit, citrus, group 10 0.40
Fruit, pome, group 11 0.2
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 0.20
Fruit, stone, group 12 0.5
Goat, meat 0.02
Goat, meat byproducts 0.04
Grain, aspirated fractions 2.0
Grain, cereal, group 15, except barley 0.02
Grape, raisin 0.30
Hog, meat 0.02
Hog, meat byproducts 0.02
Hop, dried cones 0.10
Horse, meat 0.02
Horse, meat byproducts 0.04
Mango 0.40
Milk 0.02
Millet, pearl, forage 0.02
Millet, pearl, stover 0.02
Millet, proso, forage 0.02
Millet, proso, stover 0.02
Millet, proso, straw 0.02
Mustard, seed 0.02
Nut, tree, group 14 0.02
Oat, forage 0.50
Oat, hay 0.02
Oat, straw 0.02
Onion, dry bulb 0.03
Papaya 0.40
Peanut 0.05
Peanut, hay 0.25
Peanut, meal 0.15
Pepper, black 3 0.15
Peppermint, tops 1.5
Pineapple 2 0.04
Pineapple, process residue 2 0.06
Pistachio 0.02
Potato 0.25
Radish, tops 0.80
Rapeseed, seed 0.02
Rye, forage 0.50
Rye, straw 0.02
Safflower, seed 0.02
Sapodilla 0.40
Sapote, black 0.40
Sapote, mamey 0.40
Sheep, meat 0.02
Sheep, meat byproducts 0.04
Sorghum, forage 0.02
Sorghum, grain, stover 0.02
Soybean, hulls 0.08
Spearmint, tops 1.5
Star apple 0.40
Sunflower 0.02
Tea, dried 1 20
Tomato, paste 0.80
Vegetable, cucurbit, group 9 0.2
Vegetable, fruiting, group 8 0.25
Vegetable, leafy, except brassica, group 4 4.0
Vegetable, legume, group 6 0.02
Vegetable, root, subgroup 1A 0.05
Vegetable, tuberous and corm, except potato, subgroup 1D 0.02
Wheat, forage 0.50
Wheat, hay 0.02
Wheat, straw 0.02
1 There are no U.S. registrations for these commodities as of February 15, 2017.
2 There are no U.S. registrations for these commodities as of June 15, 2022.
3 There are no U.S. registrations for these commodities as of December 19, 2025.

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the table are established for residues of the insecticide thiamethoxam, including its metabolites and degradates. Compliance with the tolerance levels specified below is to be determined by measuring only thiamethoxam 3-[(2-chloro-5-thiazolyl)methyl]tetrahydro-5-methyl-N-nitro-4H-1,3,5-oxadiazin-4-imine and its metabolite CGA-322704 N-[(2-chloro-thiazol-5-yl)methyl]-N′-methyl-N″-nitro-guanidine, calculated as the stoichiometric equivalent of thiamethoxam, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. The tolerances expire on the date specified in the table.

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration
date
Rice, grain 6 12/31/2027
Rice, straw 2 12/31/2027

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 79762, Dec. 20, 2000]

§ 180.566 Fenpyroximate; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate and its Z-isomer, (Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of fenpyroximate.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 3.0
Banana 1
Bean, snap, succulent 0.40
Berry, low growing, subgroup 13-07G 1.0
Blackeyed pea, succulent shelled 0.4
Broad bean, succulent shelled 0.4
Bushberry subgroup 13-07B 3
Caneberry subgroup 13-07A 3
Chickpea, succulent shelled 0.4
Citrus, dried pulp 4.0
Citrus, oil 15
Corn, field, forage 2.0
Corn, field, grain 0.02
Corn, field, refined oil 0.05
Corn, field, stover 7.0
Corn, pop, forage 2.0
Corn, pop, grain 0.02
Corn, pop, stover 7.0
Cotton, gin byproducts 10
Cottonseed subgroup 20C 0.1
Cowpea, succulent shelled 0.4
Crowder pea, succulent shelled 0.4
Fruit, citrus, group 10-10 1.0
Fruit, pome, group 11-10 0.30
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0
Fruit, stone, group 12-12 2.0
Goa bean, pods, succulent shelled 0.4
Grain, aspirated fractions 0.40
Hop, dried cones 10
Lablab bean, succulent shelled 0.4
Leaf petiole vegetable subgroup 22B 4
Lima bean, succulent shelled 0.4
Melon subgroup 9A 0.10
Nut, tree, group 14-12 0.1
Peanut 0.04
Peanut, hay 30
Peppermint, tops 7.0
Sapodilla 0.15
Sapote, mamey 0.15
Southern pea, succulent shelled 0.4
Soybean, edible, succulent shelled 0.4
Spearmint, tops 7.0
Squash/cucumber subgroup 9B 0.4
Succulent bean, succulent shelled 0.4
Tea, dried 1 20
Tropical and subtropical, medium to large fruit, smooth, inedible peel subgroup 24B, except banana 0.6
Vegetable, fruiting, group 8-10 0.20
Vegetable, tuberous and corm, subgroup 1C 0.10
Velvet bean, succulent shelled 0.4
1 There are no U.S. Registrations.

(2) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate and its metabolites (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)-methyleneaminooxymethyl]benzoic acid and (E)-1,1-dimethylethyl-2-hydroxyethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of fenpyroximate.

Table 2 of Paragraph (a)(2)

Commodity Parts per
million
Cattle, fat 0.1
Cattle, meat 0.03
Cattle, meat byproducts, except kidney and liver 0.03
Goat, fat 0.1
Goat, meat 0.03
Goat, meat byproducts, except kidney and liver 0.03
Horse, fat 0.1
Horse, meat 0.03
Horse, meat byproducts, except kidney and liver 0.03
Milk 0.015
Sheep, fat 0.1
Sheep, meat 0.03
Sheep, meat byproducts, except kidney and liver 0.03

(3) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate and its metabolite (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)-methyleneaminooxymethyl]benzoic acid, calculated as the stoichiometric equivalent of fenpyroximate.

Table 3 of Paragraph (a)(3)

Commodity Parts per
million
Cattle, kidney 0.5
Cattle, liver 0.7
Goat, kidney 0.5
Goat, liver 0.7
Horse, kidney 0.5
Horse, liver 0.7
Sheep, kidney 0.5
Sheep, liver 0.7

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 18568, Apr. 10, 2001, as amended at 69 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006; 72 FR 26321, May 9, 2007; 74 FR 37617, July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; 78 FR 36097, June 17, 2013; 82 FR 34875, July 27, 2017; 84 FR 66625, Dec. 5, 2019; 85 FR 36758, June 18, 2020]

§ 180.567 Zoxamide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide).

Commodity Parts per million
Banana 1 0.20
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0
Grape, raisin 15.0
Pepper/Eggplant Subgroup 8-10B 1.0
Tomato subgroup 8-10A 2.0
Vegetable, cucurbit, group 9 1.0
1 There are no U.S. registrations allowing use of zoxamide on banana as of February 9, 2018.

(2) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide) and its metabolites 3,5-dichloro-1,4-benzenedicarboxylic acid (RH-1455 and RH-141455) and 3,5-dichloro-4-hydroxymethylbenzoic acid (RH-1452 and RH-141452) calculated as the stoichiometric equivalent of zoxamide.

Commodity Parts per million
Ginseng 0.30
Onion, bulb, subgroup 3-07A 0.7
Potato, granules/flakes 0.30
Potato, wet peel 0.10
Vegetable, tuberous and corm, subgroup 1C 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, 2004; 71 FR 31104, June 1, 2006; 71 FR 76200, Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR 41915, July 18, 2014; 81 FR 12015, Mar. 8, 2016; 83 FR 5719, Feb. 9, 2018; 84 FR 12524, Apr. 2, 2019]

§ 180.568 Flumioxazin; tolerances for residues.

(a) General. Tolerances are established for residues of flumioxazin, 2-[7-fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)-2H-1,4-benzoxazin-6-yl]-4,5,6,7-tetrahydro-1H-isoindole-1,3(2H)-dione, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only flumioxazin.

Commodity Parts per
million
Alfalfa, forage 3.0
Alfalfa, hay 8.0
Almond, hulls 0.70
Artichoke, globe 0.02
Asparagus 0.02
Berry, low growing, subgroup 13-07G 0.07
Bushberry subgroup 13-07B 0.02
Caneberry, subgroup 13-07A 0.50
Citrus, group 10-10 0.02
Citrus, oil 0.1
Corn, field, forage 0.02
Corn, field, grain 0.02
Corn, field, stover 0.02
Cotton, gin byproducts 0.60
Cotton, undelinted seed 0.02
Fish, freshwater 1.5
Fruit, pome, group 11-10 0.02
Fruit, small vine climbing, except for fuzzy kiwifruit, subgroup 13-07F 0.02
Fruit, stone, group 12-12 0.02
Grain, aspirated fractions 100
Hop, dried cones 0.05
Leaf petioles subgroup 4B 0.02
Nut, tree, group 14-12 0.02
Olive 0.02
Onion, bulb subgroup 3-07A 0.02
Pea and bean, dried shelled, except soybean, subgroup 6C 0.07
Peanut 0.02
Peppermint, tops 0.04
Pomegranate 0.02
Prickly pear, fruit 0.07
Prickly pear, pads 0.06
Rapeseed subgroup 20A 0.40
Soybean forage 0.03
Soybean hay 0.02
Soybean, seed 0.02
Spearmint, tops 0.04
Sugarcane, cane 0.20
Sunflower subgroup 20B 0.50
Vegetable, brassica, head and stem, group 5-16 0.02
Vegetable, cucurbit, group 9 0.03
Vegetable, fruiting, group 8-10 0.02
Vegetable, tuberous and corm, subgroup 1C 0.02
Wheat, forage 0.02
Wheat, grain 0.40
Wheat, hay 0.02
Wheat, straw 6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of flumioxazin, 2-[7-fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)-2H-1,4-benzoxazin-6-yl]-4,5,6,7-tetrahydro-1H-isoindole-1,3(2H)-dione, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only flumioxazin.

Commodity Parts per
million
Clover, forage 0.02
Clover, hay 0.15
Grass, forage 0.40
Grass, hay 0.05

(d) Indirect or inadvertent residues. [Reserved]

[81 FR 91851, Dec. 19, 2016, as amended at 83 FR 50288, Oct. 5, 2018]

§ 180.569 Forchlorfenuron; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of forchlorfenuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only forchlorfenuron (N-(2-chloro-4-pyridinyl)-N-phenylurea).

Commodity Parts per
million
Almond 0.01
Almond, hulls 0.15
Bushberry subgroup 13-07B 0.01
Cherry, sweet 0.01
Fig 0.01
Grape 0.03
Grape, raisin 0.06
Kiwifruit 0.04
Pear 0.01
Pistachio 0.01
Plum, prune, fresh 0.01

(2) Temporary tolerances are established for residues of forchlorfenuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring on forchlorfenuron (N-(2-chloro-4-pyridinyl)-N′-phenylurea).

Commodity Parts per
million
Expiration/
revocation
date
Almond 0.01 12/31/15
Almond, hulls 0.15 12/31/15
Cherry, sweet 0.01 12/31/15
Fig 0.01 12/31/15
Pear 0.01 12/31/15
Pistachio 0.01 12/31/15
Plum, prune, fresh 0.01 12/31/15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, 2004; 73 FR 47846, Aug. 15, 2008; 78 FR 46283, July 31, 2013; 79 FR 18471, Apr. 2, 2014]

§ 180.570 Isoxadifen-ethyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of isoxadifen-ethyl (ethyl 5,5-diphenyl-2-isoxazoline-3-carboxylate, (CAS No. 163520-33-0), and its metabolite: 4,5-dihydro-5,5-diphenyl-3-isoxazolecarboxylic acid, when used as an inert ingredient (safener) in or on the following raw agricultural commodities:

Commodity Parts per million
Corn, field, forage 0.20
Corn, field, grain 0.08
Corn, field, stover 0.40
Corn, oil 0.50
Corn, pop, grain 0.04
Corn, pop, stover 0.25
Corn, sweet, forage 0.30
Corn, sweet, kernel plus cob with husk removed 0.04
Corn, sweet, stover 0.45

(2) Tolerances are established for the residues of isoxadifen-ethyl (3-isoxazolecarboxylic acid, 4,5-dihydro-5,5-diphenyl-, ethyl ester (CAS No. 164520-33-0)), and its metabolites 4,5-dihydro-5,5-diphenyl-3-isoxazolecarboxylic acid and β-hydroxy-β-benzenepropanenitrile when used as an inert ingredient (safener) in or on the following raw agricultural commodities:

Commodity Parts per million
Rice, grain 0.10
Rice, hulls 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 33187, June 21, 2001, as amended at 66 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, 2002; 69 FR 29890, May 26, 2004; 72 FR 63997, Nov. 14, 2007; 80 FR 72599, Nov. 20, 2016]

§ 180.571 Mesotrione; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide mesotrione, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only mesotrione, 2-[4-(methylsulfonyl)-2-nitrobenzoyl]-1,3-cyclohexanedione, in or on the following raw agricultural commodities:

Commodity Parts per million
Almond, hulls 0.02
Asparagus 0.01
Berry, group 13 0.01
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.5
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 1.5
Cranberry 0.02
Flax, seed 0.01
Fruit, citrus, group 10-10 0.01
Fruit, pome, group 11-10 0.01
Fruit, stone, group 12-12 0.01
Grass, forage 0.01
Grass, hay 0.01
Grass, seed screenings 0.10
Grass, straw 0.10
Lingonberry 0.01
Millet, forage 0.01
Millet, grain 0.01
Millet, hay 0.02
Millet, straw 0.02
Nut, tree, group 14-12 0.01
Oat, forage 0.01
Oat, grain 0.01
Oat, hay 0.01
Oat, straw 0.01
Okra 0.01
Rhubarb 0.01
Sorghum, grain, forage 0.01
Sorghum, grain, grain 0.01
Sorghum, grain, stover 0.01
Sorghum, sweet 0.01
Soybean, seed 0.01
Sugarcane, cane 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 33195, June 21, 2001, as amended at 67 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 69 FR 58310, Sept. 30, 2004; 70 FR 14551, Mar. 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR 67123, Dec. 18, 2009; 76 FR 34886, June 15, 2011; 80 FR 30630, May 29, 2015]

§ 180.572 Bifenazate; tolerance for residues.

(a) General.

(1) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its metabolite, diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric equivalent of bifenazate) in or on the following food commodities:

Commodity Parts per million
Acerola 0.90
Almond, hulls 15
Apple, wet pomace 1.2
Atemoya 1.6
Avocado 7.0
Bean, dry seed 0.60
Berry, low-growing subgroup 13-07G 1.5
Biriba 1.6
Black sapote 7.0
Caneberry subgroup 13-07A 5.0
Canistel 7.0
Cattle, fat 0.10
Cherimoya 1.6
Cotton, gin byproducts 35
Cotton, undelinted seed 0.75
Custard apple 1.6
Feijoa 0.90
Fruit, pome, group 11-10 0.7
Fruit, small, vine climbing subgroup 13-07F, except fuzzy kiwifruit 1.0
Fruit, stone, group 12, except plum 2.5
Goat, fat 0.10
Grape 0.75
Grape, raisin 1.2
Guava 0.9
Herb, subgroup 19A, except chervil and chive 300
Hog, fat 0.10
Hop, dried cones 15
Horse, fat 0.10
Jaboticaba 0.90
Ilama 1.6
Longan 5.0
Lychee 5.0
Mango 7.0
Nut, tree, group 14 0.20
Okra 2.0
Papaya 7.0
Passionfruit 0.90
Pea and bean, succulent shelled, subgroup 6B 0.70
Peppermint, tops 25
Pistachio 0.20
Plum 0.20
Pulasan 5.0
Rambutan 5.0
Sapodilla 7.0
Sapote, mamey 7.0
Sheep, fat 0.10
Soursop 1.6
Soybean, succulent shelled 0.70
Spanish lime 5.0
Spearmint, tops 25
Star apple 7.0
Starfruit 0.90
Strawberry 1.5
Sugar apple 1.6
Vegetable, cucurbit, group 9 0.75
Vegetable, fruiting, group 8-10 4.0
Vegetable, legume, edible-podded, subgroup 6A 6.0
Vegetable, tuberous and corm, subgroup 1C 0.10
Wax jambu 0.90

(2) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl) hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its metabolites diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester; 1,1′-biphenyl, 4-ol; and 1,1′-biphenyl, 4-oxysulfonic acid (calculated as the stoichiometric equivalent of bifenazate) in or on the following food commodities:

Commodity Parts per million
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Goat, meat 0.02
Goat, meat byproducts 0.02
Hog, meat 0.02
Hog, meat byproducts 0.02
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(l), are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its metabolite, diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric equivalent of bifenazate) in or on the following food commodities:

Commodity Parts per
million
Timothy, forage 200
Timothy, hay 150

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 34569, June 29, 2001]

§ 180.573 Tepraloxydim; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the combined residues of tepraloxydim, (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid) and OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as tepraloxydim, in or on the commodities.

Commodity Parts per
million
Expiration/
revocation
date
Cotton, undelinted seed 0.2 12/31/18
Cotton, gin byproducts 3.0 12/31/18
Flax, seed 0.10 12/31/18
Grain, aspirated fraction 1200.0 12/31/18
Pea and bean, dried shelled, except soybean, subgroup 6C 1 0.10 12/31/18
Soybean, seed 6.0 12/31/18
Soybean, hulls 8.0 12/31/18
Sunflower subgroup 20B 1 0.20 12/31/18
1 There are no U.S. registrations for commodities in this subgroup.

(2) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the combined residues of tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), and GL (3-(2-oxotetrahydropyran-4-yl)-1,5-dioic acid), calculated as tepraloxydim, in or on the commodities.

Commodity Parts per
million
Expiration/
revocation
date
Cattle, fat 0.15 12/31/18
Cattle, kidney 0.50 12/31/18
Cattle, meat 0.20 12/31/18
Cattle, meat byproducts, except kidney 0.20 12/31/18
Egg 0.20 12/31/18
Goat, fat 0.15 12/31/18
Goat, kidney 0.50 12/31/18
Goat, meat 0.20 12/31/18
Goat, meat byproducts, except kidney 0.20 12/31/18
Hog, fat 0.15 12/31/18
Hog, kidney 0.50 12/31/18
Hog, meat 0.20 12/31/18
Hog, meat byproducts, except kidney 0.20 12/31/18
Horse, fat 0.15 12/31/18
Horse, kidney 0.50 12/31/18
Horse, meat 0.20 12/31/18
Horse, meat byproducts, except kidney 0.20 12/31/18
Milk 0.10 12/31/18
Poultry, fat 0.30 12/31/18
Poultry, liver 1.00 12/31/18
Poultry, meat 0.20 12/31/18
Poultry, meat byproducts, except liver 0.20 12/31/18
Sheep, fat 0.15 12/31/18
Sheep, kidney 0.50 12/31/18
Sheep, meat 0.20 12/31/18
Sheep, meat byproducts, except kidney 0.20 12/31/18

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in § 180.1(l), is established for residues of tepraloxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the combined residues of tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid) and OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as tepraloxydim, in or on the commodities.

Commodity Parts per
million
Expiration/
revocation
date
Canola, seed 0.50 12/31/18

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 40150, Aug. 2, 2001, as amended at 72 FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; 76 FR 82152, Dec. 30, 2011; 81 FR 34906, June 1, 2016]

§ 180.574 Fluazinam; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro-4-(trifluoromethyl)phenyl]-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluazinam.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Apple 2.0
Apple, wet pomace 5.0
Bean, adzuki, dry seed 0.02
Bean, American potato, dry seed 0.02
Bean, asparagus, edible podded 0.1
Bean, asparagus, dry seed 0.02
Bean, black, dry seed 0.02
Bean, broad, dry seed 0.02
Bean, broad, succulent shelled 0.04
Bean, catjang, edible podded 0.1
Bean, catjang, dry seed 0.02
Bean, catjang, succulent shelled 0.04
Bean, cranberry, dry seed 0.02
Bean, dry, dry seed 0.02
Bean, field, dry seed 0.02
Bean, French, dry seed 0.02
Bean, French, edible podded 0.1
Bean, garden, dry seed 0.02
Bean, garden, edible podded 0.1
Bean, goa, dry seed 0.02
Bean, goa, edible podded 0.1
Bean, goa, succulent shelled 0.04
Bean, great northern, dry seed 0.02
Bean, green, dry seed 0.02
Bean, green, edible podded 0.1
Bean, guar, dry seed 0.02
Bean, guar, edible podded 0.1
Bean, kidney, dry seed 0.02
Bean, kidney, edible podded 0.1
Bean, lablab, dry seed 0.02
Bean, lablab, edible podded 0.1
Bean, lablab, succulent shelled 0.04
Bean, lima, dry seed 0.02
Bean, lima, succulent shelled 0.04
Bean, morama, dry seed 0.02
Bean, moth, dry seed 0.02
Bean, moth, edible podded 0.1
Bean, moth, succulent shelled 0.04
Bean, mung, dry seed 0.02
Bean, mung, edible podded 0.1
Bean, navy, dry seed 0.02
Bean, navy, edible podded 0.1
Bean, pink, dry seed 0.02
Bean, pinto, dry seed 0.02
Bean, red, dry seed 0.02
Bean, rice, dry seed 0.02
Bean, rice, edible podded 0.1
Bean, scarlet runner, dry seed 0.02
Bean, scarlet runner, edible podded 0.1
Bean, scarlet runner, succulent shelled 0.04
Bean, snap, edible podded 0.1
Bean, sword, dry seed 0.02
Bean, sword, edible podded 0.1
Bean, tepary, dry seed 0.02
Bean, urd, dry seed 0.02
Bean, urd, edible podded 0.1
Bean, wax, edible podded 0.1
Bean, wax, succulent shelled 0.04
Bean, yardlong, dry seed 0.02
Bean, yardlong, edible podded 0.1
Bean, yellow, dry seed 0.02
Brassica, leafy greens, subgroup 4-16B 0.01
Bushberry subgroup 13-07B 7.0
Cabbage 3.0
Carrot, roots 0.70
Chickpea, dry seed 0.04
Chickpea, edible podded 0.15
Chickpea, succulent shelled 0.03
Cowpea, dry seed 0.02
Cowpea, edible podded 0.1
Cowpea, succulent shelled 0.04
Ginseng 4.5
Gram, horse, dry seed 0.02
Grass pea, dry seed 0.04
Grass pea, edible podded 0.15
Jackbean, dry seed 0.02
Jackbean, edible podded 0.1
Jackbean, succulent shelled 0.04
Kohlrabi 0.01
Lentil, dry seed 0.04
Lentil, edible podded 0.15
Lentil, succulent shelled 0.03
Lettuce, head 0.02
Lettuce, leaf 2.0
Longbean, Chinese, dry seed 0.02
Longbean, Chinese, edible podded 0.1
Lupin, Andean, dry seed 0.02
Lupin, Andean, succulent shelled 0.04
Lupin, blue, dry seed 0.02
Lupin, blue, succulent shelled 0.04
Lupin, grain, dry seed 0.02
Lupin, grain, succulent shelled 0.04
Lupin, sweet white, dry seed 0.02
Lupin, sweet white, succulent shelled 0.04
Lupin, sweet, dry seed 0.02
Lupin, sweet, succulent shelled 0.04
Lupin, white, dry seed 0.02
Lupin, white, succulent shelled 0.04
Lupin, yellow, dry seed 0.02
Lupin, yellow, succulent shelled 0.04
Mayhaw 2.0
Onion, bulb, subgroup 3-07A 0.20
Papaya 3
Pea, blackeyed, dry seed 0.02
Pea, blackeyed, succulent shelled 0.04
Pea, crowder, dry seed 0.02
Pea, crowder, succulent shelled 0.04
Pea, dry, dry seed 0.04
Pea, dwarf, edible podded 0.15
Pea, English, succulent shelled 0.03
Pea, field, dry seed 0.04
Pea, field, hay 40
Pea, field, vines 6
Pea, garden, dry seed 0.04
Pea, garden, succulent shelled 0.03
Pea, green, dry seed 0.04
Pea, green, edible podded 0.15
Pea, green, succulent shelled 0.03
Pea, pigeon, dry seed 0.04
Pea, pigeon, edible podded 0.15
Pea, pigeon, succulent shelled 0.03
Pea, snap, edible podded 0.15
Pea, snow, edible podded 0.15
Pea, southern, dry seed 0.02
Pea, southern, succulent shelled 0.04
Pea, sugar snap, edible podded 0.15
Pea, winged, dry seed 0.02
Pea, winged, edible podded 0.1
Peanut 0.02
Pear, Asian 1 0.2
Pepper/eggplant subgroup 8-10B 0.09
Soybean, hulls 0.05
Soybean, seed 0.01
Soybean, vegetable, dry seed 0.02
Soybean, vegetable, edible podded 0.1
Soybean, vegetable, succulent shelled 0.04
Tea, dried 1 6.0
Tomato subgroup 8-10A 1.5
Vegetable, brassica, head and stem, group 5-16, except cabbage 0.01
Vegetable, cucurbit, group 9 0.07
Vegetable, tuberous and corm, subgroup 1C 0.02
Velvetbean, dry seed 0.02
Velvetbean, edible podded 0.1
Velvetbean, succulent shelled 0.04
Yam bean, African, dry seed 0.02
1 There are no U.S. registrations.

(2) Tolerances are established for residues of fluazinam, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluazinam and its metabolite AMGT (3-[[4-amino-3-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]amino]-2-nitro-6-(trifluoromethyl) phenyl]thio]-2-(beta-D-glucopyranosyloxy) propionic acid).

Commodity Parts per million
Grape, wine 1 3.0
1 No US registration as of March 15, 2002.

(3) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro-4-(trifluoromethyl)phenyl]-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluazinam, AMPA (2-(6-amino-3-chloro-α,α,α-trifluoro-2-nitro-p-toluidino)-3-chloro-5-(trifluoromethyl) pyridine), DAPA (3-chloro-2-(2,6-diamino-3-chloro-α,α,α.-trifluoro-p-toluidino)-5-(trifluoromethyl)pyridine), and their sulfamate conjugates.

Commodity Parts per
million
Cattle, fat 0.05
Cattle, meat byproducts 0.05
Goat, fat 0.05
Goat, meat byproducts 0.05
Horse, fat 0.05
Horse, meat byproducts 0.05
Sheep, fat 0.05
Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 46738, Sept. 7, 2001, as amended at 67 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, 2007; 75 FR 26667, May 12, 2010; 76 FR 3029, Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012; 81 FR 20550, Apr. 8, 2016; 81 FR 34283, May 31, 2016; 82 FR 21948, May 11, 2017; 86 FR 52081, Sept. 20, 2021; 90 FR 51118, Nov. 17, 2025]

§ 180.575 Sulfuryl fluoride; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of sulfuryl fluoride in or on the following commodities from the postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity Parts per million
All processed food commodities not otherwise listed 2.0
Barley, bran, postharvest 0.05
Barley, flour, postharvest 0.05
Barley, grain, postharvest 0.1
Barley, pearled barley, postharvest 0.05
Cacao bean, roasted bean, postharvest 0.2
Cattle, meat, dried 0.01
Cheese 2.0
Coconut, postharvest 1.0
Coffee, bean, roasted bean, postharvest 1.0
Corn, field, flour, postharvest 0.01
Corn, field, grain, postharvest 0.05
Corn, field, grits, postharvest 15.0
Corn, field, meal, postharvest 0.01
Corn, pop, grain, postharvest 0.05
Cotton, undelinted seed, postharvest 0.5
Egg, dried 1.0
Fruit, dried, postharvest 0.05
Ginger, postharvest 0.5
Grain, aspirated fractions, postharvest 0.05
Herbs and spices group 19, postharvest 0.5
Hog, meat 0.02
Milk, powdered 2.0
Millet, grain, postharvest 0.1
Nut, pine, postharvest 0.2
Nut, tree, Group 14, postharvest 3.0
Oat, flour, postharvest 0.05
Oat, grain, postharvest 0.1
Oat, groats/rolled oats, postharvest 0.1
Peanut, postharvest 0.5
Pistachio, postharvest 3.0
Rice, bran, postharvest 0.01
Rice, flour, postharvest 0.05
Rice, grain, postharvest 0.04
Rice, hulls, postharvest 0.1
Rice, polished rice, postharvest 0.01
Rice, wild, grain, postharvest 0.05
Sorghum, grain, grain, postharvest 0.1
Triticale, grain, postharvest 0.1
Vegetable, legume, group 6, postharvest 0.5
Wheat, bran, postharvest 0.05
Wheat, flour, postharvest 0.05
Wheat, germ, postharvest 0.02
Wheat, grain, postharvest 0.1
Wheat, milled byproducts, postharvest 0.05
Wheat, shorts, postharvest 0.05

(2) To assure safe use of this pesticide commodities treated with sulfuryl fluoride must be aerated for at least 24 hours prior to entering commerce.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[67 FR 5740, Feb. 7, 2002, as amended at 69 FR 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005]

§ 180.576 Cyhalofop-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of cyhalofop-butyl, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring cyhalofop butyl [R-( + )-n-butyl-2-(4(4-cyano-2-fluorophenoxy)-phenoxy)propionate], cyhalofop acid [R-( + )-2-(4(4-cyano-2-fluorophenoxy)-phenoxy)propionic acid], and the di-acid metabolite [(2R)-4-(4-(1-carboxyethoxy)phenoxy)-3-fluorobenzoic acid].

Commodity Parts per million
Rice, grain 0.40
Wild rice, grain 0.40

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 43256, June 27, 2002, as amended at 74 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, 2011]

§ 180.577 Bispyribac-sodium; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide bispyribac-sodium, including its metabolites and degradates, in or on the commodity listed below. Compliance with the tolerance level specified below is to be determined by measuring only bispyribac-sodium, (2,6-bis[(4,6-dimethoxy-2-pyrimidinyl)oxy]benzoic acid, sodium salt), in or on the following raw agricultural commodities:

Commodity Parts per million
Fish, freshwater 0.01
Rice, grain 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 48097, Sept. 18, 2001, as amended at 76 FR 5716, Feb. 2, 2011; 80 FR 72599, Nov. 20, 2015]

§ 180.578 Acetamiprid; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N'-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table below as a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be determined by measuring only acetamiprid in or on the following commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 5.0
Ambrette, seed 2 2
Angelica, seed 2 2
Angelica, dahurian, seed 2 2
Anise, seed 2 2
Annatto, seed 2 2
Asparagus 0.80
Berry, low growing subgroups 13-07G 0.60
Brassica, leafy greens, subgroup 4-16B 15
Bushberry subgroup 13-07B 1.6
Candlebush 2 2
Caneberry subgroup 13-07A 1.6
Caraway, black 2 2
Celery, seed 2 2
Celtuce 3
Chervil, seed 2 2
Chinese nutmeg tree 2 2
Citrus, dried pulp 1.20
Coriander, seed 2 2
Corn, sweet, forage 15
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 30
Cotton, gin byproducts 20.0
Cottonseed subgroup 20C 0.7
Cubeb, seed 2 2
Culantro, seed 2 2
Cumin 2 2
Dill, seed 2 2
Fennel, common, seed 2 2
Fennel, florence, fresh leaves and stalk 3
Fennel flower, seed 2 2
Fenugreek, seed 2 2
Fruit, citrus, group 10-10 1.0
Fruit, pome, group 11-10 1.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.35
Fruit, stone, group 12-12 1.5
Grain, aspirated fractions 5.0
Grains of paradise 2 2
Kohlrabi 1.2
Leaf petiole vegetable subgroup 22B 3
Leafy greens subgroup 4-16A 3
Lovage, seed 2 2
Mahaleb 2 2
Milk, thistle 2 2
Mustard, seed 2 2
Nut, tree, group 14-12 0.1
Nutmeg 2 2
Onion, bulb, subgroup 3-07A 0.02
Onion, green, subgroup 3-07B 4.5
Pea and bean, succulent shelled, subgroup 6B 0.40
Pepper, black 2 0.1
Poppy, seed 2 2
Rapeseed subgroup 20A 0.01
Sesame, seed 2 2
Soybean, hulls 0.04
Soybean, seed 0.03
Tamarind, seed 2 2
Tea, dried1 50.0
Tomato, paste 0.40
Tropical and subtropical, medium to large fruit, smooth, inedible peel, subgroup 24B 0.5
Vegetable, brassica, head and stem, group 5-16 1.2
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, group 8-10 0.20
Vegetable, legume, edible podded, subgroup 6A 0.60
Vegetable, tuberous and corm, group 1 0.01
Wattleseed 2 2
1 There are no U.S. registrations as of February 10, 2010, for the use of acetamiprid on dried tea.
2 There are no U.S. registrations for these commodities as of July 16, 2025.

(2) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table below as a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be determined by measuring acetamiprid and (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-ethanimidamide in or on the following commodities.

Commodity Parts per million
Cattle, fat 0.20
Cattle, meat 0.30
Cattle, meat byproducts 0.70
Egg 0.010
Goat, fat 0.20
Goat, meat 0.30
Goat, meat byproducts 0.70
Hog, fat 0.10
Hog, meat 0.10
Hog, meat byproducts 0.20
Horse, fat 0.20
Horse, meat 0.30
Horse, meat byproducts 0.70
Milk 0.30
Poultry, fat 0.010
Poultry, liver 0.050
Poultry, meat 0.010
Sheep, fat 0.20
Sheep, meat 0.30
Sheep, meat byproducts 0.70

(3) A tolerances of 0.01 ppm is established for residues of the insecticide acetamiprid, including its metabolites and degradates, in or on all food/feed items (other than those covered by a higher tolerance in paragraph (a)(1) or (a)(2) of this section as a result of the use on growing crops) as a result of the application of acetamiprid in food/feed handling establishments. Compliance with the 0.01 ppm tolerance level is to be determined by measuring only acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide in or on the commodities.

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the acetamiprid, (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N'-cyano-N-methylethanimidamide, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is to be determined by measuring only acetamiprid. The tolerances expire on the date specified in the table.

Commodity Parts per million Expiration date
Sugarcane, cane 45 12/31/19
Sugarcane, molasses 600 12/31/19

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table below as a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be determined by measuring only acetamiprid in or on the following commodities.

Commodity Parts per million
Clover, forage 0.30
Clover, hay 2.0

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 14659, Mar. 27, 2002, as amended at 68 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, 2005; 72 FR 67262, Nov. 28, 2007; 73 FR 2811, Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; 78 FR 36676, June 19, 2013; 80 FR 68778, Nov. 6, 2015; 82 FR 17151, Apr. 10, 2017; 85 FR 8441, Feb. 14, 2020; 90 FR 31899, July 16, 2025]

§ 180.579 Fenamidone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide, fenamidone, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring only fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), in or on the commodities:

Commodity Parts per million
Basil, dried leaves 200
Basil, fresh leaves 30
Bean, succulent, except cowpea 0.80
Celtuce 60
Cilantro, fresh leaves 60
Cotton, gin byproducts 0.02
Cottonseed subgroup 20C 0.02
Fennel, Florence, fresh leaves and stalk 60
Ginseng 0.80
Kohlrabi 5.0
Leaf petiole vegetable subgroup 22B 60
Leafy vegetable group 4-16 60
Okra 3.5
Onion, bulb, subgroup 3-07A 0.20
Onion, green, subgroup 3-07B 1.5
Pepper, nonbell 3.5
Sunflower 0.02
Tomato, paste 2.2
Tomato, puree 2.0
Turnip, greens 55
Vegetable, Brassica, head and stem, group 5-16 5.0
Vegetable, cucurbit, group 9 0.15
Vegetable, fruiting, group 8, except nonbell pepper 1.0
Vegetable, root, except sugar beet, subgroup 1B, except radish 0.15
Vegetable, tuberous and corm, subgroup 1C 0.02

(2) Tolerances are established for residues of the fungicide fenamidone, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and its metabolite RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the commodities:

Commodity Parts per million
Cattle, fat 0.10
Cattle, meat 0.10
Cattle, meat byproducts 0.10
Goat, fat 0.10
Goat, meat 0.10
Goat, meat byproducts 0.10
Milk 0.02
Sheep, fat 0.10
Sheep, meat 0.10
Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration as defined in § 180.1(l) is established for residues of the fungicide fenamidone, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring only fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylam-ino)-,(S)-), in or on the commodity:

Commodity Parts per million
Grape1 1.0
1 Applicable to grapes grown East of the Rocky Mountains.

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fenamidone, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and its metabolite RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the following commodities when present therein as a result of application of fenamidone to the crops in paragraph (a)(1).

Commodity Parts per
million
Grain, cereal, group 15, except rice 0.1
Grain, cereal, forage, fodder and straw, group 16, except rice 0.5
Soybean, forage 0.15
Soybean, hay 0.25
Soybean, seed 0.02
Strawberry 0.02

[67 FR 60976, Sept. 27, 2002, as amended at 69 FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, 2006; 72 FR 60272, Oct. 24, 2007; 74 FR 34257, July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; 79 FR 13882, Mar. 12, 2014; 82 FR 35114, July 28, 2017]

§ 180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide Iodosulfuron-Methyl-Sodium (methyl 4-iodo-2-[3-(4-methoxy-6-methyl-1,3,5 triazin-2-yl)ureidosulfonyl]benzoate, sodium salt) in or on the following commodities:

Commodity Parts per million
Corn, field, forage 0.05
Corn, field, grain 0.03
Corn, field, stover 0.05
Wheat, forage 0.10
Wheat, grain 0.02
Wheat, hay 0.05
Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 57532, Sept. 11, 2002, as amended at 74 FR 23644, May 20, 2009]

§ 180.581 Iprovalicarb; tolerances for residues.

(a) General. Tolerances are established for residues of iprovalicarb, [2-methyl-1[[[(1S)-(4-methylphenyl) ethyl] amino]carbonyl] propyl]carbamic acid methylethylester, in or on the following commodities.

Commodity Parts per million
Grape 1 2.0
Tomato 1 1.0
1 There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 54359, Aug. 22, 2002, as amended at 70 FR 55281, Sept. 21, 2005]

§ 180.582 Pyraclostrobin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide pyraclostrobin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyraclostrobin (carbamic acid, [2-[[[ 1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy] methyl]phenyl]methoxy-, methyl ester) and its desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl] phenylcarbamate), calculated as the stoichiometric equivalent of pyraclostrobin, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 10
Alfalfa, hay 30
Almond, hulls 7.0
Apple, wet pomace 8.0
Artichoke, globe 3.0
Avocado 0.6
Banana 0.04
Barley, grain 1.4
Barley, hay 25
Barley, straw 6.0
Bean, succulent shelled 0.5
Beet, sugar, dried pulp 1.0
Beet, sugar, roots 0.2
Beet, sugar, tops 8.0
Berry, low growing, subgroup 13-07G, except cranberry 1.2
Brassica, leafy greens, subgroup 4-16B, except watercress 16
Bushberry subgroup 13-07B 4.0
Caneberry subgroup 13-07A 4.0
Canistel 0.6
Celtuce 29
Citrus, dried pulp 12.5
Citrus, oil 9.0
Coffee, green bean 0.3
Corn, field, forage 5.0
Corn, field, grain 0.1
Corn, field, refined oil 0.2
Corn, field, stover 17.0
Corn, pop, grain 0.1
Corn, pop, stover 17.0
Corn, sweet, forage 5.0
Corn, sweet, kernel plus cob with husks removed 0.04
Corn, sweet, stover 23.0
Cotton, gin byproducts 30
Dill, seed 40
Endive, belgium 4.0
Fennel, Florence 29
Fruit, citrus, group 10-10 2.0
Fruit, pome, group 11-10 1.5
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 2.5
Grain, aspirated fractions 2.5
Grape, raisin 7.0
Grass, forage 10
Grass, hay 4.5
Grass, seed screenings 27
Grass, straw 14
Herb subgroup 19A 40
Hop, dried cones 23.0
Kohlrabi 5.0
Leaf petiole vegetable, subgroup 22B 29
Leafy greens, subgroup 4-16A 40
Mango 0.6
Nut, tree, group 14-12, except pistachio 0.04
Oat, grain 1.2
Oat, hay 18
Oat, straw 15
Oilseed group 20 0.45
Papaya 0.6
Pea, succulent 0.2
Pea and bean, dried shelled, except soybean, subgroup 6C 0.5
Peanut 0.05
Peanut, refined oil 0.1
Peppermint, tops 8.0
Persimmon 3.0
Pistachio 0.7
Pomegranate 0.3
Radish, tops 16
Rye, grain 0.04
Rye, straw 0.5
Sapodilla 0.6
Sapote, black 0.6
Sapote, mamey 0.6
Sorghum, grain, forage 5.0
Sorghum, grain, grain 0.60
Sorghum, grain, stover 0.80
Soybean, forage 11
Soybean, hay 14
Soybean, hulls 0.06
Soybean, seed 0.04
Spearmint, tops 8.0
Star apple 0.6
Stevia, dried leaves 150
Stevia, fresh leaves 40
Sugarcane, cane 0.20
Vegetable, Brassica, head and stem, group 5-16 5.0
Vegetable, bulb, group 3-07 0.9
Vegetable, cucurbit, group 9 0.5
Vegetable, foliage of legume, except soybean, subgroup 7A 25.0
Vegetable, fruiting, group 8-10 1.4
Vegetable, leaves of root and tuber, group 2, except sugar beet 16.0
Vegetable, legume, edible podded, subgroup 6A 0.5
Vegetable, root, except sugar beet, subgroup 1B 0.4
Vegetable, tuberous and corm, subgroup 1C 0.04
Vegetables, foliage of legume, group 7 25
Wheat, grain 0.02
Wheat, hay 6.0
Wheat, straw 8.5

(2) Tolerances are established for combined residues of the fungicide pyraclostrobin carbamic acid, [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]methoxy-, methyl ester and its metabolites convertible to 1-(4-chlorophenyl)-1H-pyrazol-3-ol and 1-(4-chloro-2-hydroxyphenyl)-1H-pyrazol-3-ol, expressed as parent compound, in or on the following raw agricultural commodities.

Commodity Parts per million
Cattle, fat 0.1
Cattle, liver 1.5
Cattle, meat 0.1
Cattle, meat byproducts, except liver 0.2
Goat, fat 0.1
Goat, liver 1.5
Goat, meat 0.1
Goat, meat byproducts, except liver 0.2
Hog, fat 0.1
Hog, liver 1.5
Hog, meat 0.1
Hog, meat byproducts, except liver 0.2
Horse, fat 0.1
Horse, liver 0.1
Horse, meat 0.1
Horse, meat byproducts, except liver 0.2
Milk 0.1
Poultry, eggs 0.10
Poultry, fat 0.10
Poultry, meat 0.10
Poultry, meat byproducts 0.10
Sheep, fat 0.1
Sheep, liver 1.5
Sheep, meat 0.1
Sheep, meat byproducts, except liver 0.2

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60901, Sept. 27, 2002]

§ 180.583 Triticonazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide triticonazole, (1RS)-(E)-5-[(4-chlorophenyl)methylene]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol, from the treatment of seed prior to planting in or on raw agricultural commodities as follows:

Commodity Parts per million
Grain, cereal, forage, fodder and straw, group 16, except rice 0.10
Grain, cereal, group 15, except rice 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60959, Sept. 27, 2002, as amended at 75 FR 4288, Jan. 27, 2010; 86 FR 52088, Sept. 20, 2021]

§ 180.584 Tolylfluanid; tolerances for residues.

(a) General. Tolerances are established for residues of tolylfluanid, 1,1-dichloro-N-[(dimethylamino)-sulfonyl]-1-fluoro-N-(4-methylphenyl)methanesulfenamide in or on the following commodities.

Commodity Parts per million
Apple 1 5.0
Grape 1 11
Hop, dried cones 1 30
Tomato 1 2.0
1 No U.S. registration as of August 31, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60141, Sept. 25, 2002]

§ 180.585 Pyraflufen-ethyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide, pyraflufen-ethyl, including its metabolites and degradates, in or on the plant commodities listed in table 1 to this paragraph (a)(1). Compliance with the plant commodity tolerance levels specified in table 1 to this paragraph (a)(1) is to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5-difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate, and its acid metabolite, E-1, 2-chloro-5-(4-chloro-5-difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, calculated as the stoichiometric equivalent of pyraflufen-ethyl in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 0.02
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Cotton, gin byproducts 1.5
Cottonseed subgroup 20C 0.04
Fruit, pome, group 11-10 0.01
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.01
Fruit, stone, group 12-12 0.01
Grass, forage, fodder and hay, group 17 1.5
Hop, dried cones 0.02
Nut, tree, group 14-12 0.01
Peanut 0.01
Peanut, hay 0.07
Pomegranate 0.01
Soybean, forage 0.05
Soybean, hay 0.1
Soybean, seed 0.01
Tropical and subtropical, small fruit, edible peel, subgroup 23A 0.01
Vegetable, tuberous and corm, subgroup 1C 0.02
Wheat, forage 0.02
Wheat, grain 0.01
Wheat, hay 0.01
Wheat, straw 0.01

(2) Tolerances are established for residues of the herbicide, pyraflufen-ethyl, including its metabolites and degradates, in or on the livestock commodities in table 2 to this paragraph (a)(2). Compliance with the livestock commodity tolerance levels specified in table 2 to this paragraph (a)(2) is to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5-difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate and its acid metabolites: E-1, 2-chloro-5-(4-chloro-5-difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, and E-9, 2-chloro-5-(4-chloro-5-difluoromethoxy-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, both calculated as the stoichiometric equivalent of pyraflufen-ethyl in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.03
Cattle, meat 0.03
Cattle, meat byproducts 0.03
Goat, fat 0.03
Goat, meat 0.03
Goat, meat byproducts 0.03
Horse, fat 0.03
Horse, meat 0.03
Horse, meat byproducts 0.03
Milk 0.03
Sheep, fat 0.03
Sheep, meat 0.03
Sheep, meat byproducts 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 23055, Apr. 30, 2003, as amended at 68 FR 27739, May 21, 2003; 69 FR 26312, May 12, 2004; 73 FR 51743, Sept. 5, 2008; 76 FR 31484, June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR 13263, Feb. 27, 2013; 84 FR 48076, Sept. 12, 2019; 91 FR 8114, Feb. 20, 2026]

§ 180.586 Clothianidin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide clothianidin, including its metabolites and degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)-N-[(2-Chloro-5-thiazolyl)methyl]-N′ -methyl-N″ -nitroguanidine, in or on the following raw agricultural commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 1.5
Beet, sugar, dried pulp 0.03
Beet, sugar, molasses 0.05
Beet, sugar, roots 0.02
Berry, low-growing, subgroup 13-07H, except strawberry 0.01
Canola, seed 0.01
Cotton, gin byproducts 4.5
Cotton, undelinted seed 0.20
Fig 0.05
Food and feed commodities (other than those covered by a higher tolerance) in food/feed handling establishments 0.01
Fruit, pome 1.0
Grain, cereal, forage, fodder and straw, group 16, except rice, forage 0.35
Grain, cereal, forage, fodder and straw, group 16, except rice, hay 0.07
Grain, cereal, forage, fodder and straw, group 16, except rice, stover 0.1
Grain, cereal, forage, fodder and straw, group 16, except rice, straw 0.05
Grain, cereal, group 15, except rice 0.01
Grape 0.60
Milk 0.01
Mustard, seed 0.01
Nut, tree, group 14 0.01
Peach 0.80
Pepper 0.80
Persimmon 1 0.5
Pomegranate 0.20
Potato, chips 0.6
Potato, granules/flakes 1.5
Rice, grain 0.01
Soybean, seed 0.02
Tea, dried 1 70
Vegetable, brassica, leafy, group 5 1.9
Vegetable, bulb, group 3-07 0.45
Vegetable, cucurbit, group 9 0.06
Vegetable, fruiting, group 8, except pepper 0.20
Vegetable, leafy, except brassica, group 4 3.0
Vegetable, root, except sugar beet, subgroup 1B 0.8
Vegetable, tuberous and corm, subgroup 1C 0.3
1 No U.S. registrations.

(2) Time-limited tolerances are established for residues of the insecticide clothianidin, including its metabolites and degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural commodity:

Commodity Parts per million Expiration/revocation date
Rice, seed 0.01 6/23/12

(b) Section 18 emergency exemptions. A time-limited tolerance specified in the following table is established for residues of clothianidin, (E)-N-[(2-chloro-5-thiazolyl)methyl]-N'-methyl-N”-nitroguanidine, in or on the specified agricultural commodity, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. This tolerance expires on the date specified in the table.

Table 3 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation date
Fruit, citrus, group 10-10 0.07 12/31/26
Rice, grain 0.5 12/31/27

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. Tolerances are established for the indirect or inadvertent residues of the insecticide clothianidin, including its metabolites and degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural commodities when present therein as a result of the application of clothianidin to crops listed in paragraph (a) of this section:

Commodity Parts per million
Animal feed, nongrass, group 18 0.02
Grass, forage, fodder and hay, group 17 0.02
Soybean, forage 0.02
Soybean, hay 0.02

[74 FR 65028, Dec. 9, 2009, as amended at 76 FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, 2011; 76 FR 34886, June 15, 2011; 77 FR 52252, Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR 10007, Feb. 25, 2015; 82 FR 57151, Dec. 4, 2017; 84 FR 53336, Oct. 7, 2019; 84 FR 64777, Nov. 25, 2019; 86 FR 8704, Feb. 9, 2021; 86 FR 56656, Oct. 12, 2021; 88 FR 75506, Nov. 3, 2023; 89 FR 85069, Oct. 25, 2024]

§ 180.587 Famoxadone; tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide famoxadone, including its metabolites and degradates, in or on the commodities listed in Table 1 to Paragraph (a). Compliance with the tolerance levels specified in Table 1 to Paragraph (a) is to be determined by measuring only famoxadone (5-methyl-5-(4-phenoxyphenyl)-3-(phenylamino)-2,4-oxazolidinedione) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Arugula 25
Caneberry subgroup 13-07A 10
Cattle, fat 0.02
Cattle, liver 0.05
Celtuce 25
Cress, garden 25
Cress, upland 25
Fennel, florence, fresh leaves and stalk 25
Goat, fat 0.02
Goat, liver 0.05
Grape, raisin 1 5
Hop, dried cone 80
Horse, fat 0.02
Horse, liver 0.05
Leaf petiole vegetable subgroup 22B 25
Leafy greens subgroup 4-16A, except spinach 25
Milk, fat 0.06
Onion, bulb, subgroup 3-07A 0.45
Onion, green, subgroup 3-07B 40
Potato 0.02
Sheep, fat 0.02
Sheep, liver 0.05
Spinach 50
Tomato 1
Vegetable, cucurbit, group 9 0.3
Vegetable, fruiting, group 8-10, except tomato 4
1 There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in § 180.1(l) are established for residues of the fungicide famoxadone, including its metabolites and degradates, in or on the commodities listed in Table 2 to Paragraph (c). Compliance with the tolerance levels specified in Table 2 to Paragraph (c) is to be determined by measuring only famoxadone (5-methyl-5-(4-phenoxyphenyl)-3-(phenylamino)-2,4-oxazolidinedione) in or on the commodity.

Table 2 to Paragraph (c)

Commodity Parts per million
Grape 2.5

(d) Indirect or inadvertant residues. [Reserved]

[68 FR 39471, July 2, 2003, as amended at 72 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, 2009; 76 FR 34885, June 15, 2011; 91 FR 8088, Feb. 20, 2026]

§ 180.588 Quinoxyfen; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide quinoxyfen, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only quinoxyfen (5,7-dichloro-4-(4-fluorophenoxy)quinoline).

Commodity Parts per million
Artichoke, globe 1.4
Berry, low growing, subgroup 13-07G 1.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12 0.70
Hop, dried cones 3.0
Gourd, edible 0.20
Lettuce, head 7.0
Lettuce, leaf 19
Melon, subgroup 9A 0.08
Pumpkin 0.20
Squash, winter 0.20
Vegetable, fruiting, group 8-10 1.7

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55858, Sept. 29, 2003, as amended at 70 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, 2006; 74 FR 14743, Apr. 1, 2009; 78 FR 57280, Sept. 18, 2013]

§ 180.589 Boscalid; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide boscalid, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), in or on the following raw agricultural commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 30.0
Alfalfa, hay 65.0
Almond, hulls 17
Apple, wet pomace 10
Artichoke, globe 6.0
Avocado 1.5
Banana, import 1 0.40
Berry, low growing, subgroup 13-07G, except cranberry 4.5
Brassica, leafy greens, subgroup 4-16B, except watercress 60
Bushberry subgroup 13-07B 13.0
Caneberry subgroup 13-07A 10.0
Canistel 1.5
Canola, refined oil 5.0
Celtuce 45
Citrus, dried pulp 4.5
Citrus, oil 85.0
Coffee, green bean, import 1 0.05
Cotton, gin byproducts 55.0
Dill, seed 100
Endive, Belgium 6.0
Fennel, Florence 45
Fruit, citrus, group 10-10 2.0
Fruit, pome, group 11-10 3.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0
Fruit, stone, group 12-12 3.5
Grain, aspirated fractions 3.0
Grape, raisin 8.5
Herb subgroup 19A 150
Hop, dried cones 35
Kohlrabi 6.0
Leaf petiole vegetable subgroup 22B 45
Leafy greens subgroup 4-16A 70
Mango 1.5
Nut, tree, group 14-12 0.70
Oilseed group 20 3.5
Papaya 1.5
Pea and bean, dried shelled, except soybean, subgroup 6C 2.5
Pea and bean, succulent shelled, subgroup 6B 0.60
Peanut 0.05
Peanut, meal 0.15
Peanut, refined oil 0.15
Peppermint, tops 30.0
Persimmon 8.0
Sapodilla 1.5
Sapote, black 1.5
Sapote, mamey 1.5
Soybean, hulls 0.2
Soybean, seed 0.1
Soybean, vegetable 2.0
Spearmint, tops 30.0
Star apple 1.5
Tea, dried 2 70
Tea, instant 2 70
Vegetable, Brassica, head and stem, group 5-16 6.0
Vegetable, bulb, group 3-07 5.0
Vegetable, cucurbit, group 9 3.0
Vegetable, fruiting, group 8-10 3.0
Vegetable, legume, edible podded subgroup 6A 5.0
Vegetable, root, except sugar beet, subgroup 1B 2.0
Vegetable, tuberous and corm, subgroup 1C 0.05
1 There are no U.S. registrations for this commodity as of September 16, 2009.
2 There are no U.S. registrations for these commodities as of August 13, 2021.

(2) Tolerances are established for residues of the fungicide boscalid, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), and metabolites 2-chloro-N-(4'-chloro-5-hydroxy-biphenyl-2-yl) nicotinamide and glucuronic acid conjugate of 2-chloro-N-(4′-chloro-5-hydroxy-biphenyl-2-yl) nicotinamide, calculated as the stoichiometric equivalent of boscalid in or on the following food commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.30
Cattle, meat 0.10
Cattle, meat byproducts 0.35
Egg 0.02
Goat, fat 0.30
Goat, meat 0.10
Goat, meat byproducts 0.35
Hog, fat 0.20
Hog, meat 0.05
Hog, meat byproducts 0.10
Horse, fat 0.30
Horse, meat 0.10
Horse, meat byproducts 0.35
Milk 0.10
Poultry, fat 0.20
Poultry, meat 0.05
Poultry, meat byproducts 0.20
Sheep, fat 0.30
Sheep, meat 0.10
Sheep, meat byproducts 0.35

(b) [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide boscalid, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), in or on the following commodities:

Table 3 to Paragraph (d)

Commodity Parts per million
Animal feed, nongrass, group 18, forage, except alfalfa 1.0
Animal feed, nongrass, group 18, hay, except alfalfa 2.0
Animal feed, nongrass, group 18, seed 0.05
Beet, sugar, roots 0.1
Grain, cereal, forage, fodder and straw, group 16, forage 2.0
Grain, cereal, forage, fodder and straw, group 16, stover 1.5
Grain, cereal, forage, fodder and straw, group 16, straw 3.0
Grain, cereal, group 15 0.20
Grass, forage, fodder, and hay, group 17, forage 2.0
Grass, forage, fodder, and hay, group 17, hay 8.0
Grass, forage, fodder, and hay, group 17, seed screenings 0.20
Grass, forage, fodder, and hay, group 17, straw 0.30
Rice, hulls 0.50
Vegetable, foliage of legume, group 7, forage 1.5
Vegetable, foliage of legume, group 7, hay 2.0
Vegetable, foliage of legume, group 7, vines 0.05
Vegetable, leafy, except brassica, group 4, except celery, lettuce and spinach 1.0
Vegetable, leaves of root and tuber, group 2 0.1

[68 FR 44651, July 30, 2003, as amended at 69 FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, 2005; 71 FR 6364, Feb. 8, 2006; 71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, 2013; 80 FR 14014, Mar. 18, 2015; 82 FR 56739, Nov. 30, 2017; 83 FR 52996, Oct. 19, 2018; 86 FR 44626, Aug. 13, 2021; 91 FR 9727, Feb. 27, 2026]

§ 180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.

(a) General. Tolerances are established for residues of the growth inhibitor 2,6-DIPN, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only 2,6-Diisopropylnaphthalene.

Commodity Parts per million
Cattle, fat 0.2
Cattle, meat 0.02
Cattle, meat byproducts, except fat 0.02
Goat, fat 0.2
Goat, meat 0.02
Goat, meat byproducts, except fat 0.02
Horse, fat 0.2
Horse, meat 0.02
Horse, meat byproducts, except fat 0.02
Milk, fat 0.02
Potato, granules/flakes 5.5
Potato, wet peel 6.0
Potato, whole 2.0
Sheep, fat 0.2
Sheep, meat 0.02
Sheep, meat byproducts, except fat 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 52011, Sept. 1, 2006, as amended at 74 FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, 2012]

§ 180.591 Trifloxysulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide trifloxysulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]-3-(2,2,2-trifluoroethoxy)-2-pyridinesulfonamide in or on the following raw agricultural commodities.

Commodity Parts per million
Almond 0.02
Almond, hulls 0.01
Fruit, citrus, Group 10 0.03
Cotton, undelinted seed 0.05
Cotton, gin byproducts 1.0
Sugarcane 0.01
Tomato 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 54386, Sept. 17, 2003]

§ 180.592 Butafenacil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million
Cotton, gin byproducts 10
Cotton, undelinted seed 0.50

(2) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) and its metabolite CGA-293731 (1-carboxy-1-methylethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate), in or on the following livestock commodities:

Commodity Parts per million
Cattle, kidney 0.05
Cattle, liver 0.50
Goat, kidney 0.05
Goat, liver 0.50
Hog, kidney 0.05
Hog, liver 0.50
Horse, kidney 0.05
Horse, liver 0.50
Sheep, kidney 0.05
Sheep, liver 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[68 FR 54827, Sept. 19, 2003]

§ 180.593 Etoxazole; tolerances for residues.

(a) General. Tolerances are established for residues of etoxazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only etoxazole (2-(2,6-difluorophenyl)-4-[4-(1,1-dimethylethyl)-2-ethoxyphenyl]-4,5-dihydrooxazole) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 3
Apple, wet pomace 0.5
Avocado 0.2
Beet, sugar, leaves 1
Beet, sugar, roots 0.02
Berry, low growing, subgroup 13-07G 0.5
Caneberry subgroup 13-07A 1.5
Canistel 0.2
Cattle, fat 0.02
Cattle, liver 0.01
Cherry subgroup 12-12A 1
Corn, field, forage 0.8
Corn, field, grain 0.01
Corn, field, refined oil 0.03
Corn, field, stover 4
Corn, pop, grain 0.01
Corn, pop, stover 4
Corn, sweet, forage 1.5
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 5
Cotton, gin byproducts 1
Cottonseed subgroup 20C 0.05
Fruit, pome, group 11-10 0.2
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.5
Goat, fat 0.02
Goat, liver 0.01
Grape, raisin 1.5
Hop, dried cones 7
Horse, fat 0.02
Horse, liver 0.01
Mango 0.2
Melon subgroup 9A 0.2
Milk, fat 0.01
Nut, tree, group 14-12 0.01
Orange 1 0.1
Orange, oil 1 1
Papaya 0.2
Peach subgroup 12-12B 1
Pepper/eggplant subgroup 8-10B 0.2
Peppermint, fresh leaves 15
Peppermint, oil 20
Plum, prune, dried 0.3
Plum subgroup 12-12C 0.15
Sapodilla 0.2
Sapote, black 0.2
Sapote, mamey 0.2
Sheep, fat 0.02
Sheep, liver 0.01
Soybean, seed 0.02
Spearmint, fresh leaves 15
Spearmint, oil 20
Squash/cucumber subgroup 9B 0.02
Star apple 0.2
Tangerine 1 0.1
Tea, dried 1 15
Tomato 0.2
1 There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[68 FR 55493, Sept. 26, 2003, as amended at 70 FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 2007; 74 FR 25160, May 27, 2009; 76 FR 20542, Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012; 80 FR 75430, Dec. 2, 2015; 81 FR 49169, July 27, 2016; 83 FR 51867, Oct. 15, 2018; 84 FR 66630, Dec. 5, 2019; 91 FR 8115, Feb. 20, 2026]

§ 180.594 Thiacloprid; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide thiacloprid, including its metabolites and degradates in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only thiacloprid ([3-[(6-chloro-3-pyridinyl)methyl]-2-thiazolidinylidene] cyanamide) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Apple, wet pomace 1 0.60
Cattle, fat 1 0.020
Cattle, kidney 1 0.050
Cattle, liver 1 0.15
Cattle, meat 1 0.030
Cattle, meat byproducts 1 0.050
Cherry subgroup 12-12A 1 0.5
Cotton, gin byproducts 1 11.0
Cotton, undelinted seed 1 0.020
Fruit, pome, group 11 1 0.30
Goat, fat 1 0.020
Goat, kidney 1 0.050
Goat, liver 1 0.15
Goat, meat 1 0.030
Goat, meat byproducts 1 0.050
Horse, fat 1 0.020
Horse, kidney 1 0.050
Horse, liver 1 0.15
Horse, meat 1 0.030
Horse, meat byproducts 1 0.050
Milk 1 0.030
Peach subgroup 12-12B 1 0.5
Pepper 1 1.0
Plum subgroup 12-12C 1 0.05
Sheep, fat 1 0.020
Sheep, kidney 1 0.050
Sheep, liver 1 0.15
Sheep, meat 1 0.030
Sheep, meat byproducts 1 0.050
1 There are no U.S. registrations for the commodity since August 6, 2014.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55512, Sept. 26, 2003, as amended at 78 FR 8416, Feb. 6, 2013; 81 FR 34907, June 1, 2016; 88 FR 46086, July 19, 2023]

§ 180.595 Flufenpyr-ethyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide, flufenpyr-ethyl; acetic acid, [2-chloro-4-fluoro-5-[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], in or on the commodities in Table 1 to paragraph (a)(1).

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Corn, field, grain 1 0.01
Soybean, seed 1 0.01
Sugarcane, cane 1 0.01
1 This tolerance expires on August 26, 2026.

(2) Tolerances are established for residues of the herbicide flufenpyr-ethyl; acetic acid, [2-chloro-4-fluoro-5-[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], and its metabolite, S-3153 acid-4-OH; [2-chloro-4-hydroxy-5-[5-methyl-6- oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-acetic acid, free and conjugated, in or on the commodities in Table 2 to paragraph (a)(2).

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Corn, field, forage 1 0.05
Corn, field, stover 1 0.05
1 This tolerance expires on August 26, 2026.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 54842, Sept. 19, 2003, as amended at 91 FR 9727, Feb. 27, 2026]

§ 180.596 Fosthiazate; tolerances for residues.

(a) General. A tolerance is established for residues of the insecticide fosthiazate, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of fosthiazate, O-ethyl S-(1-methylpropyl)(2-oxo-3-thiazolidinyl)phosphonothioate, and its metabolite, O-ethyl S-(1-methylpropyl)(2-(methylsulfonyl)ethyl)phosphoramidothioate, calculated as the stoichiometric equivalent of fosthiazate, in or on the commodity.

Commodity Parts per million
Tomato 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 18275, Apr. 7, 2004, as amended at 76 FR 23498, Apr. 27, 2011]

§ 180.597 Mesosulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide mesosulfuron-methyl, (methyl 2-[[[[(4,6-dimethoxy-2-pyrimidinyl) amino]carbonyl]amino]sulfonyl] -4-[[(methylsulfonyl)amino] methyl]benzoate]) in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, meat byproducts 0.01
Goat, meat byproducts 0.01
Grain, aspirated fractions 0.60
Horse, meat byproducts 0.01
Sheep, meat byproducts 0.01
Wheat, forage 0.60
Wheat, germ 0.10
Wheat, grain 0.03
Wheat, hay 0.06
Wheat, straw 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 18263, Apr. 7, 2004]

§ 180.598 Novaluron; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide novaluron, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table is to be determined by measuring only novaluron, (N-[[[3-chloro-4-[1,1,2-trifluoro-2- (trifluoromethoxy)ethoxy]phenyl]amino]carbonyl]-2,6-difluorobenzamide), in or on the following raw agricultural commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 15
Almond, hulls 15
Apple, wet pomace 8.0
Avocado 0.60
Bean, adzuki, dry seed 0.3
Bean, African yam, dry seed 0.3
Bean, American potato, dry seed 0.3
Bean, asparagus, dry seed 0.3
Bean, asparagus, edible podded 0.7
Bean, black, dry seed 0.3
Bean, broad, dry seed 0.3
Bean, broad, succulent shelled 0.7
Bean, catjang, dry seed 0.3
Bean, catjang edible podded 0.7
Bean, catjang, succulent shelled 0.7
Bean, cranberry, dry seed 0.3
Bean, dry bean, dry seed 0.3
Bean, field, dry seed 0.3
Bean, French, dry seed 0.3
Bean, French, edible podded 0.7
Bean, garden, dry seed 0.3
Bean, garden, edible podded 0.7
Bean, goa, dry seed 0.3
Bean, goa, edible podded 0.7
Bean, goa, succulent shelled 0.7
Bean, great northern, dry seed 0.3
Bean, green, dry seed 0.3
Bean, green, edible podded 0.7
Bean, guar, dry seed 0.3
Bean, guar, edible podded 0.7
Bean, horse gram, dry seed 0.3
Bean, kidney, dry seed 0.3
Bean, kidney, edible podded 0.7
Bean, lablab, dry seed 0.3
Bean, lablab, edible podded 0.7
Bean, lablab, succulent shelled 0.7
Bean, lima, dry seed 0.3
Bean, lima, succulent shelled 0.7
Bean, morama, dry seed 0.3
Bean, moth, dry seed 0.3
Bean, moth, edible podded 0.7
Bean, moth, succulent shelled 0.7
Bean, mung, dry seed 0.3
Bean, mung, edible podded 0.7
Bean, navy, dry seed 0.3
Bean, navy, edible podded 0.7
Bean, phaseolus, forage 15
Bean, phaseolus, hay 80
Bean, pink, dry seed 0.3
Bean, pinto, dry seed 0.3
Bean, red, dry seed 0.3
Bean, rice, dry seed 0.3
Bean, rice, edible podded 0.7
Bean, scarlet runner, dry seed 0.3
Bean, scarlet runner, edible podded 0.7
Bean, scarlet runner, succulent shelled 0.7
Bean, snap, edible podded 0.7
Bean, sword, dry seed 0.3
Bean, sword, edible podded 0.7
Bean, tepary, dry seed 0.3
Bean, urd, dry seed 0.3
Bean, urd, edible podded 0.7
Bean, wax, edible podded 0.7
Bean, wax, succulent shelled 0.7
Bean, yardlong, dry seed 0.3
Bean, yardlong, edible podded 0.7
Bean, yellow, dry seed 0.3
Berry, low growing, subgroup 13-07G, except lowbush blueberry 0.45
Brassica, leafy greens, subgroup 4-16B 25
Bushberry subgroup 13-07B 7.0
Carrot 0.05
Cattle, fat 11
Cattle, kidney 1.0
Cattle, liver 1.0
Cattle, meat 0.60
Cattle, meat byproducts, except kidney and liver 11
Cherry subgroup 12-12A 8.0
Chickpea, dry seed 0.1
Chickpea, edible podded 2
Chickpea, succulent shelled 0.05
Corn, sweet, forage 16
Corn, sweet, kernel plus cob with husks removed 0.05
Corn, sweet, stover 50
Cotton, gin byproducts 30
Cottonseed subgroup 20C 0.5
Cowpea, dry seed 0.3
Cowpea, edible podded 0.7
Cowpea, forage 15
Cowpea, hay 80
Cowpea, succulent shelled 0.7
Egg 1.5
Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food and feed handling establishments 0.01
Fruit, pome, group 11-10 3.0
Goat, fat 11
Goat, kidney 1.0
Goat, liver 1.0
Goat, meat 0.60
Goat, meat byproducts, except kidney and liver 11
Grain, aspirated fractions 25
Hog, fat 1.5
Hog, kidney 0.10
Hog, liver 0.10
Hog, meat 0.07
Hog, meat byproducts, except kidney and liver 1.5
Horse, fat 11
Horse, kidney 1.0
Horse, liver 1.0
Horse, meat 0.60
Horse, meat byproducts, except kidney and liver 11
Jackbean, dry seed 0.3
Jackbean, edible podded 0.7
Jackbean, succulent shelled 0.7
Kohlrabi 0.7
Lentil, dry seed 0.1
Lentil, edible podded 2
Lentil, succulent shelled 0.05
Longbean, Chinese, dry seed 0.3
Longbean, Chinese, edible podded 0.7
Lupin, Andean, dry seed 0.3
Lupin, Andean, succulent shelled 0.7
Lupin, blue, dry seed 0.3
Lupin, blue, succulent shelled 0.7
Lupin, grain, dry seed 0.3
Lupin, grain, succulent shelled 0.7
Lupin, sweet, dry seed 0.3
Lupin, sweet, succulent shelled 0.7
Lupin, white sweet, dry seed 0.3
Lupin, white sweet, succulent shelled 0.7
Lupin, white, dry seed 0.3
Lupin, white, succulent shelled 0.7
Lupin, yellow, dry seed 0.3
Lupin, yellow, succulent shelled 0.7
Milk 1.0
Milk, fat 20
Nut, tree, group 14-12 0.08
Pea, blackeyed, dry seed 0.3
Pea, blackeyed, succulent shelled 0.7
Pea, crowder, dry seed 0.3
Pea, crowder, succulent shelled 0.7
Pea, dry, dry seed 0.1
Pea, dwarf, edible podded 2
Pea, English, succulent shelled 0.05
Pea, field, dry seed 0.1
Pea, field, forage 15
Pea, field, hay 80
Pea, garden, dry seed 0.1
Pea, garden, succulent shelled 0.05
Pea, grass, dry seed 0.1
Pea, grass, edible podded 2
Pea, green, dry seed 0.1
Pea, green, edible podded 2
Pea, green, succulent shelled 0.05
Pea, pigeon, dry seed 0.1
Pea, pigeon, edible podded 2
Pea, pigeon, succulent shelled 0.05
Pea, snap, edible podded 2
Pea, snow, edible podded 2
Pea, southern, dry seed 0.3
Pea, southern, succulent shelled 0.7
Pea, sugar snap, edible podded 2
Pea, winged, dry seed 0.3
Pea, winged, edible podded 0.7
Peach subgroup 12-12B 1.9
Peanut 0.01
Plum, prune, dried 3.0
Plum subgroup 12-12C 1.9
Poultry, fat 7.0
Poultry, kidney 0.80
Poultry, liver 0.80
Poultry, meat 0.40
Poultry, meat byproducts, except kidney and liver 7.0
Sheep, fat 11
Sheep, kidney 1.0
Sheep, liver 1.0
Sheep, meat 0.60
Sheep, meat byproducts, except kidney and liver 11
Sorghum, grain, forage 6.0
Sorghum, grain, grain 3.0
Sorghum, grain, stover 40
Soybean, seed 0.07
Soybean, vegetable, dry seed 0.3
Soybean, vegetable, edible podded 0.7
Soybean, vegetable, succulent shelled 0.7
Sugarcane, cane 0.50
Sunflower subgroup 20B 0.07
Swiss chard 12
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 9
Vegetable, Brassica, head and stem, Group 5-16 0.7
Vegetable, cucurbit, group 9 0.20
Vegetable, fruiting, group 8-10 2
Vegetable, tuberous and corm, subgroup 1C 0.05
Velvetbean, dry seed 0.3
Velvetbean, edible podded 0.7
Velvetbean, succulent shelled 0.7

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[69 FR 31021, June 2, 2004, as amended at 71 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2006; 73 FR 74982, Dec. 10, 2008; 74 FR 637, Jan. 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26, 2010; 76 FR 55814, Sept. 9, 2011; 78 FR 40033, July 3, 2013; 80 FR 43335, July 22, 2015; 85 FR 49264, Aug. 13, 2020; 87 FR 13639, Mar. 10, 2022; 87 FR 57619, Sept. 21, 2022]

§ 180.599 Acequinocyl; tolerances for residues.

(a) General. Tolerances are established for residues of acequinocyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of acequinocyl [2-(acetyloxy)-3-dodecyl-1,4-naphthalenedione] and its metabolite, 2-dodecyl-3-hydroxy-1,4-naphthoquinone, calculated as the stoichiometric equivalent of acequinocyl, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 2
Apple, wet pomace 1
Avocado 0.5
Bean, dry, seed 0.15
Bean, edible podded 0.25
Bean, succulent shelled 0.3
Berry, low growing, subgroup 13-07G 0.5
Bushberry subgroup 13-07B 3
Caneberry subgroup 13-07A 4
Cattle, fat 0.02
Cattle, meat byproducts 0.02
Cherry, subgroup 12-12A 1
Cowpea, forage 6
Cowpea, hay 18
Fruit, citrus, group 10-10 0.35
Fruit, citrus, group 10-10, oil 30
Fruit, pome, group 11-10 0.4
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.6
Goat, fat 0.02
Goat, meat byproducts 0.02
Guava 0.9
Hop, dried cones 15
Horse, fat 0.02
Horse, meat byproducts 0.02
Nut, tree, group 14-12 0.02
Sheep, fat 0.02
Sheep, meat byproducts 0.02
Soybean, vegetable, succulent 0.25
Tea, plucked leaves 1 40
Tropical and subtropical, medium to large fruit, smooth, inedible peel subgroup 24B 4
Tropical and subtropical, small fruit, inedible peel, subgroup 24A 2
Vegetable, cucurbit, group 9 0.3
Vegetable, fruiting, group 8-10 0.7
1 There are no U.S. registrations as of January 18, 2017 for use on tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 43533, July 21, 2004, as amended at 73 FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, 2010; 77 FR 25909, May 2, 2012; 81 FR 21756, Apr. 13, 2016; 82 FR 5414, Jan. 18, 2017; 83 FR 26373, June 7, 2018; 85 FR 29340, May 15, 2020; 86 FR 48510, Aug. 31, 2021; 91 FR 8116, Feb. 20, 2026]

§ 180.600 Propoxycarbazone; tolerances for residues.

(a) General.

(1) Tolerances are established for combined residues of the herbicide propoxycarbazone methyl 2-[[[(4,5-dihydro-4-methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate and its metabolite methyl 2-[[[(4,5-dihydro-3-(2-hydroxypropoxy)-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural commodities:

Commodity Parts per million
Grass, forage 20
Grass, hay 25
Wheat, forage 17
Wheat, grain 0.02
Wheat, hay 0.15
Wheat, straw 0.05

(2) Tolerances are established for residues of the herbicide propoxycarbazone methyl 2-[[[(4,5-dihydro-4-methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural commodities:

Commodity Parts per million
Cattle, meat 0.05
Cattle, meat byproducts 0.3
Goat, meat 0.05
Goat, meat byproducts 0.3
Horse, meat 0.05
Horse, meat byproducts 0.3
Milk 0.03
Sheep, meat 0.05
Sheep, meat byproducts 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 40781, July 7, 2004, as amended at 71 FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, 2009]

§ 180.601 Cyazofamid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide cyazofamid, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of 4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite, 4-chloro-5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Brassica, leafy greens, subgroup 4-16B 15
Bulb vegetables, group 3-07 2.0
Carrot, roots 0.09
Chickpea, edible podded 0.5
Chickpea, succulent shelled 0.08
Ginseng 0.3
Herb subgroup 19A 90
Hop dried cones 10.0
Kohlrabi 1.5
Leafy greens subgroup 4-16A 10
Parsnip, roots 0.09
Vegetable, brassica, head and stem, group 5-16 1.5
Vegetable, cucurbit, group 9 0.10
Vegetable, fruiting, group 8-10 0.9
Vegetable, legume, bean, edible podded, subgroup 6-22A 0.5
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.08
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.03
Vegetable, tuberous and corm, subgroup 1C 0.02

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the fungicide cyazofamid, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of 4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite, 4-chloro-5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, in or on the following commodities:

Commodity Parts per million
Grape 1.5

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 58299, Sept. 30, 2004, as amended at 73 FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 2009; 75 FR 40751, July 14, 2010; 77 FR 4252, Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012; 81 FR 5605, Feb. 3, 2016; 85 FR 15391, Mar. 18, 2020; 89 FR 96569, Dec. 5, 2024]

§ 180.602 Spiroxamine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide spiroxamine, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following table is to be determined by measuring only spiroxamine, [(8-(1,1-dimethylethyl)-N-ethyl-N-propyl-1,4-dioxaspiro[4,5]decane-2-methanamine) in or on the commodities.

Commodity Parts per million
Artichoke, globe, import 1 0.7
Asparagus 1 0.05
Banana (import) 3.0
Grape (import) 1.0
Vegetable, fruiting , crop group 8 1 1.2
1 No U.S. registration as of December 1, 2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 42570, July 16, 2004, as amended at 75 FR 74640, Dec. 1, 2010; 80 FR 72599, Nov. 20, 2015]

§ 180.603 Dinotefuran; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea, calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below:

Commodity Parts per million
Berry, low growing, except strawberry, subgroup 13-07H 0.2
Brassica, head and stem, subgroup 5A 1.4
Brassica, leafy greens, subgroup 5B 15.0
Cotton, undelinted seed 0.4
Cotton, gin byproducts 8.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.9
Grape, raisin 2.5
Onion, bulb, subgroup 3-07A 0.15
Onion, green, subgroup 3-07B 5.0
Peach 1.0
Persimmon 1 2
Potato, chips 0.1
Potato, granules/flakes 0.15
Rice, grain 9.0
Tea, dried2 50
Tomato, paste 1.0
Turnip, greens 15.0
Vegetable, fruiting, group 8 0.7
Vegetable, cucurbit, group 9 0.5
Vegetable, leafy, except Brassica, group 4 5.0
Vegetable, tuberous and corm, subgroup 1C 0.05
Watercress 8.0
1 There are no U.S. registrations for use of dinotefuran on this commodity
2 There are no U.S. registrations for tea.

(2) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine in or on the commodities listed in the table below:

Commodity Parts per million
Cattle, fat 0.05
Cattle, meat 0.05
Cattle, meat byproducts 0.05
Egg 0.01
Goat, fat 0.05
Goat, meat 0.05
Goat, meat byproducts 0.05
Hog, fat 0.05
Hog, meat 0.05
Hog, meat byproducts 0.05
Horse, fat 0.05
Horse, meat 0.05
Horse, meat byproducts 0.05
Milk 0.05
Poultry, meat byproducts 0.01
Sheep, fat 0.05
Sheep, meat 0.05
Sheep, meat byproducts 0.05

(3) A tolerance of 0.01 parts per million is established for residues of the insecticide dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on all food and/or feed commodities (other than those covered by a higher tolerance as a result of use on growing crops or inadvertent residues) when residues result from application of dinotefuran in food and/or feed handling establishments where food and/or feed products are held, stored, processed, prepared, or served. Compliance with the tolerance level is to be determined by measuring only dinotefuran.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on the commodities in the table below resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea, calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below. The tolerances expire and are revoked on the dates specified in the table.

Commodity Parts per million Expiration/
revocation
date
Fruit, pome, Group 11 2.0 12/31/21
Fruit, stone, Group 12 2.0 12/31/21
Kiwifruit, fuzzy 0.9 12/31/2022

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 14546, Mar. 23, 2005, as amended at 74 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, 2009; 75 FR 770, Jan. 6, 2010; 77 FR 56138, Sept. 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR 24683, Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014; 80 FR 78145, Dec. 16, 2015; 83 FR 62732, Dec. 6, 2018; 84 FR 49479, Sept. 20, 2019; 84 FR 59936, Nov. 7, 2019]

§ 180.604 Mepanipyrim; tolerances for residues.

(a) General. [Reserved]

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect of inadvertent residues. [Reserved]

(e) Revoked tolerances subject to the channel of trade provisions. [Reserved]

(f) Import tolerances. Tolerances are established for the combined residues of mepanipyrim, 4-methyl-N-phenyl-6-(1-propynyl)-2-pyrimidinamine, and its metabolite, 4-methyl-N-phenyl-6-(2-hydroxypropylk)-2-pyrimidinamine, both free and conjugated in or on the following commodities:

Commodity Parts per million
Grape 1.5
Grape, raisin 3.0
Strawberry 1.5
Tomato 0.5

[68 FR 60827, Oct. 13, 2004]

§ 180.605 Penoxsulam; tolerances for residues.

(a) General. Tolerances are established for residues of penoxsulam, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only penoxsulam 2-(2,2-difluoroethoxy)-N-(5,8-dimethoxy[1,2,4]triazolo[1,5-c] pyrimidin-2-yl)-6-(trifluoromethyl) benzenesulfonamide, in or on the commodity.

Commodity Parts per
million
Almond, hulls 0.01
Artichoke, globe 0.01
Fish 0.01
Fish, shellfish, crustacean 0.01
Fish, shellfish, mollusc 0.02
Fruit, pome, group 11-10 0.01
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 0.01
Fruit, stone, group 12-12 0.01
Nut, tree, group 14-12 0.01
Olive 0.01
Pomegranate 0.01
Rice, grain 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 57197, Sept. 24, 2004, as amended at 72 FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, 2009; 80 FR 72599, Nov. 20, 2015; 81 FR 10776, Mar. 2, 2016; 85 FR 13552, Mar. 9, 2020]

§ 180.607 Spiromesifen; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate] and 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, calculated as the stoichiometric equivalent of spiromesifen, in or on the following primary crop commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Bean, dry 0.02
Bean, edible podded 0.80
Bean, succulent 0.10
Berry and small fruit, low growing berry, subgroup 13-07G 2.0
Brassica, head and stem, subgroup 5A 2.0
Brassica, leafy greens, subgroup 5B 12
Coffee, green bean 1 0.20
Corn, field, forage 5.0
Corn, field, grain 0.02
Corn, field, stover 8.0
Corn, pop, grain 0.02
Corn, pop, stover 4.0
Corn, sweet, forage 17
Corn, sweet, kernel plus cob with husks removed 0.02
Corn, sweet, stover 12
Cotton, gin byproducts 15
Cotton, undelinted seed 0.50
Cowpea, forage 30
Cowpea, hay 86
Leaf petiole subgroup 4B 6.0
Leafy greens subgroup 4A 12
Orange 2 0.15
Orange subgroup 10-10A, oil 2 10
Pea, dry, seed 0.20
Peppermint, tops 45
Spearmint, tops 45
Tea, dry 40
Tomato, paste 0.80
Vegetable, cucurbit, group 9 0.10
Vegetable, fruiting, group 8 0.45
Vegetable, tuberous and corm, subgroup 1C 0.02
1 This use has not been registered in the United States as of August 28, 2018.
2 There are no U.S. registrations for these commodities as of June 26, 2024.

(2) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate] and its metabolites containing the 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one and 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one moieties, calculated as the stoichiometric equivalent of spiromesifen, in the following livestock commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.10
Cattle, meat 0.02
Cattle, meat byproducts 0.20
Goat, fat 0.10
Goat, meat 0.02
Goat, meat byproducts 0.20
Horse, fat 0.10
Horse, meat 0.02
Horse, meat byproducts 0.20
Milk 0.01
Milk, fat 0.25
Sheep, fat 0.10
Sheep, meat 0.02
Sheep, meat byproducts 0.20

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the inadvertent or indirect residues of the insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate], 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, and its metabolites containing the 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one moiety, calculated as the stoichiometric equivalent of spiromesifen, in the following rotational crop commodities:

Table 3 to Paragraph (d)

Commodity Parts per million
Alfalfa, forage 1.5
Alfalfa, hay 3.0
Barley, grain 0.03
Barley, hay 0.25
Barley, straw 0.15
Beet, sugar, roots 0.03
Beet, sugar, tops 0.20
Oat, forage 0.20
Oat, grain 0.03
Oat, hay 0.25
Oat, straw 0.25
Vegetable, bulb, group 3-07 0.09
Wheat, forage 0.20
Wheat, grain 0.03
Wheat, hay 0.15
Wheat, straw 0.25

[70 FR 43283, July 27, 2005, as amended at 72 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, 2008; 73 FR 52606, Sept. 10, 2008; 74 FR 8492, Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 FR 81396, Dec. 28, 2011; 78 FR 3337, Jan. 16, 2013; 83 FR 45849, Sept. 11, 2018; 89 FR 53359, June 26, 2024; 91 FR 9728, Feb. 27, 2026]

§ 180.608 Spirodiclofen; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in or on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate).

Commodity Parts per million
Almond, hulls 20.0
Apple, wet pomace 2.4
Avocado 1.0
Black sapote 1.0
Canistel 1.0
Citrus, juice 0.60
Citrus, oil 35
Fruit, citrus, group 10 0.50
Fruit, pome, group 11 0.80
Fruit, stone, group 12 1.0
Grape 2.0
Grape, raisin 6.0
Hop, dried cones 30
Mamey sapote 1.0
Mango 1.0
Nut, tree, group 14 0.10
Papaya 1.0
Pistachio 0.10
Sapodilla 1.0
Star apple 1.0

(2) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in or on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate) and its metabolite 3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4,5] dec-3-en-2-one, calculated as the stoichiometric equivalent of spirodiclofen.

Commodity Parts per million
Cattle, fat 0.02
Cattle, meat byproducts 0.10
Cattle, meat 0.02
Goat, fat 0.02
Goat, meat byproducts 0.1
Goat, meat 0.02
Horse, fat 0.02
Horse, meat byproducts 0.1
Horse, meat 0.02
Milk 0.01
Milk, fat 0.03
Sheep, fat 0.02
Sheep. meat byproducts 0.1
Sheep. meat 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 40211, July 13, 2005, as amended at 73 FR 25539, May 7, 2008; 75 FR 24434, May 5, 2010; 77 FR 73939, Dec. 12, 2012; 79 FR 33464, June 11, 2014]

§ 180.609 Fluoxastrobin; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million
Avocado 1.0
Barley, grain 0.40
Barley, hay 15
Barley, straw 15
Berry, low growing, subgroup 13-07G 1.9
Corn, field, forage 3.0
Corn, field, grain 0.02
Corn, field, stover 4.5
Corn, sweet, forage 13
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 10
Cotton, gin byproducts 0.01
Cotton, undelinted seed 0.01
Grain, aspirated grain fractions 60
Leaf petioles subgroup 4B 4.0
Melon subgroup 9A 1.5
Pea and bean, dried shelled, except soybean, subgroup 6C 0.20
Peanut 0.02
Peanut, hay 20.0
Peanut, refined oil 0.06
Rapeseed, subgroup 20A 0.70
Rice, grain 4.0
Sorghum, grain, forage 5.0
Sorghum, grain, grain 1.5
Sorghum, grain, stover 5.0
Soybean, forage 9.0
Soybean, hay 1.2
Soybean, hulls 0.20
Soybean, seed 0.05
Squash/cucumber subgroup 9B 0.50
Tomato, paste 1.5
Vegetable, fruiting, group 8 1.0
Vegetable, tuberous and corm, subgroup 1C 0.010
Wheat, forage 7.0
Wheat, grain 0.15
Wheat, hay 17
Wheat, straw 11

(2) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, and its phenoxy-hydroxypyrimidine, 6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinol, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million
Cattle, fat 0.10
Cattle, meat 0.05
Cattle, meat byproducts 0.20
Goat, fat 0.10
Goat, meat 0.05
Goat, meat byproducts 0.20
Hog, fat 0.03
Hog, meat byproducts 0.06
Horse, fat 0.10
Horse, meat 0.05
Horse, meat byproducts 0.20
Milk 0.03
Milk, fat 0.75
Poultry, liver 0.06
Sheep, fat 0.10
Sheep, meat 0.05
Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of fluoxastrobin, including its metabolites and degradates, in or on the commodities in the table below, when present therein as a result of the application of fluoxastrobin to the growing crops listed in paragraph (a)(1) of this section. Compliance with the tolerance levels specified below is to be determined by measuring only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million
Alfalfa, forage 0.050
Alfalfa, hay 0.10
Cotton, gin byproducts 0.020
Grain, cereal, forage, fodder, and straw, group 16, except corn 0.10
Grass, forage 0.10
Grass, hay 0.50
Vegetable, foliage of legume, group 7 0.050

[74 FR 67113, Dec. 18, 2009, as amended at 75 FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, 2011; 77 FR 26471, May 4, 2012; 77 FR 64915, Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR 59119, Oct. 1, 2014; 82 FR 45735, Oct. 2, 2017; 84 FR 38143, Aug. 6, 2019]

§ 180.610 Aminopyralid; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2-pyridinecarboxylic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only free and conjugated aminopyralid.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Corn, field, forage 0.3
Corn, field, grain 0.2
Corn, field, stover 0.2
Grain, aspirated fractions 0.2
Grass, forage 25
Grass, hay 50
Wheat, bran 0.1
Wheat, forage 2
Wheat, grain 0.04
Wheat, hay 4
Wheat, straw 0.3

(2) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2-pyridinecarboxylic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only aminopyralid.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.02
Cattle, kidney 0.3
Cattle, meat 0.02
Cattle, meat byproducts, except kidney 0.02
Goat, fat 0.02
Goat, kidney 0.3
Goat, meat 0.02
Goat, meat byproducts, except kidney 0.02
Horse, fat 0.02
Horse, kidney 0.3
Horse, meat 0.02
Horse, meat byproducts, except kidney 0.02
Milk 0.03
Sheep, fat 0.02
Sheep, kidney 0.3
Sheep, meat 0.02
Sheep, meat byproducts, except kidney 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 46428, Aug. 10, 2005, as amended at 75 FR 17584, Apr. 7, 2010; 91 FR 8089, Feb. 20, 2026]

§ 180.611 Pinoxaden; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide pinoxaden, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in table 1 to this paragraph (a)(1) is to be determined by measuring pinoxaden (8-(2,6-diethyl-4-methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate) and its metabolites 8-(2,6-diethyl-4-methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione and free and conjugated forms of 8-(2,6-diethyl-4-hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione, and 4-(7,9-dioxo-hexahydro-pyrazolo[1,2-d] [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-benzoic acid, calculated as the stoichiometric equivalent of pinoxaden, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Barley, bran 1.6
Barley, grain 0.9
Barley, hay 3
Barley, straw 3
Egg 0.06
Poultry, fat 0.06
Poultry, meat 0.06
Poultry, meat byproducts 0.06
Wheat, bran 3
Wheat, forage 3.5
Wheat, grain 1.3
Wheat, hay 3
Wheat, straw 3

(2) Tolerances are established for residues of the herbicide pinoxaden, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in table 2 to this paragraph (a)(2) is to be determined by measuring pinoxaden (8-(2,6-diethyl-4-methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo[1,2-d][1,4,5]oxadiazepin-9-yl 2,2-dimethylpropanoate) and its metabolites 8-(2,6-diethyl-4-methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione and free and conjugated forms of 8-(2,6-diethyl-4-hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione, calculated as the stoichiometric equivalent of pinoxaden, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.04
Cattle, meat 0.04
Cattle, meat byproducts 0.04
Goat, fat 0.04
Goat, meat 0.04
Goat, meat byproducts 0.04
Hog, fat 0.04
Hog, meat 0.04
Hog, meat byproducts 0.04
Horse, fat 0.04
Horse, meat 0.04
Horse, meat byproducts 0.04
Milk 0.02
Sheep, fat 0.04
Sheep, meat 0.04
Sheep, meat byproducts 0.04

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 43322, July 27, 2005, as amended at 91 FR 8117, Feb. 20, 2026]

§ 180.612 Topramezone; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide topramezone, including its metabolites and degradates, in or on the following commodities. Compliance with the following tolerance levels is to be determined by measuring only topramezone ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl-4-(methylsulfonyl)phenyl](5-hydroxy-1-methyl-1H-pyrazol-4-yl)methanone) in or on the following commodities:

Commodity Parts per
million
Cattle, meat byproducts 0.80
Corn, field, forage 0.05
Corn, field, grain 0.01
Corn, field, stover 0.05
Corn, pop, grain 0.01
Corn, pop, stover 0.05
Corn, sweet, forage 0.05
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.05
Fish-freshwater finfish 0.05
Fish-saltwater finfish 0.05
Fish-shellfish, crustacean 0.05
Fish-shellfish, mollusk 0.05
Goat, meat byproducts 0.80
Hog, meat byproducts 0.40
Horse, meat byproducts 0.80
Poultry, meat byproducts 0.02
Sheep, meat byproducts 0.80
Sugarcane, cane 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 48074, Aug. 7, 2013, as amended at 82 FR 35120, July 28, 2017]

§ 180.613 Flonicamid; tolerances for residues.

(a) General.

(1) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its metabolites, TFNA (4-trifluoromethylnicotinic acid), TFNA-AM (4-trifluoromethylnicotinamide), and TFNG, N-(4-trifluoromethylnicotinoyl)glycine, calculated as the stoichiometric equivalent of flonicamid, in or on the following commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 10
Alfalfa, hay 7
Alfalfa, seed 1.5
Almond, hulls 9
Berry, low-growing, subgroup 13-07G 2
Brassica, leafy greens, subgroup 4-16B, except radish, tops 16
Bushberry subgroup 13-07B 1.5
Caneberry subgroup 13-07A 3
Celtuce 4
Cherry subgroup 12-12A 0.6
Corn, sweet, forage 9
Corn, sweet, kernel plus cob with husks removed 0.4
Corn, sweet, stover 20
Cotton, gin byproducts 6
Cotton, hulls 2
Cotton, meal 1
Cottonseed subgroup 20C 0.6
Fennel, florence, fresh leaves and stalk 4
Fruit, citrus, group 10-10 1.5
Fruit, pome, group 11-10 0.2
Hop, dried cones 20
Kohlrabi 1.5
Leaf petiole vegetable subgroup 22B 4
Leafy greens subgroup 4-16A, except spinach 8
Nut, tree, group 14-12 except pistachio 0.15
Peach subgroup 12-12B 1.5
Pepper/Eggplant subgroup 8-10B 3
Peppermint, fresh leaves 7
Pistachio 0.6
Plum subgroup 12-12C 0.6
Pomegranate 0.5
Potato, granules/flakes 0.4
Prickly pear, fruit 2
Prickly pear, pads 3
Radish, tops 20
Rapeseed subgroup 20A 1.5
Small fruit vine climbing (except fuzzy kiwifruit), subgroup 13-07F 3
Spearmint, fresh leaves 7
Spinach 9
Sunflower subgroup 20B 0.7
Tea 1 40
Tomato, paste 2
Tomato, puree 0.5
Tomato subgroup 8-10A 0.4
Vegetable, brassica, head and stem, group 5-16 1.5
Vegetable, cucurbit, group 9 1.5
Vegetable, legume, bean, edible podded, subgroup 6-22A 4
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 7
Vegetable, legume, pea, edible podded, subgroup 6-22B 4
Vegetable, legume, pea, succulent shelled, subgroup 6-22D 7
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 3
Vegetable, legume, pulse, pea, dried shelled, subgroup6-22F 3
Vegetable, root, except sugar beet, subgroup 1B 0.6
Vegetable, tuberous and corm, subgroup 1C 0.2
1 There are no U.S. registrations.

(2) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its metabolites, TFNA (4-trifluoromethylnicotinic acid), and TFNA-AM (4-trifluoromethylnicotinamide), calculated as the Stoichiometric equivalent of flonicamid, in or on the following commodities.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.03
Cattle, meat 0.08
Cattle, meat byproducts 0.08
Egg 0.04
Goat, fat 0.03
Goat, meat 0.08
Goat, meat byproducts 0.08
Hog, fat 0.03
Hog, meat 0.03
Hog, meat byproducts 0.03
Horse, fat 0.03
Horse, meat 0.08
Horse, meat byproducts 0.08
Milk 0.05
Poultry, fat 0.03
Poultry, meat 0.03
Poultry, meat byproducts 0.03
Sheep, fat 0.03
Sheep, meat 0.08
Sheep, meat byproducts 0.08

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by § 180.1(1), are established for the residues of the insecticide flonicamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its metabolites, TFNA (4-trifluoromethylnicotinic acid), TFNA-AM (4-trifluoromethylnicotinamide), and TFNG (N-(4-trifluoromethylnicotinoyl)glycine), calculated as the stoichiometric equivalent of flonicamid, in or on the following commodities:

Table 3 to Paragraph (c)

Commodity Parts per million
Clover, forage 0.9
Clover, hay 5

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 51614, Aug. 31, 2005, as amended at 71 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, 2008; 77 FR 67776, Nov. 14, 2012; 78 FR 75266, Dec. 11, 2013; 81 FR 52352, Aug. 8, 2016; 82 FR 21945, May 11, 2017; 82 FR 31471, July 7, 2017; 83 FR 3615, Jan. 26, 2018; 83 FR 34780, July 23, 2018; 84 FR 13808, Apr. 8, 2019; 85 FR 31986, May 28, 2020; 86 FR 8704, Feb. 9, 2021; 87 FR 30429, May 19, 2022; 88 FR 64823, Sept. 20, 2023; 89 FR 33238, Apr. 29, 2024; 91 FR 8118, Feb. 20, 2026]

§ 180.614 Kasugamycin; tolerances for residues.

(a) General. Tolerances are established for residues of kasugamycin, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by measuring only kasugamycin (3-O-[2-amino-4-[(carboxyimino-methyl)amino]-2,3,4,6-tetradeoxy-α-D-arabino-hexopyranosyl]-D-chiro-inositol) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Cherry subgroup 12-12A 0.60
Fruit, pome, group 11-10 0.20
Tea, dried 1 3
Vegetable, fruiting, group 8 2 0.04
Walnut 0.04
1 There is no U.S. registration as of August 12, 2024.
2 There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of kasugamycin, including metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified is to be determined by measuring only kasugamycin (3-O-[2-amino-4-[(carboxyimino-methyl)amino]-2,3,4,6-tetradeoxy-α-D-arabino-hexopyranosyl]-D-chiro-inositol) in or on the commodity. The tolerances expire on the date specified in the table.

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation date
Almond 0.04 12/31/26
Almond, hulls 0.4 12/31/26

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 51497, Aug. 29, 2014, as amended at 83 FR 9446, Mar. 6, 2018; 85 FR 63453, Oct. 8, 2020; 88 FR 87362, Dec. 18, 2023; 89 FR 65545, Aug. 12, 2024]

§ 180.615 Amicarbazone; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide, amicarbazone [4-amino-4, 5-dihydro- N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and its metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Cattle, fat 0.01
Cattle, liver 1.0
Cattle, meat 0.01
Cattle, meat byproducts, except liver 0.10
Corn, field, forage 0.80
Corn, field, grain 0.05
Corn, field, stover 1.0
Goat, fat 0.01
Goat, liver 1.0
Goat, meat 0.01
Goat, meat byproducts, except liver 0.10
Hog, fat 0.01
Hog, liver 0.10
Hog, meat 0.01
Hog, meat byproducts, except liver 0.01
Horse, fat 0.01
Horse, liver 1.0
Horse, meat 0.01
Horse, meat byproducts, except liver 0.10
Milk 0.01
Poultry, liver 0.10
Sheep, fat 0.01
Sheep, liver 1.0
Sheep, meat 0.01
Sheep, meat byproducts, except liver 0.10
Sugarcane, cane 1 0.2
Sugarcane, molasses 1 0.5
1 There are no current U.S. registrations

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of amicarbazone [4-amino-4, 5-dihydro-N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and its metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the following commodities when present therein as a result of application of amicarbazone to the growing crops in paragraph (a) of this section:

Commodity Parts per million
Alfalfa, forage 0.05
Alfalfa, hay 0.10
Cotton, gin byproducts 0.30
Cotton, undelinted seed 0.07
Soybean, forage 1.50
Soybean, hay 5.0
Soybean, seed 0.80
Wheat, bran 0.15
Wheat, flour 0.15
Wheat, forage 0.50
Wheat, germ 0.15
Wheat, grain 0.10
Wheat, hay 1.0
Wheat, middlings, 0.15
Wheat, shorts 0.15
Wheat, straw 0.50

[70 FR 55760, Sept. 23, 2005, as amended at 74 FR 46377, Sept. 9, 2009; 90 FR 47239, Oct. 1, 2025]

§ 180.616 Fenpropimorph; tolerances for residues.

Tolerances are established for the residues of the fungicide fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]-2,6-dimethylmorpholine) in or on the following commodity:

Commodity Parts per million
Banana* 2.0
*No U.S. registration as of February 10, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 15612, Mar. 29, 2006]

§ 180.617 Metconazole; tolerances for residues.

(a) General. Tolerances are established for residues of metconazole, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only metconazole [5-[(4-chlorophenyl)methyl]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol] as the sum of its cis- and trans-isomers in or on the following commodities:

Commodity Parts per
million
Almond, hulls 4.0
Banana 1 0.1
Barley, grain 2.5
Barley, hay 7.0
Barley, straw 7.0
Beet, sugar, dried pulp 0.70
Beet, sugar, molasses 0.08
Beet, sugar, roots 0.07
Bushberry subgroup 13-07B 0.40
Cattle, meat byproducts 0.04
Corn, field, forage 3.0
Corn, field, grain 0.02
Corn, field, stover 30
Corn, pop, grain 0.02
Corn, pop, stover 30
Corn, sweet, forage 3.0
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 30.0
Cotton, gin byproducts 8.0
Cotton, undelinted seed 0.25
Egg 0.04
Fruit, stone, group 12-12 0.2
Goat, meat byproducts 0.04
Grain, aspirated grain fractions 7.0
Horse, meat byproducts 0.04
Nut, tree, group 14-12 0.04
Oat, grain 1.0
Oat, hay 17
Oat, straw 6.0
Pea and bean, dried shelled, except soybean, subgroup 6C 0.15
Peanut 0.04
Peanut, refined oil 0.05
Rapeseed subgroup 20A 0.08
Rye, grain 0.25
Rye, straw 14
Sheep, meat byproducts 0.04
Soybean, forage 3.0
Soybean, hay 6.0
Soybean, hulls 0.08
Soybean, seed 0.05
Sugarcane, cane 0.06
Sunflower subgroup 20B 0.7
Vegetable, tuberous and corn, subgroup 1C 0.04
Wheat, grain 0.15
Wheat, hay 16
Wheat, milled byproducts 0.20
Wheat, straw 18
1 No U.S. registration as of August 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 56388, Sept. 27, 2006, as amended at 71 FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, 2008; 74 FR 21266, May 7, 2009; 76 FR 50904, Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 FR 12411, Mar. 5, 2014; 80 FR 30625. May 29, 2015]

§ 180.618 Benthiavalicarb-isopropyl; tolerance for residues.

(a) General. Tolerances are established for the combined residues of benthiavalicarb-isopropyl, isopropyl[(S)-1-[[[(1R)-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate and isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate, in or on the following raw agricultural commodities:

Commodity Parts per million
Grape, imported 0.25
Grape, raisin 1.0
Tomato 0.45
Note: There are no U.S. registrations as of July 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect of inadvertent residues. [Reserved]

[71 FR 52003, Sept. 1, 2006]

§ 180.619 Epoxiconazole; tolerances for residues.

(a) General. Tolerances are established for the residues of the fungicide epoxiconazole [(rel-1-[[(2R,3S)-3-(2-chlorophenyl)-2-(4-fluorophenyl)oxiranyl]methyl]-1H-1,2,4-triazole]) in or on the following commodities:

Commodity Parts per million
Banana * 0.5
Coffee * 0.05
* No U.S. Registration as of August 4, 2006

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional Registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 53989, Sept. 13, 2006]

§ 180.620 Etofenprox; tolerances for residues.

(a) General. A tolerance is established for residues of the insecticide etofenprox, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only etofenprox, 2-(4-ethoxyphenyl)-2-methylpropyl 3-phenoxybenzyl ether, in or on the commodity.

Commodity Parts per
million
Cattle, fat 10.0
Cattle, meat 0.40
Cattle, meat byproducts 10.0
Egg 0.40
All food commodities (including feed commodities) not otherwise listed in this subsection 5.0
Goat, fat 10.0
Goat, meat 0.40
Goat, meat byproducts 10.0
Hog, fat 4.0
Hog, meat 0.20
Hog, meat byproducts 4.0
Horse, fat 10.0
Horse, meat 0.40
Horse, meat byproducts 10.0
Milk 0.60
Poultry, fat 1.0
Poultry, meat 0.01
Poultry, meat byproducts 1.0
Rice, grain 0.01
Sheep, fat 10.0
Sheep, meat 0.40
Sheep, meat byproducts 10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23498, Apr. 27, 2011, as amended at 78 FR 70877, Nov. 27, 2013]

§ 180.621 Dithianon; tolerances for residues.

(a) General. Tolerances are established for residues of dithianon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only dithianon, 5, 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4-dithiin-2,3-dicarbonitrile.

Commodity Parts per
million
Fruit, pome, group 111 5
Grape 2 3
Hop, dried cones1 100
1 No U.S. registration as of September 5, 2006.
2 No U.S. registration as of January 29, 2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 5522, Feb. 3, 2010]

§ 180.622 Ethaboxam; tolerances for residues.

(a) General. Tolerances are established for residues of ethaboxam, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only ethaboxam (N-(cyano-2-thienylmethyl)-4-ethyl-2-(ethylamino)-5-thiazolecarboxamide) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Beet, sugar, roots 0.03
Brassica, leafy greens, subgroup 4-16B 7
Ginseng 0.10
Grape 1 6.0
Leaf petiole vegetable subgroup 22B 0.15
Pepper/eggplant subgroup 8-10B 0.90
Vegetable, Brassica, head and stem, group 5-16 3
Vegetable, cucurbit, group 9 0.30
Vegetable, tuberous and corm, subgroup 1C 0.01
1 There is no U.S. registration as of September 27, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 56392, Sept. 27, 2006, as amended at 82 FR 36090, Aug. 3, 2017; 86 FR 8713, Feb. 9, 2021; 87 FR 2728, Jan. 19, 2022; 89 FR 68117, Aug. 23, 2024]

§ 180.623 Flufenoxuron; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide, flufenoxuron, 1-[4-(2-chloro-α,α,α-trifluoro-p-tolyloxy)-2-fluorophenyl]-3-(2,6-difluorobenzoyl)urea, in or on the following food commodities.

Commodity Parts per million
Apple 1 0.50
Cattle, fat 1 4.5
Cattle, meat 1 0.10
Cattle, meat byproducts 1 0.50
Goat, fat 1 4.5
Goat, meat 1 0.10
Goat, meat byproducts 1 0.50
Grape 1 0.70
Grape, raisin 1 2.0
Horse, fat 1 4.5
Horse, meat 1 0.10
Horse, meat byproducts 1 0.50
Milk 0.20
Milk, fat 1 4.0
Orange 1 0.30
Orange, oil 1 60
Pear 1 0.50
Sheep, fat 1 4.5
Sheep, meat 1 0.10
Sheep, meat byproducts 1 0.50
1 There are no U.S. registrations as of September 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 57436, Sept. 29, 2006]

§ 180.624 Metrafenone; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide metrafenone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following table is to be determined by measuring only metrafenone (3-bromo-6-methoxy-2-methylphenyl)(2,3,4-trimethoxy-6-methylphenyl)methanone in or on the following commodities:

Commodity Parts per million
Apricot 0.70
Cherry subgroup 12-12A 2.0
Fruit, pome, group 11-10 1.5
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 4.5
Grape, raisin 17
Hop, dried cones 70
Peach subgroup 12-12B 0.70
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, group 8-10 0.90
White button mushroom 0.50

(b) Section 18 emergency exemption. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54917, Sept. 20, 2006, as amended at 75 FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, 2014; 84 FR 12520, Apr. 2, 2019]

§ 180.625 Orthosulfamuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide orthosulfamuron, including its metabolites and degradates, in or on the commodities in the table, below. Compliance with the tolerance levels specified in the following table is to be determined by measuring only orthosulfamuron, 1-(4,6-dimethoxypyrimidin-2-yl)-3-{[2-(dimethylcarbamoyl)phenyl]sulfamoyl}urea, in or on the following commodities:

Table to Paragraph (a)

Commodity Parts per million
Almond, hulls 0.03
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.01
Nut, tree, group 14-12 0.01
Rice, grain 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[72 FR 8931, Feb. 28, 2007, as amended at 80 FR 72599, Nov. 20, 2015; 86 FR 9872, Feb. 17, 2021]

§ 180.626 Prothioconazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only prothioconazole and its metabolite prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]-1H-1,2,4-triazole-1-ethanol, calculated as parent in or on the commodity.

Commodity Parts per
million
Alfalfa, forage 0.02
Alfalfa, hay 0.02
Beet, sugar, roots 0.25
Berry, low growing, except strawberry, subgroup 13-07H 0.20
Bushberry, subgroup 13-07B 2.0
Corn, sweet kernel plus cob with husks removed 0.04
Cotton, gin byproducts 4.0
Cottonseed subgroup 20C 0.4
Grain, aspirated grain fractions 11
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; forage 8.0
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; hay 7.0
Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; stover 10
Grain, cereal, forage, fodder and straw, group 16, except sorghum, straw 5.0
Grain, cereal, group 15, except sweet corn and sorghum 0.35
Pea and bean, dried shelled, except soybean, subgroup 6C 0.9
Peanut 0.02
Potato 0.02
Rapeseed subgroup 20A 0.15
Rice, hulls 0.90
Soybean, forage 4.5
Soybean, hay 17
Soybean, seed 0.15
Sunflower subgroup 20B 1 0.2
Vegetable, cucurbit, crop group 9 0.30
1 There are no U.S. registrations allowing use of prothioconazole on the commodities in the Sunflower subgroup 20B as of August 16, 2017.

(2) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only prothioconazole and its metabolites prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]-1H-1,2,4-triazole-1-ethanol, and conjugates that can be converted to these two compounds by acid hydrolysis, calculated as parent in or on the commodity.

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.02
Cattle, meat byproducts 0.2
Goat, fat 0.1
Goat, meat 0.02
Goat, meat byproducts 0.2
Hog, meat byproducts 0.05
Horse, fat 0.1
Horse, meat 0.02
Horse, meat byproducts 0.2
Milk 0.02
Poultry liver 0.02
Sheep, fat 0.1
Sheep, meat 0.02
Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 11783, Mar. 14, 2007, as amended at 73 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, 2009; 74 FR 46699, Sept. 11, 2009; 75 FR 29914, May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR 67052, Nov. 8, 2013; 81 FR 78923, Nov. 10, 2016; 82 FR 38846, Aug. 16, 2017; 83 FR 52991, Oct. 19, 2018]

§ 180.627 Fluopicolide; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or on the commodity.

Commodity Parts per million
Basil, dried, leaves 200
Basil, fresh leaves 40
Bean, moth, succulent 0.90
Bean, runner, succulent 0.90
Bean, snap, succulent 0.90
Bean, wax, succulent 0.90
Bean, yardlong, succulent 0.90
Brassica, head and stem, subgroup 5A 5.0
Citrus, dried pulp 0.03
Citrus, oil 1.0
Fruit, citrus, crop group 10-10 0.01
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Grape, raisin 6.0
Hop, dried cones 15
Potato, granules/flakes 0.15
Potato, processed potato waste 0.2
Vegetable, brassica (cole) leafy subgroup 5B 18
Vegetable, bulb, crop group 3-07 7.0
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, crop group 8-10 1.6
Vegetable, leafy, except brassica, group 4 25
Vegetable, leaves of root and tuber, group 2 15.0
Vegetable root, subgroup 1A 0.15
Vegetable, tuberous and corm, subgroup 1C 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or on the commodity.

Table 1 to Paragraph (d)

Commodity Parts per
million
Animal feed, nongrass, group 18 0.5
Cotton, gin byproducts 0.2
Grain, aspirated fractions 0.07
Grain, cereal, group 15 0.02
Grain, cereal, group 15, milled byproducts 0.07
Grain, cereal, forage, fodder, and straw, group 16 0.5
Grass, forage, fodder and hay, group 17 0.5
Oilseed group 20 0.03
Peanut 0.03
Peanut, hay 0.7
Soybean, refined oil 0.03
Vegetable, foliage of legume, group 7 0.2
Vegetable, legume, group 6 0.02

[72 FR 14447, Mar. 28, 2007, as amended at 73 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, 2008; 76 FR 22054, Apr. 20, 2011; 79 FR 12401, Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014; 81 FR 65924, Sept. 26, 2016; 83 FR 9712, Mar. 7, 2018; 87 FR 31190, May 23, 2022]

§ 180.628 Chlorantraniliprole; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide chlorantraniliprole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only chlorantraniliprole, 3-bromo-N-[4-chloro-2-methyl-6-[(methylamino)carbonyl]phenyl]-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide.

Commodity Parts per million
Acerola 2.0
Alfalfa, seed 7.0
Almond, hulls 5.0
Animal feed, nongrass, group 18, forage 25
Animal feed, nongrass, group 18, hay 90
Apple, wet pomace 2.5
Artichoke, globe 1 4.0
Artichoke, globe 2.0
Asparagus 13
Atemoya 4.0
Avocado 4.0
Banana 4.0
Beet, sugar, molasses 9.0
Berry, large shrub/tree, subgroup 13-07C 2.5
Berry, low growing, subgroup 13-07G 1.0
Biriba 4.0
Brassica, head and stem, subgroup 5A 4.0
Brassica, leafy greens, subgroup 5B 11
Bushberry, subgroup 13-07B 2.5
Cacao bean 0.08
Cacao bean, chocolate 1.5
Cacao bean, cocoa powder 1.5
Cacao bean, roasted bean 0.8
Cactus 13
Canistel 4.0
Cattle, fat 0.5
Cattle, meat 0.1
Cattle, meat byproducts 0.5
Cherimoya 4.0
Citrus, dried pulp 14
Coffee, green bean 0.4
Coffee, instant 2.0
Corn, field, grain 0.04
Corn, field, milled byproducts 0.1
Corn, pop, grain 0.04
Corn, sweet, kernel plus cobs with husk removed 0.02
Cotton, gin byproduct 30
Cotton, hulls 0.40
Cottonseed subgroup 20C 0.3
Crayfish 8.0
Custard apple 4.0
Egg 1.0
Feijoa 4.0
Fig 4.0
Fruit, caneberry, subgroup 13-07A 1.8
Fruit, citrus, group 10-10 1.4
Fruit, pome, group 11-10 1.2
Fruit, small vine climbing, subgroup 13-07F 2.5
Fruit, stone, group 12-12 2.5
Fruit, stone, group 12-12, except cherry, chickasaw plum, and damson plum 1 4.0
Goat, fat 0.5
Goat, meat 0.1
Goat, meat byproducts 0.5
Grain, aspirated grain fractions 640
Grain, cereal, except rice and corn, group 15 6.0
Grain, cereal, forage, fodder and straw, group 16 40
Grape, raisin 5.0
Grass forage, fodder and hay, group 17 90
Guava 4.0
Herb subgroup 19A, dried leaves 90
Herb subgroup 19A, fresh leaves 25
Hog, fat 0.05
Hog, meat 0.02
Hog, meat byproducts 0.05
Hop, dried cones 1 90
Hop, dried cones 40
Horse, fat 0.5
Horse, meat 0.1
Horse, meat byproducts 0.5
Ilama 4.0
Jaboticaba 2.0
Longan 4.0
Lychee 2.0
Mango 4.0
Milk 0.1
Nut, tree, group 14 1 0.04
Nut, tree, group 14-12 0.02
Olive 4.0
Olive, oil 40
Onion, bulb, subgroup 3-07A 0.30
Onion, green, subgroup 3-07B 3.0
Palm, oil 2 1.5
Papaya 4.0
Passionfruit 4.0
Peanut 0.06
Peanut, hay 90
Peppermint, tops 9.0
Persimmon 4.0
Pineapple 1.5
Pineapple, process residue 3.0
Pistachio 1 0.04
Pomegranate 4.0
Poultry, fat 0.2
Poultry, meat 0.05
Poultry, meat byproducts 0.2
Pulasan 4.0
Quinoa, forage 40
Quinoa, grain 6.0
Quinoa, hay 40
Quinoa, straw 40
Rambutan 4.0
Rapeseed subgroup 20A 2.0
Rice, grain 0.15
Rice, hulls 0.4
Sapodilla 4.0
Sapote, black 4.0
Sapote, mamey 4.0
Sapote, white 4.0
Sheep, fat 0.5
Sheep, meat 0.1
Sheep meat byproducts 0.5
Soursop 4.0
Spanish lime 4.0
Spearmint, tops 9.0
Spice, subgroup 19B 90
Star apple 4.0
Starfruit 4.0
Sugar apple 4.0
Sugarcane, cane 14
Sugarcane, molasses 420
Sunflower subgroup 20B 2.0
Tea, dried 50.0
Teff, forage 40
Teff, grain 6.0
Teff, hay 40
Teff, straw 40
Ti, leaves 13.0
Ti, root 0.3
Vegetable, cucurbit, group 9 0.5
Vegetable, foliage of legume, group 7 90
Vegetable, fruiting, group 8-10 1.4
Vegetable, leafy, except brassica, group 4 13
Vegetable, leaves of root and tuber, group 2 40.0
Vegetable, legume, group 6 2.0
Vegetable, root and tuber, group 1 0.30
Wax jambu 4.0
1 This tolerance expires on December 14, 2016.
2 There are no U.S. registrations for use of chlorantraniliprole on this commodity.

(b) Section 18 emergency exemptions. A time-limited tolerance is established for residues of chlorantraniliprole, including its metabolites and degradates, in or on the specified agricultural commodity in the table below. Compliance with the tolerance level specified in the following table is to be determined by measuring only chlorantraniliprole, 3-bromo-N-[4-chloro-2-methyl-6[(methylamino) carbonyl]phenyl]-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide, in or on the specified agricultural commodity, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemption. The tolerance expires on the date specified in the table.

Table 2 to Paragraph (b)

Commodity Parts per
million
Expiration
date
Rice, grain 15 12/31/2028

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 5532, Feb. 3, 2010, as amended at 75 FR 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; 76 FR 59909, Sept. 28, 2011; 77 FR 60315, Oct. 3, 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014; 81 FR 38604, June 14, 2016; 81 FR 61619, Sept. 7, 2016; 84 FR 53326, Oct. 7, 2019; 90 FR 51123, Nov. 17, 2025]

§ 180.629 Flutriafol; tolerances for residues.

(a) General. Tolerances are established for the residues of flutriafol, [(±)-α-(2-fluorophenyl)-α-(4-fluorophenyl)-1H-1,2,4-triazole-1-ethanol], including its metabolites and degradates in or on the following commodities. Compliance with the following tolerances is to be determined by measuring flutriafol only.

Commodity Parts per million
African tree nut 0.02
Alfalfa, forage 20
Alfalfa, hay 70
Almond 0.60
Almond, hull 15
Banana 1 0.30
Barley, grain 1.5
Barley, hay 7
Barley, straw 8
Beet sugar 0.08
Brassica, head and stem (subgroup 5A) 1.5
Brassica, leafy greens (subgroup 5B) 7.0
Brazil nut 0.02
Bur oak 0.02
Butternut 0.02
Cajou 0.02
Cashew 0.02
Castanha-do-maranhao 0.02
Cattle, fat 0.2
Cattle, liver 1.5
Cattle, meat byproducts, except liver 0.08
Cattle, muscle 0.05
Coconut 0.02
Coffee, green, bean 1 0.15
Coffee, instant 1 0.30
Coquito nut 0.02
Corn, field, forage 5.0
Corn, field, grain 0.01
Corn, field, refined oil 0.02
Corn, field, stover 15
Corn, pop 0.01
Corn, pop, stover 15
Corn, sweet, forage 9
Corn, sweet, kernel plus cob with husk removed 0.03
Corn, sweet, stover 8
Cotton, gin byproducts 6.0
Cotton, undelinted seed 0.50
Dika nut 0.02
Egg 0.02
Fruit, pome, group 11-09 0.40
Fruit, stone, group 12-10 1.5
Goat, fat 0.2
Goat, liver 1.5
Goat, meat byproducts, except liver 0.08
Goat, muscle 0.05
Grain, aspirated fractions 6.0
Grape 1.5
Grape, raisin 2.4
Guiana chestnut 0.02
Hazelnut 0.02
Heartnut 0.02
Hickory nut 0.02
Hog, fat 0.01
Hog, meat byproducts 0.05
Hog, muscle 0.01
Hop, dried cones 20
Horse, fat 0.2
Horse, liver 1.5
Horse, meat byproducts, except liver 0.08
Horse, muscle 0.05
Japanese horse-chestnut 0.02
Lettuce, head 1.5
Macadamia nut 0.02
Milk 0.02
Mongongo nut 0.02
Monkey-pot 0.02
Pachira nut 0.02
Peanut 0.09
Peanut, hay 15
Pecan 0.02
Poultry, fat 0.02
Poultry, meat byproducts 0.02
Radicchio 1.5
Sapucaia nut 0.02
Sheep, fat 0.2
Sheep, liver 1.5
Sheep, meat byproducts, except liver 0.08
Sheep, muscle 0.05
Sorghum, grain, forage 2.0
Sorghum, grain, grain 1.5
Sorghum, grain, stover 6.0
Soybean, seed 0.35
Strawberry 1.5
Tomato, paste 1.5
Vegetable, cucurbit, group 9 0.30
Vegetable, fruiting, group 8-10 1.0
Vegetable, leafy, except Brassica, crop group 4, except head lettuce and radicchio 10
Walnut, black 0.02
Walnut, English 0.02
Wheat, bran 0.30
Wheat, forage 30
Wheat, germ 0.25
Wheat, grain 0.15
Wheat, hay 15
Wheat, straw 9.0
1 There are no U.S. registrations as of October 22, 2013.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide flutriafol, including its metabolites and degradates, in or on the commodities in the table 2 to this paragraph (d) when present therein as a result of the application of flutriafol to the growing crops listed in the table to paragraph (a) of this section. Compliance with the following tolerance levels specified in table 2 to this paragraph (d) is to be determined by measuring only flutriafol ((±)-α-(2-fluorophenyl)-α-(4-fluorophenyl)-1H-1,2,4-triazole-1-ethanol) in or on the following commodities:

Table 2 to Paragraph (d)

Commodity Parts per
million
Rice, grain 0.5

[75 FR 26673, May 12, 2010, as amended at 76 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, 2012; 77 FR 48901, Aug. 15, 2012; 78 FR 75262, Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR 5951, Feb. 4, 2015; 80 FR 71952, Nov. 18, 2015; 85 FR 8467, Feb. 14, 2020]

§ 180.631 Pyrasulfotole; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pyrasulfotole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyrasulfotole ((5-hydroxy-1,3-dimethyl-1H-pyrazol-4-yl)[2-(methylsulfonyl)-4-(trifluoromethyl)phenyl]methanone) and its desmethyl metabolite (5-hydroxy-3-methyl-1H-pyrazol-4-yl)[2-(methylsulfonyl)-4-(trifluoromethyl)phenyl]methanone), calculated as the stoichiometric equivalent of pyrasulfotole, in or on the commodities:

Commodity Parts per million
Aspirated grain fractions 0.40
Barley, grain 0.02
Barley, hay 0.30
Barley, straw 0.20
Cattle, fat 0.03
Cattle, liver 3.0
Cattle, meat 0.02
Cattle, meat byproducts, except liver 0.70
Eggs 0.02
Goat, fat 0.03
Goat, liver 3.0
Goat, meat 0.02
Goat, meat byproducts, except liver 0.70
Grass, forage 25
Grass, hay 3.5
Hog, fat 0.02
Hog, liver 0.30
Hog, meat 0.02
Hog, meat byproducts, except liver 0.05
Horse, fat 0.03
Horse, liver 3.0
Horse, meat 0.02
Horse, meat byproducts, except liver 0.70
Milk 0.03
Oat, forage 0.10
Oat, grain 0.08
Oat, hay 0.50
Oat, straw 0.20
Poultry, fat 0.02
Poultry, meat 0.02
Poultry, meat byproducts 0.20
Rye, forage 0.20
Rye, grain 0.02
Rye, straw 0.20
Sheep, fat 0.03
Sheep, liver 3.0
Sheep, meat 0.02
Sheep, meat byproducts, except liver 0.70
Sorghum, grain, forage 1.5
Sorghum, grain, grain 0.70
Sorghum, grain, stover 0.80
Wheat, forage 0.20
Wheat, grain 0.02
Wheat, hay 0.80
Wheat, straw 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 45649, Aug. 15, 2007, as amended at 76 FR 23898, Apr. 29, 2011]

§ 180.632 Fenazaquin; Tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide fenazaquin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fenazaquin, or 4-[2-[4-(1,1-dimethylethyl)phenyl]-ethoxy]quinazoline.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 4
Avocado 0.15
Berry, low growing, subgroup 13-07G 2
Bushberry, subgroup 13-07B 0.8
Caneberry, subgroup 13-07A 0.7
Fruit, citrus, group 10-10 0.4
Fruit, citrus, group 10-10, oil 20
Fruit, pome, group 11-10 0.6
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.7
Fruit, stone, group 12-12 2
Grape, raisin 0.8
Hop, dried cones 30
Nuts, Tree, Group 14-12 0.02
Pea and bean, dried shelled, except soybean, subgroup 6C 0.3
Pea and bean, succulent shelled, subgroup 6B 0.03
Peppermint, fresh leaves 10
Pineapple 1 0.2
Spearmint, fresh leaves 10
Tea, dried 1 10
Tea, instant 1 10
Vegetable, cucurbit, group 9 0.3
Vegetable, fruiting, group 8-10 0.3
Vegetable, legume, edible podded, subgroup 6A 0.4
1 There are no U.S. registrations.

(b) Section is emergency exempotions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 44393, Aug. 8, 2007, as amended at 80 FR 25958, May 6, 2015; 82 FR 24071, May 25, 2017; 84 FR 14622, Apr. 11, 2019; 91 FR 8090, Feb. 20, 2026]

§ 180.633 Florasulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide florasulam, including its metabolites and degradates, in or on the commodities below. Compliance with the tolerance levels specified below is to be determined by measuring only florasulam, N-(2, 6-difluorophenyl)-8-fluoro-5-methoxy (1, 2, 4) triazole (1, 5-c)pyrimidine-2-sulfonamide, in or on the commodities.

Commodity Parts per million
Barley, grain 0.01
Barley, hay 0.05
Barley, straw 0.05
Oat, forage 0.05
Oat, grain 0.01
Oat, hay 0.05
Oat, straw 0.05
Rye, forage 0.05
Rye, grain 0.01
Rye, straw 0.05
Teff, forage 0.05
Teff, grain 0.01
Teff, hay 0.05
Teff, straw 0.05
Wheat, forage 0.05
Wheat, grain 0.01
Wheat, hay 0.05
Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of the herbicide florasulam, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (c). Compliance with the tolerance levels specified in table 2 is to be determined by measuring only florasulam, N-(2, 6-difluorophenyl)-8-fluoro-5-methoxy (1, 2, 4) triazole (1, 5-c)pyrimidine-2-sulfonamide, in or on the commodities:

Table 2 to Paragraph (c)

Commodity Parts per million
Grass, forage, fodder and hay, group 17 0.02

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 55077, Sept. 28, 2007, as amended at 83 FR 35147, July 25, 2018; 86 FR 43967, Aug. 11, 2021]

§ 180.634 Tembotrione; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and degradates, in or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]-1,3-cyclohexanedione and its metabolite, 2-[2-chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy) methyl]benzoyl]-4,6-dihydroxy-1,3-cyclohexanedione, calculated as the stoichiometric equivalent of tembotrione, in or on the following commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Cattle, liver 0.4
Cattle, meat byproducts, except liver 0.07
Corn, field, forage 0.6
Corn, field, grain 0.02
Corn, field, stover 0.45
Corn, pop, grain 0.02
Corn, pop, stover 0.35
Corn, sweet, forage 0.35
Corn, sweet, stover 0.6
Goat, liver 0.4
Goat, meat byproducts, except liver 0.07
Horse, liver 0.4
Horse, meat byproducts, except liver 0.07
Poultry, liver 0.07
Sheep, liver 0.4
Sheep, meat byproducts, except liver 0.07

(2) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and degradates, in or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]-1,3-cyclohexanedione in or on the following commodities.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Corn, sweet, kernel plus cob with husks removed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 55085, Sept. 28, 2007, as amended at 74 FR 47894, Sept. 18, 2009; 91 FR 8090, Feb. 20, 2026]

§ 180.635 Spinetoram; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide spinetoram, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of XDE-175-J: 1-H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione,2-[(6deoxy-3-O-ethyl-2,4-di-O-methyl-α-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,4,5,5a,5b,6,9,10,11,12,13,14,16a,16b-hexadecahydro-14-methyl-,(2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR); XDE-175-L: 1H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione,2-[(6deoxy-3-O-ethyl-2,4-di-O-methyl-α-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-4,14-dimethyl-,(2S,3aR,5aS,5bS,9S,13S,14R,16aS,16bS); ND-J: (2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR)-9-ethyl-14-methyl-13[[(2S,5S,6R)-6-methyl-5-(methylamino)tetrahydro-2H-pyran-2-yl]oxy]-7,15-dioxo2,3,3a,4,5,5a,5b,6,7,9,10,11,12,13,14,15,16a,16b-octadecahydro-1H-as-indaceno[3,2d]oxacyclododecin-2-yl-6-deoxy-3-O-ethyl-2,4-di-O-methyl-α-L-mannopyranoside; and NF-J: (2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S,13S,14R,16aS,16bR)-2-[(6-deoxy-3-O-ethyl-2,4-di-O-methyl-α-L-mannopyranosyl)oxy]-9-ethyl-14-methyl-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9,10,11,12,13,14,15,16a,16b-octadecahydro-1H-as-indaceno[3,2d]oxacyclododecin-13-yl]oxy)-2-methyltetrahydro-2H-pyran-3-yl(methyl)formamide, calculated as the stoichiometric equivalent of spinetoram.

Table 1 to Paragraph (a)

Commodity Parts per million
Acerola 0.30
Almond, hulls 19
Amaranth grain, grain 1.0
Animal feed, nongrass, group 18, forage 35
Animal feed, nongrass, group 18, hay 30
Apple, wet pomace 0.50
Artichoke, globe 0.30
Atemoya 0.30
Avocado 0.30
Banana 0.25
Beet, sugar, molasses 0.75
Berry, low growing, except strawberry, subgroup 13-07H 0.04
Berry, low growing, subgroup 13-07G, except cranberry 0.90
Biriba 0.30
Bushberry subgroup 13-07B 0.50
Caneberry subgroup 13-07A 0.80
Canistel 0.30
Cattle, fat 5.5
Cattle, liver 0.85
Cattle, meat 0.20
Cattle, meat byproducts (except liver) 0.60
Celtuce 8
Cherimoya 0.30
Citrus, dried pulp 0.50
Citrus, oil 3.0
Coffee, green bean 0.04
Corn, sweet, kernel plus cob with husks removed 0.04
Cotton, gin byproducts 1.5
Cottonseed subgroup 20C 0.04
Custard apple 0.30
Date 0.10
Dragon fruit 1.5
Egg 0.04
Feijoa 0.30
Fennel, Florence, fresh leaves and stalk 8
Fig 0.10
Fish, freshwater, finfish 4
Fish, shellfish, crustacean 4
Fish, shellfish, mollusk 4
Fruit, citrus, group 10-10 0.30
Fruit, pome, group 11-10 0.20
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 0.50
Fruit, stone 12-12 0.30
Goat, fat 5.5
Goat, liver 0.85
Goat, meat 0.20
Goat, meat byproducts (except liver) 0.60
Grain, aspirated fractions 20
Grain, cereal, group 15, except rice, sorghum, pearl millet and proso millet 0.04
Grain, cereal, group 16, forage 3.5
Grain, cereal, group 16, hay 10
Grain, cereal, group 16, stover 10
Grain, cereal, straw, group 16, except rice 1.0
Grape, raisin 0.70
Grass, forage, fodder and hay, group 17, forage 10
Grass, forage, fodder and hay, group 17, hay 5
Guava 0.30
Herb, dried, subgroup 19A 22
Herb, fresh, subgroup 19A 3.0
Hog, fat 0.40
Hog, meat 0.04
Hog, meat byproducts 0.04
Hop, dried cones 22
Horse, fat 5.5
Horse, liver 0.85
Horse, meat 0.20
Horse, meat byproducts (except liver) 0.60
Ilama 0.30
Jaboticaba 0.30
Kohlrabi 2
Leaf petiole vegetable subgroup 22B 8
Longan 0.30
Lychee 0.30
Mango 0.30
Milk 0.30
Milk, fat 7.5
Millet, pearl, grain 1.0
Millet, proso, grain 1.0
Nut, tree, group 14-12 0.10
Onion, bulb, subgroup 3-07A 0.10
Onion, green, subgroup 3-07B 2.0
Papaya 0.30
Passionfruit 0.30
Pea and bean, dried shelled, except soybean, subgroup 6C 0.04
Pea and bean, succulent shelled, subgroup 6B 0.04
Peanut 0.04
Peanut, hay 11
Peppermint, tops 3.5
Pineapple 0.04
Pineapple, processed residue 0.15
Pomegranate 0.30
Poultry, fat 0.10
Poultry, meat 0.04
Poultry, meat byproducts 0.04
Pulasan 0.30
Quinoa, grain 0.04
Rambutan 0.30
Sapodilla 0.30
Sapote, black 0.30
Sapote, mamey 0.30
Sapote, white 0.30
Sheep, fat 5.5
Sheep, liver 0.85
Sheep, meat 0.20
Sheep, meat products (except liver) 0.60
Sorghum, grain, grain 1.0
Soursop 0.30
Soybean, seed 0.04
Spanish lime 0.30
Spearmint, tops 3.5
Spice group 26 1.7
Stalk and stem vegetable subgroup 22A 0.4
Star apple 0.30
Star fruit 0.30
Sugar apple 0.30
Tea, dried 1 70
Tea, instant 1 70
Ti, leaves 10
Vegetable, Brassica, head and stem, group 5-16 2
Vegetable, cucurbit, group 9 0.30
Vegetable, foliage of legume, group 7 8.0
Vegetable, fruiting, group 8-10 0.40
Vegetable, leafy, group 4-16 10
Vegetable, leaves of root and tuber, group 2 10
Vegetable, legume, edible podded, subgroup 6A 0.30
Vegetable, root and tuber, group 1 0.10
Watercress 8.0
Wax jambu 0.30
1 There are no U.S. registrations as of August 8, 2018 for use on tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect and invertent residues. [Reserved]

[72 FR 57499, Oct. 10, 2007, as amended at 73 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, 2009; 80 FR 80282, Dec. 24, 2015; 83 FR 38981, Aug. 8, 2018; 86 FR 17910, Apr. 7, 2021; 86 FR 52083, Sept. 20, 2021; 86 FR 72193, Dec. 21, 2021; 88 FR 60597, Sept. 5, 2023]

§ 180.636 1,3-dichloropropene; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide cis- and trans-1,3-dichloropropene and its metabolites cis- and trans-3-chloroacrylic acid, and cis- and trans-3-chloroallyl alcohol in or on the following commodities.

Commodity Parts per million
Grape 0.018

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 8218, Feb. 13, 2008]

§ 180.637 Mandipropamid; tolerances for residues.

(a) General. Tolerances are established for residues of mandipropamid, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only mandipropamid (4-chloro-N-[2-[3-methoxy-4-(2-propynyloxy)phenyl]ethyl]-α-(2-propynyloxy)benzeneacetamide) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Asparagus bean, edible podded 0.90
Basil, dried leaves 200
Basil, fresh leaves 30
Bean (Phaseolus spp.), edible podded 0.90
Bean (Vigna spp.), edible podded 0.90
Cacao, dried bean 1 0.06
Catjang bean, edible podded 0.90
Celtuce 20
Chinese longbean, edible podded 0.90
Citrus, dried pulp 0.70
Citrus, oil 15
Cowpea, edible podded 0.90
Fennel, Florence, fresh leaves and stalk 20
French bean, edible podded 0.90
Fruit, citrus, group 10-10 0.50
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.4
Garden bean, edible podded 0.90
Ginseng 0.30
Goa bean, edible podded 0.90
Grape, raisin 3.0
Green bean, edible podded 0.90
Guar bean, edible podded 0.90
Hop, dried cones 50
Jackbean, edible podded 0.90
Kidney bean, edible podded 0.90
Kohlrabi 3.0
Lablab bean, edible podded 0.90
Leaf petiole vegetable subgroup 22B 20
Moth bean, edible podded 0.90
Mung bean, edible podded 0.90
Navy bean, edible podded 0.90
Onion, bulb, subgroup 3-07A 0.05
Onion, green, subgroup 3-07B 4.0
Papaya 2 0.9
Potato, wet peel 0.15
Rice bean, edible podded 0.90
Scarlet runner bean, edible podded 0.90
Snap bean, edible podded 0.90
Sword bean, edible podded 0.90
Urd bean, edible podded 0.90
Vegetable, Brassica, head and stem, group 5-16 3.0
Vegetable, cucurbit, group 9 0.6
Vegetable, fruiting, group 8-10 1.0
Vegetable, leafy, group 4-16 25
Vegetable soybean, edible podded 0.90
Vegetable, tuberous and corm, subgroup 1C 0.09
Velvet bean, edible podded 0.90
Wax bean, edible podded 0.90
Winged pea, edible podded 0.90
Yardlong bean, edible podded 0.90
1 There are no U.S. registrations allowing use of mandipropamid on cacao as of October 28, 2019.
2 There is no U.S. registration for use of this pesticide on papaya as of August 15, 2025.

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent tolerances. [Reserved]

[73 FR 2816, Jan. 16, 2008, as amended at 74 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, 2011; 77 FR 74119, Dec. 13, 2012; 78 FR 76992, Dec. 20, 2013; 81 FR 17088, Mar. 28, 2016; 84 FR 10700, Mar. 22, 2019; 84 FR 57621, Oct. 28, 2019; 90 FR 39339, Aug. 15, 2025; 91 FR 9728, Feb. 27, 2026]

§ 180.638 Pyroxsulam; tolerances for residues.

(a) General. Tolerances are established for residues of pyroxsulam, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only pyroxsulam, N-(5,7-dimethoxy[l, 2,4]triazolo[l, 5-a]pyrimidin-2-yl)-2-methoxy-4-(trifluoromethyl)-3-pyridinesulfonamide, in or on the commodity.

Commodity Parts per million
Teff, forage 0.06
Teff, grain 0.01
Teff, hay 0.01
Teff, straw 0.03
Wheat, forage 0.06
Wheat, grain 0.01
Wheat, hay 0.01
Wheat, straw 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 10402, Feb. 27, 2008, as amended at 82 FR 30990, July 5, 2017; 83 FR 31895, July 10, 2018]

§ 180.639 Flubendiamide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only flubendiamide N2-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4- [1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million
Almond, hulls 9.0
Apple, wet pomace 5.0
Corn, field, forage 8.0
Corn, field, grain 0.03
Corn, field, stover 15
Corn, pop, grain 0.02
Corn, pop, stover 15
Corn, sweet, forage 9.0
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 25
Cotton gin byproducts 60
Cotton, undelinted seed 0.90
Fruit, pome, group 11 1.5
Fruit, stone, group 12 1.6
Grape 1.4
Nut, tree, group 14 0.06
Okra 0.30
Tea 1 50
Vegetable, cucurbit, group 9 0.20
Vegetable, fruiting, group 8 0.60
Vegetable, leafy, except Brassica, group 4 11
1 There are no U.S. registrations as of July 5, 2017, for use of flubendiamide on tea.

(2) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only flubendiamide N2-[1,1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million
Alfalfa, forage 25
Alfalfa, hay 65
Artichoke, globe 1.6
Berry, low growing, subgroup 13-07G, except cranberry 1.5
Brassica, head and stem, subgroup 5A 3.0
Brassica, leafy greens, subgroup 5B 25
Cattle, fat 0.70
Cattle, meat 0.08
Cattle, meat byproducts 0.60
Egg 0.40
Fruit, small fruit vine climbing except fuzzy kiwifruit, subgroup 13-07F 1.4
Goat, fat 0.70
Goat, meat 0.08
Goat, meat byproducts 0.60
Grain, aspirated grain fractions 153
Hog, fat 0.15
Hog, meat 0.03
Hog, meat byproducts 0.15
Horse, fat 0.70
Horse, meat 0.08
Horse, meat byproducts 0.60
Milk 0.15
Milk, fat 1.0
Pea and bean, dried shelled, except soybean, subgroup 6C 0.60
Pea and bean, succulent shelled, subgroup 6B 0.05
Peanut, hay 60
Peanut, meal 0.03
Peanut, nutmeat 0.02
Peanut, refined oil 0.03
Pistachio 0.06
Poultry, fat 3.0
Poultry, liver 0.60
Poultry, meat 0.10
Rice, grain 1 0.50
Safflower, seed 5.0
Sheep, fat 0.70
Sheep, meat 0.08
Sheep, meat byproducts 0.60
Sorghum, grain, forage 12
Sorghum, grain, grain 5.0
Sorghum, grain, stover 14
Soybean, forage 18
Soybean, hay 60
Soybean, hulls 0.80
Soybean, seed 0.25
Sugarcane, cane 0.30
Sunflower, seed 5.0
Turnip, greens 25
Vegetable, foliage of legume, except soybean, subgroup 7A 35
Vegetable, legume, edible podded, subgroup 6A 0.50
1 There are no U.S. registrations for rice, grain.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only flubendiamide N2-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4- [1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1, 2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million
Barley, hay 0.04
Barley, straw 0.07
Buckwheat 0.07
Clover, forage 0.15
Clover, hay 0.04
Grass, forage 0.15
Grass, hay 0.04
Millet, pearl, forage 0.15
Millet, pearl, hay 0.04
Millet, proso, forage 0.15
Millet, proso, hay 0.04
Millet, proso, straw 0.07
Oats, forage 0.15
Oats, hay 0.04
Oats, straw 0.07
Rye, forage 0.15
Rye, straw 0.07
Teosinte, forage 0.15
Teosinte, hay 0.04
Teosinte, straw 0.07
Triticale, forage 0.15
Triticale, hay 0.04
Triticale, straw 0.07
Wheat, forage 0.15
Wheat, hay 0.03
Wheat, straw 0.03

[76 FR 16307, Mar. 23, 2011, as amended at 76 FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, 2012; 82 FR 30982, July 5, 2017]

§ 180.640 Pyridalyl; tolerances for residues.

(a) General. Tolerances are established for residues of pyridalyl, pyridine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2-propenyl)oxy]phenoxy]propoxy]-5-(trifluoromethyl, in or on the following raw agricultural commodities:)

Commodity Parts per million
Brassica, head and stem, subgroup 5A 3.5
Mustard greens 30
Turnip greens 30
Vegetable, fruiting, group 8 1.0
Vegetables, leafy, except Brassica, group 4 20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 25533, May 7, 2008]

§ 180.641 Spirotetramat; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide spirotetramat, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl-ethyl carbonate) and its metabolites cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl beta-D-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]decan-2-one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following commodities.

Commodity Parts per million
Acerola 2.5
Almond, hulls 9.0
Artichoke, globe 1.5
Asparagus 1 0.10
Aspirated grain fractions 10.0
Avocado 0.60
Beet, sugar, molasses 0.30
Beet, sugar, roots 0.15
Berry, low growing, except strawberry, subgroup 13-07H 0.30
Black sapote 0.60
Brassica, head and stem, subgroup 5A 2.5
Brassica, leafy, subgroup 5B 8.0
Bushberry subgroup 13-07B 3.0
Canistel 0.60
Carrot, roots 0.15
Citrus, oil 6.0
Coffee, green bean 0.20
Coffee, instant 0.50
Corn, sweet, kernel plus cob with husks removed 1.5
Cotton gin byproducts1 10.0
Cotton, undelinted seed1 0.30
Feijoa 2.5
Fruit, citrus, group 10-10 0.60
Fruit, pome, group 11-10 0.70
Fruit, stone, group 12-12 4.5
Grape, raisin 3.0
Guava 2.5
Hop, dried cones 10.0
Jaboticaba 2.5
Longan 13.0
Lychee 13.0
Mamey sapote 0.60
Mango 0.60
Nut, tree, group 14-12 0.25
Papaya 0.40
Passionfruit 2.5
Persimmon 2.5
Pineapple 0.30
Pistachio 0.25
Pomegranate 0.50
Potato, flakes 1.6
Pulasan 13.0
Rambutan 13.0
Sapodilla 0.60
Small fruit vine climbing subgroup, except fuzzy kiwifruit, subgroup 13-07F 1.3
Soybean forage 8.0
Soybean hay 16.0
Soybean seed 5.0
Spanish lime 13
Star apple 0.60
Starfruit 2.5
Strawberry1 0.40
Taro, leaves 9.0
Vegetable, bulb, group 3-07 0.80
Vegetable, cucurbit, group 9 0.30
Vegetable, foliage of legume, except soybean, subgroup 07A 7.0
Vegetable, fruiting, group 8-10 2.5
Vegetable, leafy, except brassica, group 4 9.0
Vegetable, legume, group 06, except soybean 2.5
Vegetable, tuberous and corm, subgroup 1C 0.60
Watercress 2.0
Wax jambu 2.5
White sapote 0.60
1 There are no U.S. registrations for these commodities.

(2) Tolerances are also established for residues of the insecticide spirotetramat, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl-ethyl carbonate]) and its metabolite cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following commodities:

Commodity Parts per million
Cattle, fat 0.02
Cattle, meat 0.02
Cattle, meat byproducts 0.20
Eggs 0.02
Goat, fat 0.02
Goat, meat 0.02
Goat, meat byproducts 0.20
Hog, meat byproducts 0.02
Horse, fat 0.02
Horse, meat 0.02
Horse, meat byproducts 0.20
Milk 0.01
Poultry, meat byproducts 0.02
Sheep, fat 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the insecticide spirotetramat, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl-ethyl carbonate) and its metabolites cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl beta-D-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]decan-2-one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following commodities.

Commodity Parts per million
Banana 4.0

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 39256, July 9, 2008, as amended at 76 FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, 2012; 77 FR 75859, Dec. 26, 2012; 78 FR 28512, May 15, 2013; 78 FR 66651, Nov. 6, 2013; 81 FR 73347, Oct. 25, 2016; 82 FR 27149, June 14, 2017]

§ 180.643 Uniconazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/plant growth regulator uniconazole-P, (E)-(S)-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, its R-enantiomer and its Z-isomer in or on the following raw agricultural commodities:

Commodity Parts per million
Vegetable, fruiting, group 8 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 51736, Sept. 5, 2008]

§ 180.644 Cyprosulfamide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide safener cyprosulfamide, N-[[4-[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, in or on the following raw agricultural commodities:

Commodity Parts per million
Corn, field, forage 0.20
Corn, field, grain 0.01
Corn, field, stover 0.20
Corn, pop, grain 0.01
Corn, pop, stover 0.20
Corn, sweet, forage 0.40
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.35

(2) Tolerances are established for residues of the herbicide safener cyprosulfamide, N-[[4-[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)-N-cyclopropylbenzamide, calculated as cyprosulfamide, in or on the following raw agricultural commodities:

Commodity Parts per million
Cattle, meat byproducts 0.02
Goat, meat byproducts 0.02
Horse, meat byproducts 0.02
Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 60974, Oct. 15, 2008]

§ 180.645 Thiencarbazone-methyl; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of the thiencarbazone-methyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only only thiencarbazone-methyl [methyl 4-[[[(4,5-dihydro-3-methoxy-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3-thiophenecarboxylate] in or on the following food and feed commodities.

Commodity Parts per million
Corn, field, forage 0.04
Corn, field, grain 0.01
Corn, field, stover 0.02
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.05
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.05
Wheat, forage 0.15
Wheat, grain 0.01
Wheat, hay 0.01
Wheat, straw 0.01

(2) Tolerances are established for residues of thiencarbazone-methyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiencarbazone-methyl [methyl 4-[[[(4,5-dihydro-3-methoxy-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3-thiophenecarboxylate] and its metabolite BYH 18636-MMT [5-methoxy-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one], calculated as the stoichiometric equivalent of thiencarbazone-methyl, in or on the following food commodities of animal origin:

Commodity Parts per million
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Goat, meat 0.02
Goat, meat byproducts 0.02
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of thiencarbazone-methyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiencarbazone-methyl [methyl 4-[[[(4,5-dihydro-3-methoxy-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3-thiophenecarboxylate] and its metabolite BYH 18636-MMT-glucoside [2-hexopyranosyl-5-methoxy-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one], calculated as the stoichiometric equivalent of thiencarbazone-methyl, in or on the following food commodities:

Commodity Parts per million
Soybean, forage 0.04
Soybean, hay 0.15

[73 FR 60968, Oct. 15, 2008, as amended at 83 FR 29033, June 25, 2018]

§ 180.646 Ipconazole; tolerances for residues.

(a) General. Tolerances are established for residues of ipconazole, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only ipconazole (2-[(4-chlorophenyl)methyl]-5-(1-methylethyl)-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol) in or on the commodity.

Commodity Parts per million
Cotton, gin byproducts 0.01
Cotton, undelinted seed 0.01
Grain, cereal, forage, fodder and straw, group 16, except rice 0.01
Grain, cereal group 15, except rice 0.01
Peanut 0.01
Soybean, forage 0.01
Vegetable, legume, group 6 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 69559, Nov. 19, 2008, as amended at 79 FR 15240, Mar. 19, 2014]

§ 180.647 d-Phenothrin; tolerances for residues.

(a) General. A tolerance of 0.01 parts per million is established for residues of the insecticide d-phenothrin in or on all food/feed crops following wide-area mosquito adulticide applications. Compliance with the tolerance levels specified is to be determined by measuring only d-phenothrin in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 32443, July 8, 2009, as amended at 91 FR 8119, Feb. 20, 2026]

§ 180.648 Meptyldinocap; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide meptyldinocap, 2-(1-methylheptyl)-4,6-dinitrophenyl (2E)-2-butenoate and 2,4-DNOP, 2,4-dinitro-6-(1-methylheptyl)phenol expressed as meptyldinocap in or on the following commodities:

Commodity Parts Per Million
Grape 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 48396, Sept. 23, 2009]

§ 180.649 Saflufenacil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)amino]sulfonyl]benzamide, and its metabolites N-[2-chloro-5-(2,6-dioxo-4-(trifluoromethyl)-3,6-dihydro-1(2H)-pyrimidinyl)-4-fluorobenzoyl]-N′-isopropylsulfamide and N-[4-chloro-2-fluoro-5-({[(isopropylamino)sulfonyl]amino}carbonyl)phenyl]urea, calculated as the stoichiometric equivalent of saflufenacil, in or on the commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 0.08
Alfalfa, hay 0.10
Almond, hulls 0.10
Banana 1 0.03
Barley, bran 1.5
Barley, grain 1.0
Barley, straw 15
Caneberry subgroup 13-07A 0.04
Chia, seed 0.6
Chia, straw 6
Coffee, green bean 1 0.03
Corn, field, forage 0.4
Corn, field, milled byproducts 0.2
Corn, field, stover 5
Cotton, gin byproducts 0.45
Cottonseed subgroup 20C 0.20
Fig 0.04
Fruit, citrus, group 10-10 0.03
Fruit, pome, group 11-10 0.03
Fruit, stone, group 12-12 0.03
Grain, aspirated grain fractions 50
Grain, cereal, forage, hay, stover, and straw, group 16-22, forage, except corn, field, forage 0.1
Grain, cereal, forage, hay, stover, and straw, group 16-22, hay 0.1
Grain, cereal, forage, hay, stover, and straw, group 16-22, stover, except corn, field, stover 0.1
Grain, cereal, forage, hay, stover, and straw, group 16-22, straw, except barley, chia, and wheat, straw 0.1
Grain, cereal, group 15 (except barley and wheat grain) 0.03
Grape 0.03
Grass, forage 15
Grass, hay 20
Grass, seed screenings 0.15
Grass, straw 0.15
Mango 1 0.03
Mint, dried leaves 0.03
Mint, fresh leaves 0.03
Nut, tree, group 14-12 0.03
Olive 0.03
Pea and bean, dried shelled, except soybean, subgroup 6C 0.30
Pea and bean, succulent shelled, subgroup 6B 0.03
Pea, hay 17
Pomegranate 0.03
Rapeseed subgroup 20A 0.45
Soybean, hulls 0.50
Soybean, seed 0.10
Sugarcane, cane 2 0.05
Sugarcane, molasses 2 0.08
Sunflower subgroup 20B 1.0
Vegetable, foliage of legume, group 7 (except pea, hay) 0.10
Vegetable, legume, edible podded, subgroup 6A 0.03
Wheat, grain 0.60
Wheat, straw 6.0
1 No U.S. registration as of December 7, 2011.
2 No U.S. registration as of February 21, 2014.

(2) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluoro-N-[[methyl(1-methylethyl)amino]sulfonyl]benzamide, in or on the commodities.

Commodity Parts per million
Cattle, fat 0.04
Cattle, liver 50
Cattle, meat 0.02
Cattle, meat byproducts, except liver 0.30
Fish-freshwater finfish 0.01
Fish-shellfish, crustacean 0.01
Goat, fat 0.04
Goat, liver 50
Goat, meat 0.02
Goat, meat byproducts, except liver 0.30
Hog, fat 0.01
Hog, liver 2.0
Hog, meat 0.01
Hog, meat byproducts, except liver 0.02
Horse, fat 0.04
Horse, liver 50
Horse, meat 0.02
Horse, meat byproducts, except liver 0.30
Milk 0.01
Sheep, fat 0.04
Sheep, liver 50
Sheep, meat 0.02
Sheep, meat byproducts, except liver 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 46689, Sept. 11, 2009, as amended at 76 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, 2011; 79 FR 9866, Feb. 21, 2014; 79 FR 52219, Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015; 80 FR 73667, Nov. 25, 2015; 85 FR 60365, Sept. 25, 2020; 89 FR 7294, Feb. 2, 2024; 89 FR 72997, Sept. 9, 2024]

§ 180.650 Isoxaben; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide isoxaben, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only isoxaben, N-[3-(1-ethyl-1-methylpropyl)-5-isoxazolyl]-2, 6-dimethoxybenzamide, in or on the commodity.

Commodity Parts per
million
Almond, hulls 0.40
Apple 0.01
Bushberry subgroup 13-07B 0.01
Caneberry subgroup 13-07A 0.01
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.01
Hop, dried cones 0.01
Nut, tree, group 14-12 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 69360, Nov. 12, 2010, as amended at 83 FR 5312, Feb. 7, 2018; 85 FR 29344, May 15, 2020]

§ 180.651 Imazosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide imazosulfuron, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only imazosulfuron, 2-chloro-N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]imidazo-[1,2-α]pyridine-3-sulfonamide, in or on the commodity.

Commodity Parts per million
Melon subgroup 9A 0.02
Pepper, bell 0.02
Pepper, non-bell 0.02
Rice, grain 0.02
Tomato 0.02
Vegetable, tuberous and corm, subgroup 1C 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 81884, Dec. 29, 2010, as amended at 78 FR 44444, July 24, 2013]

§ 180.652 Ethiprole; tolerances for residues.

(a) General. Tolerances are established for residues of ethiprole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only ethiprole, 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-(ethylsulfinyl)-1H-pyrazole-3-carbonitrile.

Table 1 to Paragraph (a)

Commodity Parts per
million
Coffee, green bean 1 0.1
Rice, grain 1 1.7
Sugarcane 1 0.07
Tea, dried 1 30
1 There are no U.S. registrations for this commodity as of June 28, 2019.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 18921, Apr. 6, 2011, as amended at 84 FR 30939, June 28, 2019; 89 FR 105472, Dec. 27, 2024]

§ 180.653 Indaziflam; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide indaziflam, N-[(1R,2S)-2,3-dihydro-2,6-dimethyl-1H-inden-1-yl]-6-(1-fluoroethyl)-1,3,5-triazine-2,4-diamine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only indaziflam and FDAT, 6-[(1R)-1-fluoroethyl]-1,3,5-triazine-2,4-diamine, calculated as the stoichiometric equivalent of indaziflam, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 0.15
Bushberry subgroup 13-07B 0.01
Caneberry subgroup 13-07A 0.01
Coffee, green bean 0.01
Fruit, citrus, group 10-10 0.01
Fruit, pome, group 11-10 0.01
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.01
Fruit, stone, group 12-12 0.01
Fruit, tropical and subtropical, edible peel, group 23 0.01
Fruit, tropical and subtropical, inedible peel, group 24 0.01
Grass, forage, fodder and hay, group 17, forage 40
Grass, forage, fodder and hay, group 17, hay 80
Hop, dried cones 0.06
Nut, tree, group 14-12 0.01
Palm, oil 1 0.03
Sugarcane, cane 0.01
1 No U.S. Registrations as of 12/02/2013.

(2) Tolerances are established for residues of the herbicide indaziflam, N-[(1R,2S)-2,3-dihydro-2,6-dimethyl-1H-inden-1-yl]-6-(1-fluoroethyl)-1,3,5-triazine-2,4-diamine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only indaziflam in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.1
Cattle, meat 0.01
Cattle, meat byproducts 0.3
Goat, fat 0.1
Goat, meat 0.01
Goat, meat byproducts 0.3
Horse, fat 0.1
Horse, meat 0.01
Horse, meat by-products 0.3
Milk 0.015
Milk, fat 0.4
Sheep, fat 0.1
Sheep, meat 0.01
Sheep, meat by-products 0.3

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 18905, Apr. 6, 2011, as amended at 79 FR 4630, Jan. 29, 2014; 82 FR 30987, July 5, 2017; 83 FR 8002, Feb. 23, 2018; 84 FR 54516, Oct. 10, 2019; 85 FR 37762, June 24, 2020; 88 FR 47781, July 25, 2023]

§ 180.654 Isopyrazam; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide isopyrazam, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only isopyrazam (3-(difluoromethyl)-1-methyl-N-[1,2,3,4-tetrahydro-9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide), as the sum of its syn-isomer (3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1-methylethyl)-1,4-methanonaphthalen-5-yl]-1H-pyrazole-4-carboxamide) and anti-isomer (3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9SR)-1,2,3,4-tetrahydro-9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide) in or on the commodity.

Commodity Parts per million
Apple1 0.70
Banana1 0.05
Peanut1 0.01
Pepper, bell 1 0.50
Tomato 1 0.50
Vegetable, cucurbit, subgroup 9A 1 0.30
1 There are no U.S. registrations for use of isopyrazam on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 61596, Oct. 5, 2011, as amended at 78 FR 78745, Dec. 27, 2013; 82 FR 24075, May 25, 2017]

§ 180.655 Flazasulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of flazasulfuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only flazasulfuron (N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]-3-(trifluoromethyl)-2-pyridinesulfonamide).

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 0.01
Avocado 0.01
Fruit, citrus, group 10-10 0.01
Grape 0.01
Nut, tree, group 14-12 0.01
Olive 0.01
Sugarcane 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 10968, Feb. 24, 2012, as amended at 79 FR 52989, Sept. 5, 2014; 82 FR 24066, May 25, 2017; 89 FR 81013, Oct. 7, 2024]

§ 180.656 Amisulbrom; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide amisulbrom, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels is to be determined by measuring only amisulbrom, 3-[(3-bromo-6-fluoro-2-methyl-1H-indole-1-yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4-triazole-1-sulfonamide].

Commodity 1 Parts per million
Grape 0.40
Grape, raisin 1.0
Tomato 0.50
Tomato, paste 1.2
1 There is no U.S. registration for use of amisulbrom on grape or tomato.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 59914, Sept. 28, 2011]

§ 180.657 Metaflumizone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide metaflumizone, including its metabolites and degradates, in or on the commodities listed in table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in this paragraph (a)(1) is to be determined by measuring only the sum of metaflumizone (E and Z isomers; 2-[2-(4-cyanophenyl)-1-[3-(trifluoromethyl) phenyl]ethylidene]-N-[4-(trifluoromethoxy)phenyl] hydrazinecarboxamide) and its metabolite 4-{2-oxo-2-[3-(trifluoromethyl) phenyl]ethyl}-benzonitrile, calculated as the stoichiometric equivalent of metaflumizone, in or on the following commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond, hulls 0.04
Apple 0.9
Apple, wet pomace 3
Coffee, green bean 1 0.15
Eggplant 1 1.5
Fruit, pome, group 11-10, except apple 0.04
Fruit, stone, group 12-12 0.04
Grape 5
Grape, raisin 13
Grapefruit subgroup 10-10C 0.04
Lemon/lime subgroup 10-10B 3
Lemon/lime subgroup 10-10B, oil 100
Melon subgroup 9A 1 1
Nut, tree, group 14-12 0.04
Orange subgroup 10-10A 3
Orange subgroup 10-10A, oil 100
Pepper 1 1.5
Tomato 1 0.60
Tomato, paste 1 1.2
1 There are no U.S. registrations for this commodity as of April 19, 2021.

(2) Tolerances are established for residues of the insecticide metaflumizone, including its metabolites and degradates, in or on the commodities listed in table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in this paragraph (a)(2) is to be determined by measuring only metaflumizone (E and Z isomers; 2-[2-(4-cyanophenyl)-1-[3-(trifluoromethyl) phenyl]ethylidene]-N-[4-(trifluoromethoxy)phenyl] hydrazinecarboxamide) in or on the following animal commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.15
Goat, fat 0.15
Horse, fat 0.15
Milk, fat 0.6
Sheep, fat 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 10386, Feb. 22, 2012, as amended at 79 FR 18810, Apr. 4, 2014; 80 FR 66800, Oct. 30, 2015; 86 FR 20293, Apr. 19, 2021; 86 FR 53558, Sept. 28, 2021]

§ 180.658 Penthiopyrad; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide).

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Alfalfa, forage 7.0
Alfalfa, hay 20
Almond, hulls 6.0
Apple, wet pomace 1.5
Banana 3
Barley, grain 0.15
Barley, hay 80
Barley, milled byproducts 0.90
Barley, straw 1.0
Beet, sugar, dried pulp 1.5
Beet, sugar, roots 0.5
Berry, low growing, subgroup 13-07G 3.0
Brassica, leafy greens, subgroup 4-16B 50
Buckwheat, grain 0.15
Bushberry subgroup 13-07B 6
Caneberry subgroup 13-07A 10
Celtuce 30
Corn, field, forage 40
Corn, field, grain 0.01
Corn, field, refined oil 0.05
Corn, field, stover 15
Corn, pop, grain 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Cotton, gin byproducts 15
Fennel, Florence, fresh leaves and stalk 30
Fruit, pome, group 11-10 0.50
Fruit, stone, group 12-12 4
Grain, aspirated fractions 30
Kohlrabi 5
Leaf petiole vegetable subgroup 22B 30
Leafy greens subgroup 4-16A 30
Millet, spp. 0.80
Nut, tree, group 14 1 0.06
Nut, tree, group 14-12 0.05
Oat, forage 40
Oat, grain 0.15
Oat, hay 80
Oat, straw 1.0
Oilseed group 20 1.5
Pea and bean, dried shelled, except soybean, subgroup 6C 0.40
Peanut 0.04
Peanut, hay 30
Peanut, refined oil 0.06
Persimmon 2 3
Pistachio 1 0.06
Potato, processed potato waste 0.20
Rye, forage 40
Rye, grain 0.15
Rye, straw 1.0
Sorghum, forage 40
Sorghum, grain, grain 0.80
Sorghum, stover 15
Soybean, seed 0.40
Teosinte, grain 0.15
Tomato, paste 3.5
Triticale, forage 40
Triticale, grain 0.15
Triticale, hay 80
Triticale, straw 1.0
Vegetable, brassica, head and stem, group 5-16 5
Vegetable, bulb, group 3-07 3.0
Vegetable, cucurbit, group 9 0.60
Vegetable, foliage of legume, group 7, hay 200
Vegetable, foliage of legume, group 7, vines/forage 50
Vegetable, fruiting, group 8-10 3.0
Vegetable, leaves of root and tuber, group 2 50
Vegetable, legume, edible podded, subgroup 6A 4.0
Vegetable, legume, succulent shelled, subgroup 6B 0.40
Vegetable, root, subgroup 1B, except sugar beet 3.0
Vegetable, tuber and corm, subgroup 1C 0.06
Wheat, forage 40
Wheat, grain 0.15
Wheat, hay 80
Wheat, milled byproducts 0.30
Wheat, straw 1.0
1 This tolerance expires on December 6, 2019.
2 There are no U.S. registrations for this commodity as of April 7, 2021.

(2) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide) and its metabolite (1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide), calculated as the stoichiometric equivalent of penthiopyrad, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.03
Cattle, meat 0.03
Cattle, meat byproducts 0.09
Goat, fat 0.03
Goat, meat 0.03
Goat, meat byproducts 0.09
Horse, fat 0.03
Horse, meat 0.03
Horse, meat byproducts 0.09
Milk 0.02
Sheep, fat 0.03
Sheep, meat 0.03
Sheep, meat byproducts 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 14297, Mar. 9, 2012, as amended at 84 FR 26359, June 6, 2019; 86 FR 17920, Apr. 7, 2021; 88 FR 10244, Feb. 17, 2023]

§ 180.659 Pyroxasulfone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolite, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million
Corn, field, grain 0.02
Corn, pop, grain 0.015
Corn, sweet, kernel plus cob with husks removed 0.015
Cottonseed, subgroup 20C 0.04
Wheat, grain 0.03

(2) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-1); 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid (M-3); and [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million
Corn, field, forage 0.09
Corn, field, stover 0.15
Corn, pop, stover 0.15
Corn, sweet, forage 0.10
Corn, sweet, stover 0.15
Cotton, gin byproducts 0.20
Soybean, forage 1.0
Soybean, hay 2.0
Wheat, forage 6.0
Wheat, hay 1.0
Wheat, straw 0.60

(3) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid (M-3); [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25); and 3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3-ylthio)ethylamino]-3-oxopropanoic acid (M-28), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million
Soybean, seed 0.06

(4) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of pyroxasulfone [3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole] and its metabolites [5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-1) and 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million
Milk 0.003

(5) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyroxasulfone (3-[(5-difluoromethoxy-1-methyl-3-(trifluoromethyl)pyrazol-4-ylmethylsulfonyl]-4,5-dihydro-5,5-dimethyl-1,2-oxazole), and its metabolites, M-1 (5-difluoromethoxy-1-methyl-3-trifluoromethyl-1H-pyrazol-4-yl) methanesulfonic acid), M-3 (5-difluoromethoxy-1-methyl-3-trifluoromethyl-1H-pyrazol-4-carboxylic acid), M-25 (5-difluoromethoxy-3-trifluoromethyl-1H-pyrazol-4-yl)methanesulfonic acid) and M-28 (3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3-ylthio)ethylamino]-3-oxopropanoic acid) calculated as the stoichiometric equivalent of pyroxasulfone, in or on the following commodities:

Commodity Parts per
million
Almond, hulls 0.15
Flax, seed 0.07
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.07
Leaf petiole vegetable subgroup 22B 0.80
Nut, tree, group 14-12 0.07
Pea and bean, dried shelled, except soybean, subgroup 6C 0.15
Peanut 0.30
Peanut, hay 4.0
Peanut, meal 0.40
Potato, granules/flakes 0.20
Peppermint, fresh leaves 0.20
Peppermint, oil 0.70
Soybean, vegetable, succulent shelled 0.40
Spearmint, fresh leaves 0.20
Spearmint, oil 0.70
Sunflower subgroup 20B 0.30
Vegetable, bulb, group 3-07 0.15
Vegetable, foliage of legume, except soybean, subgroup 7A 3.0
Vegetable, soybean, edible podded 0.40
Vegetable, tuberous and corm, subgroup 1C 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerance with regional registrations. Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyroxasulfone (3-[(5-difluoromethoxy-1-methyl-3-(trifluoromethyl)pyrazol-4-ylmethylsulfonyl]-4,5-dihydro-5,5-dimethyl-1,2-oxazole), and its metabolites, M-1 (5-difluoromethoxy-1-methyl-3-trifluoromethyl-1H-pyrazol-4-yl)methanesulfonic acid), M-3 (5-difluoromethoxy-1-methyl-3-trifluoromethyl-1H-pyrazol-4-carboxylic acid), M-25 (5-difluoromethoxy-3-trifluoromethyl-1H-pyrazol-4-yl)methanesulfonic acid) and M-28 (3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3-ylthio)ethylamino]-3-oxopropanoic acid) calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per
million
Grass, forage 0.50
Grass, hay 1.0

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 12213, Feb. 29, 2012, as amended at 78 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, 2013; 79 FR 34633, June 18, 2014; 82 FR 18235, Apr. 18, 2017; 83 FR 22859, May 17, 2018; 83 FR 54264, Oct. 29, 2018; 90 FR 35624, July 29, 2025]

§ 180.660 Pyriofenone; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide pyriofenone, including its metabolites and degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the table is to be determined by measuring only pyriofenone, (5-chloro-2-methoxy-4-methyl-3-pyridinyl)(2,3,4-trimethoxy-6-methylphenyl) methanone, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Apple 0.3
Apple, wet pomace 0.5
Berry, low growing, subgroup 13-07G, except cranberry 2
Bushberry subgroup 13-07B 1.5
Caneberry subgroup 13-07A 0.90
Cherry subgroup 12-12A 1.5
Fruit, small vine climbing subgroup 13-07E, except grape 1.5
Grape 0.8
Grape, raisin 2.5
Pepper/eggplant subgroup 8-10B 2
Tomato subgroup 8-10A 0.2
Tomato subgroup 8-10A 1 0.3
Vegetables, cucurbit, crop group 9 0.30
1 This tolerance expires on January 5, 2023.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 13506, Mar. 7, 2012, as amended at 82 FR 18240, Apr. 18, 2017; 84 FR 24987, May 30, 2019; 86 FR 17548, Apr. 5, 2021; 87 FR 39755, July 5, 2022; 91 FR 1396, Jan. 14, 2026]

§ 180.661 Fluopyram; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide Fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only fluopyram in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 10
Artichoke, globe 4.0
Banana 1 1.0
Beet, sugar 0.10
Berry, low growing, except cranberry, subgroup 13-07G 2.0
Brassica, leafy greens, subgroup 4-16B 50
Bushberry subgroup 13-07B 7.0
Caneberry subgroup 13-07A 5.0
Celtuce 20
Cherry subgroup 12-12A 2.0
Citrus, oil 8.0
Coffee, green beans 0.03
Corn, field, grain 0.02
Corn, pop, grain 0.02
Corn, sweet, kernel plus cob with husks removed 0.01
Cotton, gin byproducts 30
Cottonseed subgroup 20C 0.80
Cranberry 1 2
Fennel, Florence, fresh leaves and stalk 20
Fruit, citrus, group 10-10 1.0
Fruit, pome, group 11-10 0.80
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Grain, aspirated grain fractions 50
Grain, cereal, forage, fodder and straw, group 16 20
Grain, cereal, group 15, except corn and rice 0.5
Grape, raisin 3.0
Herb subgroup 19A 40
Hop, dried cones 60
Kohlrabi 4
Leaf petiole vegetable subgroup 22B 20
Leafy greens subgroup 4-16A 40
Lentil, dry seed 1 0.7
Mango 1 1.0
Melon subgroup 9A 1.0
Nut, tree, group 14-12 0.05
Onion, bulb, subgroup 3-07A 0.40
Onion, green, subgroup 3-07B 15
Papaya 1.5
Pea, dry seed 1 0.7
Peach subgroup 12-12B 1.0
Peanut 0.20
Pepper/eggplant subgroup 8-10B 4.0
Peppermint, dried leaves 0.8
Peppermint, fresh leaves 0.6
Plum subgroup 12-12C 0.50
Potato, wet peel 0.30
Rapeseed subgroup 20A 0.3
Soybean, seed 0.30
Spearmint, dried leaves 0.8
Spearmint, fresh leaves 0.6
Spice group 26 70
Squash/cucumber subgroup 9B 0.60
Sunflower subgroup 20B 0.70
Tomato subgroup 8-10A 1.0
Vegetable, Brassica, head and stem, group 5-16 4
Vegetable, leaves of root and tuber, group 2 30
Vegetable, legume, bean, edible podded, subgroup 6-22A 4
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.2
Vegetable, legume, pea, edible podded, subgroup 6-22B 4
Vegetable, legume, pea, succulent shelled, subgroup 6-22D 0.2
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.7
Vegetable, root, except sugar beet, subgroup 1B 0.30
Vegetable, tuberous and corm, subgroup 1C 0.10
1 There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates. Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of fluopyram and its metabolite, 2-(trifluoromethyl)benzamide, calculated as the stoichiometric equivalent of fluopyram, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Cattle, fat 0.3
Cattle, meat 0.3
Cattle, meat byproducts 3
Egg 0.03
Goat, fat 0.3
Goat, meat 0.3
Goat, meat byproducts 3
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.04
Horse, fat 0.3
Horse, meat 0.3
Horse, meat byproducts 3
Milk 0.15
Poultry, fat 0.01
Poultry, meat 0.02
Poultry, meat byproducts 0.06
Sheep, fat 0.3
Sheep, meat 0.3
Sheep, meat byproducts 3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in § 180.1(1), are established for indirect or inadvertent residues of fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only fluopyram in or on the commodity.

Commodity Parts per
million
Sugarcane, cane 0.08

(d) Indirect or inadvertent residues. It is recommended that tolerances be established for indirect or inadvertent residues of fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only fluopyram in or on the commodity.

Commodity Parts per
million
Alfalfa, forage 0.45
Alfalfa, hay 1.1
Soybean, seed 0.10

[81 FR 12023, Mar. 8, 2016, as amended at 84 FR 31213, July 1, 2019; 87 FR 9520, Feb. 18, 2022; 88 FR 6642, Feb. 1, 2023; 90 FR 51565, Nov. 18, 2025]

§ 180.662 Trinexapac-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator, trinexapac-ethyl, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 is to be determined by measuring only the free and conjugated forms of both trinexapac-ethyl, ethyl 4-(cyclopropylhydroxymethylene)-3,5-dioxocyclohexanecarboxylate and trinexapac, 4-(cyclopropylhydroxymethylene)-3,5-dioxocyclohexanecarboxylic acid, calculated as the stoichiometric equivalent of trinexapac-ethyl, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Barley, bran 2.5
Barley, grain 2.0
Barley, hay 0.8
Barley, straw 0.4
Cattle, fat 0.03
Cattle, meat 0.03
Cattle, meat byproducts 0.1
Egg 0.01
Goat, fat 0.03
Goat, meat 0.03
Goat, meat byproducts 0.1
Grass, forage 1.5
Grass, hay 4.0
Grass, seed screenings 40.0
Grass, straw 10.0
Hog, fat 0.02
Hog, meat 0.02
Hog, meat by-products 0.1
Horse, fat 0.02
Horse, meat 0.03
Horse, meat byproducts 0.04
Milk 0.01
Oat, forage 1.0
Oat, grain 4.0
Oat, hay 1.5
Oat, straw 0.9
Poppy, seed 1 8
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.1
Rice, bran 1.5
Rice, grain 0.4
Rice, straw 0.07
Rice, wild, grain 0.4
Rye, bran 6.0
Rye, grain 4.0
Rye, hay 1.5
Rye, straw 0.9
Sheep, fat 0.03
Sheep, meat 0.03
Sheep, meat byproducts 0.1
Sugarcane, cane 1.5
Sugarcane, molasses 5
Wheat, bran 6.0
Wheat, forage 1.0
Wheat, grain 4.0
Wheat, hay 1.5
Wheat, middlings 10.5
Wheat, straw 0.9
1 There are no U.S. registrations for Poppy, seed as of March 15, 2018.

(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in § 180.1, are established for residues of trinexapac-ethyl, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (c). Compliance with the tolerance levels specified in table 2 is to be determined by measuring only the free and conjugated forms of both trinexapac-ethyl, ethyl 4-(cyclopropylhydroxymethylene)-3,5-dioxocyclohexanecarboxylate and trinexapac, 4-(cyclopropylhydroxymethylene)-3,5-dioxocyclohexanecarboxylic acid, calculated as the stoichiometric equivalent of trinexapac-ethyl, in or on the commodity.

Table 2 to Paragraph (c)

Commodity Parts per
million
Clover, forage 8
Clover, hay 15

(d) [Reserved]

[88 FR 18434, Mar. 29, 2023]

§ 180.663 Ametoctradin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ametoctradin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only ametoctradin (5-ethyl-6-octyl[1,2,4]triazolo[1,5-a]pyrimidin-7-amine).

Commodity Parts per
million
Brassica, head and stem, subgroup 5A 9.0
Brassica, leafy greens, subgroup 5B 50
Grape 4.0
Grape, raisin 8.0
Hop, dried cones 100
Onion, bulb, subgroup 3-07A 1.5
Onion, green, subgroup 3-07B 20.0
Spinach 50.0
Vegetable, cucurbit, group 9 3.0
Vegetable, fruiting, group 8-10 1.5
Vegetable, leafy, except Brassica, group 4, except spinach 40.0
Vegetable, tuberous and corm, subgroup 1C 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 21734, May 9, 2012, as amended at 82 FR 34877, July 27, 2017]

§ 180.664 Penflufen; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide penflufen, including its metabolites and degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the table is to be determined by measuring only penflufen N-[2-(1,3-dimethylbutyl)phenyl]-5-fluoro-1,3-dimethyl-1H-pyrazole-4-carboxamide, in or on the following commodities.

Commodity Parts per million
Alfalfa, forage 0.01
Alfalfa, hay 0.01
Beet, sugar, roots 0.01 ppm
Beet, sugar, tops 0.01 ppm
Cotton, gin by-products 0.01
Grain cereal, forage, fodder and straw, group 16 0.01
Grain, cereal, group 15 0.01
Oilseed, group 20 0.01
Vegetable, bulb, group 3-07 0.01 ppm
Vegetable, foliage of legume, group 7 0.01
Vegetable, legume, group 6 0.01
Vegetable, tuberous and corm subgroup 1C 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 28281, May 14, 2012, as amended at 81 FR 72007, Oct. 19, 2016]

§ 180.665 Sedaxane; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide sedaxane, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only sedaxane, N-[2-[1,1′-bicyclopropyl]-2-ylphenyl]-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxamide, as the sum of its cis- and trans-isomers in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Beet, sugar, roots 0.01
Canola, seed 0.01
Cotton, gin byproducts 0.01
Cotton, undelinted seed 0.01
Grain, cereal, forage, fodder and straw, group 16 0.10
Grain, cereal, group 15 0.01
Onion, bulb, subgroup 3-07A 0.01
Peanut 0.01
Peanut, hay 0.08
Potato 0.02
Potato, wet peel 0.075
Rapeseed, subgroup 20A 0.01
Soybean, forage 0.05
Soybean, hay 0.04
Soybean, seed 0.01
Vegetable, cucurbit, group 9 0.01
Vegetable, foliage of legume, except soybean, subgroup 7A 0.01
Vegetable, legume, group 6 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect inadvertent residues. [Reserved]

[77 FR 36924, June 20, 2012, as amended at 78 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, 2013; 80 FR 43329, July 22, 2015; 82 FR 57871, Dec. 8, 2017; 84 FR 44707, Aug. 27, 2019; 88 FR 37771, June 9, 2023]

§ 180.666 Fluxapyroxad; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fluxapyroxad, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluxapyroxad, 3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)-1H-pyrazole-4-carboxamide in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 4.0
Apple, wet pomace 2.0
Avocado 1.5
Banana 1 3.0
Beet, sugar 0.1
Beet, sugar, dried pulp 0.1
Beet, sugar, tops 7.0
Berry, low growing, subgroup 13-07G 4.0
Bushberry, subgroup 13-07B 7.0
Caneberry, subgroup 13-07A 5.0
Cattle, fat 0.06
Cattle, meat 0.01
Cattle, meat byproduct 0.04
Citrus, dried pulp 3.0
Citrus, oil 40
Coffee, green bean 0.2
Corn, field, grain 0.01
Corn, oil 0.03
Corn, pop, grain 0.01
Corn, sweet, kernels plus cobs with husks removed 0.15
Cotton, gin byproducts 20
Cottonseed, subgroup 20C 0.5
Egg 0.01
Fish-freshwater finfish 0.01
Fish-shellfish, crustacean 0.01
Fruit, citrus, group 10-10 1.0
Fruit, pome, group 11-10 0.8
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 3.0
Goat, fat 0.06
Goat, meat 0.01
Goat, meat byproduct 0.04
Grain, aspirated fractions 20.0
Grain, cereal, forage, fodder and straw, group 16 20
Grain, cereal, group 15, (except corn, field, grain; except corn, pop, grain; except corn, kernels plus cobs with husks removed; except rice; except wheat 3.0
Grape, raisin 5.7
Grass, forage, fodder and hay, group 17 40
Hog, meat byproducts 0.01
Horse, fat 0.06
Horse, meat 0.01
Horse, meat byproduct 0.04
Mango 1 0.7
Milk 0.01
Milk, fat 0.15
Non-grass animal feed, group 18 30
Nut, tree, group 14-12 0.06
Oilseeds, group 20 (except cottonseed) 0.9
Papaya 1 0.6
Pea and bean, dried shelled except soybean, subgroup 6C 0.4
Pea and bean, succulent shelled, subgroup 6B 0.5
Peanut 0.01
Peanut, refined oil 0.02
Plum, prune, dried 3.0
Pomegranate 0.2
Potato, wet peel 0.1
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproduct 0.01
Rice, bran 4.5
Rice, bran 8.5
Rice, grain 5.0
Rice, hulls 8.0
Rice, hulls 15.0
Sheep, fat 0.06
Sheep, meat 0.01
Sheep, meat byproduct 0.04
Soybean, hulls 0.3
Soybean, seed 0.15
Stevia, dried leaves 70
Stevia, fresh leaves 20
Sugarcane, cane 3.0
Vegetable, brassica leafy, group 5 4.0
Vegetable, bulb, group 3-07 1.5
Vegetable, cucurbit, group 9 0.50
Vegetable, foliage of legume, group 7 30
Vegetable, fruiting, group 8-10 0.7
Vegetable, leafy, except brassica, group 4 30
Vegetable, legume, edible podded, subgroup 6A 2.0
Vegetable, root, except sugarbeet, subgroup 1B 0.90
Vegetable, tuberous and corm, subgroup 1C 0.02
Wheat, bran 0.6
Wheat, grain 0.3
1 There are no U.S. registrations for this commodity as of November 8, 2016.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of the fungicide fluxapyroxad, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fluxapyroxad, 3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)-1H-pyrazole-4-carboxamide in or on the commodity.

Commodity Parts per
million
Peppermint, tops 0.01
Spearmint, tops 0.01

[77 FR 28275, May 14, 2012, as amended at 77 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, 2014; 80 FR 45078, July 29, 2015; 81 FR 27025, May 5, 2016; 81 FR 78511, Nov. 8, 2016; 86 FR 36669, July 13, 2021; 88 FR 55581, Aug. 16, 2023]

§ 180.667 Cyflufenamid, tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide cyflufenamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only cyflufenamid, [N(Z)]-N-[[(cyclopropylmethoxy)amino][2,3-difluoro-6-(trifluoromethyl)phenyl]methylene]benzeneacetamide.

Table 1 to Paragraph (a)

Commodity Parts per million
Apple, wet pomace 0.10
Beet, sugar, roots 0.15
Berry, low growing, subgroup 13-07G, except cranberry 0.20
Cherry subgroup 12-12A 0.60
Fruit, pome, group 11 0.06
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.15
Grape, raisin 0.30
Hop, dried cones 5.0
Vegetable, cucurbit, group 9 0.10
Vegetable, fruiting, group 8-10 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 38210, June 27, 2012, as amended at 83 FR 5717, Feb. 9, 2018; 88 FR 30047, May 10, 2023]

§ 180.668 Sulfoxaflor; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide sulfoxaflor, including its metabolites and degradates, in or on the commodities in the table. Compliance with the tolerance levels specified is to be determined by measuring only sulfoxaflor (N-[methyloxido[1-[6-(trifluoromethyl)-3-pyridinyl]ethyl]-γ4-sulfanylidene]cyanamide).

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 7
Alfalfa, hay 20
Alfalfa, seed 40
Alfalfa, silage 9
Almond, hulls 6.0
Artichoke, globe 0.7
Asparagus 0.01
Avocado 0.15
Barley, grain 0.40
Barley, hay 1.0
Barley, straw 2.0
Bean, dry seed 0.20
Bean, succulent 4.0
Beet, sugar, dried pulp 0.07
Beet, sugar, molasses 0.25
Berry, low growing, subgroup 13-7G 0.70
Brassica, leafy greens, subgroup 4-16B, except watercress 2
Bushberry subgroup 13-07B 2
Cacao, dried bean 0.05
Caneberry subgroup 13-07A 1.5
Cattle, fat 0.2
Cattle, meat 0.4
Cattle, meat byproducts 0.8
Cauliflower 0.08
Celtuce 2
Citrus, dried pulp 3.6
Coffee, green bean 1 0.3
Corn, field, forage 0.5
Corn, field, grain 0.015
Corn, field, stover 0.8
Corn, pop, grain 0.015
Corn, pop, stover 0.8
Corn, sweet, forage 0.6
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.7
Cotton, gin byproducts 6.0
Cotton, hulls 0.35
Cottonseed subgroup 20C 0.20
Egg 0.06
Fennel, Florence, fresh leaves and stalk 2
Fruit, citrus, group 10-10 0.70
Fruit, pome, group 11-10 0.50
Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwi fruit 2.0
Fruit, stone, group 12-12 3
Goat, fat 0.2
Goat, meat 0.4
Goat, meat byproducts 0.8
Grain, aspirated fractions 20.0
Grape, raisin 6.0
Hog, fat 0.03
Hog, meat 0.3
Hog, meat byproducts 0.6
Horse, fat 0.2
Horse, meat 0.4
Horse, meat byproducts 0.8
Kohlrabi 2
Leaf petiole vegetable subgroup 22B 2
Leafy greens subgroup 4-16A 6
Milk 0.3
Millet, proso, forage 0.4
Millet, pearl, forage 0.4
Millet, proso, grain 0.3
Millet, pearl, grain 0.3
Nut, tree, group 14-12 0.015
Oat, grain 0.4
Oat, hay 1
Oat, straw 2
Onion, bulb, subgroup 3-07A 0.01
Onion, green, subgroup 3-07B 0.70
Pineapple 0.1
Poultry, fat 0.02
Poultry, meat 0.1
Poultry, meat byproducts 0.3
Rapeseed, meal 0.50
Rapeseed subgroup 20A 0.40
Rice, grain 5
Rice, hulls 15
Rye, forage 1
Rye, grain 0.08
Rye, hay 1.5
Rye, straw 2
Sheep, fat 0.2
Sheep, meat 0.4
Sheep, meat byproducts 0.8
Sorghum, grain, forage 0.4
Sorghum, grain, grain 0.3
Sorghum, grain, stover 1
Soybean, seed 0.20
Sunflower subgroup 20B 0.3
Teff, forage 1
Teff, grain 0.08
Teff, hay 1.5
Teff, straw 2
Teosinte, grain 0.015
Tomato, paste 2.60
Tomato, puree 1.20
Triticale, forage 1
Triticale, grain 0.08
Triticale, hay 1.5
Triticale, straw 2
Vegetable, brassica, head and stem, group 5-16, except cauliflower 2
Vegetable, cucurbit, group 9 0.40
Vegetable, fruiting, group 8-10 0.70
Vegetable, leaves of root and tuber, group 2 3.0
Vegetable, legume, foliage, group 7 3.0
Vegetable, root and tuber, group 1 0.05
Watercress 6.0
Wheat, forage 1.0
Wheat, grain 0.08
Wheat, hay 1.5
Wheat, straw 2.0
1 There are no U.S. registrations as of June 20, 2023.

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59565, Sept. 28, 2012, as amended at 78 FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, 2015; 82 FR 57151, Dec. 4, 2017; 84 FR 35553, July 24, 2019; 84 FR 57343, Oct. 25, 2019; 88 FR 39783, June 20, 2023]

§ 180.669 Picoxystrobin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide picoxystrobin, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring only picoxystrobin, methyl (αE)-α-(methoxymethylene)-2-[[[6-(trifluoromethyl)-2-pyridinyl]oxy]methyl]benzeneacetate.

Commodity Parts per
million
Alfalfa, forage 4.0
Alfalfa, hay 5.0
Alfalfa, seed 9.0
Almond, hulls 7.0
Barley, bran 0.5
Barley, grain 0.3
Beet, sugar, dried pulp 1.5
Bluegrass, forage 30
Bluegrass, hay 60
Bromegrass, forage 30
Bromegrass, hay 60
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Corn, field, refined oil 0.07
Cotton, gin byproducts 20
Cottonseed subgroup 20C 2.0
Eggs 0.01
Fescue, forage 30
Fescue, hay 60
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Grain, aspirated grain fractions 10
Grain, cereal, forage, fodder, and straw, group 16, forage 15
Grain, cereal, forage, fodder, and straw, group 16, hay 5
Grain, cereal, forage, fodder, and straw, group 16, stover 10
Grain, cereal, forage, fodder, and straw, group 16, straw 2
Grain, cereal, group 15, except rice and barley 0.04
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Leaf petiole vegetable subgroup 22B 20
Lettuce, head 4.0
Milk 0.01
Nut, tree, group 14-12 0.08
Onion, bulb, subgroup 3-07A 0.50
Onion, green, subgroup 3-07B 10
Orchardgrass, forage 30
Orchardgrass, hay 60
Pea and bean, dried shelled, except soybean, subgroup 6C 0.06
Pea and bean, succulent shelled, subgroup 6B 0.90
Peanut 0.05
Peanut, hay 30
Potato, wet peel 0.10
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Rapeseed subgroup 20A 0.08
Ryegrass, forage 30
Ryegrass, hay 60
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01
Soybean, forage 1
Soybean, hay 3
Soybean, hulls 0.2
Soybean, seed 0.05
Sunflower subgroup 20B 2.0
Switchgrass, forage 30
Switchgrass, hay 60
Vegetable, brassica, head and stem, group 5-16 2.0
Vegetable, cucurbit, group 9 0.30
Vegetable, foliage of legume, except soybean, subgroup 7A 40
Vegetable, fruiting, group 8-10 0.70
Vegetable, leafy, group 4-16, except lettuce, head 30
Vegetable, leaves of root and tuber, group 2 30
Vegetable, legume, edible podded, subgroup 6A 2.0
Vegetable, root, subgroup 1A 0.50
Vegetable, tuberous and corm, subgroup 1C 0.03
Wheat, bran 0.06
Wheat, germ 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 72231, Dec. 5, 2012, as amended at 83 FR 39610, Aug. 10, 2018]

§ 180.671 Fenpyrazamine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fenpyrazamine, in or on the following commodities. Compliance with the tolerance levels specified in the following table is to be determined by measuring only fenpyrazamine S-allyl 5-amino-2-isopropyl-4-(2-methylphenyl)-3-oxo-2,3-dihydropyrazole-1-carbothioate, in or on the following commodities:

Commodity Parts per
million
Almond 0.02
Almond, hulls 1.5
Berry, low growing, subgroup 13-07G 3
Bushberry subgroup 13-07B 5
Caneberry subgroup 13-07A 5
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3
Ginseng 0.7
Grape, juice 4
Lettuce, head 1.5
Lettuce, leaf 2
Pistachio 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 14465, Mar. 6, 2013]

§ 180.672 Cyantraniliprole; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide cyantraniliprole, 3-bromo-1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[((methylamino)carbonyl]phenyl]-1H-pyrazole-5-carboxamide, including its metabolites and degradates, in or on commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only cyantraniliprole in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 8.0
Artichoke, globe 1 0.10
Avocado 2 0.4
Berry, low growing, except strawberry, subgroup 13-07H, except blueberry, lowbush and lingonberry 0.08
Brassica, leafy greens, subgroup 4-16B 30
Bushberry, subgroup 13-07B 4.0
Caneberry subgroup 13-07A 4.0
Cattle, fat 0.10
Cattle, meat 0.10
Cattle, meat byproducts 0.40
Celtuce 20
Cherry, subgroup 12-12A 6.0
Citrus, oil 2.4
Coffee, green bean 0.05
Corn, field, grain 0.01
Corn, pop, grain 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Cotton, gin byproducts 10
Fennel, Florence, fresh leaves and stalk 20
Fruit, citrus, group 10-10 0.70
Fruit, pome, group 11-10 1.5
Goat, fat 0.10
Goat, meat 0.10
Goat, meat byproducts 0.40
Grain, aspirated grain fractions 200
Grape, table 2 2
Grape, wine 1 2.0
Herb, dried leaves, subgroup 25B 150
Herb, fresh leaves, subgroup 25A 40
Hop, dried cones 70
Horse, fat 0.10
Horse, meat 0.10
Horse, meat byproducts 0.40
Kohlrabi 3.0
Leaf petiole vegetable subgroup 22B 20
Leafy greens subgroup 4-16A 20
Mango 2 0.7
Milk 0.20
Nut, tree, group 14-12 0.04
Oilseed group 20 1.5
Olive 2 3
Onion, bulb, subgroup 3-07A 0.04
Onion, green, subgroup 3-07B 8.0
Papaya 1.5
Peach, subgroup 12-12B 1.5
Peanut 0.01
Peanut hay 3.0
Plum, subgroup 12-12C 0.50
Pomegranate 1 0.01
Rice, grain 0.02
Rice, hulls 0.05
Rice, straw 0.015
Sheep, fat 0.10
Sheep, meat 0.10
Sheep, meat byproducts 0.40
Soybean, forage 15
Soybean, hay 50
Soybean, hulls 1.0
Soybean, seed 0.40
Spice crop group 26 80
Strawberry 1.5
Tea 1 30
Vegetable, Brassica, head and stem, group 5-16 3.0
Vegetable, cucurbit, group 9 0.70
Vegetable, fruiting, group 8-10 2.0
Vegetable, leaves of root and tuber, group 2 40
Vegetable, legume, bean, edible podded, subgroup 6-22A 2
Vegetable, legume, bean, succulent shelled, subgroup 6-22C 0.3
Vegetable, legume, forage and hay, except soybean, subgroup 7-22A 40
Vegetable, legume, pea, edible podded, subgroup 6-22B 2
Vegetable, legume, pea, succulent shelled, subgroup 6-22D 0.3
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 1
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 1
Vegetable, root, except sugar beet, subgroup 1B 0.40
Vegetable, tuberous and corm, subgroup 1C 0.15
1 There are no U.S. registrations for these commodities.
2 There are no U.S. registrations for these commodities as of May 15, 2024.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. Tolerances are established for indirect or inadvertant tolerances for residues of cyantraniliprole, 3-bromo-1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[((methylamino)carbonyl]phenyl]-1H-pyrazole-5-carboxamide, including its metabolites and degradates, in or on commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only cyantraniliprole in or on the commodity.

Table 2 to Paragraph (d)

Commodity Parts per
million
Animal feed, nongrass, group 18 0.20
Beet, sugar, roots 0.02
Grain, cereal, forage, fodder and straw, group 16 0.50
Grass forage, fodder and hay, group 17 0.50
Sugarcane, cane 0.01

[79 FR 6833, Feb. 5, 2014, as amended at 82 FR 14629, Mar. 22, 2017; 83 FR 56267, Nov. 13, 2018; 85 FR 8457, Feb. 14, 2020; 87 FR 20335, Apr. 7, 2022; 89 FR 42386, May 15, 2024]

§ 180.673 Triforine; tolerances for residues.

(a) General. Tolerances are established for residues of triforine, including its metabolites and degradates. Compliance with the tolerance levels specified in the following table is to be determined by measuring only triforine (N,N′-[1,2-piperazinediylbis(2,2,2-trichloroehylidene)]bis[formamide]), in or on the following commodities.

Commodity Parts per
million
Blueberry 1 1.0
Tomato 1 0.5
1 There are no U.S. registrations for blueberry and tomato.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 32151, May 29, 2013. Redesignated at 78 FR 36677, June 19, 2013]

§ 180.674 Proquinazid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide, proquinazid, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only proquinazid, [6-Iodo-2-propoxy-3-propyl-3H-quinazolin-4-one), in or on the following commodities:

Commodity Parts per
million
Grape 1 0.50
Grape, raisin 1 1.0
1 No U.S. registrations for Proquinazid.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 18815, Apr. 4, 2014]

§ 180.675 Tolfenpyrad; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only tolfenpyrad (4-chloro-3-ethyl-1-methyl-N-[[4-(4-methylphenoxy)phenyl]methyl]-1H-pyrazole-5-carboxamide) in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Almond hulls 6.0
Apple, wet pomace 3.0
Artichoke, globe 5
Avocado 1.5
Berry, low growing, subgroup 13-07G, except cranberry and lowbush blueberry 3.0
Brassica, leafy greens, subgroup 4-16B 40
Bushberry, subgroup 13-07B 7.0
Caneberry, subgroup 13-07A 7.0
Celtuce 30
Citrus, dried pulp 1 8.0
Citrus, dried pulp 4.0
Citrus, oil 1 70.0
Citrus, oil 30
Cotton, gin byproducts 15.0
Cottonseed, subgroup 20C 0.70
Fennel, Florence, fresh leaves and stalk 30
Fruit, citrus, group 10-10 1 1.5
Fruit, citrus, group 10-10 0.80
Fruit, pome, group 11-10 1.0
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0
Fruit, stone, group 12-12 2.0
Grape, raisin 6.0
Leaf petiole vegetable subgroup 22B 30
Leafy greens, subgroup 4-16A 30
Nuts, tree, group 14-12 0.05
Onion, bulb, subgroup 3-07A 0.09
Onion, green, subgroup 3-07B 10
Persimmon 2.0
Plum, prune 3.0
Pomegranate 2.0
Tea 30.0
Vegetable, Brassica, head and stem, group 5-16 5.0
Vegetable, cucurbit, group 9 0.70
Vegetable, fruiting, group 8-10 1.5
Vegetable, tuberous and corm, subgroup 1C 0.01
1 This tolerance expires on December 24, 2018.

(2) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[[4-(4-methylphenoxy)phenyl]methyl]-1H-pyrazole-5-carboxamide, and its metabolite 4-[4-[(4-chloro-3-ethyl-1-methylpyrazol-5-yl)carbonylamino-methyl]phenoxy]-benzoic acid, calculated as the stoichiometric equivalent of tolfenpyrad.

Commodity Parts per million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.35
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.35
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.35
Milk 0.03
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.35

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 1605, Jan. 9, 2014, as amended at 81 FR 68944, Oct. 5, 2016; 82 FR 46934, Oct. 10, 2017; 83 FR 29023, June 22, 2018; 83 FR 65550, Dec. 21, 2018; 86 FR 31954, June 16, 2021]

§ 180.676 Fenpropidin; tolerances for residues.

(a) General. Tolerances are established for the residues of fenpropidin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only fenpropidin (1-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]piperidine).

Commodity Parts per
million
Banana 1 10
1 There are no U.S. registrations as of December 13, 2013.

(b) Section 18 tolerance. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 8096, Feb. 11, 2014]

§ 180.677 Cyflumetofen; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide cyflumetofen, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels for cyflumetofen is to be determined by measuring only cyflumetofen, 2-methoxyethyl α-cyano-α-[4-(1,1-dimethylethyl)phenyl]-β-oxo-2-(trifluoromethyl)benzenepropanoate, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 4.0
Berry, low growing, subgroup 13-07G 0.6
Cherry subgroup 12-12A 1.5
Citrus, oil 16
Coffee, green bean 2 0.08
Fruit, citrus, group 10-10 0.30
Fruit, pome, group 11-10 0.30
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.6
Hop, dried cones 30
Nut, tree, group 14-12 0.01
Peach subgroup 12-12B 0.4
Pepper/eggplant subgroup 8-10B 2
Plum subgroup 12-12C 0.3
Tea, dried 1 40
Tomato subgroup 8-10A 0.7
Vegetable, cucurbit, group 9 0.3
1 There are no U.S. registrations for this commodity as of May 8, 2019.
2 There are no U.S. registrations for these commodities as of November 25, 2019.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 29108, May 21, 2014, as amended at 84 FR 20042, May 8, 2019; 84 FR 64779, Nov. 25, 2019; 85 FR 39494, July 1, 2020; 86 FR 68918, Dec. 6, 2021; 89 FR 40399, May 10, 2024]

§ 180.678 Tricyclazole; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide tricyclazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only tricyclazole (5-methyl-1,2,4-triazolo[3,4-b ]benzothiazole).

Commodity Parts
per million
Rice, grain 1 3.0
1 There are no U.S. Registrations on Rice as of June 11, 2014.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 33468, June 11, 2014]

§ 180.679 Flupyradifurone; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide flupyradifurone, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)methyl](2,2-difluoroethyl)amino]- 2(5H)-furanone.

Table 1 to Paragraph (a)

Commodity Parts per million
Alfalfa, forage 9.0
Alfalfa, hay 20
Almond, hulls 15
Bean, succulent 0.20
Berry, low growing, except cranberry subgroup 13-07G 1.5
Brassica, leafy greens, subgroup 4-16B 40
Bushberry, except cranberry subgroup 13-07B 4.0
Cactus, pads 0.70
Caneberry subgroup 13-07A 5.0
Cattle, fat 0.20
Cattle, meat 0.30
Cattle, meat byproducts 1.0
Celtuce 9
Coffee, green bean 1.5
Corn, field, grain 0.05
Corn, pop, grain 0.05
Corn, sweet, kernels plus cobs with husks removed 0.05
Cotton, gin byproducts 40
Cottonseed, subgroup 20C 0.80
Egg 0.01
Fennel, florence, fresh leaves and stalk 9
Fruit, citrus, dried pulp 10
Fruit, citrus, group 10-10 3.0
Fruit, pome, group 11-10 0.70
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0
Fruit, stone, group 12-12 1.5
Goat, fat 0.20
Goat, meat 0.30
Goat, meat byproducts 1.0
Grain, aspirated grain fractions 40
Grain, cereal, forage, fodder and straw, group 16 30
Grain, cereal, group 15, except rice and corn 3.0
Grape, raisin 5.0
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.04
Hops, dried cones 10
Horse, fat 0.20
Horse, meat 0.30
Horse, meat byproducts 1.0
Kava, fresh leaves 40
Kava, roots 0.90
Kohlrabi 6
Leaf petiole vegetable subgroup 22B 9
Leafy greens subgroup 4-16A 30
Milk 0.15
Nut, tree, group 14-12 0.02
Onion, bulb, subgroup 3-07A 0.09
Onion, green, subgroup 3-07B 3.0
Pea and bean, dried, shelled except soybean, subgroup 6C 3.0
Pea, succulent 2.0
Peanut 0.04
Peanut, hay 20
Pineapple 0.3
Quinoa, grain 3.0
Rapeseed subgroup 20A 0.03
Sesame, seed 3
Sheep, fat 0.20
Sheep, meat 0.30
Sheep, meat byproducts 1.0
Soybean, seed 1.5
Stalk and stem vegetable subgroup 22A, except prickly pear, pads, and prickly pear, Texas, pads 0.01
Sunflower subgroup 20B 0.7
Taro leaves 30
Tropical and subtropical, inedible peel, cactus, subgroup 24D 0.3
Tropical and subtropical, medium to large fruit, smooth, inedible peel subgroup 24B 0.60
Tropical and subtropical, palm fruit, edible peel, subgroup 23C 8
Vegetable, brassica, head and stem, group 5-16 6
Vegetable, cucurbit, group 9 0.40
Vegetable, foliage of legume, group 7 30
Vegetable, fruiting, group 8-10 1.5
Vegetable, legume, edible podded, subgroup 6A 3.0
Vegetable, root, except sugar beet, subgroup 1B 0.90
Vegetable, tuberous and corm, subgroup 1C 0.05
1 No U.S. registration.

(b) Section 18 emergency exemptions. The time-limited tolerances specified in the following table are established for residues of flupyradifurone, including its metabolites and degradates, in or on the commodities in the table. Compliance with the tolerance levels specified in this paragraph (b) is to be determined by measuring only flupyradifurone,4-[[(6-chloro-3-pyridinyl)methyl](2,2-difluoroethyl)amino]-2(5H)-furanone, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemption. The tolerances expire on the date specified in the table.

Table 2 to Paragraph (b)

Commodity Parts per million Expiration date
Sugarcane, cane 3 12/31/2028
Sugarcane, molasses 90 12/31/2028

(c) Tolerances with regional restrictions. Tolerances are established for residues of the insecticide flupyradifurone, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)methyl](2,2-difluoroethyl)amino]- 2(5H)-furanone.

Table 3 to Paragraph (c)

Commodity Parts per million
Clover, forage 20
Clover, hay 30
Grass, forage, fodder and hay, group 17 15

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 3487, Jan. 23, 2015, as amended at 81 FR 65557, Sept. 23, 2016; 82 FR 13256, Mar. 10, 2017; 85 FR 5578, Jan. 31, 2020; 85 FR 51671, Aug. 21, 2020; 86 FR 21947, Apr. 26, 2021; 88 FR 75506, Nov. 3, 2023; 90 FR 59393, Dec. 19, 2025]

§ 180.680 Fluensulfone; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide fluensulfone, including its metabolites and degradates, in or on the commodities in the table 1 to § 180.680. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of fluensulfone, 5-chloro-2-[(3,4,4-trifluoro-3-buten-1-yl)sulfonyl]thiazole and its metabolite, 3,4,4-trifluoro-but-3-ene-1-sulfonic acid, calculated as the stoichiometric equivalent of fluensulfone, in or on the commodity.

Table 1 to § 180.680

Commodity Parts per million
Almond, hulls 5
Berry, low growing, subgroup 13-07G 0.5
Brassica, head and stem, subgroup 5A 1.5
Brassica, leafy greens, subgroup 4-16B 20
Celtuce 4
Fennel, Florence, fresh leaves and stalk 4
Fruit, citrus, group 10-10 0.3
Fruit, citrus, group 10-10, dried pulp 0.9
Fruit, citrus, group 10-10, oil 15
Fruit, pome, group 11-10 0.4
Fruit, small, vine climbing, subgroup 13-07D 0.8
Fruit, stone, group 12-12 0.15
Grape, raisin 1.5
Kohlrabi 1.5
Leaf petiole vegetable subgroup 22B 2
Leafy greens subgroup 4-16A 4
Nut, tree, group 14-12 0.02
Potato, chips 2
Potato, granules/flakes 2
Soybean, seed 0.07
Sugarcane, cane 0.06
Sugarcane, molasses 0.3
Tomato, paste 1.5
Vegetable, Brassica, head and stem, group 5-16 1.5
Vegetables, cucurbits, group 9 0.7
Vegetables, fruiting, group 8-10 0.7
Vegetables, leafy, except Brassica, group 4 1 4
Vegetables, leaves of root and tuber, group 2, except sugar beet 50
Vegetables, root, except sugar beet, subgroup 1B 4
Vegetables, tuberous and corm, subgroup 1C 0.8
1 This tolerance expires on May 2, 2022.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the nematicide fluensulfone, including its metabolites and degradates, in or on the commodities in table 2 to § 180.680. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of fluensulfone, 5-chloro-2-[(3,4,4-trifluoro-3-buten-1-yl)sulfonyl]thiazole and its metabolite, 3,4,4-trifluoro-but-3-ene-1-sulfonic acid, calculated as the stoichiometric equivalent of fluensulfone, in or on the commodity.

Table 2 to § 180.680

Commodity Parts per
million
Barley, bran 0.15
Barley, grain 0.1
Barley, hay 15
Barley, straw 6
Buckwheat, grain 0.1
Grain, cereal, forage, fodder and straw, group 16 3
Grain, cereal, group 15 0.05
Oat, forage 6
Oat, grain 0.1
Oat, hay 15
Oat, straw 6
Wheat, bran 0.15
Wheat, forage 6
Wheat, germ 0.1
Wheat, grain 0.1
Wheat, hay 15
Wheat, milled byproducts 0.15
Wheat, straw 6

[84 FR 24047, May 24, 2019, as amended at 86 FR 46159, Aug. 18, 2021; 86 FR 60182, Nov. 1, 2021]

§ 180.681 Isofetamid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide isofetamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only isofetamid, N-[1,1-dimethyl-2-[2-methyl-4-(1-methylethoxy)phenyl]-2-oxoethyl]-3-methyl-2-thiophenecarboxamide, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 20
Apple, wet pomace 2.0
Bean, adzuki, dry seed 0.04
Bean, American potato, dry seed 0.04
Bean, asparagus, dry seed 0.04
Bean, asparagus, edible podded 0.6
Bean, black, dry seed 0.04
Bean, broad, dry seed 0.04
Bean, broad, succulent shelled 0.04
Bean, catjang, dry seed 0.04
Bean, catjang, edible podded 0.6
Bean, catjang, succulent shelled 0.04
Bean, cranberry, dry seed 0.04
Bean, dry, dry seed 0.04
Bean, field, dry seed 0.04
Bean, French, dry seed 0.04
Bean, French, edible podded 0.6
Bean, garden, dry seed 0.04
Bean, garden, edible podded 0.6
Bean, goa, dry seed 0.04
Bean, goa, edible podded 0.6
Bean, goa, succulent shelled 0.04
Bean, great northern, dry seed 0.04
Bean, green, dry seed 0.04
Bean, green, edible podded 0.6
Bean, guar, dry seed 0.04
Bean, guar, edible podded 0.6
Bean, kidney, dry seed 0.04
Bean, kidney, edible podded 0.6
Bean, lablab, dry seed 0.04
Bean, lablab, edible podded 0.6
Bean, lablab, succulent shelled 0.04
Bean, lima, dry seed 0.04
Bean, lima, succulent shelled 0.04
Bean, morama, dry seed 0.04
Bean, moth, dry seed 0.04
Bean, moth, edible podded 0.6
Bean, moth, succulent shelled 0.04
Bean, mung, dry seed 0.04
Bean, mung, edible podded 0.6
Bean, navy, dry seed 0.04
Bean, navy, edible podded 0.6
Bean, pink, dry seed 0.04
Bean, pinto, dry seed 0.04
Bean, red, dry seed 0.04
Bean, rice, dry seed 0.04
Bean, rice, edible podded 0.6
Bean, scarlet runner, dry seed 0.04
Bean, scarlet runner, edible podded 0.6
Bean, scarlet runner, succulent shelled 0.04
Bean, snap, edible podded 0.6
Bean, sword, dry seed 0.04
Bean, sword, edible podded 0.6
Bean, tepary, dry seed 0.04
Bean, urd, dry seed 0.04
Bean, urd, edible podded 0.6
Bean, wax, edible podded 0.6
Bean, wax, succulent shelled 0.04
Bean, yardlong, dry seed 0.04
Bean, yardlong, edible podded 0.6
Bean, yellow, dry seed 0.04
Berry, low growing, subgroup 13-07G 4.0
Bushberry subgroup 13-07B 5.0
Caneberry subgroup 13-07A 4.0
Canola, refined oil 0.03
Cherry subgroup 12-12A 4.0
Chickpea, dry seed 0.04
Chickpea, edible podded 1.5
Chickpea, succulent shelled 0.04
Cowpea, dry seed 0.04
Cowpea, edible podded 0.6
Cowpea, succulent shelled 0.04
Edible podded pea, edible podded 1.5
Flax, seed, oil 0.03
Fruit, pome, group 11-10 0.60
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0
Fruit, small vine climbing, except grape, subgroup 13-07E 10.0
Ginseng 3
Gram, horse, dry seed 0.04
Grape, raisin 5.0
Grass pea, dry seed 0.04
Grass pea, edible podded 1.5
Jackbean, dry seed 0.04
Jackbean, edible podded 0.6
Jackbean, succulent shelled 0.04
Lentil, dry seed 0.04
Lentil, edible podded 1.5
Lentil, succulent shelled 0.04
Lettuce, head 5.0
Lettuce, leaf 7.0
Longbean, Chinese, dry seed 0.04
Longbean, Chinese, edible podded 0.6
Lupin, Andean, dry seed 0.04
Lupin, Andean, succulent shelled 0.04
Lupin, blue, dry seed 0.04
Lupin, blue, succulent shelled 0.04
Lupin, grain, dry seed 0.04
Lupin, grain, succulent shelled 0.04
Lupin, sweet white, dry seed 0.04
Lupin, sweet white, succulent shelled 0.04
Lupin, sweet, dry seed 0.04
Lupin, sweet, succulent shelled 0.04
Lupin, white, dry seed 0.04
Lupin, white, succulent shelled 0.04
Lupin, yellow, dry seed 0.04
Lupin, yellow, succulent shelled 0.04
Mustard, seed, oil 0.03
Nut, tree, group 14-12 0.15
Pea, blackeyed, succulent shelled 0.04
Pea, crowder, dry seed 0.04
Pea, crowder, succulent shelled 0.04
Pea, dry, dry seed 0.04
Pea, dwarf, edible podded 1.5
Pea, English, succulent shelled 0.04
Pea, field, dry seed 0.04
Pea, garden, dry seed 0.04
Pea, garden, succulent shelled 0.04
Pea, green, dry seed 0.04
Pea, green, edible podded 1.5
Pea, green, succulent shelled 0.04
Pea, pigeon, dry seed 0.04
Pea, pigeon, edible podded 1.5
Pea, pigeon, succulent shelled 0.04
Pea, snap, edible podded 1.5
Pea, snow, edible podded 1.5
Pea, southern, succulent shelled 0.04
Pea, sugar snap, edible podded 1.5
Pea, winged, dry seed 0.04
Pea, winged, edible podded 0.6
Peach subgroup 12-12B 3.0
Plum subgroup 12-12C 0.80
Plum, Prune, Dried 1.50
Rapeseed subgroup 20A 0.015
Sesame, oil 0.03
Soybean, vegetable, dry seed 0.04
Soybean, vegetable, edible podded 0.6
Soybean, vegetable, succulent shelled 0.04
Velvetbean, dry seed 0.04
Velvetbean, edible podded 0.6
Velvetbean, succulent shelled 0.04
Yam bean, African, dry seed 0.04

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 45443, July 30, 2015, as amended at 81 FR 70974, Oct. 14, 2016; 82 FR 27154, June 14, 2017; 87 FR 45668, July 29, 2022; 91 FR 49283, Aug. 4, 2026]

§ 180.682 Bicyclopyrone; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide bicyclopyrone (4-hydroxy-3-[[2-[(2-methoxyethoxy)methyl]-6-(trifluoromethyl)-3-pyridinyl]carbonyl]bicyclo[3.2.1]oct-3-en-2-one), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph (a)(1) is to be determined by measuring only the sum of the common moieties SYN503780 (2-[(2-methoxyethoxy)methyl]-6-(trifluoromethyl)-3-pyridinecarboxylic acid) and CSCD686480 (2-[(2-hydroxyethoxy)methyl]-6-(trifluoromethyl)-3-pyridinecarboxylic acid), calculated as the stoichiometric equivalent of bicyclopyrone, in or on the commodities.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Banana 0.01
Barley, bran 0.15
Barley, grain 0.07
Barley, hay 0.30
Barley, straw 0.40
Broccoli 0.01
Cattle, meat byproducts 2.0
Corn, field, forage 0.30
Corn, field, grain 0.02
Corn, field, stover 0.40
Corn, pop, grain 0.02
Corn, pop, stover 0.40
Corn, sweet, forage 0.40
Corn, sweet, kernel plus cob with husks removed 0.03
Corn, sweet, stover 0.70
Goat, meat byproducts 2.0
Grain, aspirated fractions 0.30
Hog, meat byproducts 0.40
Hop, dried cones 0.04
Horse, meat byproducts 2.0
Horseradish 0.02
Lemongrass, dried 0.5
Lemongrass, fresh 0.3
Onion, bulb 0.02
Onion, green 0.05
Papaya 0.01
Rosemary, dried 0.3
Rosemary, fresh 0.03
Sheep, meat byproducts 2.0
Strawberry 0.01
Sugarcane, cane 1 0.02
Sweet potato, tuber 0.02
Timothy, forage 1.5
Timothy, hay 2
Watermelon 0.01
Wheat, bran 0.07
Wheat, forage 0.40
Wheat, grain 0.04
Wheat, hay 0.80
Wheat, straw 0.50
Wormwood, dried 0.09
Wormwood, fresh 0.05
1 There are no U.S. Registration on Sugarcane as of March 13, 2015.

(2) [Reserved]

(b) [Reserved]

[80 FR 22654, Apr. 23, 2015, as amended at 81 FR 86965, Dec. 2, 2016; 86 FR 72851, Dec. 23, 2021; 87 FR 15339, Mar. 18, 2022]

§ 180.684 Benalaxyl-M; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide benalaxyl-M, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only benalaxyl [methyl N-(2,6-dimethylphenyl)-N-(phenylacetyl)-DL-alaninate] in or on the commodity.

Commodity Parts per million
Grape 1 3.0
Tomato 1 0.20
1 There is no U.S. registration for use on this commodity as of July 30, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 45448, July 30, 2015]

§ 180.685 Oxathiapiprolin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide oxathiapiprolin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.

Commodity Parts per million
Almond, hulls 0.05
Basil, dried leaves 80
Basil, fresh leaves 10
Berry, low growing, subgroup 13-07G, except cranberry 0.4
Brassica leafy greens subgroup 4-16B 10
Bushberry subgroup 13-07B, except lowbush blueberry 0.5
Cacao bean, dried bean 0.15
Caneberry subgroup 13-07A 0.50
Chickpea, edible podded 1
Chickpea, succulent shelled 0.05
Citrus, dried pulp 0.09
Citrus, oil 2.0
Fruit, citrus, group 10-10 0.06
Ginseng 0.15
Grape 1 0.70
Hop, dried cones 5
Leafy greens subgroup 4-16A 15
Lentil, edible podded 1
Lentil, succulent shelled 0.05
Nut, tree, group 14-12 0.01
Onion, bulb, subgroup 3-07A 0.04
Onion, green, subgroup 3-07B 2.0
Pea, dwarf, edible podded 1
Pea, edible podded 1
Pea, English, succulent shelled 0.05
Pea, garden, succulent shelled 0.05
Pea, grass, edible podded 1
Pea, green, edible podded 1
Pea, green, succulent shelled 0.05
Pea, pigeon, edible podded 1
Pea, pigeon, succulent shelled 0.05
Pea, snap, edible podded 1
Pea, snow, edible podded 1
Pea, sugar snap, edible podded 1
Potato, wet peel 0.07
Soybean, seed 0.01
Stalk and stem vegetable subgroup 22A 2.0
Sunflower, seed 0.01
Tomato, dried 3.0
Tropical and subtropical, medium to large fruit, smooth, inedible peel, subgroup 24B 0.1
Vegetable, Brassica head and stem, group 5-16 1.5
Vegetable, cucurbit, group 9 0.20
Vegetable, fruiting, group 8-10 0.50
Vegetable, tuberous and corm, subgroup 1C 0.04
1 There is no associated U.S. registration as of September 4, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide oxathiapiprolin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]-1-piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.

Table 2 to Paragraph (d)

Commodity Parts per
million
All other food commodities/feed commodities (other than those covered by a higher tolerance as a result of use on growing crops or indirect or inadvertent residues) 0.10
Peanut, hay 0.15

[80 FR 53473, Sept. 4, 2015, as amended at 81 FR 87467, Dec. 5, 2016; 82 FR 44945, Sept. 27, 2017; 85 FR 40121, July 6, 2020; 88 FR 82274, Nov. 24, 2023]

§ 180.686 Benzovindiflupyr; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide benzovindiflupyr, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only benzovindiflupyr (N-[9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalen-5-yl]-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxamide) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, grain 1.5
Barley, hay 15.0
Barley, straw 15.0
Beet, sugar, dried pulp 0.6
Beet, sugar, leaves 0.07
Beet, sugar, roots 0.08
Blueberry, lowbush 2
Bluegrass, forage 0.15
Bluegrass, hay 7.0
Bluegrass, straw 6.0
Bromegrass, forage 0.15
Bromegrass, hay 7.0
Bromegrass, straw 6.0
Cattle, fat 0.02
Cattle, liver 0.06
Cattle, meat 0.01
Cattle, meat byproducts, except liver 0.01
Coffee, green bean1 0.09
Corn, field, forage 3.0
Corn, field, grain 0.02
Corn, field, stover 15.0
Corn, pop, grain 0.02
Corn, pop, stover 15.0
Corn, sweet, forage 4.0
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 5.0
Cottonseed, subgroup 20C 0.15
Cotton, gin byproducts 3.0
Fescue, forage 0.15
Fescue, hay 7.0
Fescue, straw 6.0
Fruit, pome, group 11-10 0.20
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0
Goat, fat 0.02
Goat, liver 0.06
Goat, meat 0.01
Goat, meat byproducts, except liver 0.01
Grain, aspirated fractions 15.0
Grape, raisin 3.0
Horse, fat 0.02
Horse, liver 0.06
Horse, meat 0.01
Horse, meat byproducts, except liver 0.01
Milk 0.01
Milk, fat 0.02
Oat, grain 1.5
Oat, hay 15.0
Oat, straw 15.0
Onion, bulb, subgroup 3-07A 0.02
Onion, green, subgroup 3-07B 0.40
Orchardgrass, forage 0.15
Orchardgrass, hay 7.0
Orchardgrass, straw 6.0
Pea and bean, dried shelled, except soybean, subgroup 6C 0.20
Pea, field, hay 7.0
Pea, field, vine 1.5
Peanut 0.01
Peanut, hay 15.0
Potato, processed potato waste 0.10
Rapeseed, subgroup 20A 0.15
Rye, grain 0.1
Rye, hay 15.0
Rye, straw 15.0
Ryegrass, forage 0.15
Ryegrass, hay 7.0
Ryegrass, straw 6.0
Sheep, fat 0.02
Sheep, liver 0.06
Sheep, meat 0.01
Sheep meat byproducts, except liver 0.01
Soybean, forage 15.0
Soybean, hay 50.0
Soybean, hulls 0.20
Soybean, seed 0.07
Sugarcane, cane 0.30
Tomato, dried 4.0
Vegetable, cucurbit, group 9 0.30
Vegetable, fruiting, group 8-10 1.5
Vegetable, root, except sugar beet, subgroup 1B 0.6
Vegetable, tuberous and corm, subgroup 1C 0.02
Wheat, forage 4.0
Wheat, grain 0.10
Wheat, hay 15.0
Wheat, straw 15.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 59633, Oct. 2, 2015, as amended at 82 FR 52674, Nov. 14, 2017; 83 FR 29038, June 22, 2018; 86 FR 8707, Feb. 9, 2021; 87 FR 59027, Sept. 29, 2022]

§ 180.687 Teflubenzuron; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide teflubenzuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only teflubenzuron (N-[[(3,5-dichloro-2,4-difluorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Apple 1 1.0
Broccoli 1 0.20
Cauliflower 1 0.01
Citrus, oil 1 100
Coffee, bean, green 1 0.60
Corn, field, grain 1 0.01
Corn, field, refined oil 1 0.02
Grape 1 0.7
Grape, raisin 1 0.9
Lemon 1 0.80
Mango 1 1.5
Melon, subgroup 9A 1 0.30
Orange 1 0.60
Papaya 1 0.50
Pineapple 1 0.80
Soybean, seed 1 0.05
Soybean, hulls 1 0.15
Sugarcane, cane 1 0.01
Sunflower, seed 1 0.30
Tomato 1 1.5
1 Tolerance without U.S. registration.

(2) [Reserved]

(b)-(d) [Reserved]

[80 FR 66809, Oct. 30, 2015, as amended at 87 FR 34209, June 6, 2022]

§ 180.688 Diethofencarb; tolerance for residue.

(a) General.

(1) Tolerances are established for residues of the fungicide diethofencarb, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only diethofencarb (1-methylethyl N-(3,4-diethoxyphenyl)carbamate).

Commodity Parts per
million
Banana * 0.10
* There is no U.S. registration for use on this commodity as of November 4, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues [Reserved]

[80 FR 68261, Nov. 4, 2015]

§ 180.689 Aminocyclopyrachlor; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide aminocyclopyrachlor, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of aminocyclopyrachlor, 6-amino-5-chloro-2-cyclopropyl-4-pyrimidinecarboxylic acid, and aminocyclopyrachlor methyl ester, methyl 6-amino-5-chloro-2-cyclopropyl-4-pyrimidinecarboxylate, calculated as the stoichiometric equivalent of aminocyclopyrachlor.

Commodity Parts per million
Cattle, fat 1 0.05
Cattle, meat 1 0.01
Cattle, meat byproducts 1 0.30
Goat, fat 1 0.05
Goat, meat 1 0.01
Goat, meat byproducts 1 0.30
Horse, fat 1 0.05
Horse, meat 1 0.01
Horse, meat byproducts 1 0.30
Milk 1 0.01
Sheep, fat 1 0.05
Sheep, meat 1 0.01
Sheep, meat byproducts 1 0.30
1 There are no U.S. registrations as of August 11, 2016.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[81 FR 53018, Aug. 11, 2016]

§ 180.690 Mandestrobin; tolerances for residues.

(a) General. Tolerances are established for residues of mandestrobin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only mandestrobin, 2-[(2,5-dimethylphenoxy)methyl]-α-methoxy-N-methylbenzeneacetamide.

Table 1 to Paragraph (a)

Commodity Parts per
million
Berry, low growing, subgroup 13-07G, except cranberry 3.0
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0
Grape, raisin 7.0
Lettuce, head 0.08
Lettuce, leaf 4
Rapeseed subgroup 20A 0.2
Vegetable, tuberous and corm, except potato, subgroup 1D 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent tolerances. [Reserved]

[81 FR 70043, Oct. 11, 2016, as amended at 87 FR 29056, May 12, 2022; 88 FR 14498, Mar. 9, 2023]

§ 180.691 Halauxifen-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, halauxifen-methyl, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only halauxifen-methyl (methyl (4-amino-3-chloro-6-(4-chloro-2-fluoro-3-methoxyphenyl)-2-pyridine carboxylate).

Commodity Parts per million
Barley, grain 0.01
Barley, hay 0.01
Barley, straw 0.01
Wheat, forage 0.50
Wheat, grain 0.01
Wheat, hay 0.03
Wheat, straw 0.015

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[81 FR 53025, Aug. 11, 2016]

§ 180.692 Tioxazafen; tolerances for residues.

(a) General. Tolerances are established for residues of tioxazafen, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring the combined residues of tioxazafen [3-phenyl-5-(2-thienyl)-1,2,4-oxadiazole] and benzamidine, expressed as tioxazafen in or on the commodity.

Commodity Parts
per million
Corn, field, forage 0.02
Corn, field, grain 0.02
Corn, field, stover 0.02
Cotton, gin by-products 0.02
Cotton, undelinted seed 0.02
Soybean, forage 0.15
Soybean, hay 0.30
Soybean, meal 0.05
Soybean, seed 0.04

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 20283, May 1, 2017]

§ 180.693 Benzobicyclon; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide benzobicyclon, including its metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be determined by measuring only benzobicyclon, 3-[2-chloro-4-(methylsulfonyl)benzoyl]-4-(phenylthio)bicyclo-[3.2.1]oct-3-en-2-one), in or on the following raw agricultural commodity:

Table 1 to § 180.693(a)

Commodity Parts per
million
Rice, grain 0.15

(b)-(d) [Reserved]

[86 FR 60391, Nov. 2, 2021]

§ 180.694 Cyclaniliprole; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide cyclaniliprole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only cyclaniliprole, 3-bromo-N-[2-bromo-4-chloro-6-[[(1-cyclopropylethyl)amino]carbonyl]phenyl]-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts
per million
Almond, hulls 6.0
Apple, wet pomace 0.50
Artichoke, globe 1.5
Berry, low growing, subgroup 13-07G 0.4
Bushberry subgroup 13-07B 1.5
Caneberry subgroup 13-07A 0.8
Cattle, fat 0.015
Cattle, meat 0.01
Cattle, meat byproducts 0.015
Fruit, citrus, group 10-10, oil 30
Fruit, pome, group 11-10 0.30
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.80
Fruit, small, vine climbing, except grape, subgroup 13-07E 1
Fruit, stone, group 12-12 1.0
Goat, fat 0.015
Goat, meat 0.01
Goat, meat byproducts 0.015
Grapefruit subgroup 10-10C 0.2
Horse, fat 0.015
Horse, meat 0.01
Horse, meat byproducts 0.015
Lemon/lime subgroup 10-10B 0.3
Milk 0.015
Nut, tree, group 14-12 0.03
Orange subgroup 10-10A 0.4
Pepper/eggplant subgroup 8-10B 1.5
Potato, wet peel 0.06
Sheep, fat 0.015
Sheep, meat 0.01
Sheep, meat byproducts 0.015
Sunflower subgroup 20B 0.4
Tea, dried 1 50
Tomato subgroup 8-10A 0.7
Vegetable, Brassica, head and stem, group 5-16 1.0
Vegetable, cucurbit, group 9 0.3
Vegetable, leafy, group 4-16 15
Vegetable, tuberous and corm, subgroup 1C 0.01
1 There are no U.S. registrations for tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 36094, Aug. 3, 2017, as amended at 84 FR 50763, Sept. 26, 2019; 87 FR 69204, Nov. 18, 2022; 89 FR 30280, Apr. 23, 2024]

§ 180.696 Tolpyralate; tolerances for residues.

(a)

(1) General. Tolerances are established for residues of tolpyralate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only tolpyralate, 1-[[1-ethyl-4-[3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)benzoyl]-1H-pyrazol-5-yl]oxy]ethyl methyl carbonate, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Barley, grain 0.01
Barley, hay 0.2
Barley, straw 0.08
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 0.01
Wheat, forage 0.02
Wheat, grain 0.01
Wheat, hay 0.05
Wheat, straw 0.03

(2) Tolerances are established for residues of tolpyralate, 1-[[1-ethyl-4-[3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)benzoyl]-1H-pyrazol-5-yl]oxy]ethyl methyl carbonate and metabolite MT-2153 [1-ethyl-5-hydroxy-1H-pyrazol-4-yl-3-(2-methoxyethoxy)-4-mesyl-2-methylphenyl ketone], in or on the livestock commodities in table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in table 2 to this paragraph (a)(2) is to be determined by measuring tolpyralate, 1-[[1-ethyl-4-[3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)benzoyl]-1H-pyrazol-5-yl]oxy]ethyl methyl carbonate and metabolite MT-2153 [1-ethyl-5-hydroxy-1H-pyrazol-4-yl-3-(2-methoxyethoxy)-4-mesyl-2-methylphenyl ketone], in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Cattle, byproducts 0.02
Goat, byproducts 0.02
Horse, byproducts 0.02
Sheep, byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 34882, July 27, 2017, as amended at 88 FR 82786, Nov. 27, 2023]

§ 180.697 Flutianil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide flutianil, including its metabolites and degradates in or on food commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only flutianil, (2Z)-2-[2-fluoro-5-(trifluoromethyl)phenyl]sulfanyl-2-[3-(2-methoxyphenyl)thiazolidin-2-ylidene]acetonitrile in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Apple 0.15
Apple, wet pomace 0.30
Berry, low growing, subgroup 13-07G 0.5
Cherry subgroup 12-12A 0.4
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.7
Hop, dried cones 2
Melon subgroup 9A 0.07
Squash/cucumber subgroup 9B 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 12268, Mar. 21, 2018, as amended at 84 FR 70026, Dec. 20, 2019]

§ 180.698 Chlormequat chloride; tolerances for residues.

(a) General. Tolerances are established for the residues of the plant regulator chlormequat chloride, including its metabolites and degradates in or on food commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only chlormequat chloride [(2-chloroethyl) trimethylammonium chloride in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Barley, bran 20
Barley, grain 8
Barley, hay 150
Barley, straw 60
Cattle, meat byproducts 1
Cattle, meat 0.2
Egg 0.1
Goat, meat byproducts 1
Goat, meat 0.2
Hog, meat byproducts1 0.5
Hog, meat1 0.2
Horse, meat byproducts 1
Horse, meat 0.2
Milk 0.5
Oat, grain 40
Oat, forage 15
Oat, hay 150
Oat, straw 50
Poultry, meat byproducts 0.1
Poultry, meat 0.05
Sheep, meat byproducts 1
Sheep, meat 0.2
Wheat, bran 15
Wheat, germ 20
Wheat, grain 5
Wheat, forage 30
Wheat, hay 150
Wheat, straw 70
1 This tolerance expires December 30, 2026.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 17929, Apr. 25, 2018, as amended at 85 FR 31386, May 26, 2020, as amended at 91 FR 39493, June 30, 2026]

§ 180.699 Pydiflumetofen; tolerances for residues.

(a) General. Tolerances are established for residues of pydiflumetofen, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only pydiflumetofen (3-(difluoromethyl)-N-methoxy-1-methyl-N-[1-methyl-2-(2,4,6-trichlorophenyl)ethyl]-1H-pyrazole-4-carboxamide) in or on the commodity:

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 9
Apple, wet pomace 1
Barley, grain 4.0
Barley, hay 30
Barley, straw 30
Berry, low growing, subgroup 13-07G 1
Brassica, leafy greens, subgroup 4-16B 50
Bushberry subgroup 13-07B 5
Caneberry subgroup 13-07A 5
Cattle, fat 0.03
Cattle, meat 0.01
Cattle, meat byproducts 0.03
Cherry subgroup 12-12A 2
Coffee, green bean 1 0.2
Corn, field, flour 0.02
Corn, field, forage 6.0
Corn, field, grain 0.015
Corn, field, milled byproducts 0.06
Corn, field, stover 15
Corn, pop, forage 6.0
Corn, pop, grain 0.015
Corn, pop, stover 10
Corn, sweet, forage 5.0
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 9.0
Cotton, gin byproducts 7
Cottonseed subgroup 20C 0.4
Dragon fruit 1 0.9
Fruit, citrus, group 10-10 1
Fruit, citrus, group 10-10, oil 30
Fruit, pome, group 11-10 0.2
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.5
Goat, fat 0.03
Goat, meat 0.01
Goat, meat byproducts 0.03
Grain, aspirated fractions 100
Grape, raisin 2.0
Horse, fat 0.03
Horse, meat 0.01
Horse, meat byproducts 0.03
Leaf petiole vegetable subgroup 22B 15
Leafy greens subgroup 4-16A 40
Milk 0.03
Nut, tree, group 14-12 0.07
Oat, forage 10
Oat, grain 3.0
Oat, hay 40
Oat, straw 20
Onion, bulb, subgroup 3-07A 0.2
Onion, green, subgroup 3-07B 2
Pea and bean, succulent shelled, subgroup 6B 0.1
Pea, field, forage 6.0
Pea, field, hay 40
Peach subgroup 12-12B 1
Peanut 0.02
Peanut, hay 30
Peanut, refined oil 0.05
Peas and bean, dried shelled, except soybean, subgroup 6C 0.40
Plum, prune, dried 1
Plum subgroup 12-12C 0.6
Potato, processed potato waste 0.03
Potato, wet peel 0.03
Quinoa, grain 4.0
Rapeseed subgroup 20A 0.90
Rye, grain 0.30
Rye, hay 50
Rye, straw 30
Sheep, fat 0.03
Sheep, meat 0.01
Sheep, meat byproducts 0.03
Sorghum, grain, forage 1.5
Sorghum, grain, grain 3
Sorghum, grain, stover 10
Soybean, seed 0.40
Sunflower subgroup 20B 0.5
Tomato, dried 3.0
Vegetable, Brassica, head and stem, group 5-16 3
Vegetable, cucurbit, group 9 0.50
Vegetable, fruiting, group 8-10 0.60
Vegetable, leaves of root and tuber, group 2 10
Vegetable, legume, edible podded, subgroup 6A 1
Vegetable, root, subgroup 1A 0.5
Vegetable, tuberous and corm subgroup 1C 0.015
Wheat, forage 15
Wheat, germ 0.40
Wheat, grain 0.30
Wheat, hay 50
Wheat, milled byproducts 2.0
Wheat, straw 30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of pydiflumetofen, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (d). Compliance with the tolerance levels specified in table 2 to this paragraph (d) is to be determined by measuring only pydiflumetofen (3-(difluoromethyl)-N-methoxy-1-methyl-N-[1-methyl-2-(2,4,6-trichlorophenyl)ethyl]-1H-pyrazole-4-carboxamide) in or on the commodity:

Table 2 to Paragraph (d)

Commodity Parts per
million
Animal feed, nongrass, group 18, hay 0.04
Grass, forage, fodder and hay, group 17, except straw 0.7
Grass, forage, fodder and hay, group 17, straw 0.04
Sugarcane, cane 0.05

[83 FR 24044, May 24, 2018, as amended at 84 FR 39767, Aug. 12, 2019; 85 FR 55196, Sept. 4, 2020; 88 FR 9756, Feb. 15, 2023; 91 FR 8095, Feb. 20, 2026; 91 FR 35892, June 15, 2026]

§ 180.700 Afidopyropen; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of afidopyropen, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in this paragraph (a)(1) is to be determined by measuring only afidopyropen, [(3S,4R,4aR,6S,6aS,12R,12aS,12bS)-3-[(cyclopropylcarbonyl)oxy]-1,3,4,4a,5,6a,12,12a,12b-decahydro-6,12-dihydroxy-4,6a,12b-trimethyl-11-oxo-9-(3-pyridinyl)2H,11H-naphtho[2,1-b]pyrano[3,4-e]pyran-4-yl]methyl cyclopropanecarboxylate, in or on the following food commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Alfalfa, seed 0.3
Almond, hulls 0.3
Animal feed, nongrass, group 18, forage 4
Animal feed, nongrass, group 18, hay 9
Animal feed, nongrass, group 18, straw 5
Apple, wet pomace 0.05
Brassica, head and stem, group 5-16 0.50
Brassica, leafy greens, subgroup 4-16B 5.0
Citrus, oil 0.40
Cotton, gin byproducts 2.0
Cotton, undelinted seed 0.08
Fruit, citrus, group 10-10 0.15
Fruit, pome, group 11-10 0.02
Fruit, stone, group 12-12 0.03
Grain, aspirated fractions 60
Grass, forage, fodder and hay, group 17 10
Leafy Greens, subgroup 4-16A 2.0
Leaf petiole vegetable subgroup 22B 3.0
Lettuce, leaf 7
Nut, tree, group 14-12 0.01
Sorghum, grain, forage 0.3
Sorghum, grain, grain 0.15
Sorghum, grain, stover 0.3
Sorghum, sweet, forage 0.3
Sorghum, sweet, grain 0.15
Sorghum, sweet, stalk 0.3
Sorghum, sweet, stover 0.3
Soybean, forage 0.15
Soybean, hay 0.4
Soybean, seed 0.01
Strawberry 0.3
Tomato, dried 0.50
Vegetable, cucurbit, group 9 0.70
Vegetable, fruiting, group 8-10 0.2
Vegetable, tuberous and corm, subgroup 1C 0.01

(2) Tolerances are established for residues of afidopyropen, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in this paragraph (a)(2) is to be determined by measuring only the sum of afidopyropen, [(3S,4R,4aR,6S,6aS,12R,12aS,12bS)-3-[(cyclopropylcarbonyl)oxy]-1,3,4,4a,5,6a,12,12a,12b-decahydro-6,12-dihydroxy-4,6a,12b-trimethyl-11-oxo-9-(3-pyridinyl)2H,11H-naphtho[2,1-b]pyrano[3,4-e]pyran-4-yl]methyl cyclopropanecarboxylate and its metabolite cyclopropanecarboxylic acid carnitine (CPCA-carnitine), calculated as the stoichiometric equivalent of afidopyropen in or on the following animal commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, meat 0.2
Cattle, meat byproducts 0.2
Goat, meat 0.2
Goat, meat byproducts 0.2
Horse, meat 0.2
Horse, meat byproducts 0.2
Milk 0.04
Sheep, meat 0.2
Sheep, meat byproducts 0.2

(b) [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 46401, Sept. 13, 2018, as amended at 85 FR 63459, Oct. 8, 2020; 89 FR 51848, June 20, 2024; 90 FR 34608, July 23, 2025; 91 FR 6789, Feb. 13, 2026]

§ 180.701 Pyrifluquinazon; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide pyrifluquinazon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyrifluquinazon (1-acetyl-3,4-dihydro-3-[(3-pyridinylmethyl)amino]-6-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-2(1H)-quinazolinone) and its metabolite IV-01 (3-[(pyridin-3-ylmethyl)amino]-6-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-3,4-dihydro-1H-quinazolin-2-one), calculated as the stoichiometric equivalent of pyrifluquinazon.

Commodity Parts per
million
Almond, hulls 0.60
Cherry subgroup 12-12A 0.30
Citrus, dried pulp 2.0
Citrus, oil 30
Cotton, gin byproducts 6.0
Cotton, undelinted seed 0.30
Fruit, citrus, group 10-10 0.70
Fruit, pome, group 11-10 0.07
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.30
Leaf petiole vegetable, subgroup 22B 1.5
Peach subgroup 12-12B 0.04
Plum subgroup 12-12C 0.02
Nut, tree, group 14-12 0.02
Tea, dried1 20
Vegetable, brassica, head and stem, group 5-16 0.60
Vegetable, cucurbit, group 9 0.07
Vegetable, fruiting, group 8-10 0.30
Vegetable, leafy, group 4-16 5.0
Vegetable, tuberous and corm, subgroup 1C 0.02
1 There are no U.S. registrations as of November 26, 2018 for use on tea.

(2) Tolerances are established for residues of the insecticide pyrifluquinazon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of pyrifluquinazon (1-acetyl-3,4-dihydro-3-[(3-pyridinylmethyl)amino]-6-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-2(1H)-quinazolinone) and the free and conjugated forms of its metabolites IV-01 (3-[(pyridin-3-ylmethyl)amino]-6-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-3,4-dihydro-1H-quinazolin-2-one) and IV-203 (6-[1,2,2,2-tetrafluoro-1-trifluoromethyl)ethyl]-1H-quinazolin-2,4-dione), calculated as the stoichiometric equivalent of pyrifluquinazon.

Commodity Parts per
million
Cattle, liver 0.04
Goat, liver 0.04
Horse, liver 0.04
Sheep, liver 0.04

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 60371, Nov. 26, 2018]

§ 180.702 Bixafen; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide bixafen, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only bixafen, N-(3,4-dichloro-5-fluorobiphenyl-2-yl)-3-(difluoromethyl)-1-methylpyrazole-4-carboxamide, in or on the commodity.

Commodity Parts per million
Beet, sugar, dried pulp 1.0
Grain, aspirated grain fractions 80
Grain, cereal, forage, fodder, and straw, group 16, except rice 20
Grain, cereal, group 15, except rice and grain sorghum 0.40
Peanut 0.01
Peanut, hay 8.0
Radish, tops 3.0
Sorghum, grain, grain 3.0
Soybean, hulls 0.15
Soybean, seed 0.04
Vegetable, root, subgroup 1A 0.30
Vegetable, tuberous and corm, subgroup 1C 0.01

(2) Tolerances are established for residues of the fungicide bixafen, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of bixafen, N-(3,4-dichloro-5-fluorobiphenyl-2-yl)-3-(difluoromethyl)-1-methylpyrazole-4-carboxamide, and its desmethyl metabolite, N-(3′,4′-dichloro-5-fluoro[1,1′-biphenyl]-2-yl)-3-(difluoromethyl)-1H-pyrazole-4-carboxamide, calculated as the stoichiometric equivalent of bixafen, in or on the commodity.

Commodity Parts per million
Cattle, fat 0.08
Cattle, meat byproducts 0.40
Cattle, muscle 0.08
Goat, fat 0.08
Goat, meat byproducts 0.40
Goat, muscle 0.08
Horse, fat 0.08
Horse, meat byproducts 0.40
Horse, muscle 0.08
Milk 0.04
Sheep, fat 0.08
Sheep, meat byproducts 0.40
Sheep, muscle 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 62485, Dec. 4, 2018]

§ 180.703 6-benzyladenine; tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator, 6-benzyladenine in or on the commodities listed in the table below. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only 6-benzyladenine in or on the commodity.

Commodity Parts per
million
Avocado 0.02
Cucumber 0.01
Melon 0.01
Pepper 0.01
Squash 0.01
Tomato 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[83 FR 64030, Dec. 13, 2018]

§ 180.704 Sulfometuron-methyl; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide sulfometuron-methyl, including its metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only sulfometuron-methyl, (methyl 2-[[[[(4,6-dimethyl-2-pyrimidinyl)amino]carbonyl]amino]sulfonyl]benzoate), in or on the following raw agricultural commodities:

Commodity Parts per
million
Sugarcane, cane 1 0.1
1 There are no U.S. Registrations on Sugarcane as of September 24, 2018.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[84 FR 11420, Mar. 27, 2019]

§ 180.705 Mefentrifluconazole; tolerances for residues.

(a) General. Tolerances are established for residues of mefentrifluconazole, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only mefentrifluconazole, α-[4-(4-chlorophenoxy)-2-(trifluoromethyl)phenyl]-α-methyl-1H-1,2,4-triazole-1-ethanol, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 4
Animal feed, nongrass, group 18, forage 15
Animal feed, nongrass, group 18, hay 30
Banana 1 1.5
Beet, sugar, dried pulp 2
Beet, sugar, leaves 9
Beet, sugar, roots 0.6
Berry, low growing, subgroup 13-07G 2
Bushberry, subgroup 13-07B 5
Caneberry, subgroup 13-07A 3
Cattle, fat 1
Cattle, meat 0.15
Cattle, meat byproducts 1.5
Cherry subgroup 12-12A 4
Coffee, green bean 1 0.4
Corn, field, grain 0.01
Corn, milled byproducts 0.03
Corn, pop, grain 0.01
Corn, sweet, kernel plus cob with husks removed 0.03
Cotton, gin byproducts 10
Cottonseed subgroup 20C 0.2
Egg 0.01
Fruit, citrus, group 10-10, dried pulp 2
Fruit, citrus, group 10-10, oil 15
Fruit, pome, group 11-10 1.5
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.5
Goat, fat 1
Goat, meat 0.15
Goat, meat byproducts 1.5
Grain, aspirated grain fractions 6
Grain, cereal, forage, fodder, and straw, group 16, forage 6
Grain, cereal, forage, fodder, and straw, group 16, hay 15
Grain, cereal, forage, fodder, and straw, group 16, stover 9
Grain, cereal, forage, fodder, and straw, group 16, straw 30
Grain, cereal, group 15, except wheat and corn 4
Grape, raisin 4
Grapefruit subgroup 10-10C 0.5
Grass, forage, fodder and hay, group 17, forage 50
Grass, forage, fodder and hay, group 17, hay 100
Hog, fat 0.015
Hog, meat 0.01
Hog, meat byproducts 0.03
Horse, fat 1
Horse, meat 0.15
Horse, meat byproducts 1.5
Lemon/lime subgroup 10-10B 1
Lentil, dry, seed 2
Lettuce, head 5
Melon subgroup 9A 0.5
Milk 0.15
Milk, fat 4
Nut, tree, group 14-12 0.06
Onion, bulb, subgroup 3-07A 0.2
Onion, green, subgroup 3-07B 4
Orange subgroup 10-10A 0.6
Peach subgroup 12-12B 1.5
Peanut 0.01
Peanut, hay 30
Plum prune, dried 4
Plum subgroup 12-12C 2
Poultry, fat 0.015
Poultry, meat 0.015
Poultry, meat byproducts 0.015
Rapeseed subgroup 20A 1
Sheep, fat 1
Sheep, meat 0.15
Sheep, meat byproducts 1.5
Soybean, seed 0.4
Squash/cucumber subgroup 9B 0.2
Sugarcane, cane 1.5
Sunflower subgroup 20B 0.15
Tomato, dried 4
Vegetable, foliage of legume, group 7 20
Vegetable, fruiting, group 8-10 0.9
Vegetable, leafy, group 4-16, except head lettuce 30
Vegetable, leaves of root and tuber, group 2 20
Vegetable, legume, group 6, except lentil and soybean seed 0.15
Vegetable, root, except sugar beet, subgroup 1B 0.7
Vegetable, tuberous and corm, subgroup 1C 0.04
Wheat, grain 0.3
1 There are no U.S. registrations as of December 15, 2021.

(b)-(d) [Reserved]

[84 FR 30945, June 28, 2019, as amended at 85 FR 71000, Nov. 6, 2020; 86 FR 71158, Dec. 15, 2021]

§ 180.706 Valifenalate; tolerances for residues.

(a)

(1) Tolerances are established for residues of the fungicide valifenalate, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring only valifenalate (methyl N-(isopropoxycarbonyl)-L-valyl-(3RS)-3-(4-chlorophenyl)-β-alainate), in or on the following commodities.

Commodity Parts per
million
Celery 5
Grape 1 5
Grape, raisin 1 6
Vegetable, bulb, group 3-07 0.6
Vegetable, cucurbit, group 9 0.3
Vegetable, fruiting, group 8-10 1
1 As of July 1, 2019, valifenalate is not registered in the United States for use on this commodity.

(2) Tolerances are established for residues of the fungicide valifenalate, including its metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring only the sum of valifenalate, methyl N-(isopropoxycarbonyl)-L-valyl-(3RS)-3-(4-chlorophenyl)-β-alainate and valifenalate acid, 3-(4-chlorophenyl)-3-[[N-(isopropoxycarbonyl)-L-valyl]-amino] propionic acid calculated as the stoichiometric equivalent of valifenalate, in or on the following commodities.

Commodity Parts per
million
Potato 0.04
Potato, granules/flakes 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[84 FR 31218, July 1, 2019]

§ 180.708 Isotianil; tolerances for residues.

(a) General. Tolerances are established for residues of isotianil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance level specified in the table in this paragraph (a) is to be determined by measuring only isotianil (3,4-dichloro-N-(2-cyanophenyl)-5-isothiazolecarboxamide) in or on the commodity.

Commodity Parts per million
Banana 1 0.02
1 There are no U.S. registrations for bananas as of November 1, 2019.

(b) [Reserved]

[84 FR 58627, Nov. 1, 2019]

§ 180.709 Tetraniliprole; tolerances for residues.

(a) General. Tolerances are established for residues of tetraniliprole, including its metabolites and degradates, in or on the commodities in table 1 in this paragraph (a). Compliance with the tolerance levels specified in table 1 in this paragraph (a) is to be determined by measuring only tetraniliprole 1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-3-[[5-(trifluoromethyl)-2H-tetrazol-2-yl]methyl]-1H-pyrazole-5-carboxamide.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond, hulls 4
Cattle, fat 0.04
Cattle, meat 0.02
Cattle, meat byproducts 0.3
Corn, field, forage 4
Corn, field, grain 0.01
Corn, field, stover 15
Corn, pop, grain 0.01
Corn, pop, stover 15
Corn, sweet, forage 6
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 20
Fruit, citrus, group 10-10, oil 7
Fruit, pome, group 11-10 0.5
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.5
Fruit, stone, group 12-12 1
Goat, fat 0.04
Goat, meat 0.02
Goat, meat byproducts 0.3
Grain, aspirated fractions 50
Grain, cereal, forage, fodder and straw, group 16, except field corn, popcorn and sweet corn 0.1
Grain, cereal, group 15, except rice 0.01
Grapefruit subgroup 10-10C 0.9
Horse, fat 0.04
Horse, meat 0.02
Horse, meat byproducts 0.3
Lemon/lime subgroup 10-10B 1.5
Milk 0.05
Nut, tree, group 14-12 0.03
Orange subgroup 10-10A 1
Sheep, fat 0.04
Sheep, meat 0.02
Sheep, meat byproducts 0.3
Soybean, forage 0.07
Soybean, hay 0.2
Soybean, hulls 0.4
Soybean, seed 0.2
Tea, dried 1 80
Tomato, paste 1.5
Vegetable, brassica, head and stem, group 5-16 1.5
Vegetable, fruiting, group 8-10 0.4
Vegetable, leafy, group 4-16 20
Vegetable, tuberous and corm, subgroup 1C 0.015
1 There is no U.S. Registration for this commodity as of May 15, 2024.

(b)-(c) [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of tetraniliprole, including its metabolites and degradates, in or on the commodities in table 2 in this paragraph (d). Compliance with the tolerance levels specified in table 2 in this paragraph (d) is to be determined by measuring only tetraniliprole 1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-3-[[5-(trifluoromethyl)-2H-tetrazol-2-yl]methyl]-1H-pyrazole-5-carboxamide.

Table 2 to Paragraph (d)

Commodity Parts per
million
Alfalfa, forage 0.015
Alfalfa, hay 0.06
Cotton, gin byproducts 30
Cottonseed subgroup 20C 0.4
Vegetable, foliage of legume, except soybean, subgroup 7A 0.03

[86 FR 11138, Feb. 24, 2021, as amended at 87 FR 76948, Dec. 16, 2022; 89 FR 42390, May 15, 2024]

§ 180.710 Pethoxamid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pethoxamid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only pethoxamid, 2-chloro-N-(2-ethoxyethyl)-N-(2-methyl-1-phenyl-1-propen-1-yl) acetamide in or on the commodity.

Commodity Parts per
million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Corn, pop, grain 0.01
Corn, pop, stover 0.01
Corn, sweet, forage 0.01
Corn, sweet, kernel plus cob with husk removed 0.01
Corn, sweet, stover 0.01
Cotton, gin byproducts 0.01
Cotton, undelinted seed 0.01
Egg 0.01
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Milk 0.01
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01
Soybean, forage 0.01
Soybean, hay 0.01
Soybean, seed 0.01

(b) [Reserved]

[ 85 FR 48659, Aug. 12, 202]

§ 180.711 1-Aminocyclopropane-1-carboxylic acid (1-ACC); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for 1-aminocyclopropane-1-carboxylic acid (1-ACC) in or on apple and stone fruit when applied in accordance with good agricultural practices.

[86 FR 33892, June 28, 2021]

§ 180.712 Inpyrfluxam; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide inpyrfluxam, including its metabolites and degradates, in or on the commodities in Table 1 to this section. Compliance with the tolerance levels specified in Table 1 to this section is to be determined by measuring only inpyrfluxam (3-(difluoromethyl)-N-[(3R)-2,3-dihydro-1,1,3-trimethyl-1H-inden-4-yl]-1-methyl-1H-pyrazole-4-carboxamide), in or on the following commodities:

Table 1 to § 180.712

Commodity Parts per
million
Apple 0.01
Beet, sugar, roots 0.01
Corn, field, forage 0.02
Corn, field, grain 0.01
Corn, field, stover 0.02
Corn, pop, grain 0.01
Corn, pop, stover 0.02
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, forage 0.02
Corn, sweet, stover 0.02
Cotton, gin byproducts 0.02
Cotton, undelinted seed 0.01
Peanut 0.01
Peanut, hay 2
Rapeseed subgroup 20A 0.01
Rice, grain 0.01
Soybean, seed 0.01
Wheat, forage 0.01
Wheat, grain 0.01
Wheat, hay 1.5
Wheat, straw 0.3

(2) Tolerances are established for residues of inpyrfluxam, including its metabolites and degradates, in or on the commodities in Table 2 to this section. Compliance with the tolerance levels specified in Table 2 to this section is to be determined by measuring the free and conjugated forms of the sum of inpyrfluxam (3-(difluoromethyl)-N-[(3R)-2,3-dihydro-1,1,3-trimethyl-1H-inden-4-yl]-1-methyl-1H-pyrazole-4-carboxamide, and its metabolites 3-(difluoromethyl)-N-[1′-(hydroxymethyl)-(1′S,3′R)-1′,3′-dimethyl-2′,3′-dihydro-1′H-inden-4′-yl]-1-methyl-1H-pyrazole-4-carboxamide and 3-(difluoromethyl)-N-[1′-(hydroxymethyl)-(1′R,3′S)-1′,3′-dimethyl-2′,3′-dihydro-1′H-inden-4′-yl]-1-methyl-1H-pyrazole-4-carboxamid, calculated as the stoichiometric equivalent of inpyrfluxam, in or on the commodity:

Table 2 to § 180.712

Commodity Parts per
million
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Egg 0.01
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Milk 0.01
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01

(b)-(d) [Reserved]

[85 FR 52488, Aug. 26, 2020, as amended at 91 FR 8123, Feb. 20, 2026]

§ 180.713 Tiafenacil; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the herbicide tiafenacil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only tiafenacil, methyl N-[2-[[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenyl]thio]-1-oxopropyl]-β-alaninate, in or on the following commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Barley subgroup 15-22B 0.01
Corn, field, grain 0.01
Corn, pop, grain 0.01
Cottonseed subgroup 20C 0.3
Fruit, citrus, group 10-10 0.01
Fruit, pome, group 11-10 0.01
Fruit, stone, group 12-12 0.01
Grain sorghum and millet subgroup 15-22E 0.01
Grape 0.01
Nut, tree, group 14-12 0.01
Peanut 0.01
Rapeseed subgroup 20A 0.15
Soybean, seed 0.01
Sweet corn subgroup 15-22D 0.01
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.01
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.03
Wheat, grain 0.01

(2) Tolerances are established for residues of the herbicide tiafenacil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of tiafenacil, methyl N-[2-[[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenyl]thio]-1-oxopropyl]-β-alaninate and its metabolites 2-(2-chloro-4-fluoro-5-(3-methyl-2,6-dioxo-4-(trifluoromethyl)-2,3-dihydropyrimidin-1(6H)-yl)phenylsulfinyl)propanoic acid and 2-(2-chloro-5-(2,6-dioxo-4-(trifluoromethyl)-2,3-dihydropyrimidin-1(6H)-yl)-4-fluorophenylsulfinyl)propanoic acid, calculated as the stoichiometric equivalent of tiafenacil, in or on the following commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Almond, hulls 0.2
Barley, hay 0.03
Barley, straw 0.03
Corn, field, forage 0.05
Corn, field, stover 0.05
Corn, pop, stover 0.05
Corn, sweet, forage 0.03
Corn, sweet, stover 0.03
Cotton, gin byproducts 3
Fonio, black, forage 0.05
Fonio, black, hay 0.08
Fonio, white, forage 0.05
Fonio, white, hay 0.08
Job's tears, forage 0.05
Job's tears, hay 0.08
Millet, barnyard, forage 0.05
Millet, barnyard, hay 0.08
Millet, finger, forage 0.05
Millet, finger, hay 0.08
Millet, foxtail, forage 0.05
Millet, foxtail, hay 0.08
Millet, little, forage 0.05
Millet, little, hay 0.08
Millet, little, straw 0.07
Millet, pearl, forage 0.05
Millet, pearl, hay 0.08
Millet, pearl, straw 0.07
Millet, proso, forage 0.05
Millet, proso, hay 0.08
Millet, proso, straw 0.07
Pea, field, forage 5
Pea, field, hay 5
Sorghum, grain, forage 0.05
Sorghum, grain, stover 0.05
Soybean, forage 0.15
Soybean, hay 0.3
Teff, straw 0.07
Wheat, forage 0.05
Wheat, hay 0.08
Wheat, straw 0.07

(b)-(d) [Reserved]

[85 FR 55384, Sept. 8, 2020, as amended at 90 FR 14911, Apr. 7, 2025]

§ 180.714 Broflanilide; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of broflanilide, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only broflanilide, 3-(benzoylmethylamino)-N-[2-bromo-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Amaranth, grain, grain 0.01
Amaranth, grain, stover 0.01
Cañihua, grain 0.01
Chia, grain 0.01
Corn, field, milled byproducts 0.015
Cram-cram, grain 0.01
Grain, cereal, group 15, except rice 0.01
Food and feed commodities (other than those covered by a higher tolerance) 0.01
Grain, cereal, forage, fodder, and straw, group 16, except rice 0.01
Huauzontle, grain 0.01
Potato, wet peel 0.08
Quinoa, forage 0.01
Quinoa, grain 0.01
Quinoa, hay 0.01
Quinoa, straw 0.01
Spelt, grain 0.01
Teff, forage 0.01
Teff, grain 0.01
Teff, hay 0.01
Teff, straw 0.01
Vegetable, tuberous and corm, subgroup 1C 0.04

(2) Tolerances are established for residues of broflanilide, including its metabolites and degradates, in or on the commodities to Table 2 of this section. Compliance with the tolerance levels specified in Table 2 is to be determined by measuring the sum of broflanilide, 3-(benzoylmethylamino)-N-[2-bromo-4-[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]-6-(trifluoromethyl)phenyl]-2-fluorobenzamide, and its metabolite 3-benzamido-N-[2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl]-2-fluorobenzamide, calculated as the stoichiometric equivalent of broflanilide, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Cattle, fat 0.02
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Egg 0.02
Goat, fat 0.02
Goat, meat 0.02
Goat, meat byproducts 0.02
Hog, fat 0.02
Hog, meat 0.02
Hog, meat byproducts 0.02
Horse, fat 0.02
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.02
Poultry, fat 0.02
Poultry, meat 0.02
Poultry, meat byproducts 0.02
Sheep, fat 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.02

(b)-(d) [Reserved]

[85 FR 81805, Dec. 17, 2020]

§ 180.715 Fluxametamide; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide fluxametamide, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only residues of fluxametamide, 4-[5-(3,5-dichlorophenyl)-4,5-dihydro-5-(trifluoromethyl)-3-isoxazolyl]-N-[(methoxyamino)methylene]-2-methylbenzamide in or on the commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Tea, dried 5
Tea, instant 5

(b)-(d) [Reserved]

[86 FR 9866, Feb. 17, 2021]

§ 180.716 Fluindapyr; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the fungicide fluindapyr, including its metabolites and degradates, in or on the commodities in Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only fluindapyr, 3-(difluoromethyl)-N-(7-fluoro-1,1,3-trimethyl-2,3-dihydro-1H-inden-4-yl)-1-methyl-1H-pyrazole-4-carboxamide, in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Almond, hulls 15
Cattle, fat 0.03
Cattle, meat 0.01
Corn, field, grain 0.01
Corn, sweet, kernel plus cob with husks removed 0.01
Corn, sweet, stover 20
Egg 0.01
Goat, fat 0.03
Goat, meat 0.01
Grain, aspirated fractions 20
Grain, cereal, forage, fodder, and straw, group 16, forage, except rice 15
Grain, cereal, forage, fodder, and straw, group 16, hay, except rice 8
Grain, cereal, forage, fodder, and straw, group 16, stover, except rice 4
Grain, cereal forage, fodder, and straw, group 16, straw, except rice 20
Grain, cereal group 15, except rice and corn 0.8
Hog, fat 0.01
Hog, meat 0.01
Horse, fat 0.03
Horse, meat 0.01
Milk 0.01
Nut, tree, group 14-12 0.04
Poultry, fat 0.01
Poultry, meat 0.01
Sheep, fat 0.03
Sheep, meat 0.01
Soybean, forage 15
Soybean, hay 30
Soybean, hulls 0.6
Soybean, seed 0.2

(2) Tolerances are established for residues of the fungicide fluindapyr, including its metabolites and degradates, in or on the commodities in Table 2 of this section. Compliance with the tolerance levels specified in Table 2 is to be determined by measuring the sum of fluindapyr, 3-(difluoromethyl)-N-(7-fluoro-1,1,3-trimethyl-2,3-dihydro-1H-inden-4-yl)-1-methyl-1H-pyrazole-4-carboxamide, and 3-(difluoromethyl)-N-(7-fluoro-1-hydroxymethyl-1,3-dimethyl-2,3-dihydro-lH-inden-4-yl)-1-methyl-lH-pyrazole-4-carboxamide, calculated as the stoichiometric equivalent of fluindapyr, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Cattle, meat byproducts 0.3
Goat, meat byproducts 0.3
Horse, meat byproducts 0.3
Hog, meat byproducts 0.01
Poultry, meat byproducts 0.01
Sheep, meat byproducts 0.3

(b)-(d) [Reserved]

[86 FR 13465, Mar. 8, 2021, as amended at 89 FR 88660, Nov. 8, 2024]

§ 180.717 Trifludimoxazin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide trifludimoxazin, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only trifludimoxazin, dihydro-1,5-dimethyl-6-thioxo-3-[2,2,7-trifluoro-3,4-dihydro-3-oxo-4-(2-propyn-1-yl)-2H-1,4-benzoxazin-6-yl]-1,3,5-triazine-2,4(1H,3H)-dione, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Almond, hulls 0.15
Fruit, citrus, group 10-10 0.01
Fruit, pome, group 11-10 0.01
Grain, cereal, forage, fodder, and straw, Group 16, except rice 0.01
Grain, cereal, group 15, except rice 0.01
Nut, tree, group 14-12 0.01
Peanut 0.01
Peanut, hay 0.01
Vegetable, legume, group 6 0.01
Vegetable, foliage of legume, group 7 0.01

(b)-(d) [Reserved]

[86 FR 26677, May 17, 2021]

§ 180.718 Picarbutrazox; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide picarbutrazox, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only picarbutrazox (1,1-dimethylethyl N-[6-[[[(Z)-[(1-methyl-1H-tetrazol-5-yl)phenylmethylene]amino]oxy]methyl]-2-pyridinyl]carbamate in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Cotton, gin byproducts 0.01
Cotton, undelinted seed 0.01
Grain, cereal, except rice, group 15 0.01
Grain, cereal, forage, fodder, and straw, group 16 0.01
Herb group 25 0.01
Rapeseed subgroup 20A 0.01
Spice group 26 0.01
Vegetable, Brassica, head and stem, group 5-16 0.01
Vegetable, bulb, group 3-07 0.01
Vegetable, cucurbit, group 9 0.01
Vegetable, foliage of legume, group 7 0.01
Vegetable, fruiting, group 8-10 0.01
Vegetable, leafy, group 4-16 0.01
Vegetable, leaves of root and tuber, group 2 0.01
Vegetable, legume, group 6 0.01
Vegetable, stalk, stem, and leaf petiole group 22 0.01
Vegetable, root, subgroup 1A 0.01
Vegetable, tuberous and corm, except potato, subgroup 1D 0.01

(b)-(d) [Reserved]

[86 FR 12833, Mar. 5, 2021, as amended at 87 FR 34206, June 6, 2022]

§ 180.719 Ipflufenoquin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ipflufenoquin, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only ipflufenoquin, 2-[(7,8-difluoro-2-methyl-3-quinolinyl)oxy]-6-fluoro-α,α-dimethylbenzenemethanol, in or on the commodities.

Table 1 to Paragraph (a)

Commodity Parts per
million
Almond 0.01
Almond, hulls 3
Fruit, pome, group 11-10 0.15

(b)-(d) [Reserved]

[87 FR 11319, Mar. 1, 2022]

§ 180.720 Fluazaindolizine; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide fluazaindolizine, including its metabolites and degradates, in or on the commodities to Table 1 of this section. Compliance with the tolerance levels specified in Table 1 is to be determined by measuring only fluazaindolizine, 8-chloro-N-[(2-chloro-5-methoxyphenyl)sulfonyl]-6-(trifluoromethyl)imidazo[1,2-a]pyridine-2-carboxamide, in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per
million
Carrot 0.05
Cattle, fat 0.01
Cattle, meat 0.01
Cattle, meat byproducts 0.01
Egg 0.01
Goat, fat 0.01
Goat, meat 0.01
Goat, meat byproducts 0.01
Hog, fat 0.01
Hog, meat 0.01
Hog, meat byproducts 0.01
Horse, fat 0.01
Horse, meat 0.01
Horse, meat byproducts 0.01
Milk 0.01
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Sheep, fat 0.01
Sheep, meat 0.01
Sheep, meat byproducts 0.01
Tomato, dried 0.4
Vegetable, cucurbit, group 9 0.15
Vegetable, fruiting, group 8-10 0.07
Vegetable, tuberous and corm, subgroup 1C 0.2

(b)-(c) [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the nematicide fluazaindolizine, including its metabolites and degradates, in or on the commodities to Table 2 of this section. Compliance with the tolerance levels specified in Table 2 is to be determined by measuring only fluazaindolizine, 8-chloro-N-[(2-chloro-5-methoxyphenyl)sulfonyl]-6-(trifluoromethyl)imidazo[1,2-a]pyridine-2-carboxamide, in or on the commodity.

Table 2 to Paragraph (d)

Commodity Parts per
million
Animal feed, nongrass, group 18, forage 0.01
Animal feed, nongrass, group 18, hay 0.015
Animal feed, nongrass, group 18, straw 0.15
Berry, low growing, subgroup 13-07G 0.01
Grain, cereal, forage, hay, stover, and straw group 16-22, forage 0.01
Grain, cereal, forage, hay, stover, and straw group 16-22, hay 0.015
Grain, cereal, forage, hay, stover, and straw group 16-22, stover 0.15
Grain, cereal, forage, hay, stover, and straw group 16-22, straw 0.15
Grain, cereal, group 15-22 0.01
Grass, forage, fodder and hay, group 17, forage 0.01
Grass, forage, fodder and hay, group 17, hay 0.015
Grass, forage, fodder and hay, group 17, straw 0.15
Oilseed group 20 0.8
Rapeseed, forage 0.09
Stalk, stem and leaf petiole vegetable group 22 0.03
Vegetable, Brassica, head and stem, group 5-16 0.015
Vegetable, bulb, group 3-07 0.03
Vegetable, legume, forage and hay, group 7-22, forage 0.09
Vegetable, legume, forage and hay, group 7-22, hay 0.4
Vegetable, leafy, group 4-16 0.015
Vegetable, leaves of root and tuber, group 2 0.015
Vegetable, legume, group 6-22 0.8
Vegetable, root, subgroup 1B 0.02

[88 FR 62470, Sept. 12, 2023]

§ 180.721 Isoprothiolane; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide isoprothiolane, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only residues of isoprothiolane (bis(1-methylethyl) 2-(1,3-dithiolan-2-ylidene)propanedioate) in or on the commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
Banana 1 0.9
Rice, bran 1 15
Rice, husked 1 6
Rice, polished rice 1 1.5
1 There are no U.S. registrations as of December 6, 2021.

(b)-(d) [Reserved]

[86 FR 68925, Dec. 6, 2021]

§ 180.722 Pyflubumide; tolerances for residues.

(a) General. Tolerances are established for residues of pyflubumide, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring residues of pyflubumide (1,3,5-trimethyl-N-(2-methyl-1-oxopropyl)-N-[3-(2-methylpropyl)-4-[2,2,2-trifluoro-1-methoxy-1-(trifluoromethyl)ethyl]phenyl]-1H-pyrazole-4-carboxamide) in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Tea, dried 80
Tea, instant 80

(b)-(d) [Reserved]

[86 FR 71162, Dec. 15, 2021]

§ 180.723 Spiropidion; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide spiropidion, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in Table 1 to this paragraph (a)(1) is to be determined by measuring only the sum of spiropidion [3-(4-chloro-2,6-dimethyl-phenyl)-8-methoxy-1-methyl-2-oxo-1,8-diazaspiro[4.5]dec-3-en-4-yl ethyl carbonate] and its metabolite SYN547305 [3-(4-chloro-2,6-dimethylphenyl)-4-hydroxy-8-methoxy-1-methyl-1,8-diazaspiro[4.5]dec-3-en-2-one] calculated as the stoichiometric equivalent of spiropidion, in or on the following plant commodities:

Table 1 to Paragraph (a)(1)

Commodity Parts per
million
Cucumber 1 0.8
Muskmelon 1 0.9
Pepper, bell 1 1.5
Pepper, nonbell 1 1.5
Potato 1 1.5
Pumpkin 1 0.9
Soybean, seed 1 3
Tomato 1 0.8
Watermelon 1 0.9
1 There are no U.S. registrations for this commodity as of July 20, 2022.

(2) Tolerances are established for residues of the insecticide spiropidion, including its metabolites and degradates, in or on the commodities in Table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in Table 2 to this paragraph (a)(2) is to be determined by measuring only SYN547305 [3-(4-chloro-2,6-dimethylphenyl)-4-hydroxy-8-methoxy-1-methyl-1,8-diazaspiro[4.5]dec-3-en-2-one] calculated as the stoichiometric equivalent of spiropidion, in or on the following livestock commodities:

Table 2 to Paragraph (a)(2)

Commodity Parts per
million
Cattle, fat 1 0.03
Cattle, meat byproducts 1 0.3
Goat, fat 1 0.03
Goat, meat byproducts 1 0.3
Horse, fat 1 0.03
Horse, meat byproducts 1 0.3
Sheep, fat 1 0.03
Sheep, meat byproducts 1 0.3
1 There are no U.S. registrations for this commodity as of July 20, 2022.

(b)-(d) [Reserved]

[87 FR 43219, July 20, 2022, as amended at 88 FR 31477, May 17, 2023]

§ 180.724 Benzpyrimoxan; tolerances for residues.

(a) General. Tolerances are established for residues of benzpyrimoxan, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring residues of benzpyrimoxan (5-(1,3-dioxan-2-yl)-4-[[4-(trifluoromethyl)phenyl]methoxy]pyrimidine) in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Rice, husked 1 0.9
Rice, polished rice 1 0.15
Rice, bran 1 3
1 There are no U.S. registrations as of July 10, 2023.

(b)-(d) [Reserved]

[88 FR 43446, July 10, 2023]

§ 180.725 Pyraclonil; tolerances for residues.

(a)-(b) [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of the herbicide pyraclonil, including its metabolites and degradates, in or on the commodities to the table to this paragraph (c). Compliance with the tolerance levels specified in the table to this paragraph (c) is to be determined by measuring only pyraclonil (1-(3-chloro-4,5,6,7-tetrahydropyrazolo[1,5-a]pyridin-2-yl)-5-(methyl-2-propyn-1-ylamino)-1H-pyrazole-4-carbonitrile).

Table 1 to Paragraph (c)

Commodity Parts per
million
Rice, grain 0.01

(d) [Reserved]

[88 FR 57891, Aug. 24, 2023]

§ 180.726 Metamitron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide metamitron, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 to this paragraph (a) is to be determined by measuring residues of metamitron (4-amino-3-methyl-6-phenyl-1,2,4-triazin-5(4H)-one) in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per
million
Apple 0.01
Pear 0.01

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide metamitron, including its metabolites and degradates, in or on the specified agricultural commodities to table 1 to this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in table 1 to this paragraph (b) is to be determined by measuring residues of metamitron (4-amino-3-methyl-6-phenyl-1,2,4-triazin-5(4H)-one) in or on the listed commodities. The tolerances expire on the dates specified in table 1 to this paragraph (b).

Table 1 to Paragraph (b)

Commodity Parts per
million
Expiration/
revocation
date
Beet, sugar, roots 0.01 12/31/2027

(c)-(d) [Reserved]

[89 FR 56673, July 10, 2024, as amended at 90 FR 11674, Mar. 11, 2025]

§ 180.727 Florylpicoxamid; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of florylpicoxamid, including its metabolites and degradates, in or on the commodities in table 1 to this paragraph (a)(1). Compliance with the tolerance levels specified in table 1 is to be determined by measuring only florylpicoxamid ((1S)-2,2-bis(4-fluorophenyl)-1-methylethyl N-[[3-(acetyloxy)-4-methoxy-2-pyridinyl]carbonyl]-L-alaninate) in or on the commodity.

Table 1 to Paragraph (a)(1)

Commodity Parts per million
Barley, grain 0.03
Barley, hay 1.5
Barley, straw 0.5
Beet, sugar, leaves 0.1
Beet, sugar, roots 0.01
Canola 0.015
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.01
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.01
Vegetable, legume, forage and hay, except soybean, subgroup 7-22A 6
Wheat, forage 1.5
Wheat, grain 0.01
Wheat, hay 3
Wheat, straw 0.05

(2) Tolerances are established for residues of florylpicoxamid, including its metabolites and degradates, in or on the commodities in table 2 to this paragraph (a)(2). Compliance with the tolerance levels specified in table 2 is to be determined by measuring only the sum of florylpicoxamid ((1S)-2,2-bis(4-fluorophenyl)-1-methylethyl N-[[3-(acetyloxy)-4-methoxy-2-pyridinyl]carbonyl]-L-alaninate) and its metabolite (2S)-1,1-bis(4-fluorophenyl)propan-2-yl N-[(3-hydroxy-4-methoxypyridin-2-yl)carbonyl]-L-alaninate, calculated as the stoichiometric equivalent of florylpicoxamid, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity Parts per million
Cattle, fat 0.02
Cattle, meat 0.02
Cattle, meat byproducts 0.02
Egg 0.02
Goat, fat 0.02
Goat, meat 0.02
Goat, meat byproducts 0.02
Hog, fat 0.02
Hog, meat 0.02
Hog, meat byproducts 0.02
Horse, fat 0.02
Horse, meat 0.02
Horse, meat byproducts 0.02
Milk 0.02
Poultry, fat 0.02
Poultry, liver 0.02
Poultry, meat 0.02
Sheep, fat 0.02
Sheep, meat 0.02
Sheep, meat byproducts 0.02

(b)-(d) [Reserved]

[90 FR 22648, May 29, 2025]

§ 180.728 Diflufenican; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide diflufenican, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only diflufenican, N-(2,4-difluorophenyl)-2-[3-(trifluoromethyl)phenoxy]-3-pyridinecarboxamide, in or on the following commodities.

Table 1 to Paragraph (a)

Commodity Parts per
million
Corn, field, forage 0.01
Corn, field, grain 0.01
Corn, field, stover 0.01
Soybean, Forage 0.01
Soybean, Hay 0.015
Soybean, Seed 0.01

(b) [Reserved]

[91 FR 39506, June 30, 2026]

§ 180.729 Cyclobutrifluram; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide/fungicide cyclobutrifluram, including its metabolites and degradates, in or on the plant commodities in table 1 to this paragraph (a). Compliance with the tolerance levels specified in table 1 is to be determined by measuring the sum of cyclobutrifluram (rel-N-[(1R,2R)-2-(2,4-dichlorophenyl)cyclobutyl]-2-(trifluoromethyl)-3-pyridinecarboxamide) and its metabolite 2-trifluoromethyl-nicotinamide, calculated as the stoichiometric equivalent of cyclobutrifluram in or on plant commodities.

Table 1 to Paragraph (a)

Commodity Parts
per million
Cotton, gin byproducts 0.02
Cotton, undelinted seed 0.02
Lettuce, leaf 0.06
Soybean, seed 0.03

(b) [Reserved]

[90 FR 49259, Nov. 5, 2025]

§ 180.730 Isocycloseram; tolerances for residues.

(a) General.

(1) Tolerances are established for residues of the insecticide isocycloseram, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only isocycloseram, 4-[5-(3,5-dichloro-4-fluorophenyl)-5-(trifluoromethyl)-4,5-dihydro-1,2-oxazol-3-yl]-N-(2-ethyl-3-oxo-1,2-oxazolidin-4-yl)-2-methylbenzamide, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity Parts per million
African nut-tree 0.01
Almond 0.2
Almond, hulls 6
Almond, tropical 0.2
Apple, wet pomace 1
Barley, grain 0.01
Barley, hay 0.01
Barley, straw 0.01
Beechnut 0.2
Buckwheat, forage 0.01
Buckwheat, grain 0.01
Buckwheat, hay 0.01
Buckwheat, straw 0.01
Bunya 0.2
Bur oak 0.01
Butternut 0.01
Candlenut 0.2
Cashew 0.01
Cattle, fat 0.05
Cattle, meat 0.01
Cattle, meat byproducts 0.02
Chestnut 0.2
Chestnut, guiana 0.01
Chinquapin 0.2
Coconut 0.01
Corn, field, forage 2
Corn, field, grain 0.01
Corn, field, stover 1.5
Corn, pop, grain 0.01
Corn, pop, stover 1.5
Cotton, gin byproducts 10
Cottonseed subgroup 20C 0.5
Egg 0.01
Fruit, citrus, group 10-10 0.5
Fruit, citrus, group 10-10, dried pulp 3
Fruit, citrus, group 10-10, oil 80
Fruit, pome, group 11-10 0.4
Fruit, stone, group 12-12 1
Ginkgo 0.2
Goat, fat 0.05
Goat, meat 0.01
Goat, meat byproducts 0.02
Grain, aspirated fractions 15
Hazelnut 0.01
Heartnut 0.01
Horse, fat 0.05
Horse, meat 0.01
Horse, meat byproducts 0.02
Horse-chestnut, japanese 0.01
Milk 0.01
Milk, fat 0.3
Millet, pearl, forage 0.01
Millet, pearl, grain 0.01
Millet, pearl, hay 0.01
Millet, pearl, straw 0.01
Millet, proso, forage 0.01
Millet, proso, grain 0.01
Millet, proso, hay 0.01
Millet, proso, straw 0.01
Monkey-pot 0.01
Nut, brazil 0.01
Nut, cajou 0.01
Nut, coquito 0.01
Nut, dika 0.01
Nut, hickory 0.01
Nut, macadamia 0.01
Nut, mongongo 0.01
Nut, monkey puzzle 0.2
Nut, okari 0.2
Nut, pachira 0.01
Nut, peach palm 0.2
Nut, pili 0.2
Nut, pine 0.2
Nut, sapucaia 0.01
Oat, forage 0.01
Oat, grain 0.01
Oat, hay 0.01
Oat, straw 0.01
Onion, bulb, subgroup 3-07A 0.01
Onion, green, subgroup 3-07B 0.9
Peanut 0.01
Pecan 0.01
Pequi 0.2
Pine, brazilian 0.2
Pistachio 0.2
Plum, prune, dried 1.5
Poultry, fat 0.01
Poultry, meat 0.01
Poultry, meat byproducts 0.01
Rapeseed, seed 0.01
Rye, forage 0.01
Rye, grain 0.01
Rye, hay 0.01
Rye, straw 0.01
Sheep, fat 0.05
Sheep, meat 0.01
Sheep, meat byproducts 0.02
Soybean, hulls 0.5
Soybean, seed 0.15
Teosinte, forage 0.01
Teosinte, grain 0.01
Teosinte, hay 0.01
Teosinte, straw 0.01
Tomato, dried 2
Triticale, forage 0.01
Triticale, grain 0.01
Triticale, straw 0.01
Vegetable, brassica, head and stem, group 5-16 4
Vegetable, cucurbit, group 9 0.15
Vegetable, foliage of legume, except soybean, subgroup 7-22A 0.01
Vegetable, fruiting, group 8-10 0.6
Vegetable, leafy, group 4-16 10
Vegetable, legume, pulse, bean, dried shelled, except soybean, subgroup 6-22E 0.01
Vegetable, legume, pulse, pea, dried shelled, subgroup 6-22F 0.01
Vegetable, tuberous and corm, subgroup 1C 0.01
Walnut, black 0.01
Walnut, english 0.01
Wheat, forage 0.01
Wheat, grain 0.01
Wheat, hay 0.01
Wheat, straw 0.01
Yellowhorn 0.2

(b) [Reserved]

[90 FR 52263, Nov. 20, 2025]

§ 180.731 Epyrifenacil; tolerances for residues.

Tolerances are established for residues of the herbicide epyrifenacil, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only epyrifenacil, ethyl 2-[[3-[2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluorophenoxy]-2-pyridinyl]oxy]acetate in or on the commodity.

Table 1 to § 180.731

Commodity Parts per
million
Corn, field, forage 0.01
Corn, field, grain 0.005
Corn, field, stover 0.01
Rapeseed, seed 0.005
Soybean, forage 0.01
Soybean, hay 0.01
Soybean, seed 0.005
Wheat, forage 0.01
Wheat, grain 0.005
Wheat, hay 0.01
Wheat, straw 0.01

[91 FR 47145, July 28, 2026]

§ 180.732 Fluoxapiprolin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fluoxapiprolin, including its metabolites and degradates, in or on the commodities in table 1 to paragraph (a). Compliance with the tolerance levels specified in table 1 to paragraph (a) is to be determined by measuring the residues of fluoxapiprolin (2-[3,5-bis(difluoromethyl)-1H-pyrazol-1-yl]-1-[4-[4-[5-[2-chloro-6-[(methylsulfonyl)oxy]phenyl]-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]-1-piperidinyl]ethanone) in or on the commodity.

Table 1 to Paragraph (a)

Commodity Parts per million
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.2
Grape, raisin 0.5
Leaf petiole vegetable subgroup 22B 1.5
Lettuce, head 0.8
Onion, bulb, subgroup 3-07A 0.03
Onion, green, subgroup 3-07B 2
Vegetable, brassica, head and stem, group 5-16 0.8
Vegetable, cucurbit, group 9 0.07
Vegetable, fruiting, group 8-10 0.06
Vegetable, leafy, group 4-16, except lettuce, head 6
Vegetable, tuberous and corm, subgroup 1C 0.01

(b) [Reserved]

[91 FR 39511, June 30, 2026]