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Title 40Chapter ISubchapter EPart 180 → Subpart C


Title 40: Protection of Environment
PART 180—TOLERANCES AND EXEMPTIONS FOR PESTICIDE CHEMICAL RESIDUES IN FOOD


Subpart C—Specific Tolerances


Contents
§180.101   Specific tolerances; general provisions.
§180.103   Captan; tolerances for residues.
§180.106   Diuron; tolerances for residues.
§180.107   Triflumezopyrim; tolerance for residues.
§180.108   Acephate; tolerances for residues.
§180.109   Fenpicoxamid; Tolerances for residues.
§180.111   Malathion; tolerances for residues.
§180.114   Ferbam; tolerances for residues.
§180.116   Ziram; tolerances for residues.
§180.117   S-Ethyl dipropylthiocarbamate; tolerances for residues.
§180.123   Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.
§180.123a   Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.
§180.124   Methyl bromide; tolerances for residues.
§180.127   Piperonyl butoxide; tolerances for residues.
§180.128   Pyrethrins; tolerances for residues.
§180.129   o-Phenylphenol and its sodium salt; tolerances for residues.
§180.130   Hydrogen Cyanide; tolerances for residues.
§180.132   Thiram; tolerances for residues.
§180.142   2,4-D; tolerances for residues.
§180.145   Fluorine compounds; tolerances for residues.
§180.151   Ethylene oxide; tolerances for residues.
§180.153   Diazinon; tolerances for residues.
§180.155   1-Naphthaleneacetic acid; tolerances for residues.
§180.163   Dicofol; tolerances for residues.
§180.169   Carbaryl; tolerances for residues.
§180.172   Dodine; tolerances for residues.
§180.175   Maleic hydrazide; tolerances for residues.
§180.176   Mancozeb; tolerances for residues.
§180.178   Ethoxyquin; tolerances for residues.
§180.181   Chlorpropham; tolerances for residues.
§180.182   Endosulfan; tolerances for residues.
§180.183   Disulfoton; tolerances for residues.
§180.184   Linuron; tolerances for residues.
§180.185   DCPA; tolerances for residues.
§180.189   Coumaphos; tolerances for residues.
§180.190   Diphenylamine; tolerances for residues.
§180.191   Folpet; tolerances for residues.
§180.198   Trichlorfon; tolerances for residues.
§180.200   Dicloran; tolerances for residues.
§180.202   p-Chlorophenoxyacetic acid; tolerances for residues.
§180.204   Dimethoate; tolerances for residues.
§180.205   Paraquat; tolerances for residues.
§180.206   Phorate; tolerances for residues.
§180.207   Trifluralin; tolerances for residues.
§180.208   Benfluralin; tolerances for residues.
§180.209   Terbacil; tolerances for residues.
§180.210   Bromacil; tolerances for residues.
§180.211   Propachlor; tolerances for residues.
§180.212   S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.
§180.213   Simazine; tolerances for residues.
§180.215   Naled; tolerances for residues.
§180.217   Metiram; tolerances for residues.
§180.220   Atrazine; tolerances for residues.
§180.222   Prometryn; tolerances for residues.
§180.225   Phosphine; tolerances for residues.
§180.226   Diquat; tolerances for residues.
§180.227   Dicamba; tolerances for residues.
§180.229   Fluometuron; tolerances for residues.
§180.231   Dichlobenil; tolerances for residues.
§180.235   Dichlorvos; tolerances for residues.
§180.236   Triphenyltin hydroxide; tolerances for residues.
§180.241   Bensulide; tolerances for residues.
§180.242   Thiabendazole; tolerances for residues.
§180.243   Propazine; tolerances for residues.
§180.245   Streptomycin; tolerances for residues.
§180.249   Alachlor; tolerances for residues.
§180.252   Tetrachlorvinphos; tolerances for residues.
§180.253   Methomyl; tolerances for residues.
§180.254   Carbofuran; tolerances for residues.
§180.258   Ametryn; tolerances for residues.
§180.259   Propargite; tolerances for residues.
§180.261   Phosmet; tolerances for residues.
§180.262   Ethoprop; tolerances for residues.
§180.269   Aldicarb; tolerances for residues.
§180.272   Tribuphos; tolerances for residues.
§180.274   Propanil; tolerances for residues.
§180.275   Chlorothalonil; tolerances for residues.
§180.276   Formetanate hydrochloride; tolerances for residues.
§180.278   Phenmedipham; tolerances for residues.
§180.284   Zinc phosphide; tolerances for residues.
§180.287   Amitraz; tolerances for residues.
§180.288   2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.
§180.289   Methanearsonic acid; tolerances for residues.
§180.291   Pentachloronitrobenzene; tolerance for residues.
§180.292   Picloram; tolerances for residues.
§180.293   Endothall; tolerances for residues.
§180.297   N-1-Naphthyl phthalamic acid; tolerances for residues.
§180.298   Methidathion; tolerances for residues.
§180.299   Dicrotophos; tolerances for residues.
§180.300   Ethephon; tolerances for residues.
§180.301   Carboxin; tolerances for residues.
§180.303   Oxamyl; tolerances for residues.
§180.304   Oryzalin; tolerances for residues.
§180.314   Triallate; tolerances for residues.
§180.316   Pyrazon; tolerances for residues.
§180.317   Propyzamide; tolerances for residues.
§180.318   4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.
§180.319   Interim tolerances.
§180.324   Bromoxynil; tolerances for residues.
§180.328   Napropamide; tolerances for residues.
§180.330   S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.
§180.331   4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.
§180.332   Metribuzin;   tolerances for residues.
§180.337   Oxytetracycline; tolerances for residues.
§180.339   MCPA; tolerances for residues.
§180.341   2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.
§180.342   Chlorpyrifos; tolerances for residues.
§180.345   Ethofumesate; tolerances for residues.
§180.349   Fenamiphos; tolerances for residues.
§180.350   Nitrapyrin; tolerances for residues.
§180.352   Terbufos; tolerances for residues.
§180.353   Desmedipham; tolerances for residues.
§180.355   Bentazon; tolerances for residues.
§180.356   Norflurazon; tolerances for residues.
§180.360   Asulam; tolerance for residues.
§180.361   Pendimethalin; tolerances for residues.
§180.362   Fenbutatin-oxide; tolerances for residues.
§180.364   Glyphosate; tolerances for residues.
§180.367   n-Octyl bicycloheptenedicarboximide; tolerances for residues.
§180.368   Metolachlor; tolerances for residues.
§180.370   5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.
§180.371   Thiophanate-methyl; tolerances for residues.
§180.372   2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.
§180.373   [Reserved]
§180.377   Diflubenzuron; tolerances for residues.
§180.378   Permethrin; tolerances for residues.
§180.380   Vinclozolin; tolerances for residues.
§180.381   Oxyfluorfen; tolerances for residues.
§180.383   Sodium salt of acifluorfen; tolerances for residues.
§180.384   Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.
§180.385   Diclofop-methyl; tolerances for residues.
§§180.388-180.389   [Reserved]
§180.390   Tebuthiuron; tolerances for residues.
§180.395   Hydramethylnon; tolerances for residues.
§180.396   Hexazinone; tolerances for residues.
§180.399   Iprodione; tolerances for residues.
§180.401   Thiobencarb; tolerances for residues.
§180.403   Thidiazuron; tolerances for residues.
§180.404   Profenofos; tolerances for residues.
§180.405   Chlorsulfuron; tolerances for residues.
§180.407   Thiodicarb; tolerances for residues.
§180.408   Metalaxyl; tolerances for residues.
§180.409   Pirimiphos-methyl; tolerances for residues.
§180.410   Triadimefon; tolerances for residues.
§180.411   Fluazifop-P-butyl; tolerances for residues.
§180.412   Sethoxydim; tolerances for residues.
§180.413   Imazalil; tolerances for residues.
§180.414   Cyromazine; tolerances for residues.
§180.415   Aluminum tris (O-ethylphosphonate); tolerances for residues.
§180.416   Ethalfluralin; tolerances for residues.
§180.417   Triclopyr; tolerances for residues.
§180.418   Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.
§180.419   Chlorpyrifos-methyl; tolerances for residues.
§180.420   Fluridone; tolerances for residues.
§180.421   Fenarimol; tolerances for residues.
§180.425   Clomazone; tolerances for residues.
§180.426   2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance for residues.
§180.427   Tau-Fluvalinate; tolerances for residues.
§180.428   Metsulfuron methyl; tolerances for residues.
§180.429   Chlorimuron ethyl; tolerances for residues.
§180.430   Fenoxaprop-ethyl; tolerances for residues.
§180.431   Clopyralid; tolerances for residues.
§180.432   Lactofen; tolerances for residues.
§180.433   Fomesafen; tolerances for residues.
§180.434   Propiconazole; tolerances for residues.
§180.435   Deltamethrin; tolerances for residues.
§180.436   Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.
§180.437   Imazamethabenz-methyl; tolerances for residues.
§180.438   Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.
§180.439   Thifensulfuron methyl; tolerances for residues.
§180.440   Tefluthrin; tolerances for residues.
§180.441   Quizalofop ethyl; tolerances for residues.
§180.442   Bifenthrin; tolerances for residues.
§180.443   Myclobutanil; tolerances for residues.
§180.444   Sulfur dioxide; tolerances for residues.
§180.445   Bensulfuron methyl; tolerances for residues.
§180.446   Clofentezine; tolerances for residues.
§180.447   Imazethapyr; tolerances for residues.
§180.448   Hexythiazox; tolerance for residues.
§180.449   Avermectin B1 and its delta-8,9-isomer; tolerances for residues.
§180.450   Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.
§180.451   Tribenuron methyl; tolerances for residues.
§180.452   Primisulfuron-methyl; tolerances for residues.
§180.454   Nicosulfuron; tolerances for residues.
§180.455   Procymidone; tolerances for residues.
§180.457   Bitertanol; tolerances for residues.
§180.458   Clethodim; tolerances for residues.
§180.459   Triasulfuron; tolerances for residues.
§180.460   Benoxacor; tolerances for residues.
§180.461   Cadusafos; tolerances for residues.
§180.462   Pyridate; tolerances for residues.
§180.463   Quinclorac; tolerances for residues.
§180.464   Dimethenamid; tolerances for residues.
§180.465   4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.
§180.466   Fenpropathrin; tolerances for residues.
§180.467   Carbon disulfide; tolerances for residues.
§180.468   Flumetsulam; tolerances for residues.
§180.469   Dichlormid; tolerances for residues.
§180.470   Acetochlor; tolerances for residues.
§180.471   Furilazole; tolerances for residues.
§180.472   Imidacloprid; tolerances for residues.
§180.473   Glufosinate ammonium; tolerances for residues.
§180.474   Tebuconazole; tolerances for residues.
§180.475   Difenoconazole; tolerances for residues.
§180.476   Triflumizole; tolerances for residues.
§180.477   Flumiclorac pentyl; tolerances for residues.
§180.478   Rimsulfuron; tolerances for residues.
§180.479   Halosulfuron-methyl; tolerances for residues.
§180.480   Fenbuconazole; tolerances for residues.
§180.481   Prosulfuron; tolerances for residues.
§180.482   Tebufenozide; tolerances for residues.
§180.484   Flutolanil; tolerances for residues.
§180.485   Cyproconazole; tolerances for residues.
§180.486   Chlorethoxyfos; tolerances for residues.
§180.487   Pyrithiobac sodium; tolerances for residues.
§180.490   Imazapic; tolerances for residues.
§180.491   Propylene oxide; tolerances for residues.
§180.492   Triflusulfuron-methyl; tolerances for residues.
§180.493   Dimethomorph; tolerances for residues.
§180.494   Pyridaben; tolerance for residues.
§180.495   Spinosad; tolerances for residues.
§180.498   Sulfentrazone; tolerances for residues.
§180.499   Propamocarb; tolerances for residues.
§180.500   Imazapyr; tolerances for residues.
§180.501   Hydroprene; tolerances for residues.
§180.502   Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.
§180.503   Cymoxanil, tolerance for residues.
§180.504   [Reserved]
§180.505   Emamectin; tolerances for residues.
§180.506   Cyclanilide; tolerances for residues.
§180.507   Azoxystrobin; tolerances for residues.
§180.509   Mefenpyr-diethyl; tolerance for residues.
§180.510   Pyriproxyfen; tolerances for residues.
§180.511   Buprofezin; tolerances for residues.
§180.512   [Reserved]
§180.513   Chlorfenapyr; tolerances for residues.
§180.514   Cloransulam-methyl; tolerances for residues.
§180.515   Carfentrazone-ethyl; tolerances for residues.
§180.516   Fludioxonil; tolerances for residues.
§180.517   Fipronil; tolerances for residues.
§180.518   Pyrimethanil; tolerances for residues.
§180.519   Bromide ion and residual bromine; tolerances for residues.
§180.521   Fumigants for grain-mill machinery; tolerances for residues.
§180.522   Fumigants for processed grains used in production of fermented malt beverage; tolerances for residues.
§180.523   Metaldehyde; tolerances for residues.
§180.525   Resmethrin; tolerances for residues.
§180.526   Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.
§180.527   Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.
§180.532   Cyprodinil; tolerances for residues.
§180.533   Esfenvalerate; tolerances for residues.
§180.535   Fluroxypyr 1-methylheptyl ester; tolerances for residues.
§180.537   Isoxaflutole; tolerances for residues.
§180.539   d-Limonene; tolerances for residues.
§180.540   Fenitrothion; tolerances for residues.
§180.543   Diclosulam; tolerances for residues.
§180.544   Methoxyfenozide; tolerances for residues.
§180.545   Prallethrin; tolerances for residues.
§180.546   Mefenoxam; tolerances for residues.
§180.547   Prohexadione calcium; tolerances for residues.
§180.549   Diflufenzopyr; tolerances for residues.
§180.551   Fluthiacet-methyl; tolerances for residues.
§180.552   Sulfosulfuron; tolerances for residues.
§180.553   Fenhexamid; tolerances for residues.
§180.554   Kresoxim-methyl; tolerances for residues.
§180.555   Trifloxystrobin; tolerances for residues.
§180.556   Pymetrozine; tolerances for residues.
§180.557   Tetraconazole; tolerances for residues.
§180.559   Clodinafop-propargyl; tolerances for residues.
§180.560   Cloquintocet-mexyl; tolerances for residues.
§180.561   Acibenzolar-S-methyl; tolerances for residues.
§180.562   Flucarbazone-sodium; tolerances for residues.
§180.563   Ethametsulfuron-methyl; tolerances for residues.
§180.564   Indoxacarb; tolerances for residues.
§180.565   Thiamethoxam; tolerances for residues.
§180.566   Fenpyroximate; tolerances for residues.
§180.567   Zoxamide; tolerances for residues.
§180.568   Flumioxazin; tolerances for residues.
§180.569   Forchlorfenuron; tolerances for residues.
§180.570   Isoxadifen-ethyl; tolerances for residues.
§180.571   Mesotrione; tolerances for residues.
§180.572   Bifenazate; tolerance for residues.
§180.573   Tepraloxydim; tolerances for residues.
§180.574   Fluazinam; tolerances for residues.
§180.575   Sulfuryl fluoride; tolerances for residues.
§180.576   Cyhalofop-butyl; tolerances for residues.
§180.577   Bispyribac-sodium; tolerances for residues.
§180.578   Acetamiprid; tolerances for residues.
§180.579   Fenamidone; tolerances for residues.
§180.580   Iodosulfuron-Methyl-Sodium; tolerances for residues.
§180.581   Iprovalicarb; tolerances for residues.
§180.582   Pyraclostrobin; tolerances for residues.
§180.583   Triticonazole; tolerances for residues.
§180.584   Tolylfluanid; tolerances for residues.
§180.585   Pyraflufen-ethyl; tolerances for residues.
§180.586   Clothianidin; tolerances for residues.
§180.587   Famoxadone; tolerance for residues.
§180.588   Quinoxyfen; tolerances for residues.
§180.589   Boscalid; tolerances for residues.
§180.590   2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.
§180.591   Trifloxysulfuron; tolerances for residues.
§180.592   Butafenacil; tolerances for residues.
§180.593   Etoxazole; tolerances for residues.
§180.594   Thiacloprid; tolerances for residues.
§180.595   Flufenpyr-ethyl; tolerances for residues.
§180.596   Fosthiazate; tolerances for residues.
§180.597   Mesosulfuron-methyl; tolerances for residues.
§180.598   Novaluron; tolerances for residues.
§180.599   Acequinocyl; tolerances for residues.
§180.600   Propoxycarbazone; tolerances for residues.
§180.601   Cyazofamid; tolerances for residues.
§180.602   Spiroxamine; tolerances for residues.
§180.603   Dinotefuran; tolerances for residues.
§180.604   Mepanipyrim; tolerances for residues.
§180.605   Penoxsulam; tolerances for residues.
§180.607   Spiromesifen; tolerances for residues.
§180.608   Spirodiclofen; tolerances for residues.
§180.609   Fluoxastrobin; tolerances for residues.
§180.610   Aminopyralid; tolerances for residues.
§180.611   Pinoxaden; tolerances for residues.
§180.612   Topramezone; tolerances for residues.
§180.613   Flonicamid; tolerances for residues.
§180.614   Kasugamycin; tolerances for residues.
§180.615   Amicarbazone; tolerances for residues.
§180.616   Fenpropimorph; tolerances for residues.
§180.617   Metconazole; tolerances for residues.
§180.618   Benthiavalicarb-isopropyl; tolerance for residues.
§180.619   Epoxiconazole; tolerances for residues.
§180.620   Etofenprox; tolerances for residues.
§180.621   Dithianon; tolerances for residues.
§180.622   Ethaboxam; tolerances for residues.
§180.623   Flufenoxuron; tolerances for residues.
§180.624   Metrafenone; tolerances for residues.
§180.625   Orthosulfamuron; tolerances for residues.
§180.626   Prothioconazole; tolerances for residues.
§180.627   Fluopicolide; tolerances for residues.
§180.628   Chlorantraniliprole; tolerances for residues.
§180.629   Flutriafol; tolerances for residues.
§180.631   Pyrasulfotole; tolerances for residues.
§180.632   Fenazaquin; Tolerances for residues.
§180.633   Florasulam; tolerances for residues.
§180.634   Tembotrione; tolerances for residues.
§180.635   Spinetoram; tolerances for residues.
§180.636   1,3-dichloropropene; tolerances for residues.
§180.637   Mandipropamid; tolerances for residues.
§180.638   Pyroxsulam; tolerances for residues.
§180.639   Flubendiamide; tolerances for residues.
§180.640   Pyridalyl; tolerances for residues.
§180.641   Spirotetramat; tolerances for residues.
§180.643   Uniconazole; tolerances for residues.
§180.644   Cyprosulfamide; tolerances for residues.
§180.645   Thiencarbazone-methyl; tolerances for residues.
§180.646   Ipconazole; tolerances for residues.
§180.647   d-Phenothrin; tolerances for residues.
§180.648   Meptyldinocap; tolerances for residues.
§180.649   Saflufenacil; tolerances for residues.
§180.650   Isoxaben; tolerances for residues.
§180.651   Imazosulfuron; tolerances for residues.
§180.652   Ethiprole; tolerances for residues.
§180.653   Indaziflam; tolerances for residues.
§180.654   Isopyrazam; tolerances for residues.
§180.655   Flazasulfuron; tolerances for residues.
§180.656   Amisulbrom; tolerances for residues.
§180.657   Metaflumizone; tolerances for residues.
§180.658   Penthiopyrad; tolerances for residues.
§180.659   Pyroxasulfone; tolerances for residues.
§180.660   Pyriofenone; tolerances for residues.
§180.661   Fluopyram; tolerances for residues.
§180.662   Trinexapac-ethyl; tolerances for residues.
§180.663   Ametoctradin; tolerances for residues.
§180.664   Penflufen; tolerances for residues.
§180.665   Sedaxane; tolerances for residues.
§180.666   Fluxapyroxad; tolerances for residues.
§180.667   Cyflufenamid, tolerance for residues.
§180.668   Sulfoxaflor; tolerances for residues.
§180.669   Picoxystrobin; tolerances for residues.
§180.671   Fenpyrazamine; tolerances for residues.
§180.672   Cyantraniliprole; tolerances for residues.
§180.673   Triforine; tolerances for residues.
§180.674   Proquinazid; tolerances for residues.
§180.675   Tolfenpyrad; tolerances for residues.
§180.676   Fenpropidin; tolerances for residues.
§180.677   Cyflumetofen; tolerances for residues.
§180.678   Tricyclazole; tolerances for residues.
§180.679   Flupyradifurone; tolerances for residues.
§180.680   Fluensulfone; tolerances for residues.
§180.681   Isofetamid; tolerances for residues.
§180.682   Bicyclopyrone; tolerances for residues.
§180.684   Benalaxyl-M; tolerances for residues.
§180.685   Oxathiapiprolin; tolerances for residues.
§180.686   Benzovindiflupyr; tolerances for residues.
§180.687   Teflubenzuron; tolerances for residues.
§180.688   Diethofencarb; tolerance for residue.
§180.689   Aminocyclopyrachlor; tolerances for residues.
§180.690   Mandestrobin; tolerances for residues.
§180.691   Halauxifen-methyl; tolerances for residues.
§180.692   Tioxazafen; tolerances for residues.
§180.693   Benzobicyclon; tolerances for residues.
§180.694   Cyclaniliprole; tolerances for residues.
§180.696   Tolpyralate; tolerances for residues.
§180.697   Flutianil; tolerances for residues.
§180.698   Chlormequat chloride; tolerances for residues.
§180.699   Pydiflumetofen; tolerances for residues.
§180.700   Afidopyropen; tolerances for residues.
§180.701   Pyrifluquinazon; tolerances for residues.
§180.702   Bixafen; tolerances for residues.
§180.703   6-benzyladenine; tolerances for residues.
§180.704   Sulfometuron-methyl; tolerances for residues.
§180.705   Mefentrifluconazole; tolerances for residues.
§180.706   Valifenalate; tolerances for residues.
§180.708   Isotianil; tolerances for residues.
§180.710   Pethoxamid; tolerances for residues.
§180.711   1-Aminocyclopropane-1-carboxylic acid (ACC); temporary exemption from the requirement of a tolerance for residues.
§180.712   Inpyrfluxam; tolerances for residues.
§180.713   Tiafenacil; tolerances for residues.
§180.714   Broflanilide; tolerances for residues.
§180.715   Fluxametamide; tolerances for residues.

Editorial Note: Nomenclature changes to subpart C of part 180 appear at 67 FR 41803, June 19, 2002; 67 FR 42393, June 21, 2002; 68 FR 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 FR 60155, Oct. 10, 2008; 75 FR 56014, Sept. 15, 2010; and 76 FR 34885, June 15, 2011.

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§180.101   Specific tolerances; general provisions.

(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from their application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms of parts by weight of the pesticide chemical per one million parts by weight of the raw agricultural commodity.

(b) The poisonous and deleterious substances for which tolerances are established by the regulations in this subpart C are named by their common names wherever practicable, otherwise by their chemical names.

(c) The analytical methods to be used for determining whether pesticide residues, including negligible residues, in or on raw agricultural commodities are in compliance with the tolerances established in this part 180 are identified among the methods contained or referenced in the Food and Drug Administration's “Pesticide Analytical Manual” which is available from the Food and Drug Administration, Department of Health, Education, and Welfare, 200 C Street SW., Washington, DC 20204.

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§180.103   Captan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) in or on the following commodities:

CommodityParts per million
Almond0.25
Almond, hulls75.0
Animal feed, nongrass, group 180.05
Apple25.0
Apricot10.0
Blueberry20.0
Caneberry, subgroup 13A25.0
Cherry, sweet50.0
Cherry, tart50.0
Cotton, undelinted seed0.05
Dill, seed0.05
Flax, seed0.05
Grape25.0
Grain, cereal, forage, fodder and straw, group 160.05
Grain, cereal, group 150.05
Grass, forage0.05
Grass, hay0.05
Nectarine25.0
Okra0.05
Peach15.0
Peanut0.05
Peanut, hay0.05
Pear25.0
Plum, prune, fresh10.0
Rapeseed, forage0.05
Rapeseed, seed0.05
Safflower, seed0.05
Sesame, seed0.05
Strawberry20.0
Sunflower, seed0.05
Vegetable, brassica leafy, group 50.05
Vegetable, bulb, group 30.05
Vegetable, cucurbit, group 90.05
Vegetable, foliage of legume, group 70.05
Vegetable, fruiting, group 80.05
Vegetable, leafy, except brassica, group 40.05
Vegetable, leaves of root and tuber, group 20.05
Vegetable, legume, group 60.05
Vegetable, root and tuber, group 10.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at THPI, in or on the following commodities:

CommodityParts per million
Cattle, fat0.15
Cattle, meat0.20
Cattle, meat byproducts0.30
Goat, fat0.15
Goat, meat0.20
Goat, meat byproducts0.30
Hog, fat0.15
Hog, meat0.20
Hog, meat byproducts0.30
Horse, fat0.15
Horse, meat0.20
Horse, meat byproducts0.30
Milk0.10
Sheep, fat0.15
Sheep, meat0.20
Sheep, meat byproducts0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52016, Sept. 12, 2007]

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§180.106   Diuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food commodities, as follows:

Commodity Parts per million
Alfalfa, forage3.0
Alfalfa, hay2.0
Apple0.1
Artichoke, globe1
Asparagus7
Banana0.1
Berry group 130.1
Cattle, fat1
Cattle, meat1
Cattle, meat byproducts1
Citrus, oil3.0
Corn, field, grain0.1
Corn, pop, grain0.1
Cotton, undelinted seed0.2
Fish - freshwater finfish, farm raised2.0
Fruit, citrus, group 10, except lemon0.05
Goat, fat1
Goat, meat1
Goat, meat byproducts1
Grain, aspirated fractions5.0
Grape0.05
Grass, forage, except bermudagrass2
Grass, hay, except bermudagrass2
Hazelnut0.1
Hog, fat1
Hog, meat1
Hog, meat byproducts1
Horse, fat1
Horse, meat1
Horse, meat byproducts1
Lemon0.5
Nut, macadamia0.05
Olive1
Papaya0.5
Peach0.1
Pear1
Pea, field, seed0.1
Pea, field, vines2
Pea, field, hay2
Pecan0.05
Peppermint, tops1.5
Pineapple0.1
Pineapple, process residue0.4
Sheep, fat1
Sheep, meat1
Sheep, meat byproducts1
Sorghum, grain, forage2
Sorghum, grain, grain0.5
Sorghum, grain, stover2
Spearmint, tops1.5
Sugarcane, cane0.2
Sugarcane, molasses0.7
Walnut0.05
Wheat, bran0.7
Wheat, forage2
Wheat, grain0.5
Wheat, hay2
Wheat, straw1.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:

Commodity Parts per million
Barley, bran0.7
Barley, grain0.2
Barley, hay2
Barley, straw1.5
Cactus0.05
Clover, forage0.1
Clover, hay1.0
Oat, forage2
Oat, grain0.1
Oat, hay2
Oat, straw1.5
Trefoil, forage0.1
Trefoil, hay1.5
Vetch, forage0.1
Vetch, hay1.5

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June 13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

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§180.107   Triflumezopyrim; tolerance for residues.

(a) General. Tolerances are established for residues of the insecticide triflumezopyrim, including its metabolites and degradates, in or on the following food commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only triflumezopyrim (2,4-dioxo-1-(5-pyrimidinylmethyl)-3-[3-(trifluoromethyl)phenyl]-2H-pyrido[1,2-a] pyrimidinium inner salt) in or on the commodity.

CommodityParts per
million
Rice, grain*0.40
Rice, hulls*1.0

*There are no U.S. registrations for the use of triflumezopyrim on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48005, Oct. 16, 2017]

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§180.108   Acephate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity1Parts per million
Bean, dry, seed3.0
Brussels sprouts3.0
Cattle, fat0.1
Cattle, meat0.1
Cattle, meat byproducts0.1
Cauliflower2.0
Celery10
Cotton, hulls1.0
Cotton, meal1.0
Cotton, undelinted seed0.5
Cranberry0.5
Egg0.1
Goat, fat0.1
Goat, meat0.1
Goat, meat byproducts0.1
Hog, fat0.1
Hog, meat0.1
Hog, meat byproducts0.1
Horse, fat0.1
Horse, meat0.1
Horse, meat byproducts0.1
Lettuce, head10
Milk0.1
Peanut0.2
Pepper4.0
Peppermint, tops27
Poultry, fat0.1
Poultry, meat0.1
Poultry, meat byproducts0.1
Sheep, fat0.1
Sheep, meat0.1
Sheep, meat byproducts0.1
Spearmint, tops27
Soybean, seed1.0

1Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on all food items (other than those already covered by a higher tolerance as a result of use on growing crops) in food handling establishments where food and food products are held, processed, prepared and served, including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, where application of acephate shall be limited solely to spot and/or crack and crevice treatment (a coarse, low-pressure spray shall be used to avoid atomization or splashing of the spray for spot treatments; equipment capable of delivering a pin-stream of insecticide shall be used for crack and crevice treatments). Spray concentration shall be limited to a maximum of 1.0 percent active ingredient. Contamination of food or food-contact surfaces shall be avoided. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

(3) Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, including its metabolites and degradates, in or on the commodities in the following table as a result of the application of acephate. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the commodity.

CommodityParts per million
Bean, dry, seed1
Brussels sprouts0.5
Cauliflower0.5
Celery1
Cranberry0.1
Lettuce, head1
Pepper1
Peppermint, tops1
Spearmint, tops1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity1Parts per million
Nut, macadamia0.05

1Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010; 81 FR 34905, June 1, 2016]

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§180.109   Fenpicoxamid; Tolerances for residues.

(a) General. Tolerances are established for residues of fenpicoxamid including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels for fenpicoxamid is to be determined by measuring only fenpicoxamid ([[4-methoxy-2-[[[(3S,7R,8R,9S)-9-methyl-8-(2-methyl-1-oxopropoxy)-2,6-dioxo-7-(phenylmethyl)-1,5-dioxonan-3-yl]amino]carbonyl]-3-pyridinyl]oxy]methyl 2-methylpropanoate) in or on the commodity.

CommodityParts per
million
Banana*0.15
Wheat, grain*0.60
Rye, grain*0.60

*There are no U.S. registrations for use of fenpicoxamid on this commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48000, Oct. 16, 2017]

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§180.111   Malathion; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) in or on the following food commodities:

CommodityParts per million
Alfalfa, forage135
Alfalfa, hay135
Almond, hulls50
Almond, postharvest8
Apple8
Apricot8
Asparagus8
Avocado8
Barley, grain, postharvest8
Bean, dry, seed8
Bean, succulent8
Beet, garden, roots8
Beet, garden, tops8
Beet, sugar, roots1
Beet, sugar, tops8
Blackberry8
Blueberry8
Boysenberry8
Carrot, roots8
Chayote, fruit8
Chayote, roots8
Cherry8
Chestnut1
Clover, forage135
Clover, hay135
Corn, field, forage8
Corn, field, grain, postharvest8
Corn, pop, grain, postharvest8
Corn, sweet, forage8
Corn, sweet, kernel plus cob with husks removed2
Cowpea, forage135
Cowpea, hay135
Cranberry8
Cucumber8
Currant8
Date, dried fruit8
Dewberry8
Eggplant8
Fig8
Flax, seed0.1
Garlic, bulb8
Gooseberry8
Grape8
Grapefruit8
Guava8
Hazelnut1
Hop, dried cones1
Horseradish8
Kumquat8
Leek8
Lemon8
Lentil, seed8
Lespedeza, hay135
Lime8
Loganberry8
Lupin, seed8
Mango8
Melon8
Mushroom8
Nectarine8
Nut, macadamia1
Oat, grain, postharvest8
Okra8
Onion, bulb8
Onion, green8
Orange8
Papaya1
Parsnip8
Passionfruit8
Pea8
Pea, field, hay8
Pea, field, vines8
Peach8
Peanut, hay135
Peanut, postharvest8
Pear8
Pecan8
Pepper8
Peppermint, tops8
Pineapple8
Plum8
Plum, prune8
Potato8
Pumpkin8
Quince8
Radish8
Raspberry8
Rice, grain, postharvest8
Rice, wild8
Rutabaga8
Rye, grain, postharvest8
Safflower, seed0.2
Salsify, roots8
Salsify, tops8
Shallot, bulb8
Sorghum, grain, forage8
Sorghum, grain, grain, postharvest8
Soybean, forage135
Soybean, hay135
Soybean, seed8
Soybean, vegetable, succulent8
Spearmint, tops8
Squash, summer8
Squash, winter8
Strawberry8
Sunflower, seed, postharvest8
Sweet potato, roots1
Tangerine8
Tomato8
Trefoil, forage135
Trefoil, hay135
Turnip, greens8
Turnip, roots8
Vegetable, brassica, leafy, group 58
Vegetable, leafy, except brassica, group 48
Vetch, hay135
Walnut8
Wheat, grain, postharvest8

(2) Tolerances are established for the combined residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) and its metabolite, malaoxon (O,O-dimethyl thiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

CommodityParts per million
Barley, straw50
Corn, field, stover30.0
Cotton, undelinted seed20.0
Grass, forage200
Grass, hay270
Oat, forage4.0
Oat, straw50
Rye, forage4.0
Rye, straw50
Watercress0.2
Wheat, forage4.0
Wheat, straw50

(3) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

CommodityParts per million
Cattle, fat4
Cattle, meat14
Cattle, meat byproducts14
Egg0.1
Goat, fat4
Goat, meat14
Goat, meat byproducts14
Hog, fat4
Hog, meat14
Hog, meat byproducts14
Horse, fat4
Horse, meat14
Horse, meat byproducts14
Milk, fat0.5
Poultry, fat4
Poultry, meat14
Poultry, meat byproducts14
Sheep, fat4
Sheep, meat14
Sheep, meat byproducts14

1The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, poultry, or sheep.

(4) Malathion may be safely used in accordance with the following conditions:

(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot.

(ii) Treated paper trays are intended for use only in the drying of grape (raisins).

(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to grape before harvest shall not exceed 12 parts per million on processed ready-to-eat raisins.

(5) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not exceed 0.6 parts per million.

(6) Malathion may be safely used for the control of insects during the drying of grape (raisins) in compliance with paragraph (a)(4) of this section by incorporation into paper trays in amounts not exceeding 100 milligrams per square foot.

(7) Malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in accordance with the following conditions.

(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle feed, when present as the result of the application of the pesticide to bagged citrus pulp during storage. Whether or not tolerances for residues of malathion on the fresh fruit have been established under section 408 of the Act, the total residue of malathion in the citrus, dried pulp shall not exceed 50 parts per million.

(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate blocks resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle feed concentrate blocks.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, 2010]

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§180.114   Ferbam; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

CommodityParts per millionExpiration/Revocation Date
Apple4.01None
Bean7.0110/27/07
Cabbage7.0110/27/07
Cherry4.01None
Cranberry4.01None
Fruit, citrus, group 104.01None
Grape4.01None
Lettuce7.0110/27/07
Nectarine4.01None
Peach4.01None
Pear4.01None
Raspberry7.0110/27/07

1Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

CommodityParts per million
Mango4.01

1This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

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§180.116   Ziram; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate), including its metabolites and degradates, in or on the commodities in the table below as a result of the application of ziram. Compliance with the tolerance levels specified below is to be determined by measuring total dithiocarbamates, determined as CS2, evolved during acid digestion and expressed as zinc ethylenebisdithiocarbamate.

CommodityParts per million
Almond10.10
Apple17.0
Apricot17.0
Blueberry17.0
Cherry, sweet17.0
Cherry, tart17.0
Grape7.0
Hazelnut0.10
Huckleberry7.0
Peach7.0
Pear17.0
Pecan0.10
Quince17.0
Strawberry7.0
Tomato17.0

1Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Public Law 518, 83d Congress (68 Stat. 511).

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008; 77 FR 59123, Sept. 26, 2012; 82 FR 57860, Dec. 8, 2017]

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§180.117   S-Ethyl dipropylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl dipropylthiocarbamate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of S-ethyl dipropylthiocarbamate, S-ethyl (2-hydroxypropyl)propylcarbamothioate, S-(2-hydroxyethyl)dipropylcarbamothioate, and S-ethyl (3-hydroxypropyl)propylcarbamothioate, calculated as the stoichiometric equivalent of S-ethyl dipropylthiocarbamate, in or on the commodity.

CommodityParts per million
Alfalfa, forage0.2
Alfalfa, hay0.6
Almond0.08
Almond, hulls0.08
Bean, dry, seed0.08
Bean, succulent0.08
Beet, garden, tops0.5
Beet, sugar, molasses0.4
Beet, sugar, tops0.5
Clover, forage0.1
Clover, hay0.1
Corn, field, forage0.08
Corn, field, grain0.08
Corn, field, stover0.08
Corn, pop, grain0.08
Corn, pop, stover0.08
Corn, sweet, forage0.08
Corn, sweet, kernel plus cob with husks removed0.08
Corn, sweet, stover0.08
Cotton, gin byproducts0.20
Cotton, undelinted seed0.08
Fruit, citrus, group 100.1
Grass, forage0.60
Grass, hay0.50
Lespedeza, forage0.1
Lespedeza, hay0.1
Pea, succulent0.08
Safflower, seed0.08
Sunflower, seed0.08
Tomato0.08
Trefoil, forage0.1
Trefoil, hay0.1
Vegetable, root0.1
Walnut0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60239, Sept. 29, 2010, as amended at 82 FR 42952, Sept. 13, 2017]

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§180.123   Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on the following food commodities which have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest (with the exception of strawberry):

CommodityParts per million Expiration/Revocation Date
Alfalfa, hay, postharvest50.010/31/11
Almond, postharvest200.0None
Apple, postharvest5.0None
Apricot, postharvest20.0None
Artichoke, jerusalem, postharvest30.0None
Asparagus, postharvest100.0None
Avocado, postharvest75.0None
Barley, grain, postharvest50.0None
Bean, lima, postharvest50.0None
Bean, postharvest50.0None
Bean, snap, succulent, postharvest50.0None
Bean, succulent, postharvest50.0None
Beet, garden, roots, postharvest30.0None
Beet, sugar, roots, postharvest30.0None
Blueberry, postharvest20.0None
Butternut, postharvest200.0None
Cabbage, postharvest50.0None
Cacao bean, roasted bean, postharvest50.0None
Cantaloupe, postharvest20.0None
Carrot, roots, postharvest30.0None
Cashew, postharvest200.0None
Cherry, sweet, postharvest20.0None
Cherry, tart, postharvest20None
Chestnut, postharvest200.0None
Cippolini, bulb, postharvest50.0None
Citron, citrus, postharvest30.0None
Coconut, copra, postharvest100.0None
Coffee, bean, green, postharvest75.0None
Corn, field, grain, postharvest50.0None
Corn, pop, postharvest240.0None
Corn, sweet, kernel plus cob with husks removed, postharvest50.0None
Cotton, undelinted seed, postharvest200.010/31/11
Cucumber, postharvest30.0None
Cumin, seed, postharvest100.0None
Eggplant, postharvest20.0None
Garlic, postharvest50.0None
Ginger, postharvest100.0None
Grape, postharvest20.0None
Grapefruit, postharvest30.0None
Hazelnut, postharvest200.0None
Horseradish, postharvest30.0None
Kumquat, postharvest30.0None
Lemon, postharvest30.0None
Lime, postharvest30.0None
Melon, honeydew, postharvest20.0None
Muskmelon, postharvest20.0None
Nectarine, postharvest20.0None
Nut, brazil, postharvest200.0None
Nut, hickory, postharvest200.0None
Nut, macadamia, postharvest200.0None
Oat, postharvest50.0None
Okra, postharvest30.0None
Onion, bulb, postharvest20.0None
Onion, green, postharvest20.0None
Orange, postharvest30.0None
Parsnip, roots, postharvest30.0None
Peach, postharvest20.0None
Peanut, postharvest200.0None
Pear, postharvest5.0None
Pea, blackeyed, postharvest50.0None
Pea, postharvest50.0None
Pecan, postharvest200.0None
Pepper, postharvest30.0None
Pimento, postharvest30.0None
Pineapple, postharvest20.0None
Pistachio, postharvest200.0None
Plum, postharvest20.0None
Pomegranate, postharvest100.0None
Potato, postharvest75.0None
Pumpkin, postharvest20.0None
Quince, postharvest5.0None
Radish, postharvest30.0None
Rice, grain, postharvest50.0None
Rutabaga, roots, postharvest30.0None
Rutabaga, tops, postharvest30.0None
Rye, grain, postharvest50.0None
Salsify, roots, postharvest30.0None
Sorghum, grain, grain, postharvest50.0None
Soybean, postharvest200.0None
Squash, summer, postharvest30.0None
Squash, winter, postharvest20.0None
Squash, zucchini, postharvest20.0None
Strawberry, postharvest60.0None
Sweet potato, postharvest75.0None
Tangerine, postharvest30.0None
Timothy, hay, postharvest50.010/19/10
Tomato, postharvest20.0None
Turnip, roots, postharvest30.0None
Walnut, postharvest200.0None
Watermelon, postharvest20.0None
Wheat50.0None

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the following conditions:

(i) When inorganic bromide residues are present as a result of fumigation of the processed food with methyl bromide or from such fumigation in addition to the authorized use of methyl bromide on the source raw agricultural commodity, as provided for in this part, the total residues of inorganic bromides (calculated as Br) shall not exceed the following levels:

(A) 400 parts per million in or on egg, dried and herb, processed and spice.

(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.

(C) 250 parts per million in or on tomato, concentrated products and fig, dried fruit.

(D) 125 parts per million in or on processed food other than those listed above.

(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR 172.730(a)(2), the amount shall not exceed 25 parts per million (calculated as Br).

(iii) Where tolerances are established on both the raw agricultural commodities and processed food made therefrom, the total residues of inorganic bromides in or on the processed food shall not be greater than those designated in paragraph (a)(2) of this section, unless a higher level is established elsewhere in this part.

(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:

(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.

(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley, corn, grain sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or from carryover and concentration of residues of inorganic bromides from fumigation of the grains with methyl bromide.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of inorganic bromides (calculated as Br) in or on the following food commodity grown in soil fumigated with methyl bromide.

CommodityParts per million
Ginger, postharvest100

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74812, Dec. 13, 2006, as amended at 75 FR 60239, Sept. 29, 2010]

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§180.123a   Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been used as feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will contribute considerable residues of inorganic bromides to the meat and milk.

(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such peanut hulls as animal feed. Peanut hulls containing residues of inorganic bromides from the use of methyl bromide are unsuitable as an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.

[58 FR 65555, Dec. 15, 1993]

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§180.124   Methyl bromide; tolerances for residues.

(a) General. A tolerance is established for residues of the fumigant methyl bromide, including metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be determined by measuring only methyl bromide.

CommodityParts per
million
Cotton, undelinted seed150

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fumigant methyl bromide, including its metabolites and degradates, in or on the specified agricultural commodities in Table 2 to this paragraph (b). Compliance with the tolerance levels specified in Table 2 to this paragraph (b) is to be determined by measuring only methyl bromide, in or on the commodities, resulting from use of the pesticide pursuant to Federal Insecticide, Fungicide, Rodenticide Act (FIFRA) section 18 emergency exemptions. The tolerances expire and are revoked on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

CommodityParts per
million
Expiration/
revocation
date
Berry and small fruit, group 13-075.012/31/23
Cactus3.012/31/23
Coconut, copra8.012/31/23
Coffee, green bean15012/31/23
Cola, seed15012/31/23
Cucurbit, seed15012/31/23
Fig1012/31/23
Fruit, citrus, group 10-10212/31/23
Fruit, stone, group 12-125.012/31/23
Fruit, tropical and subtropical, edible peel, group 231012/31/23
Fruit, tropical and subtropical, inedible peel, group 245.012/31/23
Herb and spice, group 193512/31/23
Hibiscus, seed15012/31/23
Ivy gourd5.012/31/23
Kaffir lime, leaves0.5012/31/23
Kenaf, seed15012/31/23
Oilseed group 2015012/31/23
Peppermint, tops3512/31/23
Pointed gourd5.012/31/23
Spearmint, tops3512/31/23
Vegetable, bulb, group 3-072.012/31/23
Vegetable, cucurbit, group 95.012/31/23
Vegetable, foliage of legume, group 70.5012/31/23
Vegetable, fruiting, group 8-107.012/31/23
Vegetable, head and stem Brassica, group 5-161.012/31/23
Vegetable, leafy, group 4-160.5012/31/23
Vegetable, leaves of root and tuber, group 20.5012/31/23
Vegetable, legume, group 63.012/31/23
Vegetable, root and tuber, group 13.012/31/23
Vegetable, stalk, stem and leaf petiole, group 220.5012/31/23

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 35298, June 13, 2012, as amended at 83 FR 8763, Mar. 1, 2018; 85 FR 65734, Oct. 16, 2020; 86 FR 8703, Feb. 9, 2021]

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§180.127   Piperonyl butoxide; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl piperonyl)ether] are established in or on the following food commodities:

CommodityParts per million
Almond, postharvest8
Apple, postharvest8
Barley, postharvest20
Bean, postharvest8
Birdseed, mixtures, postharvest20
Blackberry, postharvest8
Blueberry, postharvest8
Boysenberry, postharvest8
Buckwheat, grain, postharvest20
Cattle, fat0.1
Cattle, meat0.1
Cattle, meat byproducts0.1
Cherry, sweet, postharvest8
Cherry, tart, postharvest8
Cacoa bean, roasted bean, postharvest8
Coconut, copra, postharvest8
Corn, field, grain, postharvest20
Corn, pop, postharvest20
Cotton, undelinted seed, postharvest8
Crabapple, postharvest8
Currant, postharvest8
Dewberry, postharvest8
Egg1
Fig, postharvest8
Flax, seed, postharvest8
Goat, fat0.1
Goat, meat0.1
Goat, meat byproducts0.1
Gooseberry, postharvest8
Grape, postharvest8
Guava, postharvest8
Hog, fat0.1
Hog, meat0.1
Hog, meat byproducts0.1
Horse, fat0.1
Horse, meat0.1
Horse, meat byproducts0.1
Loganberry, postharvest8
Mango, postharvest8
Milk, fat0.25
Muskmelon, postharvest8
Oat, postharvest8
Orange, postharvest8
Peach, postharvest8
Peanut, postharvest8
Pea, postharvest8
Pear, postharvest8
Pineapple, postharvest8
Plum, prune, fresh, postharvest8
Potato, postharvest0.25
Poultry, fat3
Poultry, meat3
Poultry, meat byproducts3
Raspberry, postharvest8
Rice, postharvest20
Rye, postharvest20
Sheep, fat0.1
Sheep, meat0.1
Sheep, meat byproducts0.1
Sorghum, grain, postharvest8
Sweet potato, postharvest0.25
Tomato, postharvest8
Walnut, postharvest8
Wheat, postharvest20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of piperonyl butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the formulation.

(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for food, dried.

(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are constructed with waxed paper liners and are to be used only for food, dried that contain 4 percent fat or less.

(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it is incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl butoxide per square foot (538 milligrams per square meter). Such treated bags are to be used only for packaging plum, prune, dried; grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12 milligrams of piperonyl butoxide per ounce of fruit (0.10 milligram of piperonyl butoxide per gram of product).

(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to such use.

(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide for insect control in accordance with 21 CFR 178.3730.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:

(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(C) Food treated in accordance with 21 CFR 178.3730.

(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the cloth of cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(v) Where tolerances are established on both raw agricultural commodities and processed food made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot.

(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth. Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried that contain 4 percent fat or less.

(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as the result of migration:

(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency.

(v) Where tolerances are established on both the raw agricultural commodities and food, processed made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74813, Dec. 13, 2006]

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§180.128   Pyrethrins; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (pyrethrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl-2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (jasmolin 1), and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles of Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1, and jasmolin 1 are not to exceed the following:

CommodityParts per million
Almond, postharvest1.0
Apple, postharvest1.0
Barley, grain, postharvest3.0
Bean, succulent, postharvest1.0
Birdseed, mixtures, postharvest3.0
Blackberry, postharvest1.0
Blueberry, postharvest1.0
Boysenberry, postharvest1.0
Buckwheat, grain, postharvest3.0
Cacao bean, roasted bean, postharvest1.0
Cattle, fat1.0
Cattle, meat0.05
Cattle, meat byproducts0.05
Cherry, sweet, postharvest1.0
Cherry, tart, postharvest1.0
Coconut, copra, postharvest1.0
Corn, field, grain, postharvest3.0
Corn, pop, grain, postharvest3.0
Cotton, undelinted seed, postharvest1.0
Crabapple, postharvest1.0
Currant, postharvest1.0
Dewberry, postharvest1.0
Fig, postharvest1.0
Flax, seed, postharvest1.0
Goat, fat1.0
Goat, meat0.05
Goat, meat byproducts0.05
Gooseberry, postharvest1.0
Grape, postharvest1.0
Guava, postharvest1.0
Hog, fat1.0
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat1.0
Horse, meat0.05
Horse, meat byproducts0.05
Loganberry, postharvest1.0
Mango, postharvest1.0
Milk, fat (reflecting negligible residues in milk)0.05
Muskmelon, postharvest1.0
Oat, grain, postharvest1.0
Orange, postharvest1.0
Pea, dry, seed, postharvest1.0
Peach, postharvest1.0
Peanut, postharvest1.0
Pear, postharvest1.0
Pineapple, postharvest1.0
Plum, prune, fresh, postharvest1.0
Potato, postharvest0.05
Raspberry, postharvest1.0
Rice, grain, postharvest3.0
Rye, grain, postharvest3.0
Sheep, fat1.0
Sheep, meat0.05
Sheep, meat byproducts0.05
Sorghum, grain, grain, postharvest1.0
Sweet potato, postharvest0.05
Tomato, postharvest1.0
Walnut, postharvest1.0
Wheat, grain, postharvest3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions derived from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served. Food must be removed or covered prior to use.

(4) Where tolerances are established on both the raw agricultural commodities and processed foods made there-from, the total residues of pyrethrins in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

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§180.129   o-Phenylphenol and its sodium salt; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide o-phenylphenol and sodium o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or on the following food commodities:

Commodity Parts per million
Apple25
Cantaloupe (NMT 10 ppm in edible portion)125
Carrot, roots20
Cherry5
Citrus fruits10
Cucumber10
Lemon10
Nectarine5
Orange10
Pepper, bell10
Peach20
Pear25.0
Pineapple10
Plum, prune, fresh20
Sweet potato, roots15
Tomato10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54960, Sept. 24, 2008]

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§180.130   Hydrogen Cyanide; tolerances for residues.

(a) General. A tolerance for residues of the insecticide hydrogen cyanide from postharvest fumigation as a result of application of sodium cyanide is established as follows: 50 parts per million in or on Fruit, citrus.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999]

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§180.132   Thiram; tolerances for residues.

(a) General. (1) A tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only thiram.

CommodityParts
per million
Avocado115

1No U.S. registrations as of September 23, 2009.

(2) Tolerances are established for residues of the fungicide thiram, tetramethyl thiuram disulfide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those thiram residues convertible to and expressed in terms of the degradate carbon disulfide, in or on the commodity.

CommodityParts
per million
Apple5
Banana12.0
Peach7.0
Strawberry13

1There are no U.S. registrations as of September 23, 2009.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 49615, July 31, 2002, as amended at 74 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015; 80 FR 72597, Nov. 20, 2015]

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§180.142   2,4-D; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

Table 1 to Paragraph (a)

CommodityParts per million
Almond hulls0.1
Asparagus5.0
Barley, bran4.0
Barley, grain2.0
Barley, straw50
Berry, group 130.2
Cattle, fat0.3
Cattle, kidney4.0
Cattle, meat0.3
Cattle, meat byproducts, except kidney0.3
Corn, field, forage6.0
Corn, field, grain0.05
Corn, field, stover50
Corn, pop, grain0.05
Corn, pop, stover50
Corn, sweet, forage6.0
Corn, sweet, kernel plus cob with husks removed0.05
Corn, sweet, stover50
Cotton, gin byproducts1.5
Cotton, undelinted seed0.08
Cranberry0.5
Fish0.1
Fruit, citrus, group 103.0
Fruit, pome, group 110.05
Fruit, stone, group 120.05
Goat, fat0.3
Goat, kidney4.0
Goat, meat0.3
Goat, meat byproducts, except kidney0.3
Grain, aspirated fractions40
Grape0.05
Grass, forage360
Grass, hay300
Hop, dried cones0.2
Horse, fat0.3
Horse, kidney4.0
Horse, meat0.3
Horse, meat byproducts, except kidney0.3
Millet, forage25
Millet, grain2.0
Millet, straw50
Milk0.05
Nut, tree, group 140.2
Oat, forage25
Oat, grain2.0
Oat, straw50
Pistachio0.05
Potato0.4
Rice, grain0.5
Rice, hulls2.0
Rye, bran4.0
Rye, forage25
Rye, grain2.0
Rye, straw50
Sesame, seed0.05
Sheep, fat0.3
Sheep, kidney4.0
Sheep, meat0.3
Sheep, meat byproducts, except kidney0.3
Shellfish1.0
Sorghum, grain, forage0.2
Sorghum, grain, grain0.2
Sorghum, grain, stover0.2
Soybean, forage0.02
Soybean, hay2.0
Soybean, seed0.02
Strawberry0.05
Sugarcane, cane0.05
Sugarcane, molasses0.2
Teff, bran4.0
Teff, forage25.0
Teff, grain2.0
Teff, straw50.0
Vegetable, leaves of root and tuber, group 20.1
Vegetable, root and tuber, except potato, group 10.1
Wheat, bran4.0
Wheat, forage25
Wheat, grain2.0
Wheat, straw50
Wheatgrass, intermediate, bran4
Wheatgrass, intermediate, forage30
Wheatgrass, intermediate, grain2
Wheatgrass, intermediate, straw50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the follow commodities:

CommodityParts per million
Rice, wild, grain0.05

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerances levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

CommodityParts per million
Animal feed, nongrass, group 180.2
Avocado0.05
Dill, seed0.05
Okra0.05
Vegetable, brassica leafy, group 50.4
Vegetable, bulb, group 30.05
Vegetable, cucurbit, group 90.05
Vegetable, foliage of legume, group 70.2
Vegetable, fruiting, group 80.05
Vegetable, leafy, except brassica, group 40.4
Vegetable, legume, group 60.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, 2009; 76 FR 55817, Sept. 9, 2011; 80 FR 72597, Nov. 20, 2015; 82 FR 9529, Feb. 7, 2017; 85 FR 82943, Dec. 21, 2020]

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§180.145   Fluorine compounds; tolerances for residues.

(a) General. (1) Tolerances are established for combined residues of the insecticidal fluorine compounds cryolite and synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:

CommodityParts per million
Apricot7
Blackberry7
Blueberry7
Boysenberry7
Broccoli7
Brussels sprouts7
Cabbage7
Cauliflower7
Collards7
Cranberry7
Cucumber7
Dewberry7
Eggplant7
Fruit, citrus7
Grape7
Kale7
Kohlrabi7
Lettuce, head7
Lettuce, leaf7
Loganberry7
Melon7
Nectarine7
Peach7
Pepper7
Plum, prune, fresh7
Pumpkin7
Raspberry7
Squash, summer7
Squash, winter7
Strawberry7
Tomato7
Youngberry7

(2) Tolerances are established for residues of fluoride in or on the following commodities from the postharvest fumigation with sulfuryl fluoride for the control of insects:

CommodityParts per million
All processed food commodities not otherwise listed70
Barley, bran, postharvest45.0
Barley, flour, postharvest45.0
Barley, grain, postharvest15.0
Barley, pearled barley, postharvest45.0
Cattle, meat, dried40
Cheese5.0
Cacao bean, roasted bean, postharvest20
Coconut, postharvest40
Coffee, bean, green, postharvest15
Corn, field, flour, postharvest35.0
Corn, field, grain, postharvest10.0
Corn, field, grits, postharvest10.0
Corn, field, meal, postharvest30.0
Corn, pop, grain, postharvest10.0
Cotton, undelinted seed, postharvest70
Egg, dried900
Fruit, dried, except grape, raisin, postharvest3.0
Ginger, postharvest70
Grain, aspirated fractions, postharvest55.0
Grape, raisin, postharvest7.0
Hog, meat20
Herbs and spices group 19, postharvest70
Milk, powdered5.0
Millet, grain, postharvest40.0
Nut, pine, postharvest20
Nut, tree, Group 14, postharvest10.0
Oat, flour, postharvest75.0
Oat, grain, postharvest25.0
Oat, groats/rolled oats75.0
Peanut, postharvest15
Pistachio, postharvest10.0
Rice, bran, postharvest31.0
Rice, flour, postharvest45
Rice, grain, postharvest12.0
Rice, hulls, postharvest35.0
Rice, polished rice, postharvest25.0
Rice, wild, grain, postharvest25.0
Sorghum, grain, postharvest40.0
Triticale, grain, postharvest40.0
Vegetable, legume, group 6, postharvest70
Wheat, bran, postharvest40.0
Wheat, flour, postharvest125.0
Wheat, germ, postharvest130.0
Wheat, grain, postharvest40.0
Wheat, milled byproducts, postharvest130.0
Wheat, shorts, postharvest40.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by §180.1(l), are established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic cryolite (sodium aluminum fluoride), in or on the following raw agricultural commodities:

CommodityParts per million
Kiwifruit15

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011]

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§180.151   Ethylene oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene oxide, when used as a postharvest fumigant in or on the following food commodities:

CommodityParts per million
Herb and spice, group 19, dried, except basil7
Licorice, roots7
Peppermint, tops, dried7
Sesame, seed7
Spearmint, tops, dried7
Vegetable, dried7
Walnut50

(2) Tolerances are established for residues of the ethylene oxide reaction product, 2-chloroethanol, commonly referred to as ethylene chlorohydrin, when ethylene oxide is used as a postharvest fumigant in or on food commodities as follows:

CommodityParts per million
Herb and spice, group 19, dried, except basil940
Licorice, roots940
Peppermint, tops, dried940
Sesame, seed940
Spearmint, tops, dried940
Vegetable, dried940

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009]

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§180.153   Diazinon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide diazinon, O,O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

CommodityParts per million
Almond, hulls3.0
Apple0.50
Apricot0.20
Bean, lima0.50
Bean, snap, succulent0.50
Beet, garden, roots0.75
Beet, garden, tops0.70
Blueberry0.50
Caneberry subgroup 13-07A0.75
Carrot, roots0.75
Cattle, fat0.50
Cherry, sweet0.20
Cherry, tart0.20
Cranberry0.50
Endive0.70
Fig0.50
Ginseng0.75
Grape0.752
Hazelnut0.50
Kiwifruit10.75
Lettuce0.70
Melon0.75
Mushroom0.752
Nectarine0.20
Onion, bulb0.75
Onion, green0.75
Pea, succulent0.50
Peach0.20
Pear0.50
Pineapple0.50
Plum, prune, fresh0.20
Radish0.50
Rutabaga0.75
Spinach0.70
Strawberry0.50
Tomato0.75
Vegetable, brassica, leafy, group 50.70
Watercress0.05

1There are no domestic registrations for kiwifruit as of March 6, 2002.

2The expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide diazinon, O, O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]-phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

CommodityParts per million
Almond0.50
Banana0.20
Celery0.70
Cucumber0.75
Parsley, leaves0.75
Parsnip0.50
Pepper0.5
Potato0.10
Squash, summer0.50
Squash, winter0.75
Sweet potato, roots0.10
Swiss chard0.70
Turnip, roots0.50
Turnip, tops0.75

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 42738, Sept. 29, 1982]

Editorial Note: For Federal Register citations affecting §180.153, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.155   1-Naphthaleneacetic acid; tolerances for residues.

(a) General. Tolerances are established for the residues of 1-naphthaleneacetic acid, including its metabolites and degradates in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring only 1-naphthaleneacetic acid and its conjugates, calculated as the Stoichiometric equivalent of 1-naphthaleneacetic acid, in or on the commodity.

Commodity Parts per
million
Avocado0.05
Cherry, sweet0.1
Fruit, pome, group 11-100.15
Mango0.05
Olive0.7
Orange0.1
Pineapple10.05
Pomegranate0.05
Potato0.01
Rambutan2.0
Sapote, mamey0.05
Tangerine0.1

1There are no U.S. registrations since 1988.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 30218, May 22, 2013, as amended at 80 FR 77260, Dec. 14, 2015]

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§180.163   Dicofol; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicofol as the sum of its p,p-dicofol and o,p-dicofol isomers: 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

CommodityParts per millionExpiration/revocation date
Apple, wet pomace38.010/31/16
Bean, dry, seed0.510/31/16
Bean, succulent3.010/31/16
Butternut0.110/31/16
Caneberry subgroup 13A5.010/31/16
Chestnut0.110/31/16
Citrus, dried pulp12.010/31/16
Citrus oil200.010/31/16
Cotton, refined oil0.510/31/16
Cotton, undelinted seed0.110/31/16
Fruit, citrus, group 106.010/31/16
Fruit, pome, group 1110.010/31/16
Fruit, stone, group 125.010/31/16
Grape5.010/31/16
Grape, raisin20.010/31/16
Hazelnut0.110/31/16
Hop, dried cones65.010/31/16
Nut, hickory0.110/31/16
Nut, macadamia0.110/31/16
Pecan0.110/31/16
Peppermint, oil30.010/31/16
Peppermint, tops25.010/31/16
Spearmint, oil30.010/31/16
Spearmint, tops25.010/31/16
Strawberry10.010/31/16
Tea, dried50.0None
Tea, plucked leaves30.0None
Vegetable, cucurbit, group 92.010/31/16
Vegetable, fruiting, group 82.010/31/16
Walnut0.110/31/16

(2) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, its isomer o,p-dicofol, 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, and its metabolites 4-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol, calculated as the stoichiometric equivalent of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

CommodityParts per millionExpiration/Revocation Date
Cattle, fat50.010/31/16
Cattle, liver5.010/31/16
Cattle, meat3.010/31/16
Cattle, meat byproducts, except liver3.010/31/16
Egg0.0510/31/16
Goat, fat50.010/31/16
Goat, liver5.010/31/16
Goat, meat3.010/31/16
Goat, meat byproducts, except liver3.010/31/16
Hog, fat50.010/31/16
Hog, liver5.010/31/16
Hog, meat3.010/31/16
Hog, meat byproducts, except liver3.010/31/16
Horse, fat50.010/31/16
Horse, liver5.010/31/16
Horse, meat3.010/31/16
Horse, meat byproducts, except liver3.010/31/16
Milk, fat (reflecting 0.75 ppm in whole milk)22.010/31/16
Poultry, fat0.110/31/16
Poultry, meat0.110/31/16
Poultry, meat byproducts0.110/31/16
Sheep, fat50.010/31/16
Sheep, liver5.010/31/16
Sheep, meat3.010/31/16
Sheep, meat byproducts, except liver3.010/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007; 77 FR 59124, Sept. 26, 2012]

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§180.169   Carbaryl; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

CommodityParts per millionExpiration/revocation date
Alfalfa, forage50None
Alfalfa, hay75None
Almond, hulls50None
Apple, wet pomace15None
Asparagus15None
Banana5.0None
Beet, sugar, roots0.5None
Beet, sugar, tops25None
Bushberry subgroup 13-07B3.0None
Cabbage21None
Cactus, fruit5.0None
Cactus, pads12None
Caneberry subgroup 13-07A12.0None
Citrus, oil20None
Clover, forage50None
Clover, hay70None
Corn, field, forage30None
Corn, field, grain0.02None
Corn, field, stover20None
Corn, pop, grain0.02None
Corn, pop, stover20None
Corn, sweet, forage185None
Corn, sweet, kernel plus cob with husks removed0.1None
Corn, sweet, stover215None
Cotton, undelinted seed5.010/31/09
Cranberry3.0None
Dandelion, leaves22None
Endive10None
Flax, seed0.5None
Fruit, citrus, group 1010None
Fruit, pome, group 1112None
Fruit, stone, group 1210None
Grain, aspirated fractions70None
Grape10None
Grape, raisin12None
Grass, forage100None
Grass, hay15None
Leaf petiole subgroup 4B3.0None
Lettuce10None
Millet, proso, grain1.0None
Millet, proso, straw20None
Nut, tree group 14, except walnut0.1None
Okra4.0None
Olive10None
Oyster0.25None
Parsley, leaves22None
Pea and bean, dried shelled, except soybean, subgroup 6C1.0None
Peanut0.05None
Peanut, hay20None
Pineapple2.0None
Pistachio0.1None
Rice, grain15None
Rice, hulls30None
Sorghum grain, forage30None
Sorghum grain, grain10None
Sorghum grain, stover30None
Soybean, forage15None
Soybean, hay15None
Soybean, seed0.5None
Spinach22None
Strawberry4.0None
Sunflower, seed0.5None
Sweet potato, roots0.2None
Trefoil, forage15None
Trefoil, hay25None
Vegetable, brassica, leafy, group 5, except cabbage10None
Vegetable, cucurbit, group 93.0None
Vegetable, foliage of legume, subgroup 7A, except soybean60None
Vegetable, fruiting, group 85.0None
Vegetable, leaves of root and tuber, group 2, except sugar beet tops75None
Vegetable, legume, edible podded, subgroup 6A10None
Vegetable, root and tuber, group 1, except sugar beet and sweet potato2.0None
Walnut1.0None
Wheat, forage30None
Wheat, grain1.0None
Wheat, hay30None
Wheat, straw20None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate, including its metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6-dihydrodihydroxy naphthol, calculated as 1-naphthyl N-methylcarbamate and the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 5-methoxy-6-hydroxy carbaryl, in or on the following food commodities:

CommodityParts per millionExpiration/revocation date
Cattle, fat0.5None
Cattle, meat1.0None
Cattle, meat byproducts3.0None
Egg0.510/31/09
Goat, fat0.5None
Goat, meat1.0None
Goat, meat byproducts3.0None
Hog, fat0.5None
Hog, meat1.0None
Hog, meat byproducts3.0None
Horse, fat0.5None
Horse, meat1.0None
Horse, meat byproducts3.0None
Milk1.0None
Poultry, fat5.010/31/09
Poultry, meat5.010/31/09
Sheep, fat0.5None
Sheep, meat1.0None
Sheep, meat byproducts3.0None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

CommodityParts per million
Dillweed, fresh leaves0.2

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009; 80 FR 72597, Nov. 20, 2015]

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§180.172   Dodine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dodine, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only dodine, N-dodecylguanidine acetate; in or on the following commodities.

CommodityParts per million
Almond, hull30.0
Apple5.0
Apple, wet pomace15.0
Banana0.50
Fruit, stone, crop group 125.0
Nuts, tree, crop group 140.3
Peanut0.013
Pear5.0
Strawberry5.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, 2012]

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§180.175   Maleic hydrazide; tolerances for residues.

(a) General. (1) Tolerances for residues of the herbicide and plant regulator maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) are established in or on the following raw agricultural commodities:

CommodityParts per million
Onion, bulb15.0
Potato50.0

(2) A food additive known as maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) may be present in potato, chips when used in accordance with the following conditions:

(i) The food additive is present as a result of the application of a pesticide formulation containing maleic hydrazide to the growing potato plant in accordance with directions registered by the U.S. Environmental Protection Agency.

(ii) The label of the pesticide formulation containing the food additive conforms to labeling registered by the U.S. Environmental Protection Agency.

(iii) The food additive is present in an amount not to exceed 160 parts per million by weight of the finished food.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 64293, Dec. 5, 1997, as amended at 64 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, 2002]

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§180.176   Mancozeb; tolerances for residues.

(a) General. Tolerances are established for residues of mancozeb (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

CommodityParts
per million
Almond0.1
Almond, hulls4
Apple0.6
Asparagus0.1
Atemoya3.0
Banana2
Barley, bran2
Barley, flour1.2
Barley, grain1
Barley, hay30
Barley, pearled barley20
Barley, straw25
Beet, sugar, dried pulp3.0
Beet, sugar, roots1.2
Beet, sugar, tops60
Broccoli7
Cabbage9
Canistel15.0
Cattle, kidney0.5
Cattle, liver0.5
Cherimoya3.0
Corn, field, forage40
Corn, field, grain0.06
Corn, field, stover15
Corn, pop, grain0.1
Corn, pop, stover40
Corn, sweet, forage70
Corn, sweet, kernel plus cob with husks removed0.1
Corn, sweet, stover40
Cotton, undelinted seed0.5
Crabapple0.6
Cranberry5
Custard apple3.0
Fennel2.5
Flax, seed0.15
Ginseng1.2
Goat, kidney0.5
Goat, liver0.5
Grape1.5
Hog, kidney0.5
Hog, liver0.5
Horse, kidney0.5
Horse, liver0.5
Lettuce, head3.5
Lettuce, leaf18
Mango15.0
Oat, flour1.2
Oat, grain1
Oat, groats/rolled oats20
Oat, hay30
Oat, straw25
Onion, bulb1.5
Papaya9
Peanut0.1
Peanut, hay65
Pear0.6
Pepper12
Potato0.2
Poultry, kidney0.5
Poultry, liver0.5
Quince0.6
Rice, grain0.06
Rye, bran2
Rye, flour1.2
Rye, grain1
Rye, straw25
Sapodilla15.0
Sapote, mamey15.0
Sapote, white15.0
Sheep, kidney0.5
Sheep, liver0.5
Sorghum, grain, forage0.15
Sorghum, grain, grain0.25
Sorghum, grain, stover0.15
Star apple15.0
Sugar apple3.0
Tangerine110
Tomato2.5
Vegetable, cucurbit, group 92.0
Walnut0.70
Wheat, bran2
Wheat, flour1.2
Wheat, germ20
Wheat, grain1
Wheat, hay30
Wheat, middlings20
Wheat, shorts2
Wheat, straw25

1There are no U.S. registrations for use of mancozeb on tangerine.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registrations, as defined in §180.1(l), is established for residues of the fungicide mancozeb, (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodity in the following table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

CommodityParts per million
Carrot, roots1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, May 14, 2014; 80 FR 72597, Nov. 20, 2015]

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§180.178   Ethoxyquin; tolerances for residues.

(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:

CommodityParts per million
Pear3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57073, Oct. 26, 1998]

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§180.181   Chlorpropham; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) in or on the following food commodities:

CommodityParts per million
Potato30
Potato, wet peel40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic acid (4-HSA) in or on the following food commodities:

CommodityParts per million
Cattle, fat0.20
Cattle, kidney0.30
Cattle, meat0.06
Cattle, meat byproducts except kidney0.06
Goat, fat0.20
Goat, kidney0.30
Goat, meat0.06
Goat, meat byproducts except kidney0.06
Hog, fat0.20
Hog, kidney0.30
Hog, meat0.06
Hog, meat byproducts except kidney0.06
Horse, fat0.20
Horse, kidney0.30
Horse, meat0.06
Horse, meat byproducts except kidney0.06
Milk0.30
Sheep, fat0.20
Sheep, kidney0.30
Sheep, meat0.06
Sheep, meat byproducts except kidney0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

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§180.182   Endosulfan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

CommodityParts per millionExpiration/
revocation
date
Almond0.37/31/12
Almond, hulls1.07/31/12
Apricot2.07/31/12
Bean2.07/31/12
Broccoli3.07/31/12
Brussels sprouts2.07/31/12
Cabbage4.07/31/12
Cantaloupe1.07/31/12
Carrot, roots0.27/31/12
Cattle, fat13.07/31/16
Cattle, liver5.07/31/16
Cattle, meat2.07/31/16
Cattle, meat byproducts, except liver1.07/31/16
Cauliflower2.07/31/12
Celery8.07/31/12
Cherry, sweet2.07/31/12
Cherry, tart2.07/31/12
Collards2.07/31/12
Cotton, gin byproducts30.07/31/12
Cotton, undelinted seed1.07/31/12
Cucumber1.07/31/12
Eggplant1.07/31/12
Goat, fat13.07/31/16
Goat, liver5.07/31/16
Goat, meat2.07/31/16
Goat, meat byproducts, except liver1.07/31/16
Hazelnut0.27/31/12
Hog, fat13.07/31/16
Hog, liver5.07/31/16
Hog, meat2.07/31/16
Hog, meat byproducts, except liver1.07/31/16
Horse, fat13.07/31/16
Horse, liver5.07/31/16
Horse, meat2.07/31/16
Horse, meat byproducts, except liver1.07/31/16
Kale2.07/31/12
Lettuce, head11.07/31/12
Lettuce, leaf6.07/31/12
Milk, fat2.07/31/16
Muskmelon1.07/31/12
Mustard greens2.07/31/12
Mustard, seed0.27/31/12
Nectarine2.07/31/12
Nut, macadamia0.27/31/12
Peach2.07/31/12
Pear2.07/31/13
Pineapple1.07/31/16
Pineapple, process residue20.07/31/16
Plum2.07/31/12
Plum, prune2.07/31/12
Sheep, fat13.07/31/16
Sheep, liver5.07/31/16
Sheep, meat2.07/31/16
Sheep, meat byproducts, except liver1.07/31/16
Squash, summer1.07/31/12
Strawberry2.07/31/16
Sweet potato, roots0.157/31/12
Walnut0.27/31/12
Watermelon1.07/31/12

(2) A tolerance is established for the combined residues of the insecticide endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3,3-dioxide in or on the commodity in the following table:

CommodityParts per millionExpiration/
revocation date
Tea, dried24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide to growing tea7/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. (1) Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph, when endosulfan is used in the state of Florida. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

CommodityParts per millionExpiration/
revocation
date
Apple1.012/31/14
Apple, wet pomace5.012/31/14
Blueberry0.312/31/14
Corn, sweet, forage12.012/31/14
Corn, sweet, kernel plus cob with husks removed0.212/31/14
Corn, sweet, stover14.012/31/14
Pepper2.012/31/14
Potato0.212/31/14
Pumpkin1.012/31/14
Squash, winter1.012/31/14
Tomato1.012/31/14

(2) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph, when endosulfan is used in the United States (except Florida). Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

CommodityParts per millionExpiration/
revocation
date
Apple1.07/31/15
Apple, wet pomace5.07/31/15
Blueberry0.37/31/15
Corn, sweet, forage12.07/31/15
Corn, sweet, kernel plus cob with husks removed0.27/31/15
Corn, sweet, stover14.07/31/15
Pepper2.07/31/15
Potato0.27/31/15
Pumpkin1.07/31/15
Squash, winter1.07/31/15
Tomato1.07/31/15

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33696, May 24, 2000, as amended at 71 FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, 2011; 78 FR 8409, Feb. 6, 2013]

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§180.183   Disulfoton; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.

CommodityParts per million Expiration/Revocation Date
Bean, lima0.7512/31/13
Bean, snap, succulent0.7512/31/13
Broccoli0.7512/31/13
Brussels sprouts0.7512/31/13
Cabbage0.7512/31/13
Cauliflower0.7512/31/13
Coffee, green bean0.26/30/14
Cotton, undelinted seed0.7512/31/13
Lettuce, head0.7512/31/14
Lettuce, leaf212/31/14

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration is established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.

CommodityParts per million Expiration/Revocation Date
Asparagus0.112/31/13

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, 2009; 75 FR 60240, Sept. 29, 2010]

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§180.184   Linuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity:

CommodityParts per million
Asparagus7.0
Carrot, roots1.0
Cattle, fat0.2
Cattle, kidney2.0
Cattle, liver2.0
Cattle, meat0.1
Cattle, meat byproducts except kidney and liver0.1
Celeriac1.0
Cilantro, dried leaves10
Cilantro, fresh leaves3.0
Coriander, seed0.01
Corn, field, forage1.0
Corn, field, grain0.1
Corn, field, stover6.0
Corn, sweet, forage1.0
Corn, sweet, kernel plus cob with husks removed0.25
Corn, sweet, stover6.0
Cotton, gin byproducts5.0
Cotton, undelinted seed0.25
Dill, oil2.0
Dill, seed0.5
Dillweed, dried leaves5.0
Dillweed, fresh leaves1.5
Goat, fat0.2
Goat, kidney2.0
Goat, liver2.0
Goat, meat0.1
Goat, meat byproducts except kidney and liver0.1
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.1
Horse, fat0.2
Horse, kidney2.0
Horse, liver2.0
Horse, meat0.1
Horse, meat byproducts except kidney and liver0.1
Horseradish0.05
Milk0.05
Parsley, dried leaves9.0
Parsley, leaves4.0
Parsnip, roots0.05
Parsnip, tops0.05
Pea, dry, seed0.09
Rhubarb0.5
Sheep, fat0.2
Sheep, kidney2.0
Sheep, liver2.0
Sheep, meat0.1
Sheep, meat byproducts except kidney and liver0.1
Sorghum, grain, forage1.0
Sorghum, grain, grain0.25
Sorghum, grain, stover1.0
Soybean, seed1.0
Soybean, vegetable1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide linuron [3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea], including its metabolites and degradates, in or on the commodities in the table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3.4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity. The tolerance expires and is revoked on the date specified in the table.

CommodityParts per
million
Expiration/revocation date
Lentil0.112/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity.

CommodityParts per million
Celery0.5
Potato0.2
Wheat, forage0.5
Wheat, grain0.05
Wheat, hay0.5
Wheat, straw2.0

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Feb. 12, 2014]

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§180.185   DCPA; tolerances for residues.

(a) General. Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid (TCP) (calculated as dimethyl tetrachloroterephthalate) are established in or on the following food commodities:

CommodityParts per million
Cantaloupe1.0
Garlic1.0
Ginseng2.0
Horseradish2.0
Muskmelon1.0
Onion, bulb1.0
Onion, green1.0
Strawberry2.0
Tomato1.0
Vegetable, brassica, leafy, group 55.0
Watermelon1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

CommodityParts per million
Radish, roots2.0
Radish, tops15.0

(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

CommodityParts per million
Basil, dried leaves20.0
Basil, fresh leaves5.0
Bean, dry2.0
Bean, mung, seed2.0
Bean, snap, succulent2.0
Celeriac2.0
Chicory, roots2.0
Chicory, tops5.0
Chive5.0
Coriander, leaves5.0
Corn, field, forage0.4
Corn, field, grain0.05
Corn, field, stover0.4
Corn, pop, forage0.4
Corn, pop, grain0.05
Corn, pop, stover0.4
Corn, sweet, forage0.4
Corn, sweet, kernel plus cob with husks removed0.05
Corn, sweet, stover0.4
Cotton, undelinted seed0.2
Cucumber1.0
Dill5.0
Eggplant1.0
Lettuce2.0
Marjoram5.0
Parsley, dried leaves20.0
Parsley, leaves5.0
Pea, blackeyed, seed2.0
Pepper2.0
Pimento2.0
Potato2.0
Radicchio5.0
Radish, oriental, roots2.0
Radish, oriental, tops2.0
Rutabaga2.0
Soybean2.0
Squash, summer1.0
Squash, winter1.0
Sweet potato2.0
Turnip, roots2.0
Turnip, tops5.0
Yam, true, tuber2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008; 74 FR 14744, Apr. 1, 2009]

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§180.189   Coumaphos; tolerances for residues.

(a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphorothioate and its oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphate) in or on food commodities as follows:

CommodityParts per million
Cattle, fat1.0
Cattle, meat1.0
Cattle, meat byproducts1.0
Goat, fat1.0
Goat, meat1.0
Goat, meat byproducts1.0
Hog, fat1.0
Hog, meat1.0
Hog, meat byproducts1.0
Honey0.15
Honeycomb45.0
Horse, fat1.0
Horse, meat1.0
Horse, meat byproducts1.0
Milk, fat ( = n in whole milk)0.5
Sheep, fat1.0
Sheep, meat1.0
Sheep, meat byproducts1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, May 23, 2007]

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§180.190   Diphenylamine; tolerances for residues.

(a) General. Tolerances for residues of the plant regulator diphenylamine are established in or on the following commodities:

Commodity Parts per million
Apple, wet pomace30.0
Apple from preharvest or postharvest use, including use of impregnated wraps10.0
Cattle, fat0.01
Cattle, liver0.1
Cattle, meat byproducts, except liver0.01
Cattle, meat0.01
Goat, fat0.01
Goat, liver0.1
Goat, meat byproducts, except liver0.01
Goat, meat0.01
Horse, fat0.01
Horse, liver0.1
Horse, meat byproducts, except liver0.01
Horse, meat0.01
Milk0.01
Pear (post harvest)5.0
Sheep, fat0.01
Sheep, liver0.1
Sheep, meat byproducts, except liver0.01
Sheep, meat0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007; 76 FR 34885, June 15, 2011]

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§180.191   Folpet; tolerances for residues.

(a) General. Tolerances are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on raw agricultural commodities as follows:

CommodityParts per million
Apple15.0
Cranberry115.0
Cucumber12.0
Grape150.0
Grape, raisin180.0
Hop, dried cones120.0
Lettuce150.0
Melon13.0
Onion,bulb12.0
Strawberry15.0
Tomato125.0

1 No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in §180.1(l) are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on the following raw agricultural commodity:

CommodityParts per million
Avocado25.0

(d) Indirect or inadvertent residues. [Reserved]

[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72 FR 41928, Aug. 1, 2007]

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§180.198   Trichlorfon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1-hydroxyethyl) phosphonate) in or on the following food commodities:

CommodityParts per million
Cattle, fat10.5
Cattle, meat10.2
Cattle, meat byproducts10.1

1There are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

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§180.200   Dicloran; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dicloran, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicloran, 2,6-dichloro-4-nitroaniline, in or on the commodity.

CommodityParts per
million
Expiration/revocation date
Apricot20None
Bean, snap, succulent20None
Carrot, roots1011/2/11
Celery15None
Cherry, sweet20None
Cucumber5None
Endive10None
Garlic5None
Grape10None
Lettuce10None
Nectarine20None
Onion10None
Peach20None
Plum, prune, fresh15None
Potato0.2512/31/14
Rhubarb10None
Sweet potato, roots10None
Tomato5None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

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§180.202   p-Chlorophenoxyacetic acid; tolerances for residues.

(a) General. A tolerance is established for the combined residues of the plant regulator p-chlorophenoxyacetic acid and its metabolite p-chlorophenol to inhibit embryonic root development in or on the following food commodity:

CommodityParts per million
Bean, mung, sprouts0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006]

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§180.204   Dimethoate; tolerances for residues.

(a) General. Tolerances are established for total residues of the insecticide dimethoate (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorodithioate) including its oxygen analog (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorothioate) in or on the following food commodities:

CommodityParts per million
Alfalfa, forage2.0
Alfalfa, hay2.0
Bean, dry, seed2.0
Bean, lima2.0
Bean, snap, succulent2.0
Blueberry11.0
Broccoli2.0
Cattle, meat byproducts0.02
Cauliflower2.0
Celery2.0
Citrus, dried pulp5.0
Corn, field, forage1.0
Corn, field, grain0.1
Corn, field, stover1.0
Corn, pop, grain0.1
Corn, pop, stover1.0
Corn, sweet, forage1.0
Cotton, undelinted seed0.1
Egg0.02
Endive2.0
Goat, meat byproducts0.02
Grapefruit2.0
Hog, meat byproducts0.02
Horse, meat byproducts0.02
Kale2.0
Lemon2.0
Lettuce, leaf2.0
Melon1.0
Milk0.002
Mustard greens2.0
Orange2.0
Pea2.0
Pear2.0
Pecan0.1
Pepper2.0
Potato0.2
Poultry, meat byproducts0.02
Safflower, seed0.1
Sheep, meat byproducts0.02
Sorghum, grain, forage0.1
Sorghum, grain, grain0.1
Sorghum, grain, stover0.1
Soybean, forage2.0
Soybean, hay2.0
Soybean, seed0.05
Swiss chard2.0
Tangerine2.0
Tomato2.0
Turnip, roots0.2
Turnip, tops2.0
Wheat, forage2.0
Wheat, grain0.04
Wheat, hay2.0
Wheat, straw2.0

1 There are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for total residues of dimethoate including its oxygen analog in or on the following food commodities:

CommodityParts per million
Asparagus0.15
Brussels sprouts5.0
Cherry, sweet2.0
Cherry, tart2.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

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§180.205   Paraquat; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat (1,1′-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

CommodityParts per million
Acerola0.05
Almond, hulls0.5
Animal feed, nongrass, group 18, forage75.0
Animal feed, nongrass, group 18, hay210.0
Artichoke, globe0.05
Asparagus0.5
Atemoya0.05
Avocado0.05
Banana0.05
Barley, grain0.05
Barley, hay3.5
Barley, straw1.0
Beet, sugar, roots0.5
Beet, sugar, tops0.05
Berry group 130.05
Biriba0.05
Cacao bean, bean0.05
Canistel0.05
Carrot, roots0.05
Cattle, fat0.05
Cattle, kidney0.5
Cattle, meat0.05
Cattle, meat byproducts, except kidney0.05
Cherimoya0.05
Coffee, bean, green0.05
Corn, field, forage3.0
Corn, field, grain0.1
Corn, field, stover10.0
Corn, pop, grain0.1
Corn, pop, stover10.0
Corn, sweet, kernel plus cob with husks removed0.05
Cotton, gin byproducts110.0
Cotton, undelinted seed3.5
Cowpea, forage0.1
Cowpea, hay0.4
Cranberry0.05
Custard apple0.05
Egg0.01
Endive0.05
Feijoa0.05
Fig0.05
Fruit, citrus, group 100.05
Fruit, pome, group 110.05
Fruit, stone, group 120.05
Goat, fat0.05
Goat, kidney0.5
Goat, meat0.05
Goat, meat byproducts, except kidney0.05
Grain, aspirated fractions65.0
Grape0.05
Grass, forage90.0
Grass, hay40.0
Guar, seed0.5
Guava0.05
Hog, fat0.05
Hog, kidney0.5
Hog, meat0.05
Hog, meat byproducts, except kidney0.05
Hop, dried cones0.5
Horse, fat0.05
Horse, kidney0.5
Horse, meat0.05
Horse, meat byproducts, except kidney0.05
Ilama0.05
Jaboticaba0.05
Kiwifruit0.05
Lentil, seed0.3
Lettuce0.05
Longan0.05
Lychee0.05
Mango0.05
Milk0.01
Nut, tree, group 140.05
Okra0.05
Olive0.05
Onion, bulb0.1
Onion, green0.05
Papaya0.05
Passionfruit0.2
Pawpaw0.05
Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean0.3
Pea and bean, succulent shelled, subgroup 6B0.05
Pea, field, hay0.8
Pea, field, vines0.2
Peanut0.05
Peanut, hay0.5
Peppermint, tops0.5
Persimmon0.05
Pineapple0.05
Pineapple, process residue0.25
Pistachio0.05
Pomegranate0.05
Pulasan0.05
Rambutan0.05
Rhubarb0.05
Rice, grain0.05
Safflower, seed0.05
Sapodilla0.05
Sapote, black0.05
Sapote, mamey0.05
Sapote, white0.05
Sheep, fat0.05
Sheep, kidney0.5
Sheep, meat0.05
Sheep, meat byproducts, except kidney0.05
Sorghum, forage, forage0.1
Sorghum, grain, forage0.1
Sorghum, grain, grain0.05
Soursop0.05
Soybean, forage0.4
Soybean, hay10.0
Soybean, hulls4.5
Soybean, seed0.7
Spanish lime0.05
Spearmint, tops0.5
Star apple0.05
Starfruit0.05
Strawberry0.25
Sugar apple0.05
Sugarcane, cane0.5
Sugarcane, molasses3.0
Sunflower, seed2.0
Turnip, greens0.05
Turnip, roots0.05
Vegetable, brassica, leafy, group 50.05
Vegetable, cucurbit, group 90.05
Vegetable, fruiting, group 80.05
Vegetable, legume, edible podded, subgroup 6A0.05
Vegetable, tuberous and corm, subgroup 1C0.50
Wax jambu0.05
Wheat, forage0.5
Wheat, grain1.1
Wheat, hay3.5
Wheat, straw50.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(l), are established for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

CommodityParts per million
Pea, pigeon, seed0.05
Taro, corm0.1
Tyfon0.05

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 51614, Oct. 21, 1981]

Editorial Note: For Federal Register citations affecting §180.205, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.206   Phorate; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide phorate (O,O-diethyl S (ethylthio) methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen analog, phorate oxygen analog sulfoxide, and phorate oxygen analog sulfone in or on the following food commodities:

CommodityParts per million
Bean, dry, seed0.05
Bean, succulent0.05
Beet, sugar, roots0.3
Beet, sugar, tops3.0
Coffee, green bean10.02
Corn, field, forage0.5
Corn, field, grain0.05
Corn, sweet, forage0.5
Corn, sweet, kernel plus cob with husks removed0.05
Cotton, undelinted seed0.05
Hop, dried cones2.0
Peanut0.1
Potato0.2
Sorghum, grain, grain0.05
Sorghum, grain, stover0.1
Soybean, seed0.05
Sugarcane, cane0.05
Wheat, forage1.5
Wheat, grain0.05
Wheat, hay1.5
Wheat, straw0.05

1 There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008]

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§180.207   Trifluralin; tolerances for residues.

(a) General. Tolerances are established for residues of trifluralin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only trifluralin (2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)benzenamine).

CommodityParts per million
Alfalfa, forage3.0
Alfalfa, hay2.0
Almond, hulls0.05
Asparagus0.05
Barley, grain0.05
Barley, hay0.05
Barley, straw0.05
Bean, mung, sprouts2.0
Carrot, roots1.0
Celery0.05
Corn, field, forage0.05
Corn, field, grain0.05
Corn, field, stover0.05
Cotton, gin byproducts0.05
Endive0.05
Fruit, citrus, group 100.05
Fruit, stone, group 120.05
Grape0.05
Hop, dried cones0.05
Nut, tree, group 140.05
Oilseed, crop group 200.05
Okra0.05
Peanut0.05
Peanut, hay0.05
Peppermint, oil2.0
Peppermint, tops0.05
Rosemary, dried leaves0.10
Rosemary, fresh leaves0.10
Rosemary, oil3.0
Sorghum, grain, forage0.05
Sorghum, grain, grain0.05
Sorghum, grain, stover0.05
Spearmint, oil2.0
Spearmint, tops0.05
Sugarcane, cane0.05
Vegetable, brassica, leafy group 50.05
Vegetable, bulb, group 30.05
Vegetable, cucurbit, group 90.05
Vegetable, foliage of legume, group 70.05
Vegetable, fruiting, group 80.05
Vegetable, leaves of root and tuber, group 20.05
Vegetable, legume, group 60.05
Vegetable, root and tuber, group 1, except carrot0.05
Wheat, grain0.05
Wheat, straw0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006; 78 FR 46274, July 31, 2013; 84 FR 4351, Feb. 15, 2019]

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§180.208   Benfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide benfluralin, N-butyl-N-ethyl-ααα-trifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities:

CommodityParts per million
Alfalfa, forage0.05
Alfalfa, hay0.05
Clover, forage0.05
Clover, hay0.05
Lettuce0.05
Trefoil, forage0.05
Trefoil, hay0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

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§180.209   Terbacil; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide terbacil, (3-tert-butyl-5-chloro-6-methyluracil) and its metabolites [3-tert-butyl-5-chloro-6-hydroxymethyluracil], [6-chloro-2,3-dihydro-7-hydroxymethyl 3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7-trimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], calculated as terbacil, in or on the following raw agricultural commodities:

CommodityParts per million
Alfalfa, forage1.0
Alfalfa, hay2.0
Apple0.3
Asparagus0.4
Blueberry0.2
Caneberry subgroup 13A0.2
Peach0.2
Peppermint, tops2.0
Spearmint, tops2.0
Strawberry0.1
Sugarcane, cane0.4
Watermelon1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 30818, May 31, 2006]

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§180.210   Bromacil; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide bromacil (5-bromo-3-sec-butyl-6-methyluracil) in or on the following food commodities:

CommodityParts per million
Fruit, citrus0.1
Pineapple0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

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§180.211   Propachlor; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propachlor (2-chloro-N-isopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloro-N-isopropylacetanilide, in or on the following raw agricultural commodities:

CommodityParts per million
Cattle, fat0.05
Cattle, kidney0.2
Cattle, meat0.02
Cattle, meat byproducts, except kidney0.05
Corn, field, forage3.0
Corn, field, grain0.2
Corn, field, stover1.0
Corn, sweet, forage3.0
Goat, fat0.05
Goat, kidney0.2
Goat, meat0.02
Goat, meat byproducts, except kidney0.05
Hog, fat0.02
Hog, meat0.02
Hog, meat byproducts0.02
Horse, fat0.05
Horse, kidney0.2
Horse, meat0.02
Horse, meat byproducts, except kidney0.05
Milk0.02
Sheep, fat0.05
Sheep, kidney0.2
Sheep, meat0.02
Sheep, meat byproducts, except kidney0.05
Sorghum, forage, forage8.0
Sorghum, grain, forage8.0
Sorghum, grain, grain0.25
Sorghum, grain, stover12.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007]

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§180.212   S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl cyclohexylethylthiocarbamate in or on the following food commodities:

CommodityParts per million
Beet, garden, roots0.05(N)
Beet, garden, tops0.05(N)
Beet, sugar, roots0.05(N)
Beet, sugar, tops0.05(N)
Spinach0.05(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

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§180.213   Simazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide simazine (2-chloro-4,6-bis(ethylamino)-s-triazine) and its two chlorinated degradates (2-amino-4-chloro-6-ethylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine), the total residue to be measured in or on the following food commodities:

CommodityParts per million
Almond0.25
Almond, hulls0.25
Apple0.20
Avocado0.20
Blackberry0.20
Blueberry0.20
Cattle, meat0.03
Cattle, meat byproducts0.03
Cherry0.25
Corn, field, forage0.20
Corn, field, grain0.20
Corn, field, stover0.25
Corn, pop, grain0.20
Corn, pop, stover0.25
Corn, sweet, forage0.20
Corn, sweet, kernel plus cob with husks removed0.25
Corn, sweet, stover0.25
Cranberry0.25
Currant0.25
Egg0.03
Goat, meat0.03
Goat, meat byproducts0.03
Grape0.20
Grapefruit0.25
Hazelnut0.20
Horse, meat0.03
Horse, meat byproducts0.03
Lemon0.25
Loganberry0.20
Milk0.03
Nut, macadamia0.25
Olive0.20
Orange0.25
Peach0.20
Pear0.25
Pecan0.20
Plum0.20
Raspberry0.20
Sheep, meat0.03
Sheep, meat byproducts0.03
Strawberry0.25
Walnut0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, 2007; 72 FR 53454, Sept. 19, 2007]

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§180.215   Naled; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as naled, resulting from the application of the pesticide to growing crops or from direct application to livestock and poultry, in or on the following raw agricultural commodities:

CommodityParts per million
Almond, hulls0.5
Almond0.5
Bean, dry, seed0.5
Bean, succulent0.5
Beet, sugar, roots0.5
Beet, sugar, tops0.5
Broccoli1
Brussels sprouts1
Cabbage1
Cauliflower1
Celery3
Collards3
Cotton, undelinted seed0.5
Cucumber0.5
Eggplant0.5
Grape0.5
Grapefruit3
Grass, forage10
Hop, dried cones0.5
Kale3
Legume, forage10
Lemon3
Melon0.5
Orange, sweet3
Peach0.5
Pea, succulent0.5
Pepper0.5
Pumpkin0.5
Safflower, seed0.5
Spinach3
Squash, summer0.5
Squash, winter0.5
Strawberry1
Swiss chard3
Tangerine3
Tomato0.5
Turnip, greens3
Walnut0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural commodities, except those otherwise listed in this section, from use of the pesticide for area pest (mosquito and fly) control.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, Sept. 26, 2012]

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§180.217   Metiram; tolerances for residues.

(a) General. Tolerances are established for residues of a metiram (a mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those metiram residues convertible to and expressed in terms of the degradate carbon disulfide.

CommodityParts per million
Apple0.5
Apple, pomace, wet2
Banana13
Grape, wine15
Potato0.2

1There are no U.S. registrations on bananas and grape, wine as of April 29, 2011.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57074, Oct. 26, 1998, as amended at 76 FR 23891, Apr. 29, 2011]

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§180.220   Atrazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4-ethylamino-6-isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylamino-s-triazine, 2-amino-4-chloro-6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the following food commodities:

CommodityParts per
million
Cattle, fat0.02
Cattle, meat0.02
Cattle, meat byproducts0.02
Corn, field, forage1.5
Corn, field, grain0.20
Corn, field, stover0.5
Corn, pop, forage1.5
Corn, pop, grain0.20
Corn, pop, stover0.5
Corn, sweet, forage15
Corn, sweet, kernel plus cob with husks removed0.20
Corn, sweet, stover2.0
Goat, fat0.02
Goat, meat0.02
Goat, meat byproducts0.02
Grass, forage4.0
Grass, hay4.0
Guava0.05
Horse, fat0.02
Horse, meat0.02
Horse, meat byproducts0.02
Milk0.02
Nut, macadamia0.20
Sheep, fat0.02
Sheep, meat0.02
Sheep, meat byproducts0.02
Sorghum, forage, forage0.25
Sorghum, grain, forage0.25
Sorghum, grain, grain0.20
Sorghum, grain, stover0.50
Sugarcane, cane0.20
Wheat, forage1.5
Wheat, grain0.10
Wheat, hay5.0
Wheat, straw0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of atrazine, 2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural commodity when present therein as a result of application of atrazine to the growing crops in paragraph (a) of this section:

CommodityParts per million
Vegetable, leafy, except brassica, group 40.25

[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011]

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§180.222   Prometryn; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities:

CommodityParts per million
Bean, snap, succulent0.05
Carrot, roots0.45
Celeriac, roots0.05
Celeriac, tops0.20
Celtuce0.50
Cilantro, leaves3.5
Coriander, dried leaves9.0
Cotton, gin byproducts1.0
Cottonseed subgroup 20C0.25
Dill, oil1.3
Dillweed, dried leaves1.1
Dillweed, fresh leaves0.30
Fennel, Florence, fresh leaves and stalk0.50
Leaf petiole vegetable subgroup 22B0.50
Okra0.05
Parsley, dried leaves1.5
Parsley, leaves0.60
Pea, pigeon, seed0.25
Sesame, seed0.05
Swiss chard0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities.

CommodityParts per million
Barley, forage0.3
Barley, hay1.0
Barley, straw0.3
Oat, forage0.3
Oat, hay1.0
Oat, straw0.3
Rye, forage0.3
Rye, hay1.0
Rye, straw0.3
Triticale, forage0.3
Triticale, hay1.0
Triticale, straw0.3
Wheat, forage0.3
Wheat, hay1.0
Wheat, straw0.3

[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013; 82 FR 57144, Dec. 4, 2017]

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§180.225   Phosphine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of phosphine in or on the following raw agricultural commodities (RACs) resulting from post-harvest fumigation for the control of insects with phosphine gas or phosphide compounds that produce phosphine gas.

CommodityParts per million
Almond0.1
Avocado0.01
Banana0.01
Barley, grain0.1
Cabbage, Chinese, bok choy0.01
Cabbage, Chinese, napa0.01
Cacao bean, dried bean0.1
Cashew0.1
Citron, citrus0.01
Coffee, bean, green0.1
Corn, field, grain0.1
Corn, pop, grain0.1
Cotton, undelinted seed0.1
Date, dried fruit0.1
Dill, seed0.01
Eggplant0.01
Endive0.01
Grapefruit0.01
Hazelnut0.1
Kumquat0.01
Lemon0.01
Lettuce0.01
Lime0.01
Mango0.01
Millet, grain0.1
Mushroom0.01
Nut, brazil0.1
Oat, grain0.1
Okra0.01
Orange, sweet0.01
Papaya0.01
Peanut0.1
Pecan0.1
Pepper0.01
Persimmon0.01
Pistachio0.1
Rice, grain0.1
Rye, grain0.1
Safflower, seed0.1
Salsify, tops0.01
Sesame, seed0.1
Sorghum, grain0.1
Soybean, seed0.1
Sunflower, seed0.1
Sweet potato, roots0.01
Tangelo0.01
Tangerine0.01
Tomato0.01
Vegetable, legume, group 6, except soybean0.01
Walnut0.1
Wheat, grain0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest treatment of pest burrows in agricultural and non-crop land areas.

CommodityParts per million
All raw agricultural commodities resulting from preharvest treatment of pest burrows0.01

(3) Residues resulting from fumigation of processed food:

CommodityParts per million
Processed food0.01

(4) Residues resulting from fumigation of animal feed:

CommodityParts per million
Animal feed0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that registered by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a restriction to aerate the finished food/feed for 48 hours before it is offered to the consumer, unless EPA specifically determines that a different time period is appropriate. Where appropriate, a warning shall state that under no condition should any formulation containing aluminum or magnesium phosphide be used so that it will come in contact with any processed food, except processed brewer's rice, malt, and corn grits stored in breweries for use in the manufacture of beer.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007; 74 FR 46372, Sept. 9, 2009]

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§180.226   Diquat; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the herbicide diquat, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a)(1) resulting from the application of the dibromide salt of diquat. Compliance with the tolerance levels specified in Table 1 to this paragraph (a)(1) is to be determined by measuring only diquat (6,7-dihydrodipyrido[1,2-a:2,1-c]pyrazinediium):

CommodityParts per million
Alfalfa, seed3.0
Cattle, fat0.05
Cattle, meat0.05
Cattle, meat byproducts0.05
Canola, meal6.0
Canola, seed2.0
Egg0.05
Goat, fat0.05
Goat, meat0.05
Goat, meat byproducts0.05
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat0.05
Horse, meat0.05
Horse, meat byproducts0.05
Milk0.02
Pea and bean, dry and shelled, except soybean, subgroup 6C10.9
Potato0.1
Poultry, fat0.05
Poultry, meat0.05
Poultry, meat byproducts0.05
Sheep, fat0.05
Sheep, meat0.05
Sheep, meat byproducts0.05

1There are no U.S. registrations for these commodities as of October 22, 2020.

(2)(i) Tolerances are established for residues of the herbicide diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) (calculated as the cation) derived from the application of the dibromide salt to ponds, lakes, reservoirs, marshes, drainage ditches, canals, streams, and rivers which are slow-moving or quiescent in programs of the Corp of Engineers or other Federal or State public agencies and to ponds, lakes and drainage ditches only where there is little or no outflow of water and which are totally under the control of the user, in or on the following food commodities:

CommodityParts per million
Avocado0.2
Berry group 130.05
Cotton, undelinted seed0.2
Cranberry0.05
Fish2.0
Fruit, citrus, group 100.05
Fruit, pome, group 110.02
Fruit, stone, group 120.02
Grain, cereal, forage, fodder and straw, group 160.02
Grain, cereal, group 150.02
Grape0.05
Grass, forage, fodder and hay, group 170.2
Hop, dried cones0.2
Nut, tree, group 140.02
Shellfish20.0
Strawberry0.05
Sugarcane, cane0.2
Vegetable, brassica, leafy, group 50.05
Vegetable, cucurbit, group 90.02
Vegetable, foliage of legume, group 70.2
Vegetable, fruiting, group 80.05
Vegetable, leafy, except brassica, group 40.05
Vegetable, root and tuber, group 10.02
Vegetable, seed and pod0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the higher tolerances applies also to residues of the aquatic uses cited in this paragraph.

(3) Tolerances are established for the plant growth regulator diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) derived from application of the dibromide salt and calculated as the cation in or on the following food commodites:

CommodityParts per million
Banana10.05
Coffee, bean, green10.05
Soybean, hulls0.6

1There are no U.S. registrations as of May 26, 2010.

(4) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and potato, chips.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29, 2010; 85 FR 67290, Oct. 22, 2020]

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§180.227   Dicamba; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the sum of the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-5-hydroxy-o-anisic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

CommodityParts per million
Barley, grain6.0
Barley, hay2.0
Barley, straw15.0
Corn, field, forage3.0
Corn, field, grain0.1
Corn, field, stover3.0
Corn, pop, grain0.1
Corn, pop, stover3.0
Corn, sweet, forage0.50
Corn, sweet, kernel plus cob with husks removed0.04
Corn, sweet, stover0.50
Grass, forage, fodder and hay, group 17, forage125.0
Grass, forage, fodder and hay, group 17, hay200.0
Millet, proso, forage90.0
Millet, proso, grain2.0
Millet, proso, hay40.0
Millet, proso, straw30.0
Oat, forage90.0
Oat, grain2.0
Oat, hay40.0
Oat, straw30.0
Rye, forage90.0
Rye, grain2.0
Rye, straw30.0
Sorghum, grain, forage3.0
Sorghum, grain, grain4.0
Sorghum, grain, stover10.0
Sugarcane, cane0.3
Sugarcane, molasses5.0
Teff, forage90.0
Teff, grain6.0
Teff, hay40.0
Teff, straw30.0
Wheat, forage90.0
Wheat, grain2.0
Wheat, hay40.0
Wheat, straw30.0

(2) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million
Asparagus4.0
Cattle, fat0.3
Cattle, kidney25.0
Cattle, meat0.25
Cattle, meat byproducts, except kidney3.0
Goat, fat0.3
Goat, kidney25.0
Goat, meat0.25
Goat, meat byproducts, except kidney3.0
Hog, fat0.3
Hog, kidney25.0
Hog, meat0.25
Hog, meat byproducts, except kidney3.0
Horse, fat0.3
Horse, kidney25.0
Horse, meat0.25
Horse, meat byproducts, except kidney3.0
Milk0.2
Sheep, fat0.3
Sheep, kidney25.0
Sheep, meat0.25
Sheep, meat byproducts, except kidney3.0

(3) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba, 3,6-dichloro-o-anisic acid, and its metabolites, 3,6-dichloro-5-hydroxy-o-anisic acid, and 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million
Cotton, gin byproducts70
Cotton, undelinted seed3.0
Grain, aspirated fractions1000
Soybean, forage60
Soybean, hay100
Soybean, hulls30.0
Soybean, seed10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011; 81 FR 88634, Dec. 8, 2016]

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§180.229   Fluometuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities:

CommodityParts per million
Cotton, gin byproducts3.5
Cotton, undelinted seed1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N,N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites: CGA-236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea; and CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or on the following food commodities:

CommodityParts per million
Cattle, meat byproducts0.1
Egg0.1
Goat, meat byproducts0.1
Hog, meat byproducts0.1
Horse, meat byproducts0.1
Milk0.02
Poultry, fat0.1
Poultry, meat0.1
Poultry, meat byproducts0.1
Sheep, meat byproducts0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities.

CommodityParts per million
Grain, cereal, forage, fodder, and straw group 16, forage3.0
Grain, cereal, forage, fodder, and straw, group 16, stover6.0
Grain, cereal, group 150.5
Peanut0.1
Peanut, hay4.0
Peanut, meal0.2
Soybean, forage3.0
Soybean, hay3.0
Soybean, seed2.0
Rice, hulls1.0
Wheat, milled byproducts1.0

[73 FR 52613, Sept. 10, 2008]

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§180.231   Dichlobenil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide dichlobenil (2,6-dichlorobenzonitrile) and its metabolite 2,6-dichlorobenzamide in or on the following raw agricultural commodities:

Commodity Parts per million
Apple0.5
Bushberry subgroup 13-07B0.15
Caneberry subgroup 13-07A0.10
Cranberry0.1
Fruit, stone, group 120.15
Grape0.15
Hazelnut0.1
Pear0.5
Rhubarb0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73 FR 50570, Aug. 27, 2008]

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§180.235   Dichlorvos; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as follows:

CommodityParts per million
Cattle, fat0.02(N)
Cattle, meat0.02(N)
Cattle, meat byproducts0.02(N)
Egg0.05(N)
Goat, fat0.02(N)
Goat, meat0.02(N)
Goat, meat byproducts0.02(N)
Horse, fat0.02(N)
Horse, meat0.02(N)
Horse, meat byproducts0.02(N)
Milk0.02(N)
Mushroom (residues expressed as naled)0.5
Poultry, fat0.05(N)
Poultry, meat0.05(N)
Poultry, meat byproducts0.05(N)
Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, postharvest0.5
Raw agricultural commodities nonperishable, packaged or bagged, containing 6 percent fat or less, postharvest0.5
Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest2
Sheep, fat0.02(N)
Sheep, meat0.02(N)
Sheep, meat byproducts0.02(N)

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2-dichlorovinyl dimethyl phosphate in hog, fat; hog, meat; hog, meat byproducts; and hog, skin covers both its use as an anthelmintic in swine feed and as an insecticide applied directly to swine.

(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged nonperishable processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). To assure safe use of the insecticide, its label and labeling shall conform to the label and labeling registered by the U.S. Environmental Protection Agency, and the usage employed shall conform with such label or labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR 59125, Sept. 26, 2012]

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§180.236   Triphenyltin hydroxide; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide (TPTH) and its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites, expressed in terms of parent TPTH, in or on the following raw agricultural commodities:

CommodityParts per million
Beet, sugar, roots0.05
Beet, sugar, tops10.0
Cattle, fat0.2
Cattle, kidney2.0
Cattle, liver4.0
Cattle, meat0.5
Goat, fat0.2
Goat, kidney2.0
Goat, liver4.0
Goat, meat0.5
Hog, fat0.3
Hog, meat0.06
Hog, meat byproducts0.3
Horse, fat0.2
Horse, kidney2.0
Horse, liver4.0
Horse, meat0.5
Milk0.06
Pecan0.05
Potato0.05
Sheep, fat0.2
Sheep, kidney2.0
Sheep, liver4.0
Sheep, meat0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 41929, Aug. 1, 2007]

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§180.241   Bensulide; tolerances for residues.

(a) General. Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

CommodityParts per million
Onion, bulb0.10
Vegetable, brassica, leafy group 50.15
Vegetable, cucurbits group 90.15
Vegetable, fruiting group 80.10
Vegetable, leafy except brassica group 40.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

CommodityParts per million
Carrot, roots0.10

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

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§180.242   Thiabendazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

CommodityParts per
million
Alfalfa, forage0.02
Alfalfa, hay0.02
Apple, wet pomace12.0
Avocado110.0
Banana, postharvest3.0
Barley, grain0.05
Barley, hay0.30
Barley, straw0.30
Bean, dry, seed20.1
Brassica, head and stem, subgroup 5A0.02
Cantaloupe115.0
Carrot, roots, postharvest10.0
Citrus, oil15.0
Corn, field, forage0.01
Corn, field, grain0.01
Corn, field, stover0.01
Corn, pop, forage0.01
Corn, pop, grain0.01
Corn, pop, stover0.01
Corn, sweet, forage0.01
Corn, sweet, kernels plus cop with husks removed0.01
Corn, sweet, stover0.01
Fruit, citrus, group 10, postharvest10.0
Fruit, pome, group 11, postharvest5.0
Mango10.0
Mushroom40.0
Oats, forage0.30
Oats, grain0.05
Oats, hay0.30
Oats, straw0.30
Onion, bulb, subgroup 3-07A0.02
Papaya, postharvest5.0
Potato, postharvest10.0
Radish, tops0.02
Rye, forage0.30
Rye, grain0.05
Rye, straw0.30
Soybean20.1
Spinach0.02
Strawberry15.0
Sweet potato (postharvest to sweet potato intended only for use as seed)0.05
Triticale, forage0.30
Triticale, grain0.05
Triticale, hay0.30
Triticale, straw0.30
Vegetable, cucurbit, group 90.02
Vegetable, foliage of legume, group 70.20
Vegetable, legume, group 60.02
Vegetable, root (except sugarbeet), subgroup 1B0.02
Wheat, forage0.30
Wheat, grain0.05
Wheat, hay0.30
Wheat, straw0.30

1There are no U.S. registrations on the indicated commodity.

2This tolerance expires on March 21, 2017.

(2) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free and conjugated) and benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

CommodityParts per million
Cattle, meat0.1
Cattle, meat byproducts0.4
Goat, meat byproducts0.4
Hog, meat byproducts0.3
Horse, meat byproducts0.4
Milk0.1
Sheep, meat byproducts0.4

(b) Section 18 emergency exemptions. Time-limited tolerances specified in table 3 to this paragraph (b) are established for residues of the thiabendazole, including its metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in table 3 to this paragraph (b) is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole. The tolerances expire on the date specified in table 3 to this paragraph (b).

CommodityParts per
million
Expiration/
revocation
date
Sweet potato1012/31/22

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 32783, June 28, 1977]

Editorial Note: For Federal Register citations affecting §180.242, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.243   Propazine; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, and its two chlorinated degradates, 2-amino-4-chloro-6-isopropylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine, calculated as the stoichiometric equivalent of propazine, in or on the commodity.

CommodityParts per million
Sorghum, grain, forage0.25
Sorghum, grain, grain0.25
Sorghum, grain, stover0.25

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60242, Sept. 29, 2010]

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§180.245   Streptomycin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide streptomycin, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only streptomycin (O-2-Deoxy-2-(methylamino)-a-Lglucopyranosyl-(1-2)-O-5-deoxy-3-Cformyl-a-L-lyxofuranosyl-(1-4)-N,N-bis(aminoiminomethyl)-D-streptamine) in or on the commodity.

Table 1 to Paragraph (a)

CommodityParts per
million
Bean, dry, seed0.5
Bean, succulent0.5
Celery0.25
Fruit, citrus, group 10-100.8
Fruit, citrus, group 10-10, dried pulp3
Fruit, pome, group 110.25
Pepper0.25
Potato0.25
Tomato0.25

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of streptomycin, in or on the agricultural commodities, as specified in Table 2 to this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels listed in Table 2 to this paragraph (b) is to be determined by measuring the levels of streptomycin only, in or on the commodities listed in this Table 2 paragraph (b). The tolerances expire on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

CommodityParts per
million
Expiration
date
Fruit, citrus, group 10-102.012/31/22
Fruit, citrus, group 10-10, dried pulp6.012/31/22

(c)-(d) [Reserved]

[86 FR 8710, Feb. 9, 2021]

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§180.249   Alachlor; tolerances for residues.

(a) General. Tolerances are established for combined residues of alachlor (2-chloro-2′,6″-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the following raw agricultural commodities.

CommodityParts per million
Beans, dry0.1
Beans, succulent lima0.1
Cattle, fat0.02
Cattle, meat byproducts0.02
Cattle, meat0.02
Corn, field, forage2.0
Corn, field, grain0.2
Corn, field, pop0.2
Corn, field, stover2.0
Corn, pop, stover2.0
Corn, sweet (K + CWHR)0.05
Corn, sweet, stover2.0
Cotton, gin byproducts0.7
Cotton, undelinted seed0.03
Cowpea, forage5.0
Cowpea, hay5.0
Egg0.02
Goat, fat0.02
Goat, meat byproducts0.02
Goat, meat0.02
Hog, fat0.02
Hog meat byproducts0.02
Hog, meat0.02
Horse, fat0.02
Horse, meat byproducts0.02
Horse, meat0.02
Milk0.02
Peanut0.5
Poultry, fat0.02
Poultry, meat byproducts0.02
Poultry, meat0.02
Sheep, fat0.02
Sheep, meat byproducts0.02
Sheep, meat0.02
Sorghum grain, forage2.0
Sorghum, grain, grain0.1
Sorghum, grain, stover1.0
Soybeans, seed1.0
Sunflower, meal3.4
Sunflower, seed2.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of alachlor (2-chloro-2′,6′-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor, in or on the following raw agricultural commodities when present therein as a result of the application of alachlor to the growing crops in paragraph (a) of this section:

CommodityParts per million
Animal feed, nongrass, group 18, forage1.4
Animal feed, nongrass, group 18, hay1.2
Grain, cereal, forage, and straw, group 16 except corn, sorghum, rice, straw0.8
Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage0.6
Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay0.8
Grain, cereal, group 15 except corn, sorghum, rice0.05

[72 FR 54584, Sept. 26, 2007]

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§180.252   Tetrachlorvinphos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tetrachlorvinphos [(Z)-2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate], including its metabolites, 1-(2,4,5-trichlorophenyl)-ethanol (free and conjugated forms), 2,4,5-trichloroacetophenone, and 1-(2,4,5-trichlorophenyl)-ethanediol, in or on the following commodities:

CommodityParts per
million
Cattle, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)0.2
Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)1.0
Cattle, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)0.5
Cattle, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)2.0
Cattle, meat byproducts, except kidney and liver1.0
Egg (of which no more than 0.05 ppm is tetrachlorvinphos per se)0.2
Hog, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)0.2
Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)1.0
Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)0.5
Hog, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)2.0
Hog, meat byproducts, except kidney and liver1.0
Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is tetrachlorvinphos per se)0.05
Poultry, fat (of which no more than 7.0 ppm is tetrachlorvinphos per se)7.0
Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)2.0
Poultry, meat (of which no more than 3.0 ppm is tetrachlorvinphos per se)3.0
Poultry, meat byproducts, except liver2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 57659, Sept. 16, 2011, as amended at 78 FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, 2013]

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§180.253   Methomyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

CommodityParts per millionExpiration/revocation date
Alfalfa, forage10None
Alfalfa, hay10None
Apple1None
Asparagus2None
Avocado2None
Barley, grain1None
Barley, hay10None
Barley, straw10None
Bean, dry, seed0.1None
Bean, forage10None
Bean, succulent2None
Beet, garden, tops6None
Bermudagrass, forage10None
Bermudagrass, hay40None
Blueberry6None
Broccoli3None
Brussels sprouts2None
Cabbage5None
Cabbage, Chinese, bok choy5None
Cabbage, Chinese, napa5None
Cauliflower2None
Celery3None
Collards6None
Corn, field, forage10None
Corn, field, grain0.1None
Corn, field, stover10None
Corn, pop, grain0.1None
Corn, pop, stover10None
Corn, sweet, forage10None
Corn, sweet, kernel plus cob with husks removed0.1None
Corn, sweet, stover10None
Cotton, undelinted seed0.1None
Dandelion, leaves6None
Endive5None
Grape512/31/16
Grapefruit2None
Hop, dried cones112None
Kale6None
Lemon2None
Lentil, seed0.1None
Lettuce5None
Mustard greens6None
Nectarine5None
Oat, forage10None
Oat, grain1None
Oat, hay10None
Oat, straw10None
Onion, dry bulb0.2None
Onion, green3None
Orange2None
Parsley, leaves6None
Pea5None
Pea, field, vines10None
Peach5None
Peanut0.1None
Pecan0.1None
Pepper, bell2None
Pepper, nonbell2None
Peppermint, tops2None
Pomegranate0.2None
Rye, forage10None
Rye, grain1None
Rye, straw10None
Sorghum, grain, forage1None
Sorghum, grain, grain0.2None
Soybean, forage10None
Soybean, seed0.2None
Spearmint, tops2None
Spinach6None
Swiss chard6None
Tangerine2None
Tomato1None
Turnip, greens6None
Vegetable, brassica, leafy, group 56.0None
Vegetable, cucurbit, group 90.2None
Vegetable, fruiting, group 80.2None
Vegetables, leafy20.2None
Vegetable, root and tuber, group 10.2None
Wheat, forage10None
Wheat, grain1None
Wheat, hay10None
Wheat, straw10None

1There are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.

2Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards, dandelions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and watercress.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

CommodityParts
per million
Pear4

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR 72598, Nov. 20, 2015]

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§180.254   Carbofuran; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide carbofuran (2,3-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benzofuranyl-N-methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on the following raw agricultural commodities:

CommodityParts per million
Banana10.1
Coffee, bean, green10.1
Rice, grain10.2
Sugarcane, cane10.1

1There are no U.S. registrations for use of carbofuran on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[39 FR 20597, June 12, 1974]

Editorial Note: For Federal Register citations affecting §180.254, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.258   Ametryn; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4-(isopropylamino)-6-(methylthio)-s-triazine in or on the following raw agricultural commodities:

CommodityParts per million Expiration/Revocation Date
Banana0.256/16/10
Corn, field, forage0.1None
Corn, field, grain0.05None
Corn, field, stover0.05None
Corn, pop, grain0.05None
Corn, pop, stover0.05None
Corn, sweet, forage0.56/16/10
Corn, sweet, kernel plus cob with husks removed0.256/16/10
Corn, sweet, stover0.56/16/10
Pineapple0.05None
Sugarcane, cane0.05None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009]

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§180.259   Propargite; tolerances for residues.

(a) General. Tolerances are established for residues of the pesticide propargite (2-(p-tert-butylphenoxy) cyclohexyl 2-propynyl sulfite) in or on the following food commodities.

Commodity Parts per million
Almond0.1
Almond, hulls55.0
Bean, dry, seed0.2
Cattle, fat0.1
Cattle, meat0.1
Cattle, meat byproducts0.1
Citrus, oil30.0
Corn, field, forage10.0
Corn, field, grain0.1
Corn, field, stover10.0
Corn, pop, grain0.1
Corn, pop, stover10.0
Corn, sweet, forage10.0
Corn, sweet, stover10.0
Cotton, undelinted seed0.1
Egg0.1
Goat, fat0.1
Goat, meat0.1
Goat, meat byproducts0.1
Grain, aspirated fractions0.4
Grape10.0
Grapefruit5.0
Hog, fat0.1
Hog, meat0.1
Hog, meat byproducts0.1
Hop, dried cones100.0
Horse, fat0.1
Horse, meat0.1
Horse, meat byproducts0.1
Lemon5.0
Milk, fat (0.08 ppm in milk)2.0
Nectarine4.0
Orange10.0
Peanut0.1
Peppermint, tops50.0
Poultry, fat0.1
Potato0.1
Sheep, fat0.1
Sheep, meat0.1
Sheep, meat byproducts0.1
Sorghum, grain, forage10.0
Sorghum, grain, grain5.0
Sorghum, grain, stover10.0
Spearmint, tops50.0
Tea, dried10.0
Walnut0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of propargite in or on the following raw agricultural commodities:

Commodity Parts per million
Corn, sweet, kernel plus cob with husks removed0.1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

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§180.261   Phosmet; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

CommodityParts per million
Alfalfa, forage20
Alfalfa, hay40
Almond, hulls10
Apple10
Apricot5
Blueberry10
Cattle, fat0.2
Cattle, meat0.1
Cattle, meat byproducts0.1
Cherry10
Cranberry10
Fruit, citrus, group 105
Goat, fat0.1
Goat, meat0.1
Goat, meat byproducts0.1
Grape10
Hog, fat0.2
Hog, meat0.04
Hog, meat byproducts0.04
Horse, fat0.1
Horse, meat0.1
Horse, meat byproducts0.1
Kiwifruit25
Milk0.1
Nectarine5
Nut, tree, group 140.1
Pea, dry, seed0.5
Pea, field, hay20
Pea, field, vines10
Pea, succulent1
Peach10
Pear10
Plum, prune, fresh5
Potato0.1
Sheep, fat0.1
Sheep, meat0.1
Sheep, meat byproducts0.1
Sweet potato, roots12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

CommodityParts per million
Crabapple20
Pistachio0.1

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, 2010]

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§180.262   Ethoprop; tolerances for residues.

(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, in or on the commodity.

CommodityParts per million
Banana0.02
Bean, lima0.02
Bean, snap, succulent0.02
Cabbage0.02
Corn, field, forage0.02
Corn, field, grain0.02
Corn, field, stover0.02
Corn, sweet, forage0.02
Corn, sweet, kernel plus cob with husks removed0.02
Corn, sweet, stover0.02
Cucumber0.02
Hop, dried cones0.02
Peppermint, tops0.02
Pineapple10.02
Potato0.02
Spearmint, tops0.02
Sugarcane, cane0.02
Sweet potato, roots0.02

1There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, distribution, and use is allowed, provided it is consistent with the terms of the cancellation order of July 9, 2009; i.e., the EPA will allow the technical registrant to continue to sell and distribute existing stocks of the amended registered product bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided that such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified product.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010]

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§180.269   Aldicarb; tolerances for residues.

(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-methyl-2-(methylthio)propionaldehyde O-(methylcarbamoyl) oxime and its cholinesterase-inhibiting metabolites 2-methyl 2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl) oxime in or on the following food commodities:

Commodity Parts per million
Bean, dry, seed0.1
Beet, sugar, roots0.05
Beet, sugar, tops1
Citrus, dried pulp0.6
Coffee, bean, green0.1
Cotton, undelinted seed0.1
Cotton, hulls0.3
Grapefruit0.3
Lemon0.3
Lime0.3
Orange, sweet0.3
Peanut0.05
Pecan0.5
Potato1
Soybean0.02
Sugarcane, cane0.02
Sweet potato, roots0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016]

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§180.272   Tribuphos; tolerances for residues.

(a) General. Tolerances are established for residues of the defoliant tribuphos (S,S,S-tributyl phosphorotrithioate) in or on food commodities as follows:

CommodityParts per million
Cattle, fat0.15
Cattle, meat0.02
Cattle, meat byproducts0.02
Cotton, gin byproducts40.0
Cotton, undelinted seed4.0
Goat, fat0.15
Goat, meat0.02
Goat, meat byproducts0.02
Hog, fat0.15
Hog, meat0.02
Hog, meat byproducts0.02
Horse, fat0.15
Horse, meat0.02
Horse, meat byproducts0.02
Milk0.01
Sheep, fat0.15
Sheep, meat0.02
Sheep, meat byproducts0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

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§180.274   Propanil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propanil (3′, 4′-dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the following food commodities:

CommodityParts per million
Cattle, fat0.10
Cattle, meat0.05
Cattle, meat byproducts1.0
Crayfish0.05
Egg0.30
Goat, fat0.10
Goat, meat0.05
Goat, meat byproducts1.0
Hog, fat0.10
Hog, meat0.05
Hog, meat byproducts1.0
Horse, fat0.10
Horse, meat0.05
Horse, meat byproducts1.0
Milk0.05
Poultry, fat0.05
Poultry, meat0.10
Poultry, meat byproducts0.50
Rice, bran40
Rice, grain10
Rice, hulls30
Sheep, fat0.10
Sheep, meat0.05
Sheep, meat byproducts1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007; 80 FR 72598, Nov. 20, 2015]

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§180.275   Chlorothalonil; tolerances for residues.

(a) General. (1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

CommodityParts per million
Almond0.05
Almond, hulls1.0
Apricot0.5
Asparagus0.1
Banana (NMT 0.05 ppm in edible pulp)0.5
Bean, dry, seed0.1
Bean, snap, succulent5
Blueberry1.0
Brassica, head and stem, subgroup 5A5.0
Carrot, roots1
Celery15
Cherry, sweet0.5
Cherry, tart0.5
Cocoa bean, dried bean0.05
Coffee, bean, green0.20
Corn, sweet, kernel plus cob with husks removed1
Cranberry5.0
Ginseng4.0
Horseradish4.0
Lentil0.10
Lychee15
Mango1.0
Mushroom1.0
Nectarine0.5
Okra6.0
Onion, bulb0.5
Onion, green5
Papaya15
Parsnip, roots1
Passionfruit3
Pea, edible podded5
Peach0.5
Peanut0.3
Pistachio0.2
Plum0.2
Plum, prune0.2
Potato0.1
Rhubarb4.0
Soybean0.2
Starfruit3.0
Tomato5
Vegetable, cucurbit, group 95.0
Vegetable, fruiting, group 8, except tomato6.0
Yam, true0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity Parts per million
Cattle, fat0.1
Cattle, kidney0.5
Cattle, meat byproducts, except kidney0.05
Cattle, meat0.03
Goat, fat0.1
Goat, kidney0.5
Goat, meat byproducts, except kidney0.05
Goat, meat0.03
Hog, fat0.1
Hog, kidney0.5
Hog, meat byproducts, except kidney0.05
Hog, meat0.03
Horse, fat0.1
Horse, kidney0.5
Horse, meat byproducts, except kidney0.05
Horse, meat0.03
Milk0.1
Sheep, fat0.1
Sheep, kidney0.5
Sheep, meat byproducts, except kidney0.05
Sheep, meat0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined residues of chlorothalonil and its metabolite in or on the following raw agricultural commodities:

CommodityParts per million
Hazelnut0.1
Peppermint, tops2
Persimmon1.5
Spearmint, tops2

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 56114, Oct. 21, 1977]

Editorial Note: For Federal Register citations affecting §180.275, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.276   Formetanate hydrochloride; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide formetanate hydrochloride, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only formetanate hydrochloride, N,N-dimethyl-N'-[3-[(methylamino)carbonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity.

CommodityParts per
million
Expiration/revocation date
Apple0.5012/31/13
Apple, wet pomace1.512/31/13
Grapefruit1.5None
Lemon0.60None
Lime0.03None
Nectarine0.40None
Orange1.5None
Peach0.4012/31/13
Pear0.5012/31/13
Tangelo0.03None
Tangerine0.03None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

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§180.278   Phenmedipham; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide phenmedipham (3-methoxycarbonylaminophenyl-3′-methylcarbanilate) in or on the following food commodities:

CommodityParts per million
Beet, garden, roots0.2
Beet, garden, tops0.2
Beet, sugar, dried pulp0.5
Beet, sugar, molasses0.2
Beet, sugar, roots0.1
Beet, sugar, tops0.1
Spinach4.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007]

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§180.284   Zinc phosphide; tolerances for residues.

(a) General. Tolerances are established for residues of the phosphine resulting from the use of the rodenticide zinc phosphide in or on the raw agricultural commodities as follows:

CommodityParts per million
Alfalfa, forage0.2
Alfalfa, hay0.2
Barley, grain0.05
Barley, hay0.2
Barley, straw0.2
Bean, dry, seed0.05
Beet, sugar, roots0.05
Beet, sugar, tops0.2
Grape0.01
Grass, rangeland, forage0.1
Grass, rangeland, hay0.1
Potato0.05
Sugarcane, cane0.01
Timothy, hay0.5
Timothy, forage0.5
Wheat, forage0.05
Wheat, grain0.05
Wheat, hay0.05
Wheat, straw0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on the following raw agricultural commodities as follows:

CommodityParts per million
Artichoke, globe0.01
Beet, sugar, roots0.04
Beet, sugar, tops0.02

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011]

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§180.287   Amitraz; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N-[[(2,4-dimethylphenyl)imino]methyl]]-N-methylmethanimidamide), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring amitraz residues convertible to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, in or on the following raw agricultural commodities:

CommodityParts per million
Cattle, fat0.1
Cattle, meat0.02
Cattle, meat byproducts0.2
Hog, fat0.1
Hog, kidney0.1
Hog, liver0.1
Hog, meat0.05
Hog, meat byproducts0.3
Honey0.2
Honeycomb9
Milk0.03
Milk, fat0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013; 80 FR 72598, Nov. 20, 2015]

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§180.288   2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole in or on the following food commodities:

CommodityParts per million
Barley, grain0.1(N)
Barley, straw0.1(N)
Beet, sugar, roots0.1(N)
Beet, sugar, tops0.1(N)
Corn, field, forage0.1(N)
Corn, field, grain0.1
Corn, field, stover0.1
Corn, pop, grain0.1
Corn, pop, stover0.1
Cotton, forage0.1(N)
Cotton, undelinted seed0.1(N)
Oat, forage0.1(N)
Oat, grain0.1(N)
Oat, hay0.1(N)
Oat, straw0.1(N)
Rice, grain0.1(N)
Safflower, seed0.1(N)
Sorghum, grain, forage0.1(N)
Sorghum, grain, grain0.1(N)
Sorghum, grain, stover0.1(N)
Wheat, forage0.1(N)
Wheat, grain0.1(N)
Wheat, hay0.1(N)
Wheat, straw0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 74 FR 46374, Sept. 9, 2009; 80 FR 72598, Nov. 20, 2015]

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§180.289   Methanearsonic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide methanearsonic acid, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methanearsonic acid, from application of the disodium and monosodium salts of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, in or on the commodity.

CommodityParts per millionExpiration/Revocation Date
Cotton, undelinted seed0.7None
Cotton, hulls0.9None
Fruit, citrus0.3512/31/12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 77 FR 59126, Sept. 26, 2012]

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§180.291   Pentachloronitrobenzene; tolerance for residues.

(a) General. Tolerances are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

CommodityParts per million
Bean0.1
Brassica, head and stem, subgroup 5A0.1
Cotton, undelinted seed0.1
Garlic, bulb0.1
Peanut1.0
Potato0.1
Soybean, forage0.02
Soybean, hay0.02
Soybean, seed0.02
Vegetable, fruiting, group 80.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

CommodityParts per million
Collards0.2
Kale0.2
Mustard, greens0.2

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47456, Sept. 16, 2009]

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§180.292   Picloram; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide picloram, 4-amino-3,5,6-trichloropicolinic acid, including its metabolites and degradates, in or on the commodities in the following table from its application in the acid form or in the form of its salts. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only picloram, 4-amino-3,5,6-trichloropicolinic acid, in or on the commodity.

CommodityParts per million
Barley, grain0.5
Barley, pearled barley3.0
Barley, straw1.0
Cattle, fat0.4
Cattle, meat0.4
Cattle, meat byproducts15
Egg0.05
Goat, fat0.4
Goat, meat0.4
Goat, meat byproducts15
Grain, aspirated fractions4.0
Grass, forage400
Grass, hay225
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat0.4
Horse, meat0.4
Horse, meat byproducts15
Milk0.25
Oat, forage1.0
Oat, grain0.5
Oat, groats/rolled oats3.0
Oat, straw1.0
Poultry, fat0.05
Poultry, meat0.05
Poultry, meat byproducts0.05
Sheep, fat0.4
Sheep, meat0.4
Sheep, meat byproducts15
Wheat, bran3.0
Wheat, forage1.0
Wheat, germ3.0
Wheat, grain0.5
Wheat, middlings3.0
Wheat, shorts3.0
Wheat, straw1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, 2007; 75 FR 60243, Sept. 29, 2010]

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§180.293   Endothall; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of endothall, including its metabolites and degradates, in or on the commodities in the table, below. Compliance with the tolerance levels specified, below, is to be determined by measuring only endothall (7-oxabicylco [2.2.1] heptanes-2,3-dicarboxylic acid) and its mono-methyl ester.

CommodityParts per million
Apple0.05
Apple, wet pomace0.15
Cotton, undelinted seed0.1
Fish0.1
Hop, dried cones0.1
Potato0.1
Rice, grain0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di-N, N-dimethylalkylamine, and mono-N-N,-dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potential sources of water, potable.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent combined residues of the herbicide, endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in potable water from use of its potassium, sodium, di-N, N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potable water sources that may lead to endothall residues in or on the following commodities:

CommodityParts per million
Almond, hulls15.0
Animal feed, nongrass, group 18, forage4.0
Animal feed, nongrass, group 18, hay10
Apple, wet pomace0.15
Beet, sugar, molasses1.5
Brassica, head and stem subgroup 5A0.1
Brassica, leafy, subgroup 5B2.0
Bushberry subgroup 13-07B0.6
Caneberry subgroup 13-07A0.6
Cattle, fat0.05
Cattle, kidney0.05
Cattle, kidney10.20
Cattle, liver10.10
Cattle, liver0.05
Cattle, meat0.05
Corn, field, grain0.07
Corn, pop, grain0.07
Corn, sweet, kernel plus cob with husks removed0.3
Citrus, dried pulp0.1
Egg0.05
Feed commodities not otherwise listed10.0
Food commodities not otherwise listed5.0
Fruit, citrus group 100.05
Fruit, pome, group 110.05
Fruit, stone, group 120.3
Goat, fat0.05
Goat, kidney10.15
Goat, kidney0.05
Goat, liver0.05
Goat, meat0.05
Grain, aspirated fractions35.0
Grain cereal, forage, fodder and straw, group 1610.0
Grain, cereal, group 15, except corn4.0
Grape1.0
Grape, raisin5.0
Grass, forage, fodder, and hay group 17, forage3.5
Grass, forage, fodder, and hay group 17, hay18.0
Herb and spice, group 195.0
Hog, fat0.05
Hog, kidney10.10
Hog, kidney0.05
Hog, liver0.05
Hog, meat0.05
Milk10.03
Milk0.01
Nut, tree, group 140.05
Okra0.05
Pea and bean, dried shelled, subgroup 6C0.2
Pea and bean, succulent shelled, subgroup 6B2.0
Peppermint, tops5.0
Pistachio0.05
Poultry, fat0.05
Poultry, liver0.05
Poultry, meat0.05
Poultry, meat byproducts10.20
Poultry, meat byproducts0.05
Rice, hulls8.0
Sheep, fat0.05
Sheep, kidney10.15
Sheep, kidney0.05
Sheep, liver0.05
Sheep, meat0.05
Soybean, hulls0.5
Soybean, seed0.2
Spearmint, tops5.0
Tomato, paste0.1
Tomato, puree0.1
Vegetable, bulb, group 3-070.5
Vegetable, cucurbit, group 91.5
Vegetable, foliage of legume, group 74.0
Vegetable, fruiting, group 80.05
Vegetable, leafy, except brassica, group 42.0
Vegetable, leaves of root and tuber, group 23.0
Vegetable, legume, edible, podded, subgroup 6A2.0
Vegetable, root and tuber, group 11.0
Wheat, milled byproducts5.0

1This tolerance expires on May 22, 2017.

[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013; 80 FR 72598, Nov. 20, 2015; 81 FR 83169, Nov. 21, 2016]

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§180.297   N-1-Naphthyl phthalamic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide N-1-naphthyl phthalamic acid from application of its sodium salt in or on the following raw agricultural commodities:

CommodityParts per million
Cantaloupe0.1(N)
Cucumber0.1(N)
Muskmelon0.1(N)
Watermelon0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

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§180.298   Methidathion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in or on the commodity.

CommodityParts per millionExpiration/revocation date
Almond, hulls6.012/31/16
Artichoke, globe0.0512/31/16
Citrus, oil420.012/31/16
Cotton, undelinted seed0.212/31/16
Fruit, citrus, group 10, except tangerine4.012/31/16
Fruit, pome, group 110.0512/31/16
Fruit, stone, group 120.0512/31/16
Mango0.0512/31/16
Nut, tree, group 140.0512/31/16
Olive0.0512/31/16
Safflower, seed0.512/31/16
Sorghum, forage, forage2.012/31/16
Sorghum, grain, forage2.012/31/16
Sorghum, grain, grain0.212/31/16
Sorghum, grain, stover2.012/31/16
Sunflower, seed0.512/31/16
Tangerine6.012/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in or on the commodity.

CommodityParts per
million
Expiration/
revocation
date
Kiwifruit0.112/31/16
Longan0.112/31/16
Starfruit0.112/31/16
Sugar apple0.212/31/16

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 44845, Sept. 29, 1978]

Editorial Note: For Federal Register citations affecting §180.298, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.299   Dicrotophos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of 3-hydroxy-N,N-dimethyl-cis-crotonamide, in or on the following food commodities:

CommodityParts per million
Cotton, gin byproducts2.0
Cotton, undelinted seed0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52613, Sept. 10, 2008]

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§180.300   Ethephon; tolerances for residues.

(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl) phosphonic acid] in or on food commodities as follows:

CommodityParts per million
Apple5.0
Apple, juice10.0
Barley, bran5.0
Barley, grain2.0
Barley, straw10.0
Blackberry30.0
Blueberry20.0
Cantaloupe2.0
Cattle, fat0.02
Cattle, kidney1.0
Cattle, meat0.02
Cattle, meat byproducts, except kidney0.2
Cherry10.0
Coffee, bean, green0.5
Cotton, gin byproducts180.0
Cotton, undelinted seed6.0
Egg0.002
Goat, fat0.02
Goat, kidney1.0
Goat, meat0.02
Goat, meat byproducts, except kidney0.2
Grape2.0
Grape, raisin12.0
Hazelnut0.80
Hog, fat0.02
Hog, kidney1.0
Hog, meat0.02
Hog, meat byproducts, except kidney0.2
Horse, fat0.02
Horse, kidney1.0
Horse, meat0.02
Horse, meat byproducts, except kidney0.2
Milk0.01
Nut, macadamia0.5
Pepper30.0
Pineapple2.0
Poultry, fat0.02
Poultry, liver0.05
Poultry, meat0.01
Poultry, meat byproducts, except liver0.01
Sheep, fat0.02
Sheep, kidney1.0
Sheep, meat0.02
Sheep, meat byproducts, except kidney0.2
Sugarcane, molasses1.5
Tomato2.0
Walnut0.5
Wheat, bran5.0
Wheat, germ5.0
Wheat, grain2.0
Wheat, middlings5.0
Wheat, shorts5.0
Wheat, straw10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(m), of 0.1 part per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic acid] in or on the food commodity sugarcane.

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010; 80 FR 72598, Nov. 20, 2015]

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§180.301   Carboxin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide carboxin (5,6-dihydro-2-methyl-1,4-oxathiin-3-carboxanilide) and its metabolites determined as aniline and expressed as parent compound, in or on food commodities as follows:

CommodityParts per million
Barley, grain0.2
Barley, straw0.2
Bean, dry, seed0.2
Bean, succulent0.2
Canola, seed0.03
Cattle, fat0.05
Cattle, meat byproducts0.1
Cattle, meat0.05
Corn, field, forage0.2
Corn, field, grain0.2
Corn, field, stover0.2
Corn, pop, grain0.2
Corn, pop, stover0.2
Corn, sweet, forage0.2
Corn, sweet, kernel plus cob with husks removed0.2
Corn, sweet, stover0.2
Cotton, undelinted seed0.2
Egg0.05
Goat, fat0.05
Goat, meat byproducts0.1
Goat, meat0.05
Hog, fat0.05
Hog, meat byproducts0.1
Hog, meat0.05
Horse, fat0.05
Horse, meat byproducts0.1
Horse, meat0.05
Milk0.05
Oat, forage0.5
Oat, grain0.2
Oat, straw0.2
Onion, bulb0.2
Peanut0.2
Peanut, hay0.2
Poultry, fat0.1
Poultry, meat byproducts0.1
Poultry, meat0.1
Rice, grain0.2
Safflower, seed0.2
Sheep, fat0.05
Sheep, meat byproducts0.1
Sheep, meat0.05
Soybean, seed0.2
Wheat, forage0.5
Wheat, grain0.2
Wheat, straw0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006; 80 FR 72598, Nov. 20, 2015]

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§180.303   Oxamyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide oxamyl, methyl N,N-dimethyl-N-[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N-dimethyl-N-hydroxy-1-thiooxamimidate calculated as oxamyl in or on the following food commodities:

Commodity Parts per million
Apple2
Banana0.3
Cantaloupe2.0
Carrot0.1
Celery10.0
Cotton, undelinted seed0.2
Cucumber2.0
Eggplant2.0
Fruit, citrus, group 103
Garlic, bulb0.2
Melon, honeydew2.0
Onion, bulb0.2
Peanut0.05
Peanut, hay2.0
Pear2.0
Peppermint, tops10.0
Pepper, bell2.0
Pepper, nonbell5.0
Pineapple1
Pineapple, process residue2.0
Pumpkin2.0
Spearmint, tops10.0
Squash, summer2.0
Squash, winter2.0
Tomato2
Vegetable, tuberous and corm, subgroup 1C0.1
Watermelon2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 72598, Nov. 20, 2015]

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§180.304   Oryzalin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

CommodityParts per million
Almond, hulls0.05
Avocado0.05
Berry group 130.05
Cranberry0.05
Fig0.05
Fruit, citrus, group 100.05
Fruit, pome, group 110.05
Fruit, stone, group 120.05
Grape0.05
Kiwifruit0.05
Nut, tree, group 140.05
Olive0.05
Pistachio0.05
Pomegranate0.05
Strawberry0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

CommodityParts per million
Guava0.05
Papaya0.05

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011]

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§180.314   Triallate; tolerances for residues.

(a) General. Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl diisopropylthiocarbamate and its metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodity:

CommodityParts per million
Bermudagrass, hay0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in 180.1(l),are established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its metabolite 2, 3, 3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:

CommodityParts per million
Barley, grain0.05
Barley, hay1.0
Barley, straw0.3
Beet, sugar, dried pulp0.2
Beet, sugar, roots0.1
Beet, sugar, tops0.5
Pea, dry0.2
Pea, field, hay1.0
Pea, field, vines0.5
Pea, succulent0.2
Wheat, forage0.5
Wheat, grain0.05
Wheat, hay1.0
Wheat, straw1.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24, 2009]

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§180.316   Pyrazon; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the following food commodities:

CommodityParts per million
Beet, garden, roots0.9
Beet, garden, tops7.0
Beet, sugar, molasses1.5
Beet, sugar, roots0.2
Beet, sugar, tops3.0
Cattle, fat0.10
Cattle, liver0.15
Cattle, meat0.10
Cattle, meat byproducts, except liver0.10
Goat, fat0.10
Goat, liver0.15
Goat, meat0.10
Goat, meat byproducts, except liver0.10
Horse, fat0.10
Horse, liver0.15
Horse, meat0.10
Horse, meat byproducts, except liver0.10
Milk0.02
Sheep, fat0.10
Sheep, liver0.15
Sheep, meat0.10
Sheep, meat byproducts, except liver0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for combined residues of the herbicide pyrazon, 5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone, and its metabolites (calculated as pyrazon), in or on the following food commodities:

CommodityParts per million
Corn, field, forage0.5
Corn, field, stover0.5
Soybean, forage0.5
Soybean, hay0.5
Wheat, forage0.3
Wheat, hay0.2
Wheat, straw0.1

[68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008]

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§180.317   Propyzamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

CommodityParts per million
Alfalfa, seed10.0
Animal feed, nongrass, group 1810.0
Apple0.1
Artichoke, globe0.01
Blackberry0.05
Blueberry0.05
Boysenberry0.05
Cattle, fat0.2
Cattle, kidney0.4
Cattle, liver0.4
Cattle, meat0.02
Cattle, meat byproducts, except kidney and liver0.02
Egg0.02
Endive1.0
Fruit, stone, group 120.1
Goat, fat0.2
Goat, kidney0.4
Goat, liver0.4
Goat, meat0.02
Goat, meat byproducts, except kidney and liver0.02
Grape0.1
Hog, fat0.2
Hog, kidney0.4
Hog, liver0.4
Hog, meat0.02
Hog, meat byproducts, except kidney and liver0.02
Horse, fat0.2
Horse, kidney0.4
Horse, liver0.4
Horse, meat0.02
Horse, meat byproducts, except kidney and liver0.02
Lettuce, head1.0
Lettuce, leaf1.0
Milk0.02
Pear0.1
Poultry, fat0.02
Poultry, liver0.2
Poultry, meat0.02
Poultry, meat byproducts, except liver0.02
Radicchio2.0
Raspberry0.05
Sheep, fat0.2
Sheep, kidney0.4
Sheep, liver0.4
Sheep, meat0.02
Sheep, meat byproducts, except kidney and liver0.02

(b) Section 18 emergency exemptions. The time-limited tolerance specified in the table in this paragraph (b) is established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the specified agricultural commodity in the table in this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance level specified in the table in this paragraph (b) is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide in or on the commodity. The time-limited tolerance expires on the date specified in the table in this paragraph (b).

CommodityParts per
million
Expiration/revocation date
Cranberry1December 31, 2022

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

CommodityParts per million
Pea, field, seed0.05
Rhubarb0.1

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

CommodityParts per million
Grain, cereal, forage, group 160.6
Grain, cereal, hay, group 160.2
Grain, cereal, straw, group 160.3

[72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011; 81 FR 1531, Jan. 13, 2016; 84 FR 60943, Nov. 12, 2019]

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§180.318   4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.

(a) General. (1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or on the following food commodity:

CommodityParts per million
Pea0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4-(4-chloro-2-methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic acid, in or on the following food commodities:

CommodityParts per million
Peppermint, tops0.20
Spearmint, tops0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

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§180.319   Interim tolerances.

(a) General. While petitions for tolerances for negligible residues are pending and until action is completed on these petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the following raw agricultural commodities:

SubstancesUsesTolerance in parts per millionRaw
agricultural
commodity
Expiration/
revocation
date
Endothall (7-oxabicyclo-(2,2,1)heptane 2,3-dicarboxylic acidHerbicide0.2Beet, sugarNone
Methyl parathionHerbicide0.5Rye12/31/13

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014]

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§180.324   Bromoxynil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide bromoxynil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

CommodityParts per million
Alfalfa, forage0.1
Alfalfa, hay0.5
Barley, grain0.05
Barley, hay9.0
Barley, straw4.0
Corn, field, forage0.3
Corn, field, grain0.05
Corn, field, stover0.2
Corn, pop, grain0.05
Corn, pop, stover0.2
Flax, seed0.1
Garlic0.1
Grain, aspirated fractions1.2
Grass, forage18
Grass, hay5.0
Oat, forage0.3
Oat, grain0.05
Oat, hay9.0
Oat, straw4.0
Onion, bulb0.1
Peppermint, hay0.1
Rye, forage1.0
Rye, grain0.05
Rye, straw2.0
Sorghum, grain, forage0.8
Sorghum, grain, grain0.2
Sorghum, grain, stover0.2
Spearmint, hay0.1
Wheat, forage1.0
Wheat, grain0.05
Wheat, hay4.0
Wheat, straw2.0

(2) Tolerances are established for residues of the herbicide bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil and its metabolite, 3,5-dibromo-4-hydroxybenzoic acid (DBHA), resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

CommodityParts per million
Cattle, fat1
Cattle, meat byproducts3.5
Cattle, meat0.5
Cotton, gin byproducts7.0
Cotton, hulls5.0
Cotton, undelinted seed1.5
Egg0.05
Goat, fat1
Goat, meat byproducts3.5
Goat, meat0.5
Hog, fat1
Hog, meat byproducts3.5
Hog, meat0.5
Horse, fat1
Horse, meat byproducts3.5
Horse, meat0.5
Milk0.4
Poultry, fat0.05
Poultry, meat byproducts0.3
Poultry, meat0.05
Sheep, fat1
Sheep, meat byproducts3.5
Sheep, meat0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR 31491, June 1, 2011]

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§180.328   Napropamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide napropamide, N,N-diethyl-2-(1-napthalenyloxy) propionamide, in or on the following food commodities:

CommodityParts per millionExpiration/revocation date
Almond, hulls0.1None
Asparagus0.1None
Basil0.1None
Berry group 130.1None
Coffee, green bean0.1None
Cranberry0.1None
Grape0.1None
Kiwifruit0.1None
Marjoram0.1None
Nut, tree, group 140.1None
Peppermint, tops0.1None
Persimmon0.1None
Rhubarb0.1None
Rosemary0.1None
Savory, summer0.1None
Savory, winter0.1None
Spearmint, tops0.1None
Strawberry0.1None
Sweet potato, roots0.1None
Vegetable, brassica, leafy, group 50.1None
Vegetable, fruiting, group 80.1None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52614, Sept. 10, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.330   S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

CommodityParts per million
Alfalfa, forage5.0
Alfalfa, hay11.0
Bean, lima0.2
Beet, sugar, roots0.3
Beet, sugar, tops0.5
Broccoli1.0
Brussels sprouts1.0
Cabbage2.0
Cauliflower1.0
Clover, forage5.0
Clover, hay10.0
Corn, sweet, forage1.0
Corn, sweet, kernel plus cob with husks removed0.5
Corn, sweet, stover3.0
Cotton, undelinted seed0.02
Cucumber1.0
Eggplant1.0
Grapefruit1.0
Hazelnut0.05
Lemon1.0
Lettuce, head2.0
Melon0.2
Onion, bulb0.05
Orange1.0
Pepper0.75
Peppermint, tops12.5
Pumpkin0.2
Safflower, seed1.0
Sorghum, forage, forage2.0
Sorghum, grain, forage2.0
Sorghum, grain, grain0.75
Spearmint, tops12.5
Squash, summer1.0
Squash, winter0.3
Strawberry2.0
Walnut0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following food commodities:

CommodityParts per million
Cattle, fat0.01
Cattle, meat0.01
Cattle, meat byproducts0.01
Egg0.01
Goat, fat0.01
Goat, meat0.01
Goat, meat byproducts0.01
Hog, fat0.01
Hog, meat0.01
Hog, meat byproducts0.01
Horse, fat0.01
Horse, meat0.01
Horse, meat byproducts0.01
Milk0.01
Poultry, fat0.01
Poultry, meat0.01
Poultry, meat byproducts0.01
Sheep, fat0.01
Sheep, meat0.01
Sheep, meat byproducts0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

CommodityParts per million
Broccoli raab2.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

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§180.331   4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid (2,4-DB), both free and conjugated, determined as the acid, in or on food commodities, as follows:

Commodity Parts per million
Alfalfa, forage0.7
Alfalfa, hay2.0
Cattle, meat byproducts0.05
Clover, forage0.2
Clover, hay0.2
Goat, meat byproducts0.05
Hog, meat byproducts0.05
Horse, meat byproducts0.05
Peanut0.2
Peppermint, tops0.2
Sheep, meat byproducts0.05
Soybean, forage0.7
Soybean, hay2.0
Soybean, seed0.5
Spearmint, tops0.2
Trefoil, forage0.7
Trefoil, hay2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 74 FR 46374, Sept. 9, 2009]

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§180.332   Metribuzin;   tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1-dimethyl- ethyl)-3-(methylthio)-;1,2,4-triazin-5(4H)-one) and its triazinone metabolites in or on food commodities:

Commodity Parts per million
Alfalfa, forage2.0
Alfalfa, hay7.0
Asparagus0.1
Barley, grain0.75
Barley, hay7.0
Barley, pearled barley3.0
Barley, straw1.0
Carrot, roots0.3
Cattle, fat0.7
Cattle, meat0.7
Cattle, meat byproducts0.7
Corn, field, forage0.1
Corn, field, grain0.05
Corn, field, stover0.1
Corn, pop, grain0.05
Corn, sweet, forage0.1
Corn, sweet, kernel plus cob with husks removed0.05
Corn, sweet, stover0.1
Egg0.01
Goat, fat0.7
Goat, meat0.7
Goat, meat byproducts0.7
Grass, forage2.0
Grass, hay7.0
Hog, fat0.7
Hog, meat0.7
Hog, meat byproducts0.7
Horse, fat0.7
Horse, meat0.7
Horse, meat byproducts0.7
Lentil0.05
Milk0.05
Pea, dry, seed0.05
Pea, field, hay4.0
Pea, field, vines0.5
Pea, succulent0.1
Potato0.6
Potato, chips3.0
Potato, processed potato waste3.0
Poultry, fat0.7
Poultry, meat0.7
Poultry, meat byproducts0.7
Sainfoin, forage2.0
Sainfoin, hay7.0
Sheep, fat0.7
Sheep, meat0.7
Sheep, meat byproducts0.7
Soybean, seed0.3
Soybean, forage4.0
Soybean, hay4.0
Sugarcane, cane0.1
Sugarcane, molasses2.0
Tomato0.1
Wheat, bran3.0
Wheat, forage2.0
Wheat, germ3.0
Wheat, grain0.75
Wheat, hay7.0
Wheat, middlings3.0
Wheat, shorts3.0
Wheat, straw1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, July 31, 2002]

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§180.337   Oxytetracycline; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the commodity.

CommodityParts per million
Apple0.35
Fruit, citrus, group 10-100.01
Peach0.35
Pear0.35

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire on the dates specified in the table.

CommodityParts per
million
Expiration/
revocation date
Fruit, citrus, group 10-100.4012/31/19

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23493, Apr. 27, 2011, as amended at 82 FR 13251, Mar. 10, 2017; 83 FR 62493, Dec. 4, 2018]

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§180.339   MCPA; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid), both free and conjugated, resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following food commodities:

CommodityParts per million
Alfalfa, forage0.5
Alfalfa, hay2.0
Barley, grain1.0
Barley, hay40
Barley, straw25
Clover, forage0.5
Clover, hay2.0
Flax, seed0.1
Grain, aspirated fractions3.0
Grass, forage300
Grass, hay20
Lespedeza, forage0.5
Lespedeza, hay2.0
Oat, forage20
Oat, grain1.0
Oat, hay115
Oat, straw25
Pea, dry0.1
Pea, field, hay0.1
Pea, succulent0.1
Pea, field, vines0.1
Rye, forage20
Rye, grain1.0
Rye, straw25
Trefoil, forage0.5
Trefoil, hay2.0
Vetch, forage0.5
Vetch, hay2.0
Wheat, forage20
Wheat, grain1.0
Wheat, hay115
Wheat, straw25

(2) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid) resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following food commodities:

CommodityParts per million
Cattle, fat0.1
Cattle, meat0.1
Cattle, meat byproducts0.1
Goat, fat0.1
Goat, meat0.1
Goat, meat byproducts0.1
Hog, fat0.1
Hog, meat0.1
Hog, meat byproducts0.1
Horse, fat0.1
Horse, meat0.1
Horse, meat byproducts0.1
Milk0.1
Sheep, fat0.1
Sheep meat0.1
Sheep meat byproducts0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008]

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§180.341   2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.

(a) General. Tolerances are established for combined negligible residues of a fungicide and insecticide that is a mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw agricultural commodities as follows:

CommodityParts per million
Apple10.1
Grape10.1

1There are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

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§180.342   Chlorpyrifos; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

CommodityParts per million
Alfalfa, forage3.0
Alfalfa, hay13
Almond0.2
Almond, hulls12
Apple0.01
Apple, wet pomace0.02
Banana0.1
Beet, sugar, dried pulp5.0
Beet, sugar, molasses15
Beet, sugar, roots1.0
Beet, sugar, tops8.0
Cattle, fat0.3
Cattle, meat0.05
Cattle, meat byproducts0.05
Cherry, sweet1.0
Cherry, tart1.0
Citrus, dried pulp5.0
Citrus, oil20
Corn, field, forage8.0
Corn, field, grain0.05
Corn, field, refined oil0.25
Corn, field, stover8.0
Corn, sweet, forage8.0
Corn, sweet, kernel plus cob with husk removed0.05
Corn, sweet, stover8.0
Cotton, undelinted seed0.2
Cranberry1.0
Cucumber0.05
Egg0.01
Fig0.01
Fruit, citrus, group 101.0
Goat, fat0.2
Goat, meat0.05
Goat, meat byproducts0.05
Hazelnut0.2
Hog, fat0.2
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat0.25
Horse, meat0.25
Horse, meat byproducts0.25
Kiwifruit2.0
Milk, fat (Reflecting 0.01 ppm in whole milk)0.25
Nectarine0.05
Onion, bulb0.5
Peach0.05
Peanut0.2
Peanut, refined oil0.2
Pear0.05
Pecan0.2
Pepper1.0
Peppermint, tops0.8
Peppermint, oil8.0
Plum, prune, fresh0.05
Poultry, fat0.1
Poultry, meat0.1
Poultry, meat byproducts0.1
Pumpkin0.05
Radish2.0
Rutabaga0.5
Sheep, fat0.2
Sheep, meat0.05
Sheep, meat byproducts0.05
Spearmint, tops0.8
Spearmint, oil8.0
Sorghum, grain, forage0.5
Sorghum, grain, grain0.5
Sorghum, grain, stover2.0
Soybean, seed0.3
Strawberry0.2
Sunflower, seed0.1
Sweet potato, roots0.05
Turnip, roots1.0
Turnip, tops0.3
Vegetable, brassica, leafy, group 51.0
Vegetable, legume, group 6. except soybean0.05
Walnut0.2
Wheat, forage3.0
Wheat, grain0.5
Wheat, straw6.0

(2) Chlorpyrifos [O,O-diethyl O-(3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in accordance with the following prescribed conditions.

(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are held, processed, prepared or served. Contamination of food or food contact surfaces shall be avoided. Food must be removed or covered during treatment.

(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active ingredient by weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the spray.

(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active ingredient by weight.

(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by weight. Equipment capable of delivering a pin-stream of insecticide shall be used.

(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release product in food-handling establishments where food and food products are held, processed, prepared, or served. A maximum of 36 strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor space. The strips are not to be placed in exposed areas where direct contact with food, utensils, and food-contact surfaces would be likely to occur.

(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food commodities (other than those already covered by a higher tolerance as a result of use on growing crops) in food service establishments where food and food products are prepared and served, as a result of the application of chlorpyrifos in microencapsulated form.

(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are prepared and served. All treatments shall be applied in such a manner as to avoid contamination of food or food contact surfaces.

(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight.

(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into cracks and crevices or capable of applying small amounts of insecticide into cracks and crevices shall be used.

(iv) For spot treatment, an individual spot shall not exceed 2 square feet.

(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in 180.1(l), are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl- O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

CommodityParts per million
Asparagus5.0
Grape0.01

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, Sept. 14, 2011]

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§180.345   Ethofumesate; tolerances for residues.

(a) General. Tolerance are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the following food commodities.

CommodityParts per million
Beet, garden, roots0.5
Beet, garden, tops5.0
Beet, sugar, molasses2.0
Beet, sugar, roots1.5
Beet, sugar, tops4.0
Cattle, fat0.05
Cattle, meat0.05
Cattle, meat byproducts0.05
Garlic0.25
Goat, fat0.05
Goat, meat0.05
Goat, meat byproducts0.05
Grass, straw1.0
Horse, fat0.05
Horse, meat0.05
Horse, meat byproducts0.05
Onion, bulb0.25
Shallot, bulb0.25
Shallot, fresh leaves0.25
Sheep, fat0.05
Sheep, meat0.05
Sheep, meat byproducts0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in §180.1(l) are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the raw agricultural commodities.

CommodityParts per million
Carrot, roots7.0

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007; 82 FR 57158, Dec. 4, 2017]

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§180.349   Fenamiphos; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide/insecticide fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, and its cholinesterase inhibiting metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl 1-(methylethyl)phosphoramidate and ethyl 3-methyl-4-(methylsulfonyl)phenyl 1-(methylethyl)phosphoramidate, calculated as the stoichiometric equivalent of fenamiphos, in or on the commodity.

CommodityParts per million
Banana10.1
Grape10.1
Grape, raisin10.3
Pineapple10.3

1There are no U.S. registrations as of May 31, 2007.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, 2010]

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§180.350   Nitrapyrin; tolerances for residues.

(a) General. Tolerances are established for residues of the nitrification inhibitor nitrapyrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of nitrapyrin (2-chloro-6-(trichloromethyl) pyridine) and its 6-CPA metabolite (6-chloro-picolinic acid), calculated as the stoichiometric equivalent of nitrapyrin, in or on the commodity:

CommodityParts per million
Almond, hulls0.06
Beet, sugar, molasses0.5
Beet, sugar, roots0.3
Beet, sugar, tops0.7
Corn, field, forage1.0
Corn, field, grain0.1
Corn, field, milled byproducts0.2
Corn, field, stover1.0
Corn, pop, grain0.1
Corn, pop, stover1.0
Corn, sweet, forage1.0
Corn, sweet, kernel plus cob with husks removed0.1
Corn, sweet, stover1.0
Fruit, citrus, group 10-100.06
Fruit, citrus, group 10-10, dried pulp0.5
Fruit, citrus, group 10-10, oil2
Leaf petiole vegetable subgroup 22B0.5
Nut, tree, group 14-120.02
Rapeseed, seed0.3
Sorghum, forage, forage0.5
Sorghum, grain, forage0.5
Sorghum, grain, grain0.1
Sorghum, grain, stover0.5
Vegetable, Brassica, head and stem, group 5-160.1
Vegetable, bulb, group 3-070.3
Vegetable, leafy, group 4-160.4
Vegetable, tuberous and corm, crop subgroup 1C0.6
Wheat, bran3.0
Wheat, forage2.0
Wheat, grain0.5
Wheat, milled byproducts, except flour2.0
Wheat, straw6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007; 82 FR 56744, Nov. 30, 2017; 84 FR 44712, Aug. 27, 2019; 85 FR 48654, Aug. 12, 2020]

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§180.352   Terbufos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide terbufos (phosphorodithioic acid, S-(t-butylthio)methyl O,O-diethyl ester) and its phosphorylated (cholinesterase-inhibiting) metabolites (phosphorothioic acid, S-(t-butylthio)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester; phosphorodithioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; and phosphorodithioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester) in or on food commodities:

CommodityParts per million
Banana0.025
Beet, sugar, roots0.05
Beet, sugar, tops0.1
Coffee, green bean10.05
Corn, field, forage0.5
Corn, field, grain0.5
Corn, field, stover0.5
Corn, pop, grain0.5
Corn, pop, stover0.5
Corn, sweet, kernel plus cob with husks removed0.05
Corn, sweet, forage0.5
Corn, sweet, stover0.5
Sorghum, grain, forage0.5
Sorghum, grain, grain0.05
Sorghum, grain, stover0.5

1 There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 53740, Sept. 17, 2008]

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§180.353   Desmedipham; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide desmedipham, (ethyl-m-hydroxycarbanilate carbanilate) in or on the following raw agricultural commodities in the table that follows:

CommodityParts per million
Beet, garden, roots0.05
Beet, garden, tops1.0
Beet, sugar, roots0.1
Beet, sugar, tops5.0
Spinach6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

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§180.355   Bentazon; tolerances for residues.

(a) General. (1) Tolerances are established for residues of bentazon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring for only the sum of bentazon (3-(1-methylethyl)-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide), 6-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide, and 8-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide calculated as the stoichiometric equivalent of bentazon.

CommodityParts per million
Bean, dry, seed0.05
Bean, succulent0.5
Corn, field, forage3.0
Corn, field, grain0.05
Corn, field, stover3.0
Corn, pop, grain0.05
Corn, sweet, kernel plus cob with husks removed0.05
Cowpea, forage10.0
Cowpea, hay3.0
Flax, seed1.0
Pea, dry, seed3
Pea, field, hay8.0
Pea, field, vines3.0
Pea, succulent3.0
Peanut0.05
Peanut, hay3.0
Pepper, nonbell0.05
Peppermint, tops1.0
Rice, grain0.05
Rice, hulls0.25
Sorghum, forage0.20
Sorghum, grain, grain0.05
Sorghum, grain, stover0.05
Soybean, forage8.0
Soybean, hay8.0
Soybean, seed0.05
Spearmint, tops1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl benzamide (AIBA) in or on the following food commodities:

Commodity Parts per million
Cattle, fat0.05
Cattle, meat byproducts0.05
Cattle, meat0.05
Egg0.05
Goat, fat0.05
Goat, meat byproducts0.05
Goat, meat0.05
Hog, fat0.05
Hog, meat byproducts0.05
Hog, meat0.05
Milk0.02
Poultry, fat0.05
Poultry, meat byproducts0.05
Poultry, meat0.05
Sheep, fat0.05
Sheep, meat byproducts0.05
Sheep, meat0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(m), are established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

CommodityParts per million
Clover, forage1.0
Clover, hay2.0

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 26979, May 26, 1977]

Editorial Note: For Federal Register citations affecting §180.355, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.356   Norflurazon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro-5-(methylamino)-2-(alpha, alpha, alpha-trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its desmethyl metabolite 4-chloro-5-(amino)-2-alpha, alpha, alpha-trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural commodities:

CommodityParts per million
Alfalfa, forage3.0
Alfalfa, hay5.0
Alfalfa, seed0.1
Almond, hulls1.0
Almond0.1
Apple0.1
Apricot0.1
Asparagus0.05
Avocado0.20
Blackberry0.1
Blueberry0.2
Cattle, fat0.1
Cattle, liver0.50
Cattle, meat0.1
Cattle, meat byproducts, except liver0.1
Cherry0.1
Citrus, dried pulp0.4
Citrus, molasses1.0
Cotton, undelinted seed0.1
Cranberry0.1
Fruit, citrus0.2
Goat, fat0.1
Goat, liver0.50
Goat, meat0.1
Goat, meat byproducts, except liver0.1
Grape0.1
Hazelnut0.1
Hog, fat0.1
Hog, liver0.50
Hog, meat0.1
Hog, meat byproducts, except liver0.1
Hop, dried cones3.0
Hop, vines1.0
Horse, fat0.1
Horse, liver0.50
Horse, meat0.1
Horse, meat byproducts, except liver0.1
Milk0.1
Nectarine0.1
Peach0.1
Peanut0.05
Peanut, hay5.50
Peanut, hay1.5
Pear0.1
Pecan0.1
Plum, prune, fresh0.1
Poultry, fat0.1
Poultry, meat0.1
Poultry, meat byproducts0.1
Raspberry0.2
Sheep, fat0.1
Sheep, liver0.50
Sheep, meat0.1
Sheep, meat byproducts, except liver0.1
Soybean0.1
Soybean, forage1.0
Soybean, hay1.0
Walnut0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 14909, Apr. 7, 1982]

Editorial Note: For Federal Register citations affecting §180.356, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.360   Asulam; tolerance for residues.

(a) General. Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate) and its sulfanilamide containing metabolites in or on the following food commodities:

CommodityParts per million
Cattle, fat0.05
Cattle, meat0.05
Cattle, meat byproducts0.2
Goat, fat0.05
Goat, meat0.05
Goat, meat byproducts0.2
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.2
Horse, fat0.05
Horse, meat0.05
Horse, meat byproducts0.2
Milk0.05
Sheep, fat0.05
Sheep, meat0.05
Sheep, meat byproducts0.2
Sugarcane, cane1.0
Sugarcane, molasses30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

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§180.361   Pendimethalin; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on the commodities. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine] and its metabolite, 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

Commodity Parts per million
Alfalfa, forage80
Alfalfa, hay150
Alfalfa, seed0.10
Almond, hulls6.0
Apple, wet pomace0.20
Artichoke, globe0.1
Asparagus0.15
Beans0.10
Beans, forage0.10
Beans, hay0.10
Berry, low growing subgroup 13-07G0.1
Brassica head and stem, subgroup 5-A0.1
Brassica, leafy greens, subgroup 5B0.20
Bushberry subgroup 13-07B0.10
Caneberry subgroup 13-07A0.10
Carrot0.5
Citrus, oil0.5
Corn, field, forage0.1
Corn, field, grain0.1
Corn, field, stover0.1
Corn, pop, grain0.1
Corn, sweet, forage0.1
Corn, sweet, kernel plus cob with husks removed0.1
Corn, sweet, stover0.1
Cotton, gin byproducts3.0
Cotton, undelinted seed0.1
Crayfish0.05
Fruit, citrus, group 10-100.1
Fruit, pome, group 11-100.1
Fruit, small vine climbing, except grape, subgroup 13-07E0.10
Fruit, stone, group 12-120.1
Grape0.1
Grass, forage, fodder, and hay crop group 17, forage1,000
Grass, forage, fodder, and hay crop group 17, hay2,000
Hop, dried cones0.1
Leaf petiole vegetable subgroup 22B0.2
Lettuce, leaf4.0
Melon subgroup 9A0.10
Monarda, fresh leaves0.2
Monarda, oil1
Nut, tree, group 14-120.10
Olive0.1
Onion, bulb subgroup 3-07A0.1
Onion, green subgroup 3-07B0.2
Peanut0.1
Peanut, hay0.1
Peas (except field peas)0.10
Peppermint, oil1.0
Peppermint, tops0.2
Pomegranate0.10
Potato0.1
Rice, grain0.1
Rosemary, fresh leaves0.2
Rosemary, oil1
Sorghum, forage0.1
Sorghum, grain, grain0.1
Sorghum, grain, stover0.1
Soybean, forage0.1
Soybean, hay0.1
Soybean, seed0.1
Spearmint, oil1.0
Spearmint, tops0.2
Sugarcane, cane0.1
Sunflower subgroup 20B0.1
Turnip greens0.20
Vegetable, fruiting, group 8-100.1
Vegetable, soybean, succulent0.10
Wheat, grain0.10
Wheat, forage3.0
Wheat, hay0.60
Wheat, straw0.30

(2) Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on commodities listed in the following table. Compliance with the tolerance levels is to be determined by measuring only the sum of pendimethalin (N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine)) and its metabolite, 1-(1-ethylpropyl)-5, 6-dimethyl-7-nitro-1H-benzimidazole (metabolite 6), calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

CommodityParts
per
million
Cattle, fat0.30
Cattle, meat0.10
Cattle, meat byproduct3.0
Goats, fat0.30
Goats, meat0.10
Goats, meat byproduct3.0
Horse, fat0.30
Horse, meat0.10
Horse, byproduct3.0
Milk0.04
Sheep, fat0.30
Sheep, meat0.10
Sheep, meat byproduct3.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for combined residues of the herbicide pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the table.

CommodityParts per millionExpiration/revocation date
Bermuda grass, forage2512/31/10
Bermuda grass, hay6012/31/10

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 15293, Apr. 18, 1984]

Editorial Note: For Federal Register citations affecting §180.361, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.362   Fenbutatin-oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

CommodityParts per million
Almond, hulls80.0
Apple15.0
Apple, wet pomace100.0
Cherry, sweet6.0
Cherry, tart6.0
Citrus, dried pulp100.0
Citrus, oil140.0
Cucumber4.0
Eggplant6.0
Fruit, citrus, group 1020.0
Grape5.0
Grape, raisin20.0
Nut, tree, group 140.5
Papaya2.0
Peach10.0
Pear15.0
Pistachio0.5
Plum, prune, fresh4.0
Plum, prune, dried20.0
Strawberry10.0

(2) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the animal commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, and its organotin metabolites, dihydroxybis(2-methyl-2-phenylpropyl) stannane and 2-methyl-2-phenylpropylstannoic acid, calculated as the stoichiometric equivalent of fenbutatin-oxide, in or on the commodity.

CommodityParts per million
Cattle, fat0.5
Cattle, meat0.5
Cattle, meat byproducts0.5
Egg0.1
Goat, fat0.5
Goat, meat0.5
Goat, meat byproducts0.5
Hog, fat0.5
Hog, meat0.5
Hog, meat byproducts0.5
Horse, fat0.5
Horse, meat0.5
Horse, meat byproducts0.5
Milk, fat0.1
Poultry, fat0.1
Poultry, meat0.1
Poultry, meat byproducts0.1
Sheep, fat0.5
Sheep, meat0.5
Sheep, meat byproducts0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity Parts per million
Raspberry10.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011]

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§180.364   Glyphosate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine).

CommodityParts per million
Acerola0.2
Alfalfa, seed0.5
Almond, hulls25
Aloe vera0.5
Ambarella0.2
Animal feed, nongrass, group 18400
Artichoke, globe0.2
Asparagus0.5
Atemoya0.2
Avocado0.2
Bamboo, shoots0.2
Banana0.2
Barley, bran30
Beet, sugar, dried pulp25
Beet, sugar, roots10
Beet, sugar, tops10
Berry and small fruit, group 13-070.20
Betelnut1.0
Biriba0.2
Blimbe0.2
Breadfruit0.2
Cacao bean, bean0.2
Cactus, fruit0.5
Cactus, pads0.5
Canistel0.2
Carrot5.0
Chaya1.0
Cherimoya0.2
Citrus, dried pulp1.5
Coconut0.1
Coffee, bean, green1.0
Corn, pop, grain0.1
Corn, sweet, kernel plus cob with husk removed3.5
Cotton, gin byproducts210
Custard apple0.2
Date, dried fruit0.2
Dokudami2.0
Durian0.2
Epazote1.3
Feijoa0.2
Fig0.2
Fish0.25
Fruit, citrus, group 10-100.50
Fruit, pome, group 11-100.20
Fruit, stone, group 120.2
Galangal, roots0.2
Ginger, white, flower0.2
Gourd, buffalo, seed0.1
Governor's plum0.2
Gow kee, leaves0.2
Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover100
Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice30
Grass, forage, fodder and hay, group 17300
Guava0.2
Herbs subgroup 19A0.2
Hop, dried cones7.0
Ilama0.2
Imbe0.2
Imbu0.2
Jaboticaba0.2
Jackfruit0.2
Kava, roots0.2
Kenaf, forage200
Leucaena, forage200
Longan0.2
Lychee0.2
Mamey apple0.2
Mango0.2
Mangosteen0.2
Marmaladebox0.2
Mioga, flower0.2
Noni0.20
Nut, pine1.0
Nut, tree, group 141.0
Oilseeds, group 20, except canola40
Okra0.5
Olive0.2
Oregano, Mexican, leaves2.0
Palm heart0.2
Palm heart, leaves0.2
Palm, oil0.1
Papaya0.2
Papaya, mountain0.2
Passionfruit0.2
Pawpaw0.2
Pea, dry8.0
Peanut0.1
Peanut, hay0.5
Pepper leaf, fresh leaves0.2
Peppermint, tops200
Perilla, tops1.8
Persimmon0.2
Pineapple0.1
Pistachio1.0
Pomegranate0.2
Pulasan0.2
Quinoa, grain5.0
Rambutan0.2
Rice, grain0.1
Rice, wild, grain0.1
Rose apple0.2
Sapodilla0.2
Sapote, black0.2
Sapote, mamey0.2
Sapote, white0.2
Shellfish3.0
Soursop0.2
Spanish lime0.2
Spearmint, tops200
Spice subgroup 19B7.0
Star apple0.2
Starfruit0.2
Stevia, dried leaves1.0
Sugar apple0.2
Sugarcane, cane2.0
Sugarcane, molasses30
Surinam cherry0.2
Sweet potato3.0
Tamarind0.2
Tea, dried1.0
Tea, instant7.0
Teff, forage100
Teff, grain5.0
Teff, hay100
Ti, leaves0.2
Ti, roots0.2
Ugli fruit0.5
Vegetable, bulb, group 3-070.20
Vegetable, cucurbit, group 90.5
Vegetable, foliage of legume, subgroup 7A, except soybean0.2
Vegetable, fruiting, group 8-10 (except okra)0.10
Vegetable, leafy, brassica, group 50.2
Vegetable, leafy, except brassica, group 40.2
Vegetable, leaves of root and tuber, group 2, except sugar beet tops0.2
Vegetable, legume, group 6 except soybean and dry pea5.0
Vegetables, root and tuber, group 1, except carrot, sweet potato, and sugar beet0.20
Wasabi, roots0.2
Water spinach, tops0.2
Watercress, upland0.2
Wax jambu0.2
Yacon, tuber0.2

(2) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine) and its metabolite N-acetyl-glyphosate (N-acetyl-N-(phosphonomethyl)glycine; calculated as the stoichiometric equivalent of glyphosate).

CommodityParts per Million
Canola, seed20
Cattle, meat byproducts5.0
Corn, field, forage13
Corn, field, grain5.0
Corn, field, stover100
Egg0.05
Goat, meat byproducts5.0
Grain aspirated fractions310.0
Hog, meat byproducts5.0
Horse, meat byproducts5.0
Poultry, meat0.10
Poultry, meat byproducts1.0
Sheep, meat byproducts5.0
Soybean, forage100.0
Soybean, hay200.0
Soybean, hulls120.0
Soybean, seed20.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 64911, Oct. 1, 1980]

Editorial Note: For Federal Register citations affecting §180.364, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.367   n-Octyl bicycloheptenedicarboximide; tolerances for residues.

(a) General. A tolerance of 5 parts per million is established for residues of the insecticide synergist N-octyl bicycloheptene dicarboximide, including its metabolites and degradates, in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served, provided that the food is removed or covered prior to such use, except for bagged food in warehouse storage which need not be removed or covered prior to applications of formulations containing N-octyl bicycloheptene dicarboximide. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only N-octyl bicycloheptene dicarboximide, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 75 FR 60243, Sept. 29, 2010]

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§180.368   Metolachlor; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2- ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

CommodityParts per million
Almond, hulls0.30
Animal feed, nongrass, group 181.0
Cattle, fat0.02
Cattle, kidney0.20
Cattle, liver0.05
Cattle, meat0.02
Cattle, meat byproducts, except kidney and liver0.04
Corn, field, forage6.0
Corn, field, grain0.10
Corn, field, stover6.0
Corn, pop, grain0.10
Corn, pop, stover6.0
Corn, sweet, forage6.0
Corn, sweet, kernel plus cob with husks removed0.10
Corn, sweet, stover6.0
Cotton, gin byproducts4.0
Cotton, undelinted seed0.10
Dillweed0.50
Egg0.02
Goat, fat0.02
Goat, kidney0.20
Goat, liver0.05
Goat, meat0.02
Goat, meat byproducts, except kidney and liver0.04
Grass, forage10
Grass, hay0.20
Horse, fat0.02
Horse, kidney0.20
Horse, liver0.05
Horse, meat0.02
Horse, meat byproducts, except kidney and liver0.04
Milk0.02
Nut, tree, group 140.10
Okra0.50
Peanut0.20
Peanut, hay20
Peanut, meal0.40
Potato0.20
Poultry, fat0.02
Poultry, meat0.02
Poultry, meat byproducts0.05
Safflower, seed0.10
Sheep, fat0.02
Sheep, kidney0.20
Sheep, liver0.05
Sheep, meat0.02
Sheep, meat byproducts, except kidney and liver0.04
Sorghum, grain, forage1.0
Sorghum, grain, grain0.30
Sorghum, grain, stover4.0
Soybean, forage5.0
Soybean, hay8.0
Soybean, seed0.20
Tomato0.10
Vegetable, foliage of legume, subgroup 7A, except soybean15.0
Vegetable, legume, group 60.30

(2) Tolerances are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodity(s), as defined. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Table 2 to Paragraph (a)(2)

CommodityParts per
million
Beet, sugar, molasses2.0
Beet, sugar, roots0.5
Beet, sugar, tops15.0
Brassica, leafy greens, subgroup 4-16B1.8
Bushberry subgroup 13-07B0.15
Caneberry subgroup 13-07A0.10
Carrot, roots0.40
Cattle, fat0.02
Cattle, kidney0.20
Cattle, liver0.05
Cattle, meat0.02
Cattle, meat byproducts, except kidney and liver0.04
Cilantro, leaves8.0
Coriander, seed0.13
Corn, field, forage40
Corn, field, grain0.10
Corn, field, stover40
Corn, pop, grain0.10
Corn, pop, stover40
Corn, sweet, forage40
Corn, sweet, kernel plus cob with husks removed0.10
Corn, sweet, stover40
Cotton, gin byproducts4.0
Cottonseed subgroup 20C0.10
Dill, seed15
Dillweed5
Dillweed, dried leaves9
Egg0.02
Goat, fat0.02
Goat, kidney0.20
Goat, liver0.05
Goat, meat0.02
Goat, meat byproducts, except kidney and liver0.04
Grain, aspirated fractions4
Grass, forage10.0
Grass, hay0.20
Horse, fat0.02
Horse, kidney0.20
Horse, liver0.05
Horse, meat0.02
Horse, meat byproducts, except kidney and liver0.04
Kohlrabi0.60
Leaf petiole vegetable subgroup 22B0.10
Lettuce1.5
Low growing berry subgroup 13-07G, except cranberry0.40
Milk0.02
Onion, bulb, subgroup 3-07A0.10
Onion, green, subgroup 3-07B2.0
Peanut0.20
Peanut, hay20.0
Peanut, meal0.40
Poultry, fat0.02
Poultry, meat0.02
Poultry, meat byproducts0.05
Rosemary, dried leaves2
Rosemary, fresh leaves1.5
Safflower, seed0.10
Sesame, seed0.13
Sheep, fat0.02
Sheep, kidney0.20
Sheep, liver0.05
Sheep, meat0.02
Sheep, meat byproducts, except kidney and liver0.04
Sorghum, grain, forage1.0
Sorghum, grain, grain0.3
Sorghum, grain, stover4.0
Sorghum, sweet, stalk4.0
Soybean, forage5.0
Soybean, hay8.0
Soybean, meal1.5
Soybean, seed0.9
Spinach0.50
Stalk and stem vegetable subgroup 22A, except kohlrabi0.10
Stevia, dried leaves15
Sugarcane, cane0.20
Sugarcane, molasses1.5
Sunflower, meal1.0
Sunflower subgroup 20B1.0
Swiss chard0.15
Tomato, paste0.30
Vegetable, Brassica, head and stem, group 5-160.60
Vegetable, cucurbit group 90.50
Vegetable, foliage of legume, except soybean, subgroup 7A15.0
Vegetable, fruiting, group 8-10, except tabasco pepper0.10
Vegetable, leaves of root and tuber, group 2, except sugar beet2.0
Vegetable, legume, group 60.30
Vegetable, root, except sugar beet, subgroup 1B, except carrot0.30
Vegetable, tuberous and corm, subgroup 1C0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. (1) Tolerances with regional registration as defined in 180.1(l) are established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound, in or on the following raw agricultural commodities:

CommodityParts per million
Pepper, nonbell0.50

(2) Tolerances with regional registration are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

CommodityParts per million
Pepper, tabasco0.50

(d) Indirect or inadvertent residues. (1) Tolerances are established for the indirect or inadvertent combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2-ethyl-6- methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

CommodityParts per million
Animal feed, nongrass, group 181.0
Barley, grain0.10
Barley, hay0.80
Barley, straw0.80
Buckwheat, grain0.10
Millet, forage0.50
Millet, grain0.10
Millet, hay0.80
Millet, straw0.80
Oat, forage0.50
Oat, grain0.10
Oat, hay0.80
Oat, straw0.80
Rice, grain0.10
Rye, forage0.50
Rye, grain0.10
Rye, straw0.80
Wheat, forage0.50
Wheat, grain0.10
Wheat, hay0.80
Wheat, straw0.80

(2) Tolerances for are established for the indirect or inadvertent residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

CommodityParts per million
Animal feed, nongrass, group 181.0
Barley, grain0.10
Barley, hay0.50
Barley, straw0.50
Buckwheat, grain0.10
Millet, forage0.50
Millet, grain0.10
Millet, hay0.50
Millet, straw0.50
Oat, forage0.50
Oat, grain0.10
Oat, hay0.50
Oat, straw0.50
Rice, grain0.10
Rye, forage0.50
Rye, grain0.10
Rye, straw0.50
Wheat, forage0.50
Wheat, grain0.10
Wheat, hay0.50
Wheat, straw0.50

[73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015; 83 FR 12274, Mar. 21, 2018; 84 FR 8617, Mar. 11, 2019; 85 FR 40131, July 6, 2020]

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§180.370   5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole and its monoacid metabolite 3-carboxy-5-ethoxy-1,2,4-thiadiazole in or on the following raw agricultural commodities:

CommodityParts per
million
Cotton, gin byproducts0.1
Cotton, undelinted seed0.1
Tomato0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016]

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§180.371   Thiophanate-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

CommodityParts per million
Almond0.1
Almond, hulls0.5
Apple2.0
Apricot15.0
Banana2.0
Bean, dry, seed0.2
Bean, snap, succulent2.0
Beet, sugar, roots0.2
Cherry, sweet20.0
Cherry, tart20.0
Grain, aspirated fractions12
Grape5.0
Onion, bulb0.5
Onion, green3.0
Peach3.0
Peanut0.1
Peanut, hay5.0
Pear3.0
Pecan0.1
Pistachio0.1
Plum0.5
Potato0.1
Soybean, hulls1.5
Soybean, seed0.2
Strawberry7.0
Vegetable, cucurbit, group 91.0
Wheat, forage1.1
Wheat, grain0.1
Wheat, hay0.1
Wheat, straw0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis(iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

CommodityParts per million
Canola, seed0.1

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60244, Sept. 29, 2010]

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§180.372   2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.

(a) General. A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in or on the following food commodity:

Commodity Parts per million
Banana11.0

1There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008]

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§180.373   [Reserved]

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§180.377   Diflubenzuron; tolerances for residues.

(a) General. (1) Tolerances are established for residues of diflubenzuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

Commodity Parts per million
Artichoke, globe6.0
Cattle, fat0.05
Cattle, meat0.05
Cottonseed subgroup 20C0.20
Egg0.07
Goat, fat0.05
Goat, meat0.05
Hog, fat0.05
Hog, meat0.05
Horse, fat0.05
Horse, meat0.05
Milk0.05
Mushroom0.2
Poultry, fat0.10
Poultry, meat byproducts0.08
Poultry, meat0.05
Sheep, fat0.05
Sheep, meat0.05
Soybean0.05
Soybean, hulls0.5

(2) Tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

CommodityParts per million
Almond, hulls6.0
Barley, grain0.06
Barley, hay3.0
Barley, straw1.8
Brassica, leafy greens, subgroup 5B9.0
Carrot, roots0.20
Cattle, meat byproducts0.15
Citrus, oil32
Fruit, citrus, group 10-103.0
Goat, meat byproducts0.15
Grain, aspirated fractions11
Grass, forage, fodder, and hay, group 176.0
Hog, meat byproducts0.15
Horse, meat byproducts0.15
Oat, forage7.0
Oat, grain0.06
Oat, hay6.0
Oat, straw3.5
Peanut0.10
Peanut, hay55
Peanut, refined oil0.20
Peach subgroup 12-12B0.50
Pear0.50
Pepper/Eggplant subgroup 8-10B1.0
Plum Subgroup 12-12C0.50
Nut, tree, group 14-120.20
Rice, grain0.02
Sheep, meat byproducts0.15
Turnip greens9.0
Wheat, forage7.0
Wheat, grain0.06
Wheat, hay6.0
Wheat, straw3.5

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6- difluorobenzamide) and its metabolites, in connection with use of the pesticide under section 18 emergency exemptions granted by EPA. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity. The tolerances are specified in the following table, and will expire and are revoked on the dates specified.

CommodityParts per millionExpiration/revocation date
Alfalfa, forage6.012/31/17
Alfalfa, hay6.012/31/17
Lemon0.812/31/10

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

CommodityParts per million
Alfalfa, forage6.0
Alfalfa, hay20
Alfalfa, seed0.90

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33699, May 24, 2000]

Editorial Note: For Federal Register citations affecting §180.377, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.378   Permethrin; tolerances for residues.

(a) General. Tolerances are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

CommodityParts per million
Alfalfa, forage20
Alfalfa, hay45
Almond0.05
Almond, hulls20
Artichoke, globe5.0
Asparagus2.0
Avocado1.0
Broccoli2.0
Brussels sprouts1.0
Cabbage6.0
Cattle, fat1.5
Cattle, meat0.10
Cattle, meat byproducts0.10
Cauliflower0.5
Celtuce5
Cherry subgroup 12-12A4
Corn, field, forage50
Corn, field, grain0.05
Corn, field, stover30
Corn, pop, grain0.05
Corn, pop, stover30
Corn, sweet, forage50
Corn, sweet, kernel plus cob with husks removed0.10
Corn, sweet, stover30
Egg0.10
Eggplant0.50
Fennel, Florence, fresh leaves and stalks5
Fruit, pome, group 110.05
Garlic, bulb0.10
Grain, aspirated fractions0.50
Goat, fat1.5
Goat, meat0.10
Goat, meat byproducts0.10
Hazelnut0.05
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat1.5
Horse, meat0.10
Horse, meat byproducts0.10
Horseradish0.50
Kiwifruit2.0
Leaf petiole vegetable subgroup 22B5
Leafy greens subgroup 4A20
Lettuce, head20
Milk, fat (reflecting 0.88 ppm in whole milk)3.0
Mushroom5.0
Onion, bulb0.10
Peach subgroup 12-12B2
Pepper, bell0.50
Pistachio0.10
Poultry, fat0.15
Poultry, meat0.05
Poultry, meat byproducts0.05
Sheep, fat1.5
Sheep, meat0.10
Sheep, meat byproducts0.10
Soybean, seed0.05
Spinach20
Swiss chard5
Tea, plucked leaves120
Tomato2.0
Vegetable, cucurbit, group 91.5
Vegetable, tuberous and corm, subgroup 1C0.05
Walnut0.05
Watercress5.0

1There are no United States registrations for use of permethrin on tea, plucked leaves as of July 28, 2020.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

CommodityParts per million
Collards15
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F2
Grass, forage15
Grass, hay15
Papaya1.0
Turnip, tops10
Turnip, roots0.20

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52019, Sept. 12, 2007, as amended at 85 FR 45335, July 28, 2020]

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§180.380   Vinclozolin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5-dichloroaniline moiety in or on the food commodities in the table below. There are no U.S. registrations for grape (wine) as of July 30, 1997.

CommodityParts per millionExpiration/Revocation Date
Bean, succulent2.011/30/05
Canola, seed1.011/30/08
Cattle, fat0.0511/30/08
Cattle, meat0.0511/30/08
Cattle, meat byproducts0.0511/30/08
Egg0.0511/30/08
Goat, fat0.0511/30/08
Goat, meat0.0511/30/08
Goat, meat byproducts0.0511/30/08
Grape, wine6. 0None
Hog, fat0.0511/30/08
Hog, meat0.0511/30/08
Hog, meat byproducts0.0511/30/08
Horse, fat0.0511/30/08
Horse, meat0.0511/30/08
Horse, meat byproducts0.0511/30/08
Lettuce, head10.011/30/05
Lettuce, leaf10.011/30/05
Milk0.0511/30/08
Poultry, fat0.111/30/08
Poultry, meat0.111/30/08
Poultry, meat byproducts0.111/30/08
Sheep, fat0.0511/30/08
Sheep, meat0.0511/30/08
Sheep, meat byproducts0.0511/30/08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities with residues of vinclozolin resulting from lawful use are subject to the channels of trade provisions of section 408(l)(5) of the FFDCA:

Commodity Parts per million
Cucumber1.0
Fruit, stone, except plum, prune, fresh25.0
Pepper, bell3.0
Strawberry10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005]

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§180.381   Oxyfluorfen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

CommodityParts per million
Almond, hulls0.1
Artichoke, globe0.05
Avocado0.05
Banana0.05
Broccoli0.05
Cabbage0.05
Cacao bean, dried bean0.05
Cattle, fat0.01
Cattle, meat0.01
Cattle, meat byproducts0.01
Cauliflower0.05
Coffee, bean, green0.05
Corn, field, grain0.05
Cotton, undelinted seed0.05
Date, dried fruit0.05
Egg0.03
Feijoa0.05
Fig0.05
Fruit, pome, group 110.05
Fruit, stone, group 120.05
Goat, fat0.01
Goat, meat0.01
Goat, meat byproducts0.01
Grape0.05
Hog, fat0.01
Hog, meat0.01
Hog, meat byproducts0.01
Horse, fat0.01
Horse, meat0.01
Horse, meat byproducts0.01
Horseradish0.05
Kiwifruit0.05
Milk0.01
Nut, tree, group 140.05
Olive0.05
Onion, bulb0.05
Peppermint, tops0.05
Persimmon0.05
Pistachio0.05
Pomegranate0.05
Poultry, fat0.2
Poultry, meat0.01
Poultry, meat byproducts0.01
Sheep, fat0.01
Sheep, meat0.01
Sheep, meat byproducts0.01
Soybean0.05
Spearmint, tops0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

CommodityParts per million
Blackberry0.05
Chickpea, seed0.05
Grass, forage0.05
Grass, hay0.05
Grass, seed screenings0.05
Guava0.05
Papaya0.05
Raspberry0.05
Taro, corm0.05
Taro, leaves0.05

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 85022, Dec. 24, 1980]

Editorial Note: For Federal Register citations affecting §180.381, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.383   Sodium salt of acifluorfen; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen, sodium 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding acid, methyl ester, and amino analogues) in or on the following raw agricultural commodities:

CommodityParts per million
Peanut0.1
Rice, grain0.1
Soybean, seed0.1
Strawberry0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006; 80 FR 72598, Nov. 20, 2015]

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§180.384   Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator mepiquat, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only mepiquat, N,N-dimethylpiperidinium, in or on the commodity.

CommodityParts
per million
Cattle, meat byproducts0.1
Cotton, gin byproducts6.0
Cotton, undelinted seed2.0
Goat, meat byproducts0.1
Grape1.0
Grape, raisin5.0
Hog, meat byproducts0.1
Horse, meat byproducts0.1
Sheep, meat byproducts0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 3118, Jan. 23, 2002, as amended at 80 FR 72598, Nov. 20, 2015]

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§180.385   Diclofop-methyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoic acid and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agricultural commodities:

CommodityParts per million
Barley, grain0.1
Barley, straw0.1
Wheat, grain0.1
Wheat, straw0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

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§§180.388-180.389   [Reserved]

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§180.390   Tebuthiuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

CommodityParts per million
Grass, forage10.0
Grass, hay10.0

(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino-1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

CommodityParts per million
Cattle, fat1.0
Cattle, meat1.0
Cattle, meat byproducts5.0
Goat, fat1.0
Goat, meat1.0
Goat, meat byproducts5.0
Horse, fat1.0
Horse, meat1.0
Horse, meat byproducts5.0
Sheep, fat1.0
Sheep, meat1.0
Sheep, meat byproducts5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

CommodityParts per million
Milk0.8

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 53461, Sept. 19, 2007]

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§180.395   Hydramethylnon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)hydrazone in or on the following raw agricultural commodities:

CommodityParts per million
Grass, forage2.0
Grass, hay2.0
Pineapple0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug. 1, 2007]

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§180.396   Hexazinone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant metabolites: metabolite A, 3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite D, 3-cyclohexyl-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

CommodityParts per million
Alfalfa, forage2.0
Alfalfa, hay4.0
Alfalfa, seed2.0
Blueberry0.6
Grass, forage250
Grass, hay230
Pineapple0.6
Sugarcane, cane0.6
Sugarcane, molasses4.0

(2) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its animal tissue metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

CommodityParts per million
Cattle, fat0.1
Cattle, meat0.5
Cattle, meat byproducts4.0
Goat, fat0.1
Goat, meat0.5
Goat, meat byproducts4.0
Hog, fat0.1
Hog, meat0.5
Hog, meat byproducts4.0
Horse, fat0.1
Horse, meat0.5
Horse, meat byproducts4.0
Sheep, fat0.1
Sheep, meat0.5
Sheep, meat byproducts4.0

(3) A tolerance is established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C-2, 3-(3-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

CommodityParts per million
Milk11

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, 2010]

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§180.399   Iprodione; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide in or on the following food commodities:

CommodityParts per million
Almond, hulls2.0
Almond0.3
Apricot20.0
Bean, dry, seed2.0
Bean, forage90.0
Bean, succulent2.0
Blueberry15.0
Boysenberry15.0
Broccoli25.0
Caneberry subgroup 13A25.0
Carrot, roots5.0
Cherry, sweet, postharvest20.0
Cherry, tart20.0
Cotton, undelinted seed0.10
Cowpea, hay90.0
Currant15.0
Garlic0.1
Ginseng2.0
Ginseng, dried root4.0
Grape60.0
Grape, raisin300
Kiwifruit10.0
Lettuce25.0
Nectarine, postharvest20.0
Onion, bulb0.5
Peach, postharvest20.0
Peanut0.5
Peanut, hay150.0
Plum, postharvest20.0
Plum, prune20.0
Potato0.5
Raspberry15.0
Rice, bran30.0
Rice, grain10.0
Rice, hulls50.0
Strawberry15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide] and [N-(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as iprodione equivalents in or on the following food commodities of animal origin:

CommodityParts per million
Cattle, fat0.5
Cattle, kidney3.0
Cattle, liver3.0
Cattle, meat0.5
Cattle, meat byproducts, except kidney and liver0.5
Egg1.5
Goat, fat0.5
Goat, kidney3.0
Goat, liver3.0
Goat, meat0.5
Goat, meat byproducts, except kidney and liver0.5
Hog, fat0.5
Hog, kidney3.0
Hog, liver3.0
Hog, meat0.5
Hog, meat byproducts, except kidney and liver0.5
Horse, fat0.5
Horse, kidney3.0
Horse, liver3.0
Horse, meat0.5
Horse, meat byproducts, except kidney and liver0.5
Milk0.5
Poultry, fat3.5
Poultry, liver5.0
Poultry, meat1.0
Poultry, meat byproducts, except liver1.0
Sheep, fat0.5
Sheep, kidney3.0
Sheep, liver3.0
Sheep, meat0.5
Sheep, meat byproducts, except kidney and liver0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide], and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide] in or on the following food commodity:

CommodityParts per million
Mustard greens15.0

(d) Indirect or inadvertent residues. [Reserved]

[48 FR 40385, Sept. 7, 1983]

Editorial Note: For Federal Register citations affecting §180.399, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

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§180.401   Thiobencarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide thiobencarb (S-[(4-chlorophenyl)methyl]diethyl-carbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

CommodityPart per million
Cattle, fat0.2
Cattle, meat byproducts0.2
Cattle, meat0.2
Egg0.2
Goat, fat0.2
Goat, meat byproducts0.2
Goat, meat0.2
Hog, fat0.2
Hog, meat byproducts0.2
Hog, meat0.2
Horse, fat0.2
Horse, meat byproducts0.2
Horse, meat0.2
Milk0.05
Poultry, fat0.2
Poultry, meat byproducts0.2
Poultry, meat0.2
Rice, grain0.2
Sheep, fat0.2
Sheep, meat byproducts0.2
Sheep, meat0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide thiobencarb (S-[(4-chloro-phenyl)methyl]diethylcarbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

CommodityParts per million
Celery0.2
Endive0.2
Lettuce0.2

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015]

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§180.403   Thidiazuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenyl-N-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities:

CommodityParts per million
Cattle, fat0.4
Cattle, meat0.4
Cattle, meat byproducts0.4
Cotton, gin byproducts24.0
Cotton, undelinted seed0.3
Goat, fat0.4
Goat, meat0.4
Goat, meat byproducts0.4
Hog, fat0.4
Hog, meat0.4
Hog, meat byproducts0.4
Horse, fat0.4
Horse, meat0.4
Horse, meat byproducts0.4
Milk0.05
Sheep, fat0.4
Sheep, meat0.4
Sheep, meat byproducts0.4

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

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§180.404   Profenofos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2-chlorophenyl)-O-ethyl-S-propyl phosphorothioate) in or on the following food commodities:

CommodityParts per million
Cattle, fat0.05
Cattle, meat0.05
Cattle, meat byproducts0.05
Cotton, gin byproducts55.0
Cotton, undelinted seed2.0
Goat, fat0.05
Goat, meat0.05
Goat, meat byproducts0.05
Horse, fat0.05
Horse, meat0.05
Horse, meat byproducts0.05
Milk0.01
Sheep, fat0.05
Sheep, meat0.05
Sheep, meat byproducts0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007]

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§180.405   Chlorsulfuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5-hydroxy-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the following raw agricultural commodities:

Commodity Parts per million
Barley, grain0.1
Barley, straw0.5
Oat, forage20.0
Oat, grain0.1
Oat, straw0.5
Wheat, forage20.0
Wheat, grain0.1
Wheat, straw0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2- yl)aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities.

Commodity Parts per million
Cattle, fat0.3
Cattle, meat0.3
Cattle, meat byproducts0.3
Goat, fat0.3
Goat, meat0.3
Goat, meat byproducts0.3
Grass, forage11.0
Grass, hay19.0
Hog, fat0.3
Hog, meat0.3
Hog, meat byproducts0.3
Horse, fat0.3
Horse, meat0.3
Horse, meat byproducts0.3
Milk0.1
Sheep, fat0.3
Sheep, meat0.3
Sheep, meat byproducts0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 52873, Aug. 14, 2002]

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§180.407   Thiodicarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl N,N′-[thiobis[[(methylimino)carbonyloxy]]      bis[ethanimidothioate]) and its metabolite methomyl (S-methyl N-[(methylcarbamoyl)      oxy]thioacetimidate) in or on the following food commodities or groups. The time-limited tolerances expire and are revoked on the dates listed in the following table:

CommodityParts per millionExpiration/revocation date
Broccoli7.0None
Cabbage7.0None
Cauliflower7.0None
Corn, sweet, kernel plus cob with husks removed2.0None
Cotton, undelinted seed0.4None
Soybean, hulls0.8None
Soybean0.2None
Vegetable, leafy, except brassica, group 435None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 44595, Aug. 22, 1997, as amended at 75 FR 60245, Sept. 29, 2010]

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§180.408   Metalaxyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [N-(2,6-dmethylphyenyl)-N-(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methylphenyl)-N-(methoxyacetyl)-alanine methyl ester, each expressed as metalaxyl equivalents, in or on the following food commodities:

Commodity Parts per million
Alfalfa, forage6.0
Alfalfa, hay20.0
Almond0.5
Almond, hulls10.0
Apple0.2
Apple, wet pomace0.4
Apricot, dried4.0
Asparagus7.0
Avocado4.0
Beet, garden, roots0.1
Beet, garden, tops0.1
Beet, sugar0.1
Beet, sugar, molasses1.0
Beet, sugar, roots0.5
Beet, sugar, tops10.0
Blueberry2.0
Broccoli2.0
Brussels sprouts2.0
Cabbage1.0
Cattle, fat0.4
Cattle, kidney0.4
Cattle, liver0.4
Cattle, meat0.05
Cattle, meat byproducts, except kidney and liver0.05
Cauliflower1.0
Citrus, oil7.0
Citrus, dried pulp7.0
Clover, forage1.0
Clover, hay2.5
Cotton, undelinted seed0.1
Cranberry4.0
Egg0.05
Fruit, citrus1.0
Fruit, stone, group 121.0
Ginseng3.0
Goat, fat0.4
Goat, kidney0.4
Goat, liver0.4
Goat, meat0.05
Goat, meat byproducts, except kidney and liver0.05
Grain, cereal, group 15, except barley, oat and wheat0.1
Grain, crop0.1
Grape2.0
Grape, raisin6.0
Grass, forage10.0
Grass, hay25.0
Hog, fat0.4
Hog, kidney0.4
Hog, liver0.4
Hog, meat0.05
Hog, meat byproducts, except kidney and liver0.05
Hop, dried cones20
Hop, vines2.0
Horse, fat0.4
Horse, kidney0.4
Horse, liver0.4
Horse, meat0.05
Horse, meat byproducts, except kidney and liver0.05
Lettuce, head5.0
Milk0.02
Mustard greens5.0
Onion, bulb3.0
Onion, green10.0
Peanut0.2
Peanut, hay20.0
Peanut, meal1.0
Peanut, hulls2.0
Pineapple0.1
Pineapple, fodder0.1
Pineapple, forage0.1
Plum, prune, dried4.0
Potato, chips4.0
Potato, granules, flakes4.0
Potato, processed potato waste4.0
Potato, wet peel4.0
Poultry, fat0.4
Poultry, kidney0.4
Poultry, liver0.4
Poultry, meat0.05
Poultry, meat byproducts, except kidney and liver0.05
Potato0.5
Raspberry0.5
Sheep, fat0.4
Sheep, kidney0.4
Sheep, liver0.4
Sheep, meat0.05
Sheep, meat byproducts, except kidney and liver0.05
Soybean, hulls2.0
Soybean, meal2.0
Soybean, seed1.0
Spinach10.0
Strawberry10.0
Sunflower, seed0.1
Sunflower, forage0.1
Tomato, paste3.0
Tomato, puree3.0
Vegetable, brassica, leafy, group 5, except broccoli, cabbage, cauliflower, brussels sprouts, and mustard greens0.1
Vegetable, cucurbit, group 91.0
Vegetable, foilage of legume, group 78.0
Vegetable, fruiting, group 81.0
Vegetable, leafy, except brassica, group 4, except spinach5.0
Vegetable, leaves of root and tuber, group 215.0
Vegetable, legume, cannery waste5.0
Vegetable, legume, group 60.2
Vegetable, root and tuber, group 10.5
Walnut0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration (refer to §180.1(m)) are established for the combined residues of the fungicide metalaxyl [N-(2,6-dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N-(methoxyacetyl)-alanine methylester, each expressed as metalaxyl, in or on the following raw agricultural commodity:

Commodity Parts per million
Papaya0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of metalaxyl in or on the food commodities when present therein as a result of the application of metalaxyl to growing crops listed in paragraph (a) of this section and other non-food crops to read as follows:

Commodity Part per million
Barley, bran1.0
Barley, flour1.0
Barley, grain0.2
Barley, pearled barley1.0
Barley, straw2.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; stover1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; straw1.0
Oat, flour1.0
Oat, forage2.0
Oat, grain0.2
Oat, groats, rolled oats1.0
Oat, straw2.0
Wheat, bran1.0
Wheat, flour1.0
Wheat, forage2.0
Wheat, germ1.0
Wheat, grain0.2
Wheat, middlings1.0
Wheat, shorts1.0
Wheat, straw2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, 2009; 75 FR 56015, Sept. 15, 2010]

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§180.409   Pirimiphos-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2-diethylamino-6-methyl-4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural commodities:

CommodityParts per million
Cattle, fat0.02
Cattle, meat byproducts0.02
Corn, field, grain8.0
Corn, pop, grain8.0
Goat, fat0.02
Goat, meat byproducts0.02
Grain, aspirated fractions20.0
Hog, fat0.02
Hog, meat byproducts0.02
Horse, fat0.02
Horse, meat byproducts0.02
Poultry, fat0.02
Sheep, fat0.02
Sheep, meat byproducts0.02
Sorghum, grain, grain8.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Sept. 19, 2007]

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§180.410   Triadimefon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date
Pineapple2.0None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.411   Fluazifop-P-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.

CommodityParts per million
Banana0.01
Beans, dry, seed50
Beet, sugar, dried pulp1.0
Beet, sugar, molasses3.5
Beet, sugar, roots0.25
Bushberry subgroup 13-07B0.30
Caneberry subgroup 13-07A0.08
Carrot, roots2.0
Cattle, fat0.05
Cattle, meat0.05
Cattle, meat byproducts0.05
Citrus, dried pulp0.40
Citrus, juice0.06
Citrus, oil30.0
Cotton, gin byproducts1.5
Cotton, refined oil1.3
Cotton, undelinted seed1.0
Egg0.05
Endive6.0
Fruit, citrus, group 100.03
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F0.03
Fruit, stone0.05
Goat, fat0.05
Goat, meat0.05
Goat, meat byproducts0.05
Hog, fat0.05
Hog, meat0.05
Hog, meat byproducts0.05
Horse, fat0.05
Horse, meat0.05
Horse, meat byproducts0.05
Lettuce, head3.0
Lettuce, leaf5.0
Milk0.05
Nut, macadamia0.1
Onion, bulb, subgroup 3-07A0.50
Onion, green1.5
Peanut1.5
Peanut, meal2.2
Pecans0.05
Poultry, fat0.05
Poultry, meat0.05
Poultry, meat byproducts0.05
Potato11.0
Potato, chips12.0
Potato, granules/flakes14.0
Rhubarb0.50
Sheep, fat0.05
Sheep, meat0.05
Sheep, meat byproducts0.05
Soybean, seed2.5
Strawberry3.0
Vegetable, tuberous and corm, except potato, subgroup 1D1.5

1No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.

CommodityParts per million
Asparagus3.0
Coffee, bean0.1
Fescue, forage4.0
Fescue, hay15
Pepper, tabasco1.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33714, May 24, 2000, as amended at 74 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR 46822, Aug. 6, 2015; 82 FR 44942, Sept. 27, 2017]

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§180.412   Sethoxydim; tolerances for residues.

(a) Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No. 74051-80-2) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

Table 1 to Paragraph (a)

CommodityParts per
million
Alfalfa, forage40
Alfalfa, hay40
Almond, hulls2.0
Apricot0.2
Apple, wet pomace0.8
Asparagus4.0
Basil, dried leaves20
Basil, fresh leaves8
Bean, succulent15
Beet, sugar, molasses10
Beet, sugar, tops3.0
Berry, low growing, subgroup 13-07H, except strawberry2.5
Borage, meal40
Buckwheat, flour25
Buckwheat, grain19
Bushberry subgroup 13-07B4.0
Calendula, meal20
Caneberry subgroup 13-07A5.0
Canola, meal40
Castor oil plant, meal20
Cattle, fat0.2
Cattle, meat0.2
Cattle, meat byproducts1.0
Cherry, sweet0.2
Cherry, tart0.2
Chinese tallowtree, meal20
Citrus, dried pulp1.5
Clover, forage35
Clover, hay55
Coriander, leaves4.0
Corn, field, forage2.0
Corn, field, grain0.5
Corn, field, stover2.5
Corn, sweet, forage3.0
Corn, sweet, kernel plus cob with husk removed0.4
Corn, sweet, stover3.5
Cottonseed subgroup 20C5.0
Cowpea, forage15
Cowpea, hay50
Crambe, meal40
Cuphea, meal40
Dillweed, fresh leaves10
Echium, meal40
Egg2.0
Euphorbia, meal20
Evening primrose, meal20
Flax seed, meal40
Fruit, citrus, group 10-100.5
Fruit, pome, group 11-100.2
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F1.0
Goat, fat0.2
Goat, meat0.2
Goat, meat byproducts1.0
Gold of pleasure, meal40
Grape, raisin2.0
Hare's ear mustard, meal40
Hog, fat0.2
Hog, meat0.2
Hog, meat byproducts1.0
Horse, fat0.2
Horse, meat0.2
Horse, meat byproducts1.0
Jojoba, meal20
Juneberry15.0
Lesquerella, meal40
Lingonberry15.0
Lunaria, meal40
Meadowfoam, meal40
Milk0.5
Milkweed, meal40
Mustard, meal40
Nectarine0.2
Niger seed, meal20
Nut, tree, group 140.2
Oil radish, meal40
Pea and bean, dried shelled, except soybean, subgroup 6C25
Pea, field, hay40
Pea, field, vines20
Pea, succulent10
Peach0.2
Peanut25
Peppermint, tops30
Pistachio0.2
Poppy seed, meal40
Potato granules/flakes8.0
Potato waste, processed8.0
Poultry, fat0.2
Poultry, meat0.2
Poultry, meat byproducts2.0
Radish, tops4.5
Rapeseed, meal40
Rapeseed subgroup 20A35
Rose hip, meal20
Safflower, seed15
Salal15.0
Sesame, meal40
Sheep, fat0.2
Sheep, meat0.2
Sheep, meat byproducts1.0
Soybean, hay10
Soybean, seed16
Spearmint, tops30
Strawberry10
Stokes aster, meal20
Sunflower, meal20
Sunflower subgroup 20B, except safflower7.0
Sweet rocket, meal40
Tallowwood, meal20
Tea oil plant, meal20
Turnip, tops5.0
Vegetable, brassica, leafy, group 55.0
Vegetable, bulb, group 3-071.0
Vegetable, cucurbit, group 94.0
Vegetable, fruiting, group 8-104.0
Vegetable, leafy, except brassica, group 44.0
Vegetable, root and tuber, group 14.0
Vernonia, meal20

1The individual tolerances for Juneberry, Lingonberry, and Salal expire on December 15, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

CommodityParts per
million
Artichoke, globe5.0
Fescue, forage7.0
Fescue, hay4.0
Rhubarb0.3

(d) Indirect and inadvertent residues. [Reserved]

[80 FR 34077, June 15, 2015, as amended at 85 FR 78002, Dec. 3, 2020]

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§180.413   Imazalil; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1H-imidazole-1-yl)-1-ethanol, in or on the following food commodities:

CommodityParts per million
Banana3.0
Barley, grain0.1
Barley, hay0.5
Barley, straw0.5
Citrus, dried pulp25.0
Citrus, oil200.0
Fruit, citrus, postharvest10.0
Wheat, forage0.5
Wheat, grain0.1
Wheat, hay0.5
Wheat, straw0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2-(2,3-dihydroxypropoxy)ethyl]-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]-2,4-imidazolidinedione (FK284), in or on the following food commodities:

CommodityParts per million
Cattle, fat0.01
Cattle, meat0.01
Cattle, meat byproducts0.2
Goat, fat0.01
Goat, meat0.01
Goat, meat byproducts0.2
Horse, fat0.01
Horse, meat0.01
Horse, meat byproducts0.2
Milk0.02
Sheep, fat0.01
Sheep, meat0.01
Sheep, meat byproducts0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

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§180.414   Cyromazine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine.

Commodity Parts per million
Bean, dry, except cowpea3.0
Bean, lima1.0
Bean, succulent2.0
Brassica, leafy greens, subgroup 4-16B35
Broccoli1.0
Cattle, fat0.05
Cattle, kidney0.2
Cattle, meat0.05
Cattle, meat byproducts, except kidney0.05
Celtuce10
Chickpea, edible podded0.4
Chickpea, succulent shelled0.3
Dwarf pea, edible podded0.4
Edible podded pea, edible podded0.4
Egg0.25
English pea, succulent shelled0.3
Fennel, Florence, fresh leaves and stalk10
Garden pea, succulent shelled0.3
Goat, fat0.05
Goat, kidney0.2
Goat, meat0.05
Goat, meat byproducts, except kidney0.05
Grass-pea, edible podded0.4
Green pea, edible podded0.4
Green pea, succulent shelled0.3
Hog, fat0.05
Hog, kidney0.2
Hog, meat0.05
Hog, meat byproducts, except kidney0.05
Horse, fat0.05
Horse, kidney0.2
Horse, meat0.05
Horse, meat byproducts, except kidney0.05
Kohlrabi35
Leaf petiole vegetable subgroup 22B10
Leafy greens subgroup 4-16A10
Lentil, edible podded0.4
Lentil, succulent shelled0.3
Mango10.3
Milk0.05
Mushroom1.0
Onion, bulb, subgroup 3-07A0.3
Onion, green, subgroup 3-07B3
Onion, potato23.0
Pepper/eggplant subgroup 8-10B3
Pigeon pea, edible podded0.4
Pigeon pea, succulent shelled0.3
Poultry, fat (from chicken layer hens and chicken breeder hens only)0.05
Poultry, meat (from chicken layer hens and chicken breeder hens only)0.05
Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only)0.05
Sheep, fat0.05
Sheep, kidney0.2
Sheep, meat0.05
Sheep, meat byproducts, except kidney0.05
Snap pea, edible podded0.4
Snow pea, edible podded0.4
Sugar snap pea, edible podded0.4
Tomato subgroup 8-10A1
Vegetable, brassica, head and stem, group 5-16, except broccoli35
Vegetable, cucurbit, group 91.0
Vegetable, tuberous and corm, subgroup 1C0.8

1There are no U.S. registrations on mango as of May 4, 2000.

2This tolerance expires on April 7, 2020.

(2) A tolerance of 5.0 parts per million is established for residues of the insecticide cyromazine, including its metabolites and degradates, in or on poultry feed when used as a feed additive only in feed for chicken layer hens and chicken breeder hens at the rate of not more than 0.01 pound of cyromazine per ton of poultry feed for control of flies in manure of treated chicken layer hens and chicken breeder hens, provided the feeding of cyromazine-treated feed must stop at least 3 days (72 hours) before slaughter. If the feed is formulated by any person other than the end user, the formulator must inform the end user, in writing, of the 3-day (72 hours) pre-slaughter interval. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph when present therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of this section. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

Commodity Parts per million
Cotton, undelinted seed0.1
Corn, sweet, kernel plus cob with husks removed0.5
Corn, sweet, forage0.5
Corn, sweet, stover0.5
Radish, roots0.5
Radish, tops0.5

[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Apr. 27, 2011; 84 FR 53322, Oct. 7, 2019]

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§180.415   Aluminum tris (O-ethylphosphonate); tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

CommodityParts per million
Avocado25
Banana3.0
Bushberry subgroup 13B40
Caneberry subgroup 13A0.1
Cranberry0.5
Fruit, citrus, group 10-109.0
Fruit, pome, group 1110
Ginseng0.1
Hop, dried cones45
Juneberry40
Lingonberry40
Nut, macadamia0.20
Onion, bulb0.5
Onion, green10.0
Pea, succulent0.3
Pepper/eggplant, subgroup 8-10B10.01
Pineapple0.1
Salal40
Strawberry75
Tomato3
Turnip, greens40
Turnip, roots15
Vegetable, brassica, leafy, group 560
Vegetable, cucurbit, group 915
Vegetable, leafy, except brassica, group 4100

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Commodity Parts per million
Asparagus0.1
Grape10

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015; 83 FR 12265, Mar. 21, 2018]

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§180.416   Ethalfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide ethalfluralin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the residues of ethalfluralin, N-ethyl-N-(2-methyl-2-propenyl)-2,6-dinitro-4-(trifluoromethyl)benzenamine.

CommodityParts per million
Bean, dry, seed0.05
Dill, dried leaves0.05
Dill, fresh leaves0.05
Peanut0.05
Pea, dry, seed0.05
Potato0.01
Potato10.05
Rapeseed subgroup 20A0.05
Soybean0.05
Sunflower subgroup 20B0.05
Vegetable, cucurbit, group 90.05

1This tolerance expires on January 28, 2021.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, 2013; 85 FR 45341, July 28, 2020]

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§180.417   Triclopyr; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide triclopyr, including its metabolites and degradates, in or on the commodities in the table below resulting from the application of the butoxyethyl ester of triclopyr, triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified below is to be determined by measuring only triclopyr, 2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid.

CommodityParts per million
Egg0.05
Fish3.0
Grass, forage700.0
Grass, hay200.0
Milk0.60
Poultry, fat0.1
Poultry, meat0.1