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Title 40 → Chapter I → Subchapter E → Part 180 → Subpart C

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Title 40: Protection of Environment
PART 180—TOLERANCES AND EXEMPTIONS FOR PESTICIDE CHEMICAL RESIDUES IN FOOD

Subpart C—Specific Tolerances

Editorial Note: Nomenclature changes to subpart C of part 180 appear at 67 FR 41803, June 19, 2002; 67 FR 42393, June 21, 2002; 68 FR 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 FR 60155, Oct. 10, 2008; 75 FR 56014, Sept. 15, 2010; and 76 FR 34885, June 15, 2011.

§180.101 Specific tolerances; general provisions.

(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from their application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms of parts by weight of the pesticide chemical per one million parts by weight of the raw agricultural commodity.

(b) The poisonous and deleterious substances for which tolerances are established by the regulations in this subpart C are named by their common names wherever practicable, otherwise by their chemical names.

(c) The analytical methods to be used for determining whether pesticide residues, including negligible residues, in or on raw agricultural commodities are in compliance with the tolerances established in this part 180 are identified among the methods contained or referenced in the Food and Drug Administration's “Pesticide Analytical Manual” which is available from the Food and Drug Administration, Department of Health, Education, and Welfare, 200 C Street SW., Washington, DC 20204.

§180.103 Captan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) in or on the following commodities:

Commodity	Parts per million
Almond	0.25
Almond, hulls	75.0
Animal feed, nongrass, group 18	0.05
Apple	25.0
Apricot	10.0
Blueberry	20.0
Caneberry, subgroup 13A	25.0
Cherry, sweet	50.0
Cherry, tart	50.0
Cotton, undelinted seed	0.05
Dill, seed	0.05
Flax, seed	0.05
Grape	25.0
Grain, cereal, forage, fodder and straw, group 16	0.05
Grain, cereal, group 15	0.05
Grass, forage	0.05
Grass, hay	0.05
Nectarine	25.0
Okra	0.05
Peach	15.0
Peanut	0.05
Peanut, hay	0.05
Pear	25.0
Plum, prune, fresh	10.0
Rapeseed, forage	0.05
Rapeseed, seed	0.05
Safflower, seed	0.05
Sesame, seed	0.05
Strawberry	20.0
Sunflower, seed	0.05
Vegetable, brassica leafy, group 5	0.05
Vegetable, bulb, group 3	0.05
Vegetable, cucurbit, group 9	0.05
Vegetable, foliage of legume, group 7	0.05
Vegetable, fruiting, group 8	0.05
Vegetable, leafy, except brassica, group 4	0.05
Vegetable, leaves of root and tuber, group 2	0.05
Vegetable, legume, group 6	0.05
Vegetable, root and tuber, group 1	0.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4-cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at THPI, in or on the following commodities:

Commodity	Parts per million
Cattle, fat	0.15
Cattle, meat	0.20
Cattle, meat byproducts	0.30
Goat, fat	0.15
Goat, meat	0.20
Goat, meat byproducts	0.30
Hog, fat	0.15
Hog, meat	0.20
Hog, meat byproducts	0.30
Horse, fat	0.15
Horse, meat	0.20
Horse, meat byproducts	0.30
Milk	0.10
Sheep, fat	0.15
Sheep, meat	0.20
Sheep, meat byproducts	0.30

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52016, Sept. 12, 2007]

§180.106 Diuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food commodities, as follows:

Commodity	Parts per million
Alfalfa, forage	3.0
Alfalfa, hay	2.0
Apple	0.1
Artichoke, globe	1
Asparagus	7
Banana	0.1
Berry group 13	0.1
Cattle, fat	1
Cattle, meat	1
Cattle, meat byproducts	1
Citrus, oil	3.0
Corn, field, grain	0.1
Corn, pop, grain	0.1
Cotton, undelinted seed	0.2
Fish - freshwater finfish, farm raised	2.0
Fruit, citrus, group 10, except lemon	0.05
Goat, fat	1
Goat, meat	1
Goat, meat byproducts	1
Grain, aspirated fractions	5.0
Grape	0.05
Grass, forage, except bermudagrass	2
Grass, hay, except bermudagrass	2
Hazelnut	0.1
Hog, fat	1
Hog, meat	1
Hog, meat byproducts	1
Horse, fat	1
Horse, meat	1
Horse, meat byproducts	1
Lemon	0.5
Nut, macadamia	0.05
Olive	1
Papaya	0.5
Peach	0.1
Pear	1
Pea, field, seed	0.1
Pea, field, vines	2
Pea, field, hay	2
Pecan	0.05
Peppermint, tops	1.5
Pineapple	0.1
Pineapple, process residue	0.4
Sheep, fat	1
Sheep, meat	1
Sheep, meat byproducts	1
Sorghum, grain, forage	2
Sorghum, grain, grain	0.5
Sorghum, grain, stover	2
Spearmint, tops	1.5
Sugarcane, cane	0.2
Sugarcane, molasses	0.7
Walnut	0.05
Wheat, bran	0.7
Wheat, forage	2
Wheat, grain	0.5
Wheat, hay	2
Wheat, straw	1.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:

Commodity	Parts per million
Barley, bran	0.7
Barley, grain	0.2
Barley, hay	2
Barley, straw	1.5
Cactus	0.05
Clover, forage	0.1
Clover, hay	1.0
Oat, forage	2
Oat, grain	0.1
Oat, hay	2
Oat, straw	1.5
Trefoil, forage	0.1
Trefoil, hay	1.5
Vetch, forage	0.1
Vetch, hay	1.5

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001; 67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June 13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

§180.107 Triflumezopyrim; tolerance for residues.

(a) General. Tolerances are established for residues of the insecticide triflumezopyrim, including its metabolites and degradates, in or on the following food commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only triflumezopyrim (2,4-dioxo-1-(5-pyrimidinylmethyl)-3-[3-(trifluoromethyl)phenyl]-2H-pyrido[1,2-a] pyrimidinium inner salt) in or on the commodity.

Commodity	Parts per million
Rice, grain*	0.40
Rice, hulls*	1.0

*There are no U.S. registrations for the use of triflumezopyrim on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48005, Oct. 16, 2017]

§180.108 Acephate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity¹	Parts per million
Bean, dry, seed	3.0
Brussels sprouts	3.0
Cattle, fat	0.1
Cattle, meat	0.1
Cattle, meat byproducts	0.1
Cauliflower	2.0
Celery	10
Cotton, hulls	1.0
Cotton, meal	1.0
Cotton, undelinted seed	0.5
Cranberry	0.5
Egg	0.1
Goat, fat	0.1
Goat, meat	0.1
Goat, meat byproducts	0.1
Hog, fat	0.1
Hog, meat	0.1
Hog, meat byproducts	0.1
Horse, fat	0.1
Horse, meat	0.1
Horse, meat byproducts	0.1
Lettuce, head	10
Milk	0.1
Peanut	0.2
Pepper	4.0
Peppermint, tops	27
Poultry, fat	0.1
Poultry, meat	0.1
Poultry, meat byproducts	0.1
Sheep, fat	0.1
Sheep, meat	0.1
Sheep, meat byproducts	0.1
Spearmint, tops	27
Soybean, seed	1.0

¹Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on all food items (other than those already covered by a higher tolerance as a result of use on growing crops) in food handling establishments where food and food products are held, processed, prepared and served, including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, where application of acephate shall be limited solely to spot and/or crack and crevice treatment (a coarse, low-pressure spray shall be used to avoid atomization or splashing of the spray for spot treatments; equipment capable of delivering a pin-stream of insecticide shall be used for crack and crevice treatments). Spray concentration shall be limited to a maximum of 1.0 percent active ingredient. Contamination of food or food-contact surfaces shall be avoided. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

(3) Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, including its metabolites and degradates, in or on the commodities in the following table as a result of the application of acephate. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the commodity.

Commodity	Parts per million
Bean, dry, seed	1
Brussels sprouts	0.5
Cauliflower	0.5
Celery	1
Cranberry	0.1
Lettuce, head	1
Pepper	1
Peppermint, tops	1
Spearmint, tops	1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than methamidophos, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity¹	Parts per million
Nut, macadamia	0.05

¹Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from methamidophos application are regulated under 40 CFR 180.315.

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010; 81 FR 34905, June 1, 2016]

§180.109 Fenpicoxamid; Tolerances for residues.

(a) General. Tolerances are established for residues of fenpicoxamid including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels for fenpicoxamid is to be determined by measuring only fenpicoxamid ([[4-methoxy-2-[[[(3S,7R,8R,9S)-9-methyl-8-(2-methyl-1-oxopropoxy)-2,6-dioxo-7-(phenylmethyl)-1,5-dioxonan-3-yl]amino]carbonyl]-3-pyridinyl]oxy]methyl 2-methylpropanoate) in or on the commodity.

Commodity	Parts per million
Banana*	0.15
Wheat, grain*	0.60
Rye, grain*	0.60

*There are no U.S. registrations for use of fenpicoxamid on this commodity.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[82 FR 48000, Oct. 16, 2017]

§180.111 Malathion; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	135
Alfalfa, hay	135
Almond, hulls	50
Almond, postharvest	8
Apple	8
Apricot	8
Asparagus	8
Avocado	8
Barley, grain, postharvest	8
Bean, dry, seed	8
Bean, succulent	8
Beet, garden, roots	8
Beet, garden, tops	8
Beet, sugar, roots	1
Beet, sugar, tops	8
Blackberry	8
Blueberry	8
Boysenberry	8
Carrot, roots	8
Chayote, fruit	8
Chayote, roots	8
Cherry	8
Chestnut	1
Clover, forage	135
Clover, hay	135
Corn, field, forage	8
Corn, field, grain, postharvest	8
Corn, pop, grain, postharvest	8
Corn, sweet, forage	8
Corn, sweet, kernel plus cob with husks removed	2
Cowpea, forage	135
Cowpea, hay	135
Cranberry	8
Cucumber	8
Currant	8
Date, dried fruit	8
Dewberry	8
Eggplant	8
Fig	8
Flax, seed	0.1
Garlic, bulb	8
Gooseberry	8
Grape	8
Grapefruit	8
Guava	8
Hazelnut	1
Hop, dried cones	1
Horseradish	8
Kumquat	8
Leek	8
Lemon	8
Lentil, seed	8
Lespedeza, hay	135
Lime	8
Loganberry	8
Lupin, seed	8
Mango	8
Melon	8
Mushroom	8
Nectarine	8
Nut, macadamia	1
Oat, grain, postharvest	8
Okra	8
Onion, bulb	8
Onion, green	8
Orange	8
Papaya	1
Parsnip	8
Passionfruit	8
Pea	8
Pea, field, hay	8
Pea, field, vines	8
Peach	8
Peanut, hay	135
Peanut, postharvest	8
Pear	8
Pecan	8
Pepper	8
Peppermint, tops	8
Pineapple	8
Plum	8
Plum, prune	8
Potato	8
Pumpkin	8
Quince	8
Radish	8
Raspberry	8
Rice, grain, postharvest	8
Rice, wild	8
Rutabaga	8
Rye, grain, postharvest	8
Safflower, seed	0.2
Salsify, roots	8
Salsify, tops	8
Shallot, bulb	8
Sorghum, grain, forage	8
Sorghum, grain, grain, postharvest	8
Soybean, forage	135
Soybean, hay	135
Soybean, seed	8
Soybean, vegetable, succulent	8
Spearmint, tops	8
Squash, summer	8
Squash, winter	8
Strawberry	8
Sunflower, seed, postharvest	8
Sweet potato, roots	1
Tangerine	8
Tomato	8
Trefoil, forage	135
Trefoil, hay	135
Turnip, greens	8
Turnip, roots	8
Vegetable, brassica, leafy, group 5	8
Vegetable, leafy, except brassica, group 4	8
Vetch, hay	135
Walnut	8
Wheat, grain, postharvest	8

(2) Tolerances are established for the combined residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) and its metabolite, malaoxon (O,O-dimethyl thiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

Commodity	Parts per million
Barley, straw	50
Corn, field, stover	30.0
Cotton, undelinted seed	20.0
Grass, forage	200
Grass, hay	270
Oat, forage	4.0
Oat, straw	50
Rye, forage	4.0
Rye, straw	50
Watercress	0.2
Wheat, forage	4.0
Wheat, straw	50

(3) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate), in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	4
Cattle, meat¹	4
Cattle, meat byproducts¹	4
Egg	0.1
Goat, fat	4
Goat, meat¹	4
Goat, meat byproducts¹	4
Hog, fat	4
Hog, meat¹	4
Hog, meat byproducts¹	4
Horse, fat	4
Horse, meat¹	4
Horse, meat byproducts¹	4
Milk, fat	0.5
Poultry, fat	4
Poultry, meat¹	4
Poultry, meat byproducts¹	4
Sheep, fat	4
Sheep, meat¹	4
Sheep, meat byproducts¹	4

¹The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, poultry, or sheep.

(4) Malathion may be safely used in accordance with the following conditions:

(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot.

(ii) Treated paper trays are intended for use only in the drying of grape (raisins).

(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to grape before harvest shall not exceed 12 parts per million on processed ready-to-eat raisins.

(5) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not exceed 0.6 parts per million.

(6) Malathion may be safely used for the control of insects during the drying of grape (raisins) in compliance with paragraph (a)(4) of this section by incorporation into paper trays in amounts not exceeding 100 milligrams per square foot.

(7) Malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in accordance with the following conditions.

(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle feed, when present as the result of the application of the pesticide to bagged citrus pulp during storage. Whether or not tolerances for residues of malathion on the fresh fruit have been established under section 408 of the Act, the total residue of malathion in the citrus, dried pulp shall not exceed 50 parts per million.

(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate blocks resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle feed concentrate blocks.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980; 47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR 47455, Sept. 16, 2009; 75 FR 60238, Sept. 29, 2010]

§180.114 Ferbam; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

Commodity	Parts per million	Expiration/Revocation Date
Apple	4.0¹	None
Bean	7.0¹	10/27/07
Cabbage	7.0¹	10/27/07
Cherry	4.0¹	None
Cranberry	4.0¹	None
Fruit, citrus, group 10	4.0¹	None
Grape	4.0¹	None
Lettuce	7.0¹	10/27/07
Nectarine	4.0¹	None
Peach	4.0¹	None
Pear	4.0¹	None
Raspberry	7.0¹	10/27/07

¹Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on the following food commodities:

Commodity	Parts per million
Mango	4.0¹

¹This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

§180.116 Ziram; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate), including its metabolites and degradates, in or on the commodities in the table below as a result of the application of ziram. Compliance with the tolerance levels specified below is to be determined by measuring total dithiocarbamates, determined as CS2, evolved during acid digestion and expressed as zinc ethylenebisdithiocarbamate.

Commodity	Parts per million
Almond	¹0.10
Apple	¹7.0
Apricot	¹7.0
Blueberry	¹7.0
Cherry, sweet	¹7.0
Cherry, tart	¹7.0
Grape	7.0
Hazelnut	0.10
Huckleberry	7.0
Peach	7.0
Pear	¹7.0
Pecan	0.10
Quince	¹7.0
Strawberry	7.0
Tomato	¹7.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008; 77 FR 59123, Sept. 26, 2012; 82 FR 57860, Dec. 8, 2017]

§180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl dipropylthiocarbamate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of S-ethyl dipropylthiocarbamate, S-ethyl (2-hydroxypropyl)propylcarbamothioate, S-(2-hydroxyethyl)dipropylcarbamothioate, and S-ethyl (3-hydroxypropyl)propylcarbamothioate, calculated as the stoichiometric equivalent of S-ethyl dipropylthiocarbamate, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	0.2
Alfalfa, hay	0.6
Almond	0.08
Almond, hulls	0.08
Bean, dry, seed	0.08
Bean, succulent	0.08
Beet, garden, tops	0.5
Beet, sugar, molasses	0.4
Beet, sugar, tops	0.5
Clover, forage	0.1
Clover, hay	0.1
Corn, field, forage	0.08
Corn, field, grain	0.08
Corn, field, stover	0.08
Corn, pop, grain	0.08
Corn, pop, stover	0.08
Corn, sweet, forage	0.08
Corn, sweet, kernel plus cob with husks removed	0.08
Corn, sweet, stover	0.08
Cotton, gin byproducts	0.20
Cotton, undelinted seed	0.08
Fruit, citrus, group 10	0.1
Grass, forage	0.60
Grass, hay	0.50
Lespedeza, forage	0.1
Lespedeza, hay	0.1
Pea, succulent	0.08
Safflower, seed	0.08
Sunflower, seed	0.08
Tomato	0.08
Trefoil, forage	0.1
Trefoil, hay	0.1
Vegetable, root	0.1
Walnut	0.08

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60239, Sept. 29, 2010, as amended at 82 FR 42952, Sept. 13, 2017]

§180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on the following food commodities which have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest (with the exception of strawberry):

Commodity	Parts per million	Expiration/Revocation Date
Alfalfa, hay, postharvest	50.0	10/31/11
Almond, postharvest	200.0	None
Apple, postharvest	5.0	None
Apricot, postharvest	20.0	None
Artichoke, jerusalem, postharvest	30.0	None
Asparagus, postharvest	100.0	None
Avocado, postharvest	75.0	None
Barley, grain, postharvest	50.0	None
Bean, lima, postharvest	50.0	None
Bean, postharvest	50.0	None
Bean, snap, succulent, postharvest	50.0	None
Bean, succulent, postharvest	50.0	None
Beet, garden, roots, postharvest	30.0	None
Beet, sugar, roots, postharvest	30.0	None
Blueberry, postharvest	20.0	None
Butternut, postharvest	200.0	None
Cabbage, postharvest	50.0	None
Cacao bean, roasted bean, postharvest	50.0	None
Cantaloupe, postharvest	20.0	None
Carrot, roots, postharvest	30.0	None
Cashew, postharvest	200.0	None
Cherry, sweet, postharvest	20.0	None
Cherry, tart, postharvest	20	None
Chestnut, postharvest	200.0	None
Cippolini, bulb, postharvest	50.0	None
Citron, citrus, postharvest	30.0	None
Coconut, copra, postharvest	100.0	None
Coffee, bean, green, postharvest	75.0	None
Corn, field, grain, postharvest	50.0	None
Corn, pop, postharvest	240.0	None
Corn, sweet, kernel plus cob with husks removed, postharvest	50.0	None
Cotton, undelinted seed, postharvest	200.0	10/31/11
Cucumber, postharvest	30.0	None
Cumin, seed, postharvest	100.0	None
Eggplant, postharvest	20.0	None
Garlic, postharvest	50.0	None
Ginger, postharvest	100.0	None
Grape, postharvest	20.0	None
Grapefruit, postharvest	30.0	None
Hazelnut, postharvest	200.0	None
Horseradish, postharvest	30.0	None
Kumquat, postharvest	30.0	None
Lemon, postharvest	30.0	None
Lime, postharvest	30.0	None
Melon, honeydew, postharvest	20.0	None
Muskmelon, postharvest	20.0	None
Nectarine, postharvest	20.0	None
Nut, brazil, postharvest	200.0	None
Nut, hickory, postharvest	200.0	None
Nut, macadamia, postharvest	200.0	None
Oat, postharvest	50.0	None
Okra, postharvest	30.0	None
Onion, bulb, postharvest	20.0	None
Onion, green, postharvest	20.0	None
Orange, postharvest	30.0	None
Parsnip, roots, postharvest	30.0	None
Peach, postharvest	20.0	None
Peanut, postharvest	200.0	None
Pear, postharvest	5.0	None
Pea, blackeyed, postharvest	50.0	None
Pea, postharvest	50.0	None
Pecan, postharvest	200.0	None
Pepper, postharvest	30.0	None
Pimento, postharvest	30.0	None
Pineapple, postharvest	20.0	None
Pistachio, postharvest	200.0	None
Plum, postharvest	20.0	None
Pomegranate, postharvest	100.0	None
Potato, postharvest	75.0	None
Pumpkin, postharvest	20.0	None
Quince, postharvest	5.0	None
Radish, postharvest	30.0	None
Rice, grain, postharvest	50.0	None
Rutabaga, roots, postharvest	30.0	None
Rutabaga, tops, postharvest	30.0	None
Rye, grain, postharvest	50.0	None
Salsify, roots, postharvest	30.0	None
Sorghum, grain, grain, postharvest	50.0	None
Soybean, postharvest	200.0	None
Squash, summer, postharvest	30.0	None
Squash, winter, postharvest	20.0	None
Squash, zucchini, postharvest	20.0	None
Strawberry, postharvest	60.0	None
Sweet potato, postharvest	75.0	None
Tangerine, postharvest	30.0	None
Timothy, hay, postharvest	50.0	10/19/10
Tomato, postharvest	20.0	None
Turnip, roots, postharvest	30.0	None
Walnut, postharvest	200.0	None
Watermelon, postharvest	20.0	None
Wheat	50.0	None

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the following conditions:

(i) When inorganic bromide residues are present as a result of fumigation of the processed food with methyl bromide or from such fumigation in addition to the authorized use of methyl bromide on the source raw agricultural commodity, as provided for in this part, the total residues of inorganic bromides (calculated as Br) shall not exceed the following levels:

(A) 400 parts per million in or on egg, dried and herb, processed and spice.

(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.

(D) 125 parts per million in or on processed food other than those listed above.

(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR 172.730(a)(2), the amount shall not exceed 25 parts per million (calculated as Br).

(iii) Where tolerances are established on both the raw agricultural commodities and processed food made therefrom, the total residues of inorganic bromides in or on the processed food shall not be greater than those designated in paragraph (a)(2) of this section, unless a higher level is established elsewhere in this part.

(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:

(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.

(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley, corn, grain sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or from carryover and concentration of residues of inorganic bromides from fumigation of the grains with methyl bromide.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of inorganic bromides (calculated as Br) in or on the following food commodity grown in soil fumigated with methyl bromide.

Commodity	Parts per million
Ginger, postharvest	100

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74812, Dec. 13, 2006, as amended at 75 FR 60239, Sept. 29, 2010]

§180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been used as feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will contribute considerable residues of inorganic bromides to the meat and milk.

(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such peanut hulls as animal feed. Peanut hulls containing residues of inorganic bromides from the use of methyl bromide are unsuitable as an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.

[58 FR 65555, Dec. 15, 1993]

§180.124 Methyl bromide; tolerances for residues.

(a) General. A tolerance is established for residues of the fumigant methyl bromide, including metabolites and degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be determined by measuring only methyl bromide.

Commodity	Parts per million
Cotton, undelinted seed	150

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fumigant methyl bromide, including its metabolites and degradates, in or on the specified agricultural commodities in Table 2 to this paragraph (b). Compliance with the tolerance levels specified in Table 2 to this paragraph (b) is to be determined by measuring only methyl bromide, in or on the commodities, resulting from use of the pesticide pursuant to Federal Insecticide, Fungicide, Rodenticide Act (FIFRA) section 18 emergency exemptions. The tolerances expire and are revoked on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

Commodity	Parts per million	Expiration/ revocation date
Berry and small fruit, group 13-07	5.0	12/31/23
Cactus	3.0	12/31/23
Coconut, copra	8.0	12/31/23
Coffee, green bean	150	12/31/23
Cola, seed	150	12/31/23
Cucurbit, seed	150	12/31/23
Fig	10	12/31/23
Fruit, citrus, group 10-10	2	12/31/23
Fruit, stone, group 12-12	5.0	12/31/23
Fruit, tropical and subtropical, edible peel, group 23	10	12/31/23
Fruit, tropical and subtropical, inedible peel, group 24	5.0	12/31/23
Herb and spice, group 19	35	12/31/23
Hibiscus, seed	150	12/31/23
Ivy gourd	5.0	12/31/23
Kaffir lime, leaves	0.50	12/31/23
Kenaf, seed	150	12/31/23
Oilseed group 20	150	12/31/23
Peppermint, tops	35	12/31/23
Pointed gourd	5.0	12/31/23
Spearmint, tops	35	12/31/23
Vegetable, bulb, group 3-07	2.0	12/31/23
Vegetable, cucurbit, group 9	5.0	12/31/23
Vegetable, foliage of legume, group 7	0.50	12/31/23
Vegetable, fruiting, group 8-10	7.0	12/31/23
Vegetable, head and stem Brassica, group 5-16	1.0	12/31/23
Vegetable, leafy, group 4-16	0.50	12/31/23
Vegetable, leaves of root and tuber, group 2	0.50	12/31/23
Vegetable, legume, group 6	3.0	12/31/23
Vegetable, root and tuber, group 1	3.0	12/31/23
Vegetable, stalk, stem and leaf petiole, group 22	0.50	12/31/23

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 35298, June 13, 2012, as amended at 83 FR 8763, Mar. 1, 2018; 85 FR 65734, Oct. 16, 2020; 86 FR 8703, Feb. 9, 2021]

§180.127 Piperonyl butoxide; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl piperonyl)ether] are established in or on the following food commodities:

Commodity	Parts per million
Almond, postharvest	8
Apple, postharvest	8
Barley, postharvest	20
Bean, postharvest	8
Birdseed, mixtures, postharvest	20
Blackberry, postharvest	8
Blueberry, postharvest	8
Boysenberry, postharvest	8
Buckwheat, grain, postharvest	20
Cattle, fat	0.1
Cattle, meat	0.1
Cattle, meat byproducts	0.1
Cherry, sweet, postharvest	8
Cherry, tart, postharvest	8
Cacoa bean, roasted bean, postharvest	8
Coconut, copra, postharvest	8
Corn, field, grain, postharvest	20
Corn, pop, postharvest	20
Cotton, undelinted seed, postharvest	8
Crabapple, postharvest	8
Currant, postharvest	8
Dewberry, postharvest	8
Egg	1
Fig, postharvest	8
Flax, seed, postharvest	8
Goat, fat	0.1
Goat, meat	0.1
Goat, meat byproducts	0.1
Gooseberry, postharvest	8
Grape, postharvest	8
Guava, postharvest	8
Hog, fat	0.1
Hog, meat	0.1
Hog, meat byproducts	0.1
Horse, fat	0.1
Horse, meat	0.1
Horse, meat byproducts	0.1
Loganberry, postharvest	8
Mango, postharvest	8
Milk, fat	0.25
Muskmelon, postharvest	8
Oat, postharvest	8
Orange, postharvest	8
Peach, postharvest	8
Peanut, postharvest	8
Pea, postharvest	8
Pear, postharvest	8
Pineapple, postharvest	8
Plum, prune, fresh, postharvest	8
Potato, postharvest	0.25
Poultry, fat	3
Poultry, meat	3
Poultry, meat byproducts	3
Raspberry, postharvest	8
Rice, postharvest	20
Rye, postharvest	20
Sheep, fat	0.1
Sheep, meat	0.1
Sheep, meat byproducts	0.1
Sorghum, grain, postharvest	8
Sweet potato, postharvest	0.25
Tomato, postharvest	8
Walnut, postharvest	8
Wheat, postharvest	20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of piperonyl butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the formulation.

(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for food, dried.

(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are constructed with waxed paper liners and are to be used only for food, dried that contain 4 percent fat or less.

(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it is incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl butoxide per square foot (538 milligrams per square meter). Such treated bags are to be used only for packaging plum, prune, dried; grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12 milligrams of piperonyl butoxide per ounce of fruit (0.10 milligram of piperonyl butoxide per gram of product).

(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to such use.

(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide for insect control in accordance with 21 CFR 178.3730.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:

(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the cloth of cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(v) Where tolerances are established on both raw agricultural commodities and processed food made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams per square foot.

(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth. Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried that contain 4 percent fat or less.

(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as the result of migration:

(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. Environmental Protection Agency.

(v) Where tolerances are established on both the raw agricultural commodities and food, processed made therefrom, the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74813, Dec. 13, 2006]

§180.128 Pyrethrins; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (pyrethrin 1), (1S)-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2), (1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl-2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (jasmolin 1), and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles of Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1, and jasmolin 1 are not to exceed the following:

Commodity	Parts per million
Almond, postharvest	1.0
Apple, postharvest	1.0
Barley, grain, postharvest	3.0
Bean, succulent, postharvest	1.0
Birdseed, mixtures, postharvest	3.0
Blackberry, postharvest	1.0
Blueberry, postharvest	1.0
Boysenberry, postharvest	1.0
Buckwheat, grain, postharvest	3.0
Cacao bean, roasted bean, postharvest	1.0
Cattle, fat	1.0
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Cherry, sweet, postharvest	1.0
Cherry, tart, postharvest	1.0
Coconut, copra, postharvest	1.0
Corn, field, grain, postharvest	3.0
Corn, pop, grain, postharvest	3.0
Cotton, undelinted seed, postharvest	1.0
Crabapple, postharvest	1.0
Currant, postharvest	1.0
Dewberry, postharvest	1.0
Fig, postharvest	1.0
Flax, seed, postharvest	1.0
Goat, fat	1.0
Goat, meat	0.05
Goat, meat byproducts	0.05
Gooseberry, postharvest	1.0
Grape, postharvest	1.0
Guava, postharvest	1.0
Hog, fat	1.0
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	1.0
Horse, meat	0.05
Horse, meat byproducts	0.05
Loganberry, postharvest	1.0
Mango, postharvest	1.0
Milk, fat (reflecting negligible residues in milk)	0.05
Muskmelon, postharvest	1.0
Oat, grain, postharvest	1.0
Orange, postharvest	1.0
Pea, dry, seed, postharvest	1.0
Peach, postharvest	1.0
Peanut, postharvest	1.0
Pear, postharvest	1.0
Pineapple, postharvest	1.0
Plum, prune, fresh, postharvest	1.0
Potato, postharvest	0.05
Raspberry, postharvest	1.0
Rice, grain, postharvest	3.0
Rye, grain, postharvest	3.0
Sheep, fat	1.0
Sheep, meat	0.05
Sheep, meat byproducts	0.05
Sorghum, grain, grain, postharvest	1.0
Sweet potato, postharvest	0.05
Tomato, postharvest	1.0
Walnut, postharvest	1.0
Wheat, grain, postharvest	3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions derived from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for milled cereal grain products.

(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served. Food must be removed or covered prior to use.

(4) Where tolerances are established on both the raw agricultural commodities and processed foods made there-from, the total residues of pyrethrins in or on the processed food shall not be greater than that permitted by the larger of the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

§180.129 o-Phenylphenol and its sodium salt; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide o-phenylphenol and sodium o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or on the following food commodities:

Commodity	Parts per million
Apple	25
Cantaloupe (NMT 10 ppm in edible portion)	125
Carrot, roots	20
Cherry	5
Citrus fruits	10
Cucumber	10
Lemon	10
Nectarine	5
Orange	10
Pepper, bell	10
Peach	20
Pear	25.0
Pineapple	10
Plum, prune, fresh	20
Sweet potato, roots	15
Tomato	10

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54960, Sept. 24, 2008]

§180.130 Hydrogen Cyanide; tolerances for residues.

(a) General. A tolerance for residues of the insecticide hydrogen cyanide from postharvest fumigation as a result of application of sodium cyanide is established as follows: 50 parts per million in or on Fruit, citrus.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999]

§180.132 Thiram; tolerances for residues.

(a) General. (1) A tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only thiram.

Commodity	Parts per million
Avocado¹	15

¹No U.S. registrations as of September 23, 2009.

(2) Tolerances are established for residues of the fungicide thiram, tetramethyl thiuram disulfide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those thiram residues convertible to and expressed in terms of the degradate carbon disulfide, in or on the commodity.

Commodity	Parts per million
Apple	5
Banana¹	2.0
Peach	7.0
Strawberry	13

¹There are no U.S. registrations as of September 23, 2009.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 49615, July 31, 2002, as amended at 74 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, 2014; 79 FR 18822, Apr. 4, 2014; 80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015; 80 FR 72597, Nov. 20, 2015]

§180.142 2,4-D; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

Table 1 to Paragraph (a)

Commodity	Parts per million
Almond hulls	0.1
Asparagus	5.0
Barley, bran	4.0
Barley, grain	2.0
Barley, straw	50
Berry, group 13	0.2
Cattle, fat	0.3
Cattle, kidney	4.0
Cattle, meat	0.3
Cattle, meat byproducts, except kidney	0.3
Corn, field, forage	6.0
Corn, field, grain	0.05
Corn, field, stover	50
Corn, pop, grain	0.05
Corn, pop, stover	50
Corn, sweet, forage	6.0
Corn, sweet, kernel plus cob with husks removed	0.05
Corn, sweet, stover	50
Cotton, gin byproducts	1.5
Cotton, undelinted seed	0.08
Cranberry	0.5
Fish	0.1
Fruit, citrus, group 10	3.0
Fruit, pome, group 11	0.05
Fruit, stone, group 12	0.05
Goat, fat	0.3
Goat, kidney	4.0
Goat, meat	0.3
Goat, meat byproducts, except kidney	0.3
Grain, aspirated fractions	40
Grape	0.05
Grass, forage	360
Grass, hay	300
Hop, dried cones	0.2
Horse, fat	0.3
Horse, kidney	4.0
Horse, meat	0.3
Horse, meat byproducts, except kidney	0.3
Millet, forage	25
Millet, grain	2.0
Millet, straw	50
Milk	0.05
Nut, tree, group 14	0.2
Oat, forage	25
Oat, grain	2.0
Oat, straw	50
Pistachio	0.05
Potato	0.4
Rice, grain	0.5
Rice, hulls	2.0
Rye, bran	4.0
Rye, forage	25
Rye, grain	2.0
Rye, straw	50
Sesame, seed	0.05
Sheep, fat	0.3
Sheep, kidney	4.0
Sheep, meat	0.3
Sheep, meat byproducts, except kidney	0.3
Shellfish	1.0
Sorghum, grain, forage	0.2
Sorghum, grain, grain	0.2
Sorghum, grain, stover	0.2
Soybean, forage	0.02
Soybean, hay	2.0
Soybean, seed	0.02
Strawberry	0.05
Sugarcane, cane	0.05
Sugarcane, molasses	0.2
Teff, bran	4.0
Teff, forage	25.0
Teff, grain	2.0
Teff, straw	50.0
Vegetable, leaves of root and tuber, group 2	0.1
Vegetable, root and tuber, except potato, group 1	0.1
Wheat, bran	4.0
Wheat, forage	25
Wheat, grain	2.0
Wheat, straw	50
Wheatgrass, intermediate, bran	4
Wheatgrass, intermediate, forage	30
Wheatgrass, intermediate, grain	2
Wheatgrass, intermediate, straw	50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the follow commodities:

Commodity	Parts per million
Rice, wild, grain	0.05

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerances levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the following commodities:

Commodity	Parts per million
Animal feed, nongrass, group 18	0.2
Avocado	0.05
Dill, seed	0.05
Okra	0.05
Vegetable, brassica leafy, group 5	0.4
Vegetable, bulb, group 3	0.05
Vegetable, cucurbit, group 9	0.05
Vegetable, foliage of legume, group 7	0.2
Vegetable, fruiting, group 8	0.05
Vegetable, leafy, except brassica, group 4	0.4
Vegetable, legume, group 6	0.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, 2009; 76 FR 55817, Sept. 9, 2011; 80 FR 72597, Nov. 20, 2015; 82 FR 9529, Feb. 7, 2017; 85 FR 82943, Dec. 21, 2020]

§180.145 Fluorine compounds; tolerances for residues.

(a) General. (1) Tolerances are established for combined residues of the insecticidal fluorine compounds cryolite and synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:

Commodity	Parts per million
Apricot	7
Blackberry	7
Blueberry	7
Boysenberry	7
Broccoli	7
Brussels sprouts	7
Cabbage	7
Cauliflower	7
Collards	7
Cranberry	7
Cucumber	7
Dewberry	7
Eggplant	7
Fruit, citrus	7
Grape	7
Kale	7
Kohlrabi	7
Lettuce, head	7
Lettuce, leaf	7
Loganberry	7
Melon	7
Nectarine	7
Peach	7
Pepper	7
Plum, prune, fresh	7
Pumpkin	7
Raspberry	7
Squash, summer	7
Squash, winter	7
Strawberry	7
Tomato	7
Youngberry	7

(2) Tolerances are established for residues of fluoride in or on the following commodities from the postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity	Parts per million
All processed food commodities not otherwise listed	70
Barley, bran, postharvest	45.0
Barley, flour, postharvest	45.0
Barley, grain, postharvest	15.0
Barley, pearled barley, postharvest	45.0
Cattle, meat, dried	40
Cheese	5.0
Cacao bean, roasted bean, postharvest	20
Coconut, postharvest	40
Coffee, bean, green, postharvest	15
Corn, field, flour, postharvest	35.0
Corn, field, grain, postharvest	10.0
Corn, field, grits, postharvest	10.0
Corn, field, meal, postharvest	30.0
Corn, pop, grain, postharvest	10.0
Cotton, undelinted seed, postharvest	70
Egg, dried	900
Fruit, dried, except grape, raisin, postharvest	3.0
Ginger, postharvest	70
Grain, aspirated fractions, postharvest	55.0
Grape, raisin, postharvest	7.0
Hog, meat	20
Herbs and spices group 19, postharvest	70
Milk, powdered	5.0
Millet, grain, postharvest	40.0
Nut, pine, postharvest	20
Nut, tree, Group 14, postharvest	10.0
Oat, flour, postharvest	75.0
Oat, grain, postharvest	25.0
Oat, groats/rolled oats	75.0
Peanut, postharvest	15
Pistachio, postharvest	10.0
Rice, bran, postharvest	31.0
Rice, flour, postharvest	45
Rice, grain, postharvest	12.0
Rice, hulls, postharvest	35.0
Rice, polished rice, postharvest	25.0
Rice, wild, grain, postharvest	25.0
Sorghum, grain, postharvest	40.0
Triticale, grain, postharvest	40.0
Vegetable, legume, group 6, postharvest	70
Wheat, bran, postharvest	40.0
Wheat, flour, postharvest	125.0
Wheat, germ, postharvest	130.0
Wheat, grain, postharvest	40.0
Wheat, milled byproducts, postharvest	130.0
Wheat, shorts, postharvest	40.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by §180.1(l), are established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic cryolite (sodium aluminum fluoride), in or on the following raw agricultural commodities:

Commodity	Parts per million
Kiwifruit	15

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011]

§180.151 Ethylene oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene oxide, when used as a postharvest fumigant in or on the following food commodities:

Commodity	Parts per million
Herb and spice, group 19, dried, except basil	7
Licorice, roots	7
Peppermint, tops, dried	7
Sesame, seed	7
Spearmint, tops, dried	7
Vegetable, dried	7
Walnut	50

(2) Tolerances are established for residues of the ethylene oxide reaction product, 2-chloroethanol, commonly referred to as ethylene chlorohydrin, when ethylene oxide is used as a postharvest fumigant in or on food commodities as follows:

Commodity	Parts per million
Herb and spice, group 19, dried, except basil	940
Licorice, roots	940
Peppermint, tops, dried	940
Sesame, seed	940
Spearmint, tops, dried	940
Vegetable, dried	940

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009]

§180.153 Diazinon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide diazinon, O,O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity	Parts per million
Almond, hulls	3.0
Apple	0.50
Apricot	0.20
Bean, lima	0.50
Bean, snap, succulent	0.50
Beet, garden, roots	0.75
Beet, garden, tops	0.70
Blueberry	0.50
Caneberry subgroup 13-07A	0.75
Carrot, roots	0.75
Cattle, fat	0.50
Cherry, sweet	0.20
Cherry, tart	0.20
Cranberry	0.50
Endive	0.70
Fig	0.50
Ginseng	0.75
Grape	0.75²
Hazelnut	0.50
Kiwifruit¹	0.75
Lettuce	0.70
Melon	0.75
Mushroom	0.75²
Nectarine	0.20
Onion, bulb	0.75
Onion, green	0.75
Pea, succulent	0.50
Peach	0.20
Pear	0.50
Pineapple	0.50
Plum, prune, fresh	0.20
Radish	0.50
Rutabaga	0.75
Spinach	0.70
Strawberry	0.50
Tomato	0.75
Vegetable, brassica, leafy, group 5	0.70
Watercress	0.05

¹There are no domestic registrations for kiwifruit as of March 6, 2002.

²The expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide diazinon, O, O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]-phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity	Parts per million
Almond	0.50
Banana	0.20
Celery	0.70
Cucumber	0.75
Parsley, leaves	0.75
Parsnip	0.50
Pepper	0.5
Potato	0.10
Squash, summer	0.50
Squash, winter	0.75
Sweet potato, roots	0.10
Swiss chard	0.70
Turnip, roots	0.50
Turnip, tops	0.75

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 42738, Sept. 29, 1982]

Editorial Note: For Federal Register citations affecting §180.153, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.155 1-Naphthaleneacetic acid; tolerances for residues.

(a) General. Tolerances are established for the residues of 1-naphthaleneacetic acid, including its metabolites and degradates in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring only 1-naphthaleneacetic acid and its conjugates, calculated as the Stoichiometric equivalent of 1-naphthaleneacetic acid, in or on the commodity.

Commodity	Parts per million
Avocado	0.05
Cherry, sweet	0.1
Fruit, pome, group 11-10	0.15
Mango	0.05
Olive	0.7
Orange	0.1
Pineapple¹	0.05
Pomegranate	0.05
Potato	0.01
Rambutan	2.0
Sapote, mamey	0.05
Tangerine	0.1

¹There are no U.S. registrations since 1988.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 30218, May 22, 2013, as amended at 80 FR 77260, Dec. 14, 2015]

§180.163 Dicofol; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicofol as the sum of its p,p-dicofol and o,p-dicofol isomers: 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

Commodity	Parts per million	Expiration/revocation date
Apple, wet pomace	38.0	10/31/16
Bean, dry, seed	0.5	10/31/16
Bean, succulent	3.0	10/31/16
Butternut	0.1	10/31/16
Caneberry subgroup 13A	5.0	10/31/16
Chestnut	0.1	10/31/16
Citrus, dried pulp	12.0	10/31/16
Citrus oil	200.0	10/31/16
Cotton, refined oil	0.5	10/31/16
Cotton, undelinted seed	0.1	10/31/16
Fruit, citrus, group 10	6.0	10/31/16
Fruit, pome, group 11	10.0	10/31/16
Fruit, stone, group 12	5.0	10/31/16
Grape	5.0	10/31/16
Grape, raisin	20.0	10/31/16
Hazelnut	0.1	10/31/16
Hop, dried cones	65.0	10/31/16
Nut, hickory	0.1	10/31/16
Nut, macadamia	0.1	10/31/16
Pecan	0.1	10/31/16
Peppermint, oil	30.0	10/31/16
Peppermint, tops	25.0	10/31/16
Spearmint, oil	30.0	10/31/16
Spearmint, tops	25.0	10/31/16
Strawberry	10.0	10/31/16
Tea, dried	50.0	None
Tea, plucked leaves	30.0	None
Vegetable, cucurbit, group 9	2.0	10/31/16
Vegetable, fruiting, group 8	2.0	10/31/16
Walnut	0.1	10/31/16

(2) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, its isomer o,p-dicofol, 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, and its metabolites 4-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol, calculated as the stoichiometric equivalent of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, in or on the commodity.

Commodity	Parts per million	Expiration/Revocation Date
Cattle, fat	50.0	10/31/16
Cattle, liver	5.0	10/31/16
Cattle, meat	3.0	10/31/16
Cattle, meat byproducts, except liver	3.0	10/31/16
Egg	0.05	10/31/16
Goat, fat	50.0	10/31/16
Goat, liver	5.0	10/31/16
Goat, meat	3.0	10/31/16
Goat, meat byproducts, except liver	3.0	10/31/16
Hog, fat	50.0	10/31/16
Hog, liver	5.0	10/31/16
Hog, meat	3.0	10/31/16
Hog, meat byproducts, except liver	3.0	10/31/16
Horse, fat	50.0	10/31/16
Horse, liver	5.0	10/31/16
Horse, meat	3.0	10/31/16
Horse, meat byproducts, except liver	3.0	10/31/16
Milk, fat (reflecting 0.75 ppm in whole milk)	22.0	10/31/16
Poultry, fat	0.1	10/31/16
Poultry, meat	0.1	10/31/16
Poultry, meat byproducts	0.1	10/31/16
Sheep, fat	50.0	10/31/16
Sheep, liver	5.0	10/31/16
Sheep, meat	3.0	10/31/16
Sheep, meat byproducts, except liver	3.0	10/31/16

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007; 77 FR 59124, Sept. 26, 2012]

§180.169 Carbaryl; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

Commodity	Parts per million	Expiration/revocation date
Alfalfa, forage	50	None
Alfalfa, hay	75	None
Almond, hulls	50	None
Apple, wet pomace	15	None
Asparagus	15	None
Banana	5.0	None
Beet, sugar, roots	0.5	None
Beet, sugar, tops	25	None
Bushberry subgroup 13-07B	3.0	None
Cabbage	21	None
Cactus, fruit	5.0	None
Cactus, pads	12	None
Caneberry subgroup 13-07A	12.0	None
Citrus, oil	20	None
Clover, forage	50	None
Clover, hay	70	None
Corn, field, forage	30	None
Corn, field, grain	0.02	None
Corn, field, stover	20	None
Corn, pop, grain	0.02	None
Corn, pop, stover	20	None
Corn, sweet, forage	185	None
Corn, sweet, kernel plus cob with husks removed	0.1	None
Corn, sweet, stover	215	None
Cotton, undelinted seed	5.0	10/31/09
Cranberry	3.0	None
Dandelion, leaves	22	None
Endive	10	None
Flax, seed	0.5	None
Fruit, citrus, group 10	10	None
Fruit, pome, group 11	12	None
Fruit, stone, group 12	10	None
Grain, aspirated fractions	70	None
Grape	10	None
Grape, raisin	12	None
Grass, forage	100	None
Grass, hay	15	None
Leaf petiole subgroup 4B	3.0	None
Lettuce	10	None
Millet, proso, grain	1.0	None
Millet, proso, straw	20	None
Nut, tree group 14, except walnut	0.1	None
Okra	4.0	None
Olive	10	None
Oyster	0.25	None
Parsley, leaves	22	None
Pea and bean, dried shelled, except soybean, subgroup 6C	1.0	None
Peanut	0.05	None
Peanut, hay	20	None
Pineapple	2.0	None
Pistachio	0.1	None
Rice, grain	15	None
Rice, hulls	30	None
Sorghum grain, forage	30	None
Sorghum grain, grain	10	None
Sorghum grain, stover	30	None
Soybean, forage	15	None
Soybean, hay	15	None
Soybean, seed	0.5	None
Spinach	22	None
Strawberry	4.0	None
Sunflower, seed	0.5	None
Sweet potato, roots	0.2	None
Trefoil, forage	15	None
Trefoil, hay	25	None
Vegetable, brassica, leafy, group 5, except cabbage	10	None
Vegetable, cucurbit, group 9	3.0	None
Vegetable, foliage of legume, subgroup 7A, except soybean	60	None
Vegetable, fruiting, group 8	5.0	None
Vegetable, leaves of root and tuber, group 2, except sugar beet tops	75	None
Vegetable, legume, edible podded, subgroup 6A	10	None
Vegetable, root and tuber, group 1, except sugar beet and sweet potato	2.0	None
Walnut	1.0	None
Wheat, forage	30	None
Wheat, grain	1.0	None
Wheat, hay	30	None
Wheat, straw	20	None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate, including its metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6-dihydrodihydroxy naphthol, calculated as 1-naphthyl N-methylcarbamate and the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 5-methoxy-6-hydroxy carbaryl, in or on the following food commodities:

Commodity	Parts per million	Expiration/revocation date
Cattle, fat	0.5	None
Cattle, meat	1.0	None
Cattle, meat byproducts	3.0	None
Egg	0.5	10/31/09
Goat, fat	0.5	None
Goat, meat	1.0	None
Goat, meat byproducts	3.0	None
Hog, fat	0.5	None
Hog, meat	1.0	None
Hog, meat byproducts	3.0	None
Horse, fat	0.5	None
Horse, meat	1.0	None
Horse, meat byproducts	3.0	None
Milk	1.0	None
Poultry, fat	5.0	10/31/09
Poultry, meat	5.0	10/31/09
Sheep, fat	0.5	None
Sheep, meat	1.0	None
Sheep, meat byproducts	3.0	None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food commodities:

Commodity	Parts per million
Dillweed, fresh leaves	0.2

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009; 80 FR 72597, Nov. 20, 2015]

§180.172 Dodine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dodine, including its metabolites and degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only dodine, N-dodecylguanidine acetate; in or on the following commodities.

Commodity	Parts per million
Almond, hull	30.0
Apple	5.0
Apple, wet pomace	15.0
Banana	0.50
Fruit, stone, crop group 12	5.0
Nuts, tree, crop group 14	0.3
Peanut	0.013
Pear	5.0
Strawberry	5.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, 2012]

§180.175 Maleic hydrazide; tolerances for residues.

(a) General. (1) Tolerances for residues of the herbicide and plant regulator maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) are established in or on the following raw agricultural commodities:

Commodity	Parts per million
Onion, bulb	15.0
Potato	50.0

(2) A food additive known as maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) may be present in potato, chips when used in accordance with the following conditions:

(i) The food additive is present as a result of the application of a pesticide formulation containing maleic hydrazide to the growing potato plant in accordance with directions registered by the U.S. Environmental Protection Agency.

(ii) The label of the pesticide formulation containing the food additive conforms to labeling registered by the U.S. Environmental Protection Agency.

(iii) The food additive is present in an amount not to exceed 160 parts per million by weight of the finished food.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 64293, Dec. 5, 1997, as amended at 64 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, 2002]

§180.176 Mancozeb; tolerances for residues.

(a) General. Tolerances are established for residues of mancozeb (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity	Parts per million
Almond	0.1
Almond, hulls	4
Apple	0.6
Asparagus	0.1
Atemoya	3.0
Banana	2
Barley, bran	2
Barley, flour	1.2
Barley, grain	1
Barley, hay	30
Barley, pearled barley	20
Barley, straw	25
Beet, sugar, dried pulp	3.0
Beet, sugar, roots	1.2
Beet, sugar, tops	60
Broccoli	7
Cabbage	9
Canistel	15.0
Cattle, kidney	0.5
Cattle, liver	0.5
Cherimoya	3.0
Corn, field, forage	40
Corn, field, grain	0.06
Corn, field, stover	15
Corn, pop, grain	0.1
Corn, pop, stover	40
Corn, sweet, forage	70
Corn, sweet, kernel plus cob with husks removed	0.1
Corn, sweet, stover	40
Cotton, undelinted seed	0.5
Crabapple	0.6
Cranberry	5
Custard apple	3.0
Fennel	2.5
Flax, seed	0.15
Ginseng	1.2
Goat, kidney	0.5
Goat, liver	0.5
Grape	1.5
Hog, kidney	0.5
Hog, liver	0.5
Horse, kidney	0.5
Horse, liver	0.5
Lettuce, head	3.5
Lettuce, leaf	18
Mango	15.0
Oat, flour	1.2
Oat, grain	1
Oat, groats/rolled oats	20
Oat, hay	30
Oat, straw	25
Onion, bulb	1.5
Papaya	9
Peanut	0.1
Peanut, hay	65
Pear	0.6
Pepper	12
Potato	0.2
Poultry, kidney	0.5
Poultry, liver	0.5
Quince	0.6
Rice, grain	0.06
Rye, bran	2
Rye, flour	1.2
Rye, grain	1
Rye, straw	25
Sapodilla	15.0
Sapote, mamey	15.0
Sapote, white	15.0
Sheep, kidney	0.5
Sheep, liver	0.5
Sorghum, grain, forage	0.15
Sorghum, grain, grain	0.25
Sorghum, grain, stover	0.15
Star apple	15.0
Sugar apple	3.0
Tangerine¹	10
Tomato	2.5
Vegetable, cucurbit, group 9	2.0
Walnut	0.70
Wheat, bran	2
Wheat, flour	1.2
Wheat, germ	20
Wheat, grain	1
Wheat, hay	30
Wheat, middlings	20
Wheat, shorts	2
Wheat, straw	25

¹There are no U.S. registrations for use of mancozeb on tangerine.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registrations, as defined in §180.1(l), is established for residues of the fungicide mancozeb, (a coordination product of zinc ion and maneb (manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodity in the following table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity	Parts per million
Carrot, roots	1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 50913, Aug. 18, 2010; 76 FR 18915, Apr. 6, 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, May 14, 2014; 80 FR 72597, Nov. 20, 2015]

§180.178 Ethoxyquin; tolerances for residues.

(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6-ethoxy-2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:

Commodity	Parts per million
Pear	3

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57073, Oct. 26, 1998]

§180.181 Chlorpropham; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) in or on the following food commodities:

Commodity	Parts per million
Potato	30
Potato, wet peel	40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide chlorpropham (isopropyl m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic acid (4-HSA) in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.20
Cattle, kidney	0.30
Cattle, meat	0.06
Cattle, meat byproducts except kidney	0.06
Goat, fat	0.20
Goat, kidney	0.30
Goat, meat	0.06
Goat, meat byproducts except kidney	0.06
Hog, fat	0.20
Hog, kidney	0.30
Hog, meat	0.06
Hog, meat byproducts except kidney	0.06
Horse, fat	0.20
Horse, kidney	0.30
Horse, meat	0.06
Horse, meat byproducts except kidney	0.06
Milk	0.30
Sheep, fat	0.20
Sheep, kidney	0.30
Sheep, meat	0.06
Sheep, meat byproducts except kidney	0.06

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

§180.182 Endosulfan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

Commodity	Parts per million	Expiration/ revocation date
Almond	0.3	7/31/12
Almond, hulls	1.0	7/31/12
Apricot	2.0	7/31/12
Bean	2.0	7/31/12
Broccoli	3.0	7/31/12
Brussels sprouts	2.0	7/31/12
Cabbage	4.0	7/31/12
Cantaloupe	1.0	7/31/12
Carrot, roots	0.2	7/31/12
Cattle, fat	13.0	7/31/16
Cattle, liver	5.0	7/31/16
Cattle, meat	2.0	7/31/16
Cattle, meat byproducts, except liver	1.0	7/31/16
Cauliflower	2.0	7/31/12
Celery	8.0	7/31/12
Cherry, sweet	2.0	7/31/12
Cherry, tart	2.0	7/31/12
Collards	2.0	7/31/12
Cotton, gin byproducts	30.0	7/31/12
Cotton, undelinted seed	1.0	7/31/12
Cucumber	1.0	7/31/12
Eggplant	1.0	7/31/12
Goat, fat	13.0	7/31/16
Goat, liver	5.0	7/31/16
Goat, meat	2.0	7/31/16
Goat, meat byproducts, except liver	1.0	7/31/16
Hazelnut	0.2	7/31/12
Hog, fat	13.0	7/31/16
Hog, liver	5.0	7/31/16
Hog, meat	2.0	7/31/16
Hog, meat byproducts, except liver	1.0	7/31/16
Horse, fat	13.0	7/31/16
Horse, liver	5.0	7/31/16
Horse, meat	2.0	7/31/16
Horse, meat byproducts, except liver	1.0	7/31/16
Kale	2.0	7/31/12
Lettuce, head	11.0	7/31/12
Lettuce, leaf	6.0	7/31/12
Milk, fat	2.0	7/31/16
Muskmelon	1.0	7/31/12
Mustard greens	2.0	7/31/12
Mustard, seed	0.2	7/31/12
Nectarine	2.0	7/31/12
Nut, macadamia	0.2	7/31/12
Peach	2.0	7/31/12
Pear	2.0	7/31/13
Pineapple	1.0	7/31/16
Pineapple, process residue	20.0	7/31/16
Plum	2.0	7/31/12
Plum, prune	2.0	7/31/12
Sheep, fat	13.0	7/31/16
Sheep, liver	5.0	7/31/16
Sheep, meat	2.0	7/31/16
Sheep, meat byproducts, except liver	1.0	7/31/16
Squash, summer	1.0	7/31/12
Strawberry	2.0	7/31/16
Sweet potato, roots	0.15	7/31/12
Walnut	0.2	7/31/12
Watermelon	1.0	7/31/12

(2) A tolerance is established for the combined residues of the insecticide endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3,3-dioxide in or on the commodity in the following table:

Commodity	Parts per million	Expiration/ revocation date
Tea, dried	24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide to growing tea	7/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. (1) Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph, when endosulfan is used in the state of Florida. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

Commodity	Parts per million	Expiration/ revocation date
Apple	1.0	12/31/14
Apple, wet pomace	5.0	12/31/14
Blueberry	0.3	12/31/14
Corn, sweet, forage	12.0	12/31/14
Corn, sweet, kernel plus cob with husks removed	0.2	12/31/14
Corn, sweet, stover	14.0	12/31/14
Pepper	2.0	12/31/14
Potato	0.2	12/31/14
Pumpkin	1.0	12/31/14
Squash, winter	1.0	12/31/14
Tomato	1.0	12/31/14

(2) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities in the table in this paragraph, when endosulfan is used in the United States (except Florida). Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in or on the commodity.

Commodity	Parts per million	Expiration/ revocation date
Apple	1.0	7/31/15
Apple, wet pomace	5.0	7/31/15
Blueberry	0.3	7/31/15
Corn, sweet, forage	12.0	7/31/15
Corn, sweet, kernel plus cob with husks removed	0.2	7/31/15
Corn, sweet, stover	14.0	7/31/15
Pepper	2.0	7/31/15
Potato	0.2	7/31/15
Pumpkin	1.0	7/31/15
Squash, winter	1.0	7/31/15
Tomato	1.0	7/31/15

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33696, May 24, 2000, as amended at 71 FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, 2011; 78 FR 8409, Feb. 6, 2013]

§180.183 Disulfoton; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.

Commodity	Parts per million	Expiration/Revocation Date
Bean, lima	0.75	12/31/13
Bean, snap, succulent	0.75	12/31/13
Broccoli	0.75	12/31/13
Brussels sprouts	0.75	12/31/13
Cabbage	0.75	12/31/13
Cauliflower	0.75	12/31/13
Coffee, green bean	0.2	6/30/14
Cotton, undelinted seed	0.75	12/31/13
Lettuce, head	0.75	12/31/14
Lettuce, leaf	2	12/31/14

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration is established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.

Commodity	Parts per million	Expiration/Revocation Date
Asparagus	0.1	12/31/13

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67 FR 41806, June 19, 2002; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, 2009; 75 FR 60240, Sept. 29, 2010]

§180.184 Linuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity:

Commodity	Parts per million
Asparagus	7.0
Carrot, roots	1.0
Cattle, fat	0.2
Cattle, kidney	2.0
Cattle, liver	2.0
Cattle, meat	0.1
Cattle, meat byproducts except kidney and liver	0.1
Celeriac	1.0
Cilantro, dried leaves	10
Cilantro, fresh leaves	3.0
Coriander, seed	0.01
Corn, field, forage	1.0
Corn, field, grain	0.1
Corn, field, stover	6.0
Corn, sweet, forage	1.0
Corn, sweet, kernel plus cob with husks removed	0.25
Corn, sweet, stover	6.0
Cotton, gin byproducts	5.0
Cotton, undelinted seed	0.25
Dill, oil	2.0
Dill, seed	0.5
Dillweed, dried leaves	5.0
Dillweed, fresh leaves	1.5
Goat, fat	0.2
Goat, kidney	2.0
Goat, liver	2.0
Goat, meat	0.1
Goat, meat byproducts except kidney and liver	0.1
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.1
Horse, fat	0.2
Horse, kidney	2.0
Horse, liver	2.0
Horse, meat	0.1
Horse, meat byproducts except kidney and liver	0.1
Horseradish	0.05
Milk	0.05
Parsley, dried leaves	9.0
Parsley, leaves	4.0
Parsnip, roots	0.05
Parsnip, tops	0.05
Pea, dry, seed	0.09
Rhubarb	0.5
Sheep, fat	0.2
Sheep, kidney	2.0
Sheep, liver	2.0
Sheep, meat	0.1
Sheep, meat byproducts except kidney and liver	0.1
Sorghum, grain, forage	1.0
Sorghum, grain, grain	0.25
Sorghum, grain, stover	1.0
Soybean, seed	1.0
Soybean, vegetable	1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide linuron [3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea], including its metabolites and degradates, in or on the commodities in the table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3.4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity. The tolerance expires and is revoked on the date specified in the table.

Commodity	Parts per million	Expiration/revocation date
Lentil	0.1	12/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity.

Commodity	Parts per million
Celery	0.5
Potato	0.2
Wheat, forage	0.5
Wheat, grain	0.05
Wheat, hay	0.5
Wheat, straw	2.0

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008; 76 FR 81396, Dec. 28, 2011; 79 FR 8307, Feb. 12, 2014]

§180.185 DCPA; tolerances for residues.

(a) General. Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid (TCP) (calculated as dimethyl tetrachloroterephthalate) are established in or on the following food commodities:

Commodity	Parts per million
Cantaloupe	1.0
Garlic	1.0
Ginseng	2.0
Horseradish	2.0
Muskmelon	1.0
Onion, bulb	1.0
Onion, green	1.0
Strawberry	2.0
Tomato	1.0
Vegetable, brassica, leafy, group 5	5.0
Watermelon	1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

Commodity	Parts per million
Radish, roots	2.0
Radish, tops	15.0

(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

Commodity	Parts per million
Basil, dried leaves	20.0
Basil, fresh leaves	5.0
Bean, dry	2.0
Bean, mung, seed	2.0
Bean, snap, succulent	2.0
Celeriac	2.0
Chicory, roots	2.0
Chicory, tops	5.0
Chive	5.0
Coriander, leaves	5.0
Corn, field, forage	0.4
Corn, field, grain	0.05
Corn, field, stover	0.4
Corn, pop, forage	0.4
Corn, pop, grain	0.05
Corn, pop, stover	0.4
Corn, sweet, forage	0.4
Corn, sweet, kernel plus cob with husks removed	0.05
Corn, sweet, stover	0.4
Cotton, undelinted seed	0.2
Cucumber	1.0
Dill	5.0
Eggplant	1.0
Lettuce	2.0
Marjoram	5.0
Parsley, dried leaves	20.0
Parsley, leaves	5.0
Pea, blackeyed, seed	2.0
Pepper	2.0
Pimento	2.0
Potato	2.0
Radicchio	5.0
Radish, oriental, roots	2.0
Radish, oriental, tops	2.0
Rutabaga	2.0
Soybean	2.0
Squash, summer	1.0
Squash, winter	1.0
Sweet potato	2.0
Turnip, roots	2.0
Turnip, tops	5.0
Yam, true, tuber	2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008; 74 FR 14744, Apr. 1, 2009]

§180.189 Coumaphos; tolerances for residues.

(a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphorothioate and its oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosphate) in or on food commodities as follows:

Commodity	Parts per million
Cattle, fat	1.0
Cattle, meat	1.0
Cattle, meat byproducts	1.0
Goat, fat	1.0
Goat, meat	1.0
Goat, meat byproducts	1.0
Hog, fat	1.0
Hog, meat	1.0
Hog, meat byproducts	1.0
Honey	0.15
Honeycomb	45.0
Horse, fat	1.0
Horse, meat	1.0
Horse, meat byproducts	1.0
Milk, fat ( = n in whole milk)	0.5
Sheep, fat	1.0
Sheep, meat	1.0
Sheep, meat byproducts	1.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69 FR 29458, May 24, 2004; 72 FR 28876, May 23, 2007]

§180.190 Diphenylamine; tolerances for residues.

(a) General. Tolerances for residues of the plant regulator diphenylamine are established in or on the following commodities:

Commodity	Parts per million
Apple, wet pomace	30.0
Apple from preharvest or postharvest use, including use of impregnated wraps	10.0
Cattle, fat	0.01
Cattle, liver	0.1
Cattle, meat byproducts, except liver	0.01
Cattle, meat	0.01
Goat, fat	0.01
Goat, liver	0.1
Goat, meat byproducts, except liver	0.01
Goat, meat	0.01
Horse, fat	0.01
Horse, liver	0.1
Horse, meat byproducts, except liver	0.01
Horse, meat	0.01
Milk	0.01
Pear (post harvest)	5.0
Sheep, fat	0.01
Sheep, liver	0.1
Sheep, meat byproducts, except liver	0.01
Sheep, meat	0.01

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007; 76 FR 34885, June 15, 2011]

§180.191 Folpet; tolerances for residues.

(a) General. Tolerances are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on raw agricultural commodities as follows:

Commodity	Parts per million
Apple¹	5.0
Cranberry¹	15.0
Cucumber¹	2.0
Grape¹	50.0
Grape, raisin¹	80.0
Hop, dried cones	120.0
Lettuce¹	50.0
Melon¹	3.0
Onion,bulb¹	2.0
Strawberry¹	5.0
Tomato¹	25.0

¹ No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in §180.1(l) are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on the following raw agricultural commodity:

Commodity	Parts per million
Avocado	25.0

(d) Indirect or inadvertent residues. [Reserved]

[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72 FR 41928, Aug. 1, 2007]

§180.198 Trichlorfon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1-hydroxyethyl) phosphonate) in or on the following food commodities:

Commodity	Parts per million
Cattle, fat¹	0.5
Cattle, meat¹	0.2
Cattle, meat byproducts¹	0.1

¹There are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

§180.200 Dicloran; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dicloran, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only dicloran, 2,6-dichloro-4-nitroaniline, in or on the commodity.

Commodity	Parts per million	Expiration/revocation date
Apricot	20	None
Bean, snap, succulent	20	None
Carrot, roots	10	11/2/11
Celery	15	None
Cherry, sweet	20	None
Cucumber	5	None
Endive	10	None
Garlic	5	None
Grape	10	None
Lettuce	10	None
Nectarine	20	None
Onion	10	None
Peach	20	None
Plum, prune, fresh	15	None
Potato	0.25	12/31/14
Rhubarb	10	None
Sweet potato, roots	10	None
Tomato	5	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

§180.202 p-Chlorophenoxyacetic acid; tolerances for residues.

(a) General. A tolerance is established for the combined residues of the plant regulator p-chlorophenoxyacetic acid and its metabolite p-chlorophenol to inhibit embryonic root development in or on the following food commodity:

Commodity	Parts per million
Bean, mung, sprouts	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006]

§180.204 Dimethoate; tolerances for residues.

(a) General. Tolerances are established for total residues of the insecticide dimethoate (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorodithioate) including its oxygen analog (O,O-dimethyl S-(N- methylcarbamoylmethyl) phosphorothioate) in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	2.0
Alfalfa, hay	2.0
Bean, dry, seed	2.0
Bean, lima	2.0
Bean, snap, succulent	2.0
Blueberry¹	1.0
Broccoli	2.0
Cattle, meat byproducts	0.02
Cauliflower	2.0
Celery	2.0
Citrus, dried pulp	5.0
Corn, field, forage	1.0
Corn, field, grain	0.1
Corn, field, stover	1.0
Corn, pop, grain	0.1
Corn, pop, stover	1.0
Corn, sweet, forage	1.0
Cotton, undelinted seed	0.1
Egg	0.02
Endive	2.0
Goat, meat byproducts	0.02
Grapefruit	2.0
Hog, meat byproducts	0.02
Horse, meat byproducts	0.02
Kale	2.0
Lemon	2.0
Lettuce, leaf	2.0
Melon	1.0
Milk	0.002
Mustard greens	2.0
Orange	2.0
Pea	2.0
Pear	2.0
Pecan	0.1
Pepper	2.0
Potato	0.2
Poultry, meat byproducts	0.02
Safflower, seed	0.1
Sheep, meat byproducts	0.02
Sorghum, grain, forage	0.1
Sorghum, grain, grain	0.1
Sorghum, grain, stover	0.1
Soybean, forage	2.0
Soybean, hay	2.0
Soybean, seed	0.05
Swiss chard	2.0
Tangerine	2.0
Tomato	2.0
Turnip, roots	0.2
Turnip, tops	2.0
Wheat, forage	2.0
Wheat, grain	0.04
Wheat, hay	2.0
Wheat, straw	2.0

¹ There are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for total residues of dimethoate including its oxygen analog in or on the following food commodities:

Commodity	Parts per million
Asparagus	0.15
Brussels sprouts	5.0
Cherry, sweet	2.0
Cherry, tart	2.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

§180.205 Paraquat; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat (1,1′-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity	Parts per million
Acerola	0.05
Almond, hulls	0.5
Animal feed, nongrass, group 18, forage	75.0
Animal feed, nongrass, group 18, hay	210.0
Artichoke, globe	0.05
Asparagus	0.5
Atemoya	0.05
Avocado	0.05
Banana	0.05
Barley, grain	0.05
Barley, hay	3.5
Barley, straw	1.0
Beet, sugar, roots	0.5
Beet, sugar, tops	0.05
Berry group 13	0.05
Biriba	0.05
Cacao bean, bean	0.05
Canistel	0.05
Carrot, roots	0.05
Cattle, fat	0.05
Cattle, kidney	0.5
Cattle, meat	0.05
Cattle, meat byproducts, except kidney	0.05
Cherimoya	0.05
Coffee, bean, green	0.05
Corn, field, forage	3.0
Corn, field, grain	0.1
Corn, field, stover	10.0
Corn, pop, grain	0.1
Corn, pop, stover	10.0
Corn, sweet, kernel plus cob with husks removed	0.05
Cotton, gin byproducts	110.0
Cotton, undelinted seed	3.5
Cowpea, forage	0.1
Cowpea, hay	0.4
Cranberry	0.05
Custard apple	0.05
Egg	0.01
Endive	0.05
Feijoa	0.05
Fig	0.05
Fruit, citrus, group 10	0.05
Fruit, pome, group 11	0.05
Fruit, stone, group 12	0.05
Goat, fat	0.05
Goat, kidney	0.5
Goat, meat	0.05
Goat, meat byproducts, except kidney	0.05
Grain, aspirated fractions	65.0
Grape	0.05
Grass, forage	90.0
Grass, hay	40.0
Guar, seed	0.5
Guava	0.05
Hog, fat	0.05
Hog, kidney	0.5
Hog, meat	0.05
Hog, meat byproducts, except kidney	0.05
Hop, dried cones	0.5
Horse, fat	0.05
Horse, kidney	0.5
Horse, meat	0.05
Horse, meat byproducts, except kidney	0.05
Ilama	0.05
Jaboticaba	0.05
Kiwifruit	0.05
Lentil, seed	0.3
Lettuce	0.05
Longan	0.05
Lychee	0.05
Mango	0.05
Milk	0.01
Nut, tree, group 14	0.05
Okra	0.05
Olive	0.05
Onion, bulb	0.1
Onion, green	0.05
Papaya	0.05
Passionfruit	0.2
Pawpaw	0.05
Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean	0.3
Pea and bean, succulent shelled, subgroup 6B	0.05
Pea, field, hay	0.8
Pea, field, vines	0.2
Peanut	0.05
Peanut, hay	0.5
Peppermint, tops	0.5
Persimmon	0.05
Pineapple	0.05
Pineapple, process residue	0.25
Pistachio	0.05
Pomegranate	0.05
Pulasan	0.05
Rambutan	0.05
Rhubarb	0.05
Rice, grain	0.05
Safflower, seed	0.05
Sapodilla	0.05
Sapote, black	0.05
Sapote, mamey	0.05
Sapote, white	0.05
Sheep, fat	0.05
Sheep, kidney	0.5
Sheep, meat	0.05
Sheep, meat byproducts, except kidney	0.05
Sorghum, forage, forage	0.1
Sorghum, grain, forage	0.1
Sorghum, grain, grain	0.05
Soursop	0.05
Soybean, forage	0.4
Soybean, hay	10.0
Soybean, hulls	4.5
Soybean, seed	0.7
Spanish lime	0.05
Spearmint, tops	0.5
Star apple	0.05
Starfruit	0.05
Strawberry	0.25
Sugar apple	0.05
Sugarcane, cane	0.5
Sugarcane, molasses	3.0
Sunflower, seed	2.0
Turnip, greens	0.05
Turnip, roots	0.05
Vegetable, brassica, leafy, group 5	0.05
Vegetable, cucurbit, group 9	0.05
Vegetable, fruiting, group 8	0.05
Vegetable, legume, edible podded, subgroup 6A	0.05
Vegetable, tuberous and corm, subgroup 1C	0.50
Wax jambu	0.05
Wheat, forage	0.5
Wheat, grain	1.1
Wheat, hay	3.5
Wheat, straw	50.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(l), are established for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity	Parts per million
Pea, pigeon, seed	0.05
Taro, corm	0.1
Tyfon	0.05

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 51614, Oct. 21, 1981]

Editorial Note: For Federal Register citations affecting §180.205, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.206 Phorate; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide phorate (O,O-diethyl S (ethylthio) methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen analog, phorate oxygen analog sulfoxide, and phorate oxygen analog sulfone in or on the following food commodities:

Commodity	Parts per million
Bean, dry, seed	0.05
Bean, succulent	0.05
Beet, sugar, roots	0.3
Beet, sugar, tops	3.0
Coffee, green bean¹	0.02
Corn, field, forage	0.5
Corn, field, grain	0.05
Corn, sweet, forage	0.5
Corn, sweet, kernel plus cob with husks removed	0.05
Cotton, undelinted seed	0.05
Hop, dried cones	2.0
Peanut	0.1
Potato	0.2
Sorghum, grain, grain	0.05
Sorghum, grain, stover	0.1
Soybean, seed	0.05
Sugarcane, cane	0.05
Wheat, forage	1.5
Wheat, grain	0.05
Wheat, hay	1.5
Wheat, straw	0.05

¹ There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008]

§180.207 Trifluralin; tolerances for residues.

(a) General. Tolerances are established for residues of trifluralin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only trifluralin (2,6-dinitro-N,N-dipropyl-4-(trifluoromethyl)benzenamine).

Commodity	Parts per million
Alfalfa, forage	3.0
Alfalfa, hay	2.0
Almond, hulls	0.05
Asparagus	0.05
Barley, grain	0.05
Barley, hay	0.05
Barley, straw	0.05
Bean, mung, sprouts	2.0
Carrot, roots	1.0
Celery	0.05
Corn, field, forage	0.05
Corn, field, grain	0.05
Corn, field, stover	0.05
Cotton, gin byproducts	0.05
Endive	0.05
Fruit, citrus, group 10	0.05
Fruit, stone, group 12	0.05
Grape	0.05
Hop, dried cones	0.05
Nut, tree, group 14	0.05
Oilseed, crop group 20	0.05
Okra	0.05
Peanut	0.05
Peanut, hay	0.05
Peppermint, oil	2.0
Peppermint, tops	0.05
Rosemary, dried leaves	0.10
Rosemary, fresh leaves	0.10
Rosemary, oil	3.0
Sorghum, grain, forage	0.05
Sorghum, grain, grain	0.05
Sorghum, grain, stover	0.05
Spearmint, oil	2.0
Spearmint, tops	0.05
Sugarcane, cane	0.05
Vegetable, brassica, leafy group 5	0.05
Vegetable, bulb, group 3	0.05
Vegetable, cucurbit, group 9	0.05
Vegetable, foliage of legume, group 7	0.05
Vegetable, fruiting, group 8	0.05
Vegetable, leaves of root and tuber, group 2	0.05
Vegetable, legume, group 6	0.05
Vegetable, root and tuber, group 1, except carrot	0.05
Wheat, grain	0.05
Wheat, straw	0.05

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980; 46 FR 37250, July 20, 1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006; 78 FR 46274, July 31, 2013; 84 FR 4351, Feb. 15, 2019]

§180.208 Benfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide benfluralin, N-butyl-N-ethyl-ααα-trifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	0.05
Alfalfa, hay	0.05
Clover, forage	0.05
Clover, hay	0.05
Lettuce	0.05
Trefoil, forage	0.05
Trefoil, hay	0.05

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

§180.209 Terbacil; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide terbacil, (3-tert-butyl-5-chloro-6-methyluracil) and its metabolites [3-tert-butyl-5-chloro-6-hydroxymethyluracil], [6-chloro-2,3-dihydro-7-hydroxymethyl 3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7-trimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], calculated as terbacil, in or on the following raw agricultural commodities:

Commodity	Parts per million
Alfalfa, forage	1.0
Alfalfa, hay	2.0
Apple	0.3
Asparagus	0.4
Blueberry	0.2
Caneberry subgroup 13A	0.2
Peach	0.2
Peppermint, tops	2.0
Spearmint, tops	2.0
Strawberry	0.1
Sugarcane, cane	0.4
Watermelon	1.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 30818, May 31, 2006]

§180.210 Bromacil; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide bromacil (5-bromo-3-sec-butyl-6-methyluracil) in or on the following food commodities:

Commodity	Parts per million
Fruit, citrus	0.1
Pineapple	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

§180.211 Propachlor; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propachlor (2-chloro-N-isopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloro-N-isopropylacetanilide, in or on the following raw agricultural commodities:

Commodity	Parts per million
Cattle, fat	0.05
Cattle, kidney	0.2
Cattle, meat	0.02
Cattle, meat byproducts, except kidney	0.05
Corn, field, forage	3.0
Corn, field, grain	0.2
Corn, field, stover	1.0
Corn, sweet, forage	3.0
Goat, fat	0.05
Goat, kidney	0.2
Goat, meat	0.02
Goat, meat byproducts, except kidney	0.05
Hog, fat	0.02
Hog, meat	0.02
Hog, meat byproducts	0.02
Horse, fat	0.05
Horse, kidney	0.2
Horse, meat	0.02
Horse, meat byproducts, except kidney	0.05
Milk	0.02
Sheep, fat	0.05
Sheep, kidney	0.2
Sheep, meat	0.02
Sheep, meat byproducts, except kidney	0.05
Sorghum, forage, forage	8.0
Sorghum, grain, forage	8.0
Sorghum, grain, grain	0.25
Sorghum, grain, stover	12.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47 FR 46701, Oct. 20, 1982; 63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007]

§180.212 S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl cyclohexylethylthiocarbamate in or on the following food commodities:

Commodity	Parts per million
Beet, garden, roots	0.05(N)
Beet, garden, tops	0.05(N)
Beet, sugar, roots	0.05(N)
Beet, sugar, tops	0.05(N)
Spinach	0.05(N)

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

§180.213 Simazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide simazine (2-chloro-4,6-bis(ethylamino)-s-triazine) and its two chlorinated degradates (2-amino-4-chloro-6-ethylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine), the total residue to be measured in or on the following food commodities:

Commodity	Parts per million
Almond	0.25
Almond, hulls	0.25
Apple	0.20
Avocado	0.20
Blackberry	0.20
Blueberry	0.20
Cattle, meat	0.03
Cattle, meat byproducts	0.03
Cherry	0.25
Corn, field, forage	0.20
Corn, field, grain	0.20
Corn, field, stover	0.25
Corn, pop, grain	0.20
Corn, pop, stover	0.25
Corn, sweet, forage	0.20
Corn, sweet, kernel plus cob with husks removed	0.25
Corn, sweet, stover	0.25
Cranberry	0.25
Currant	0.25
Egg	0.03
Goat, meat	0.03
Goat, meat byproducts	0.03
Grape	0.20
Grapefruit	0.25
Hazelnut	0.20
Horse, meat	0.03
Horse, meat byproducts	0.03
Lemon	0.25
Loganberry	0.20
Milk	0.03
Nut, macadamia	0.25
Olive	0.20
Orange	0.25
Peach	0.20
Pear	0.25
Pecan	0.20
Plum	0.20
Raspberry	0.20
Sheep, meat	0.03
Sheep, meat byproducts	0.03
Strawberry	0.25
Walnut	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, 2007; 72 FR 53454, Sept. 19, 2007]

§180.215 Naled; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as naled, resulting from the application of the pesticide to growing crops or from direct application to livestock and poultry, in or on the following raw agricultural commodities:

Commodity	Parts per million
Almond, hulls	0.5
Almond	0.5
Bean, dry, seed	0.5
Bean, succulent	0.5
Beet, sugar, roots	0.5
Beet, sugar, tops	0.5
Broccoli	1
Brussels sprouts	1
Cabbage	1
Cauliflower	1
Celery	3
Collards	3
Cotton, undelinted seed	0.5
Cucumber	0.5
Eggplant	0.5
Grape	0.5
Grapefruit	3
Grass, forage	10
Hop, dried cones	0.5
Kale	3
Legume, forage	10
Lemon	3
Melon	0.5
Orange, sweet	3
Peach	0.5
Pea, succulent	0.5
Pepper	0.5
Pumpkin	0.5
Safflower, seed	0.5
Spinach	3
Squash, summer	0.5
Squash, winter	0.5
Strawberry	1
Swiss chard	3
Tangerine	3
Tomato	0.5
Turnip, greens	3
Walnut	0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural commodities, except those otherwise listed in this section, from use of the pesticide for area pest (mosquito and fly) control.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 77 FR 59124, Sept. 26, 2012]

§180.217 Metiram; tolerances for residues.

(a) General. Tolerances are established for residues of a metiram (a mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those metiram residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity	Parts per million
Apple	0.5
Apple, pomace, wet	2
Banana¹	3
Grape, wine¹	5
Potato	0.2

¹There are no U.S. registrations on bananas and grape, wine as of April 29, 2011.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57074, Oct. 26, 1998, as amended at 76 FR 23891, Apr. 29, 2011]

§180.220 Atrazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4-ethylamino-6-isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylamino-s-triazine, 2-amino-4-chloro-6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.02
Cattle, meat	0.02
Cattle, meat byproducts	0.02
Corn, field, forage	1.5
Corn, field, grain	0.20
Corn, field, stover	0.5
Corn, pop, forage	1.5
Corn, pop, grain	0.20
Corn, pop, stover	0.5
Corn, sweet, forage	15
Corn, sweet, kernel plus cob with husks removed	0.20
Corn, sweet, stover	2.0
Goat, fat	0.02
Goat, meat	0.02
Goat, meat byproducts	0.02
Grass, forage	4.0
Grass, hay	4.0
Guava	0.05
Horse, fat	0.02
Horse, meat	0.02
Horse, meat byproducts	0.02
Milk	0.02
Nut, macadamia	0.20
Sheep, fat	0.02
Sheep, meat	0.02
Sheep, meat byproducts	0.02
Sorghum, forage, forage	0.25
Sorghum, grain, forage	0.25
Sorghum, grain, grain	0.20
Sorghum, grain, stover	0.50
Sugarcane, cane	0.20
Wheat, forage	1.5
Wheat, grain	0.10
Wheat, hay	5.0
Wheat, straw	0.50

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of atrazine, 2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural commodity when present therein as a result of application of atrazine to the growing crops in paragraph (a) of this section:

Commodity	Parts per million
Vegetable, leafy, except brassica, group 4	0.25

[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63 FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; 72 FR 53454, Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011]

§180.222 Prometryn; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities:

Commodity	Parts per million
Bean, snap, succulent	0.05
Carrot, roots	0.45
Celeriac, roots	0.05
Celeriac, tops	0.20
Celtuce	0.50
Cilantro, leaves	3.5
Coriander, dried leaves	9.0
Cotton, gin byproducts	1.0
Cottonseed subgroup 20C	0.25
Dill, oil	1.3
Dillweed, dried leaves	1.1
Dillweed, fresh leaves	0.30
Fennel, Florence, fresh leaves and stalk	0.50
Leaf petiole vegetable subgroup 22B	0.50
Okra	0.05
Parsley, dried leaves	1.5
Parsley, leaves	0.60
Pea, pigeon, seed	0.25
Sesame, seed	0.05
Swiss chard	0.50

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the following raw agricultural commodities.

Commodity	Parts per million
Barley, forage	0.3
Barley, hay	1.0
Barley, straw	0.3
Oat, forage	0.3
Oat, hay	1.0
Oat, straw	0.3
Rye, forage	0.3
Rye, hay	1.0
Rye, straw	0.3
Triticale, forage	0.3
Triticale, hay	1.0
Triticale, straw	0.3
Wheat, forage	0.3
Wheat, hay	1.0
Wheat, straw	0.3

[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60 FR 20434, Apr. 26, 1995; 63 FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; 74 FR 67108, Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013; 82 FR 57144, Dec. 4, 2017]

§180.225 Phosphine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of phosphine in or on the following raw agricultural commodities (RACs) resulting from post-harvest fumigation for the control of insects with phosphine gas or phosphide compounds that produce phosphine gas.

Commodity	Parts per million
Almond	0.1
Avocado	0.01
Banana	0.01
Barley, grain	0.1
Cabbage, Chinese, bok choy	0.01
Cabbage, Chinese, napa	0.01
Cacao bean, dried bean	0.1
Cashew	0.1
Citron, citrus	0.01
Coffee, bean, green	0.1
Corn, field, grain	0.1
Corn, pop, grain	0.1
Cotton, undelinted seed	0.1
Date, dried fruit	0.1
Dill, seed	0.01
Eggplant	0.01
Endive	0.01
Grapefruit	0.01
Hazelnut	0.1
Kumquat	0.01
Lemon	0.01
Lettuce	0.01
Lime	0.01
Mango	0.01
Millet, grain	0.1
Mushroom	0.01
Nut, brazil	0.1
Oat, grain	0.1
Okra	0.01
Orange, sweet	0.01
Papaya	0.01
Peanut	0.1
Pecan	0.1
Pepper	0.01
Persimmon	0.01
Pistachio	0.1
Rice, grain	0.1
Rye, grain	0.1
Safflower, seed	0.1
Salsify, tops	0.01
Sesame, seed	0.1
Sorghum, grain	0.1
Soybean, seed	0.1
Sunflower, seed	0.1
Sweet potato, roots	0.01
Tangelo	0.01
Tangerine	0.01
Tomato	0.01
Vegetable, legume, group 6, except soybean	0.01
Walnut	0.1
Wheat, grain	0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest treatment of pest burrows in agricultural and non-crop land areas.

Commodity	Parts per million
All raw agricultural commodities resulting from preharvest treatment of pest burrows	0.01

(3) Residues resulting from fumigation of processed food:

Commodity	Parts per million
Processed food	0.01

(4) Residues resulting from fumigation of animal feed:

Commodity	Parts per million
Animal feed	0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that registered by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a restriction to aerate the finished food/feed for 48 hours before it is offered to the consumer, unless EPA specifically determines that a different time period is appropriate. Where appropriate, a warning shall state that under no condition should any formulation containing aluminum or magnesium phosphide be used so that it will come in contact with any processed food, except processed brewer's rice, malt, and corn grits stored in breweries for use in the manufacture of beer.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007; 74 FR 46372, Sept. 9, 2009]

§180.226 Diquat; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the herbicide diquat, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a)(1) resulting from the application of the dibromide salt of diquat. Compliance with the tolerance levels specified in Table 1 to this paragraph (a)(1) is to be determined by measuring only diquat (6,7-dihydrodipyrido[1,2-a:2′,1′-c]pyrazinediium):

Commodity	Parts per million
Alfalfa, seed	3.0
Cattle, fat	0.05
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Canola, meal	6.0
Canola, seed	2.0
Egg	0.05
Goat, fat	0.05
Goat, meat	0.05
Goat, meat byproducts	0.05
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	0.05
Horse, meat	0.05
Horse, meat byproducts	0.05
Milk	0.02
Pea and bean, dry and shelled, except soybean, subgroup 6C¹	0.9
Potato	0.1
Poultry, fat	0.05
Poultry, meat	0.05
Poultry, meat byproducts	0.05
Sheep, fat	0.05
Sheep, meat	0.05
Sheep, meat byproducts	0.05

¹There are no U.S. registrations for these commodities as of October 22, 2020.

(2)(i) Tolerances are established for residues of the herbicide diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) (calculated as the cation) derived from the application of the dibromide salt to ponds, lakes, reservoirs, marshes, drainage ditches, canals, streams, and rivers which are slow-moving or quiescent in programs of the Corp of Engineers or other Federal or State public agencies and to ponds, lakes and drainage ditches only where there is little or no outflow of water and which are totally under the control of the user, in or on the following food commodities:

Commodity	Parts per million
Avocado	0.2
Berry group 13	0.05
Cotton, undelinted seed	0.2
Cranberry	0.05
Fish	2.0
Fruit, citrus, group 10	0.05
Fruit, pome, group 11	0.02
Fruit, stone, group 12	0.02
Grain, cereal, forage, fodder and straw, group 16	0.02
Grain, cereal, group 15	0.02
Grape	0.05
Grass, forage, fodder and hay, group 17	0.2
Hop, dried cones	0.2
Nut, tree, group 14	0.02
Shellfish	20.0
Strawberry	0.05
Sugarcane, cane	0.2
Vegetable, brassica, leafy, group 5	0.05
Vegetable, cucurbit, group 9	0.02
Vegetable, foliage of legume, group 7	0.2
Vegetable, fruiting, group 8	0.05
Vegetable, leafy, except brassica, group 4	0.05
Vegetable, root and tuber, group 1	0.02
Vegetable, seed and pod	0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the higher tolerances applies also to residues of the aquatic uses cited in this paragraph.

(3) Tolerances are established for the plant growth regulator diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) derived from application of the dibromide salt and calculated as the cation in or on the following food commodites:

Commodity	Parts per million
Banana¹	0.05
Coffee, bean, green¹	0.05
Soybean, hulls	0.6

¹There are no U.S. registrations as of May 26, 2010.

(4) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and potato, chips.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29, 2010; 85 FR 67290, Oct. 22, 2020]

§180.227 Dicamba; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the sum of the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-5-hydroxy-o-anisic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity	Parts per million
Barley, grain	6.0
Barley, hay	2.0
Barley, straw	15.0
Corn, field, forage	3.0
Corn, field, grain	0.1
Corn, field, stover	3.0
Corn, pop, grain	0.1
Corn, pop, stover	3.0
Corn, sweet, forage	0.50
Corn, sweet, kernel plus cob with husks removed	0.04
Corn, sweet, stover	0.50
Grass, forage, fodder and hay, group 17, forage	125.0
Grass, forage, fodder and hay, group 17, hay	200.0
Millet, proso, forage	90.0
Millet, proso, grain	2.0
Millet, proso, hay	40.0
Millet, proso, straw	30.0
Oat, forage	90.0
Oat, grain	2.0
Oat, hay	40.0
Oat, straw	30.0
Rye, forage	90.0
Rye, grain	2.0
Rye, straw	30.0
Sorghum, grain, forage	3.0
Sorghum, grain, grain	4.0
Sorghum, grain, stover	10.0
Sugarcane, cane	0.3
Sugarcane, molasses	5.0
Teff, forage	90.0
Teff, grain	6.0
Teff, hay	40.0
Teff, straw	30.0
Wheat, forage	90.0
Wheat, grain	2.0
Wheat, hay	40.0
Wheat, straw	30.0

(2) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity	Parts per million
Asparagus	4.0
Cattle, fat	0.3
Cattle, kidney	25.0
Cattle, meat	0.25
Cattle, meat byproducts, except kidney	3.0
Goat, fat	0.3
Goat, kidney	25.0
Goat, meat	0.25
Goat, meat byproducts, except kidney	3.0
Hog, fat	0.3
Hog, kidney	25.0
Hog, meat	0.25
Hog, meat byproducts, except kidney	3.0
Horse, fat	0.3
Horse, kidney	25.0
Horse, meat	0.25
Horse, meat byproducts, except kidney	3.0
Milk	0.2
Sheep, fat	0.3
Sheep, kidney	25.0
Sheep, meat	0.25
Sheep, meat byproducts, except kidney	3.0

(3) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only the residues of dicamba, 3,6-dichloro-o-anisic acid, and its metabolites, 3,6-dichloro-5-hydroxy-o-anisic acid, and 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity	Parts per million
Cotton, gin byproducts	70
Cotton, undelinted seed	3.0
Grain, aspirated fractions	1000
Soybean, forage	60
Soybean, hay	100
Soybean, hulls	30.0
Soybean, seed	10.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73 FR 54960, Sept. 24, 2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011; 81 FR 88634, Dec. 8, 2016]

§180.229 Fluometuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities:

Commodity	Parts per million
Cotton, gin byproducts	3.5
Cotton, undelinted seed	1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N,N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites: CGA-236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea; and CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or on the following food commodities:

Commodity	Parts per million
Cattle, meat byproducts	0.1
Egg	0.1
Goat, meat byproducts	0.1
Hog, meat byproducts	0.1
Horse, meat byproducts	0.1
Milk	0.02
Poultry, fat	0.1
Poultry, meat	0.1
Poultry, meat byproducts	0.1
Sheep, meat byproducts	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the following food commodities.

Commodity	Parts per million
Grain, cereal, forage, fodder, and straw group 16, forage	3.0
Grain, cereal, forage, fodder, and straw, group 16, stover	6.0
Grain, cereal, group 15	0.5
Peanut	0.1
Peanut, hay	4.0
Peanut, meal	0.2
Soybean, forage	3.0
Soybean, hay	3.0
Soybean, seed	2.0
Rice, hulls	1.0
Wheat, milled byproducts	1.0

[73 FR 52613, Sept. 10, 2008]

§180.231 Dichlobenil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide dichlobenil (2,6-dichlorobenzonitrile) and its metabolite 2,6-dichlorobenzamide in or on the following raw agricultural commodities:

Commodity	Parts per million
Apple	0.5
Bushberry subgroup 13-07B	0.15
Caneberry subgroup 13-07A	0.10
Cranberry	0.1
Fruit, stone, group 12	0.15
Grape	0.15
Hazelnut	0.1
Pear	0.5
Rhubarb	0.06

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73 FR 50570, Aug. 27, 2008]

§180.235 Dichlorvos; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as follows:

Commodity	Parts per million
Cattle, fat	0.02(N)
Cattle, meat	0.02(N)
Cattle, meat byproducts	0.02(N)
Egg	0.05(N)
Goat, fat	0.02(N)
Goat, meat	0.02(N)
Goat, meat byproducts	0.02(N)
Horse, fat	0.02(N)
Horse, meat	0.02(N)
Horse, meat byproducts	0.02(N)
Milk	0.02(N)
Mushroom (residues expressed as naled)	0.5
Poultry, fat	0.05(N)
Poultry, meat	0.05(N)
Poultry, meat byproducts	0.05(N)
Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, postharvest	0.5
Raw agricultural commodities nonperishable, packaged or bagged, containing 6 percent fat or less, postharvest	0.5
Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest	2
Sheep, fat	0.02(N)
Sheep, meat	0.02(N)
Sheep, meat byproducts	0.02(N)

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2-dichlorovinyl dimethyl phosphate in hog, fat; hog, meat; hog, meat byproducts; and hog, skin covers both its use as an anthelmintic in swine feed and as an insecticide applied directly to swine.

(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged nonperishable processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). To assure safe use of the insecticide, its label and labeling shall conform to the label and labeling registered by the U.S. Environmental Protection Agency, and the usage employed shall conform with such label or labeling.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991; 63 FR 57075, Oct. 26, 1998; 65 FR 33697, May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR 59125, Sept. 26, 2012]

§180.236 Triphenyltin hydroxide; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide (TPTH) and its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites, expressed in terms of parent TPTH, in or on the following raw agricultural commodities:

Commodity	Parts per million
Beet, sugar, roots	0.05
Beet, sugar, tops	10.0
Cattle, fat	0.2
Cattle, kidney	2.0
Cattle, liver	4.0
Cattle, meat	0.5
Goat, fat	0.2
Goat, kidney	2.0
Goat, liver	4.0
Goat, meat	0.5
Hog, fat	0.3
Hog, meat	0.06
Hog, meat byproducts	0.3
Horse, fat	0.2
Horse, kidney	2.0
Horse, liver	4.0
Horse, meat	0.5
Milk	0.06
Pecan	0.05
Potato	0.05
Sheep, fat	0.2
Sheep, kidney	2.0
Sheep, liver	4.0
Sheep, meat	0.5

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 41929, Aug. 1, 2007]

§180.241 Bensulide; tolerances for residues.

(a) General. Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity	Parts per million
Onion, bulb	0.10
Vegetable, brassica, leafy group 5	0.15
Vegetable, cucurbits group 9	0.15
Vegetable, fruiting group 8	0.10
Vegetable, leafy except brassica group 4	0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity	Parts per million
Carrot, roots	0.10

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

§180.242 Thiabendazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	0.02
Alfalfa, hay	0.02
Apple, wet pomace	12.0
Avocado¹	10.0
Banana, postharvest	3.0
Barley, grain	0.05
Barley, hay	0.30
Barley, straw	0.30
Bean, dry, seed²	0.1
Brassica, head and stem, subgroup 5A	0.02
Cantaloupe¹	15.0
Carrot, roots, postharvest	10.0
Citrus, oil	15.0
Corn, field, forage	0.01
Corn, field, grain	0.01
Corn, field, stover	0.01
Corn, pop, forage	0.01
Corn, pop, grain	0.01
Corn, pop, stover	0.01
Corn, sweet, forage	0.01
Corn, sweet, kernels plus cop with husks removed	0.01
Corn, sweet, stover	0.01
Fruit, citrus, group 10, postharvest	10.0
Fruit, pome, group 11, postharvest	5.0
Mango	10.0
Mushroom	40.0
Oats, forage	0.30
Oats, grain	0.05
Oats, hay	0.30
Oats, straw	0.30
Onion, bulb, subgroup 3-07A	0.02
Papaya, postharvest	5.0
Potato, postharvest	10.0
Radish, tops	0.02
Rye, forage	0.30
Rye, grain	0.05
Rye, straw	0.30
Soybean²	0.1
Spinach	0.02
Strawberry¹	5.0
Sweet potato (postharvest to sweet potato intended only for use as seed)	0.05
Triticale, forage	0.30
Triticale, grain	0.05
Triticale, hay	0.30
Triticale, straw	0.30
Vegetable, cucurbit, group 9	0.02
Vegetable, foliage of legume, group 7	0.20
Vegetable, legume, group 6	0.02
Vegetable, root (except sugarbeet), subgroup 1B	0.02
Wheat, forage	0.30
Wheat, grain	0.05
Wheat, hay	0.30
Wheat, straw	0.30

¹There are no U.S. registrations on the indicated commodity.

²This tolerance expires on March 21, 2017.

(2) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free and conjugated) and benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

Commodity	Parts per million
Cattle, meat	0.1
Cattle, meat byproducts	0.4
Goat, meat byproducts	0.4
Hog, meat byproducts	0.3
Horse, meat byproducts	0.4
Milk	0.1
Sheep, meat byproducts	0.4

(b) Section 18 emergency exemptions. Time-limited tolerances specified in table 3 to this paragraph (b) are established for residues of the thiabendazole, including its metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in table 3 to this paragraph (b) is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole. The tolerances expire on the date specified in table 3 to this paragraph (b).

Commodity	Parts per million	Expiration/ revocation date
Sweet potato	10	12/31/22

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 32783, June 28, 1977]

Editorial Note: For Federal Register citations affecting §180.242, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.243 Propazine; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of propazine, 2-chloro-4,6-bis(isopropylamino)-s-triazine, and its two chlorinated degradates, 2-amino-4-chloro-6-isopropylamino-s-triazine and 2,4-diamino-6-chloro-s-triazine, calculated as the stoichiometric equivalent of propazine, in or on the commodity.

Commodity	Parts per million
Sorghum, grain, forage	0.25
Sorghum, grain, grain	0.25
Sorghum, grain, stover	0.25

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60242, Sept. 29, 2010]

§180.245 Streptomycin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide streptomycin, including its metabolites and degradates, in or on the commodities in Table 1 to this paragraph (a). Compliance with the tolerance levels specified in Table 1 to this paragraph (a) is to be determined by measuring only streptomycin (O-2-Deoxy-2-(methylamino)-a-Lglucopyranosyl-(1-2)-O-5-deoxy-3-Cformyl-a-L-lyxofuranosyl-(1-4)-N,N′-bis(aminoiminomethyl)-D-streptamine) in or on the commodity.

Table 1 to Paragraph (a)

Commodity	Parts per million
Bean, dry, seed	0.5
Bean, succulent	0.5
Celery	0.25
Fruit, citrus, group 10-10	0.8
Fruit, citrus, group 10-10, dried pulp	3
Fruit, pome, group 11	0.25
Pepper	0.25
Potato	0.25
Tomato	0.25

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of streptomycin, in or on the agricultural commodities, as specified in Table 2 to this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance levels listed in Table 2 to this paragraph (b) is to be determined by measuring the levels of streptomycin only, in or on the commodities listed in this Table 2 paragraph (b). The tolerances expire on the dates specified in Table 2 to this paragraph (b).

Table 2 to Paragraph (b)

Commodity	Parts per million	Expiration date
Fruit, citrus, group 10-10	2.0	12/31/22
Fruit, citrus, group 10-10, dried pulp	6.0	12/31/22

(c)-(d) [Reserved]

[86 FR 8710, Feb. 9, 2021]

§180.249 Alachlor; tolerances for residues.

(a) General. Tolerances are established for combined residues of alachlor (2-chloro-2′,6″-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the following raw agricultural commodities.

Commodity	Parts per million
Beans, dry	0.1
Beans, succulent lima	0.1
Cattle, fat	0.02
Cattle, meat byproducts	0.02
Cattle, meat	0.02
Corn, field, forage	2.0
Corn, field, grain	0.2
Corn, field, pop	0.2
Corn, field, stover	2.0
Corn, pop, stover	2.0
Corn, sweet (K + CWHR)	0.05
Corn, sweet, stover	2.0
Cotton, gin byproducts	0.7
Cotton, undelinted seed	0.03
Cowpea, forage	5.0
Cowpea, hay	5.0
Egg	0.02
Goat, fat	0.02
Goat, meat byproducts	0.02
Goat, meat	0.02
Hog, fat	0.02
Hog meat byproducts	0.02
Hog, meat	0.02
Horse, fat	0.02
Horse, meat byproducts	0.02
Horse, meat	0.02
Milk	0.02
Peanut	0.5
Poultry, fat	0.02
Poultry, meat byproducts	0.02
Poultry, meat	0.02
Sheep, fat	0.02
Sheep, meat byproducts	0.02
Sheep, meat	0.02
Sorghum grain, forage	2.0
Sorghum, grain, grain	0.1
Sorghum, grain, stover	1.0
Soybeans, seed	1.0
Sunflower, meal	3.4
Sunflower, seed	2.5

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of alachlor (2-chloro-2′,6′-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor, in or on the following raw agricultural commodities when present therein as a result of the application of alachlor to the growing crops in paragraph (a) of this section:

Commodity	Parts per million
Animal feed, nongrass, group 18, forage	1.4
Animal feed, nongrass, group 18, hay	1.2
Grain, cereal, forage, and straw, group 16 except corn, sorghum, rice, straw	0.8
Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage	0.6
Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay	0.8
Grain, cereal, group 15 except corn, sorghum, rice	0.05

[72 FR 54584, Sept. 26, 2007]

§180.252 Tetrachlorvinphos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tetrachlorvinphos [(Z)-2-chloro-1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate], including its metabolites, 1-(2,4,5-trichlorophenyl)-ethanol (free and conjugated forms), 2,4,5-trichloroacetophenone, and 1-(2,4,5-trichlorophenyl)-ethanediol, in or on the following commodities:

Commodity	Parts per million
Cattle, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)	0.2
Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)	1.0
Cattle, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)	0.5
Cattle, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)	2.0
Cattle, meat byproducts, except kidney and liver	1.0
Egg (of which no more than 0.05 ppm is tetrachlorvinphos per se)	0.2
Hog, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se)	0.2
Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se)	1.0
Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)	0.5
Hog, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se)	2.0
Hog, meat byproducts, except kidney and liver	1.0
Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is tetrachlorvinphos per se)	0.05
Poultry, fat (of which no more than 7.0 ppm is tetrachlorvinphos per se)	7.0
Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se)	2.0
Poultry, meat (of which no more than 3.0 ppm is tetrachlorvinphos per se)	3.0
Poultry, meat byproducts, except liver	2.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 57659, Sept. 16, 2011, as amended at 78 FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, 2013]

§180.253 Methomyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

Commodity	Parts per million	Expiration/revocation date
Alfalfa, forage	10	None
Alfalfa, hay	10	None
Apple	1	None
Asparagus	2	None
Avocado	2	None
Barley, grain	1	None
Barley, hay	10	None
Barley, straw	10	None
Bean, dry, seed	0.1	None
Bean, forage	10	None
Bean, succulent	2	None
Beet, garden, tops	6	None
Bermudagrass, forage	10	None
Bermudagrass, hay	40	None
Blueberry	6	None
Broccoli	3	None
Brussels sprouts	2	None
Cabbage	5	None
Cabbage, Chinese, bok choy	5	None
Cabbage, Chinese, napa	5	None
Cauliflower	2	None
Celery	3	None
Collards	6	None
Corn, field, forage	10	None
Corn, field, grain	0.1	None
Corn, field, stover	10	None
Corn, pop, grain	0.1	None
Corn, pop, stover	10	None
Corn, sweet, forage	10	None
Corn, sweet, kernel plus cob with husks removed	0.1	None
Corn, sweet, stover	10	None
Cotton, undelinted seed	0.1	None
Dandelion, leaves	6	None
Endive	5	None
Grape	5	12/31/16
Grapefruit	2	None
Hop, dried cones¹	12	None
Kale	6	None
Lemon	2	None
Lentil, seed	0.1	None
Lettuce	5	None
Mustard greens	6	None
Nectarine	5	None
Oat, forage	10	None
Oat, grain	1	None
Oat, hay	10	None
Oat, straw	10	None
Onion, dry bulb	0.2	None
Onion, green	3	None
Orange	2	None
Parsley, leaves	6	None
Pea	5	None
Pea, field, vines	10	None
Peach	5	None
Peanut	0.1	None
Pecan	0.1	None
Pepper, bell	2	None
Pepper, nonbell	2	None
Peppermint, tops	2	None
Pomegranate	0.2	None
Rye, forage	10	None
Rye, grain	1	None
Rye, straw	10	None
Sorghum, grain, forage	1	None
Sorghum, grain, grain	0.2	None
Soybean, forage	10	None
Soybean, seed	0.2	None
Spearmint, tops	2	None
Spinach	6	None
Swiss chard	6	None
Tangerine	2	None
Tomato	1	None
Turnip, greens	6	None
Vegetable, brassica, leafy, group 5	6.0	None
Vegetable, cucurbit, group 9	0.2	None
Vegetable, fruiting, group 8	0.2	None
Vegetables, leafy²	0.2	None
Vegetable, root and tuber, group 1	0.2	None
Wheat, forage	10	None
Wheat, grain	1	None
Wheat, hay	10	None
Wheat, straw	10	None

¹There are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.

²Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards, dandelions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and watercress.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

Commodity	Parts per million
Pear	4

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR 72598, Nov. 20, 2015]

§180.254 Carbofuran; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide carbofuran (2,3-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benzofuranyl-N-methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on the following raw agricultural commodities:

Commodity	Parts per million
Banana¹	0.1
Coffee, bean, green¹	0.1
Rice, grain¹	0.2
Sugarcane, cane¹	0.1

¹There are no U.S. registrations for use of carbofuran on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[39 FR 20597, June 12, 1974]

Editorial Note: For Federal Register citations affecting §180.254, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.258 Ametryn; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4-(isopropylamino)-6-(methylthio)-s-triazine in or on the following raw agricultural commodities:

Commodity	Parts per million	Expiration/Revocation Date
Banana	0.25	6/16/10
Corn, field, forage	0.1	None
Corn, field, grain	0.05	None
Corn, field, stover	0.05	None
Corn, pop, grain	0.05	None
Corn, pop, stover	0.05	None
Corn, sweet, forage	0.5	6/16/10
Corn, sweet, kernel plus cob with husks removed	0.25	6/16/10
Corn, sweet, stover	0.5	6/16/10
Pineapple	0.05	None
Sugarcane, cane	0.05	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52 FR 33237, Sept. 2, 1987; 63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009]

§180.259 Propargite; tolerances for residues.

(a) General. Tolerances are established for residues of the pesticide propargite (2-(p-tert-butylphenoxy) cyclohexyl 2-propynyl sulfite) in or on the following food commodities.

Commodity	Parts per million
Almond	0.1
Almond, hulls	55.0
Bean, dry, seed	0.2
Cattle, fat	0.1
Cattle, meat	0.1
Cattle, meat byproducts	0.1
Citrus, oil	30.0
Corn, field, forage	10.0
Corn, field, grain	0.1
Corn, field, stover	10.0
Corn, pop, grain	0.1
Corn, pop, stover	10.0
Corn, sweet, forage	10.0
Corn, sweet, stover	10.0
Cotton, undelinted seed	0.1
Egg	0.1
Goat, fat	0.1
Goat, meat	0.1
Goat, meat byproducts	0.1
Grain, aspirated fractions	0.4
Grape	10.0
Grapefruit	5.0
Hog, fat	0.1
Hog, meat	0.1
Hog, meat byproducts	0.1
Hop, dried cones	100.0
Horse, fat	0.1
Horse, meat	0.1
Horse, meat byproducts	0.1
Lemon	5.0
Milk, fat (0.08 ppm in milk)	2.0
Nectarine	4.0
Orange	10.0
Peanut	0.1
Peppermint, tops	50.0
Poultry, fat	0.1
Potato	0.1
Sheep, fat	0.1
Sheep, meat	0.1
Sheep, meat byproducts	0.1
Sorghum, grain, forage	10.0
Sorghum, grain, grain	5.0
Sorghum, grain, stover	10.0
Spearmint, tops	50.0
Tea, dried	10.0
Walnut	0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of propargite in or on the following raw agricultural commodities:

Commodity	Parts per million
Corn, sweet, kernel plus cob with husks removed	0.1

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 76 FR 34885, June 15, 2011]

§180.261 Phosmet; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	20
Alfalfa, hay	40
Almond, hulls	10
Apple	10
Apricot	5
Blueberry	10
Cattle, fat	0.2
Cattle, meat	0.1
Cattle, meat byproducts	0.1
Cherry	10
Cranberry	10
Fruit, citrus, group 10	5
Goat, fat	0.1
Goat, meat	0.1
Goat, meat byproducts	0.1
Grape	10
Hog, fat	0.2
Hog, meat	0.04
Hog, meat byproducts	0.04
Horse, fat	0.1
Horse, meat	0.1
Horse, meat byproducts	0.1
Kiwifruit	25
Milk	0.1
Nectarine	5
Nut, tree, group 14	0.1
Pea, dry, seed	0.5
Pea, field, hay	20
Pea, field, vines	10
Pea, succulent	1
Peach	10
Pear	10
Plum, prune, fresh	5
Potato	0.1
Sheep, fat	0.1
Sheep, meat	0.1
Sheep, meat byproducts	0.1
Sweet potato, roots	12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

Commodity	Parts per million
Crabapple	20
Pistachio	0.1

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52 FR 48539, Dec. 23, 1987; 53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 46698, Sept. 11, 2009; 75 FR 60242, Sept. 29, 2010]

§180.262 Ethoprop; tolerances for residues.

(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only ethoprop, O-ethyl S,S-dipropyl phosphorodithioate, in or on the commodity.

Commodity	Parts per million
Banana	0.02
Bean, lima	0.02
Bean, snap, succulent	0.02
Cabbage	0.02
Corn, field, forage	0.02
Corn, field, grain	0.02
Corn, field, stover	0.02
Corn, sweet, forage	0.02
Corn, sweet, kernel plus cob with husks removed	0.02
Corn, sweet, stover	0.02
Cucumber	0.02
Hop, dried cones	0.02
Peppermint, tops	0.02
Pineapple¹	0.02
Potato	0.02
Spearmint, tops	0.02
Sugarcane, cane	0.02
Sweet potato, roots	0.02

¹There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, distribution, and use is allowed, provided it is consistent with the terms of the cancellation order of July 9, 2009; i.e., the EPA will allow the technical registrant to continue to sell and distribute existing stocks of the amended registered product bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided that such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified product.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988; 63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731, Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010]

§180.269 Aldicarb; tolerances for residues.

(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-methyl-2-(methylthio)propionaldehyde O-(methylcarbamoyl) oxime and its cholinesterase-inhibiting metabolites 2-methyl 2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde O-(methylcarbamoyl) oxime in or on the following food commodities:

Commodity	Parts per million
Bean, dry, seed	0.1
Beet, sugar, roots	0.05
Beet, sugar, tops	1
Citrus, dried pulp	0.6
Coffee, bean, green	0.1
Cotton, undelinted seed	0.1
Cotton, hulls	0.3
Grapefruit	0.3
Lemon	0.3
Lime	0.3
Orange, sweet	0.3
Peanut	0.05
Pecan	0.5
Potato	1
Soybean	0.02
Sugarcane, cane	0.02
Sweet potato, roots	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016]

§180.272 Tribuphos; tolerances for residues.

(a) General. Tolerances are established for residues of the defoliant tribuphos (S,S,S-tributyl phosphorotrithioate) in or on food commodities as follows:

Commodity	Parts per million
Cattle, fat	0.15
Cattle, meat	0.02
Cattle, meat byproducts	0.02
Cotton, gin byproducts	40.0
Cotton, undelinted seed	4.0
Goat, fat	0.15
Goat, meat	0.02
Goat, meat byproducts	0.02
Hog, fat	0.15
Hog, meat	0.02
Hog, meat byproducts	0.02
Horse, fat	0.15
Horse, meat	0.02
Horse, meat byproducts	0.02
Milk	0.01
Sheep, fat	0.15
Sheep, meat	0.02
Sheep, meat byproducts	0.02

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

§180.274 Propanil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propanil (3′, 4′-dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.10
Cattle, meat	0.05
Cattle, meat byproducts	1.0
Crayfish	0.05
Egg	0.30
Goat, fat	0.10
Goat, meat	0.05
Goat, meat byproducts	1.0
Hog, fat	0.10
Hog, meat	0.05
Hog, meat byproducts	1.0
Horse, fat	0.10
Horse, meat	0.05
Horse, meat byproducts	1.0
Milk	0.05
Poultry, fat	0.05
Poultry, meat	0.10
Poultry, meat byproducts	0.50
Rice, bran	40
Rice, grain	10
Rice, hulls	30
Sheep, fat	0.10
Sheep, meat	0.05
Sheep, meat byproducts	1.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007; 80 FR 72598, Nov. 20, 2015]

§180.275 Chlorothalonil; tolerances for residues.

(a) General. (1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity	Parts per million
Almond	0.05
Almond, hulls	1.0
Apricot	0.5
Asparagus	0.1
Banana (NMT 0.05 ppm in edible pulp)	0.5
Bean, dry, seed	0.1
Bean, snap, succulent	5
Blueberry	1.0
Brassica, head and stem, subgroup 5A	5.0
Carrot, roots	1
Celery	15
Cherry, sweet	0.5
Cherry, tart	0.5
Cocoa bean, dried bean	0.05
Coffee, bean, green	0.20
Corn, sweet, kernel plus cob with husks removed	1
Cranberry	5.0
Ginseng	4.0
Horseradish	4.0
Lentil	0.10
Lychee	15
Mango	1.0
Mushroom	1.0
Nectarine	0.5
Okra	6.0
Onion, bulb	0.5
Onion, green	5
Papaya	15
Parsnip, roots	1
Passionfruit	3
Pea, edible podded	5
Peach	0.5
Peanut	0.3
Pistachio	0.2
Plum	0.2
Plum, prune	0.2
Potato	0.1
Rhubarb	4.0
Soybean	0.2
Starfruit	3.0
Tomato	5
Vegetable, cucurbit, group 9	5.0
Vegetable, fruiting, group 8, except tomato	6.0
Yam, true	0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities.

Commodity	Parts per million
Cattle, fat	0.1
Cattle, kidney	0.5
Cattle, meat byproducts, except kidney	0.05
Cattle, meat	0.03
Goat, fat	0.1
Goat, kidney	0.5
Goat, meat byproducts, except kidney	0.05
Goat, meat	0.03
Hog, fat	0.1
Hog, kidney	0.5
Hog, meat byproducts, except kidney	0.05
Hog, meat	0.03
Horse, fat	0.1
Horse, kidney	0.5
Horse, meat byproducts, except kidney	0.05
Horse, meat	0.03
Milk	0.1
Sheep, fat	0.1
Sheep, kidney	0.5
Sheep, meat byproducts, except kidney	0.05
Sheep, meat	0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined residues of chlorothalonil and its metabolite in or on the following raw agricultural commodities:

Commodity	Parts per million
Hazelnut	0.1
Peppermint, tops	2
Persimmon	1.5
Spearmint, tops	2

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 56114, Oct. 21, 1977]

Editorial Note: For Federal Register citations affecting §180.275, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.276 Formetanate hydrochloride; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide formetanate hydrochloride, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only formetanate hydrochloride, N,N-dimethyl-N'-[3-[(methylamino)carbonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity.

Commodity	Parts per million	Expiration/revocation date
Apple	0.50	12/31/13
Apple, wet pomace	1.5	12/31/13
Grapefruit	1.5	None
Lemon	0.60	None
Lime	0.03	None
Nectarine	0.40	None
Orange	1.5	None
Peach	0.40	12/31/13
Pear	0.50	12/31/13
Tangelo	0.03	None
Tangerine	0.03	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

§180.278 Phenmedipham; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide phenmedipham (3-methoxycarbonylaminophenyl-3′-methylcarbanilate) in or on the following food commodities:

Commodity	Parts per million
Beet, garden, roots	0.2
Beet, garden, tops	0.2
Beet, sugar, dried pulp	0.5
Beet, sugar, molasses	0.2
Beet, sugar, roots	0.1
Beet, sugar, tops	0.1
Spinach	4.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007]

§180.284 Zinc phosphide; tolerances for residues.

(a) General. Tolerances are established for residues of the phosphine resulting from the use of the rodenticide zinc phosphide in or on the raw agricultural commodities as follows:

Commodity	Parts per million
Alfalfa, forage	0.2
Alfalfa, hay	0.2
Barley, grain	0.05
Barley, hay	0.2
Barley, straw	0.2
Bean, dry, seed	0.05
Beet, sugar, roots	0.05
Beet, sugar, tops	0.2
Grape	0.01
Grass, rangeland, forage	0.1
Grass, rangeland, hay	0.1
Potato	0.05
Sugarcane, cane	0.01
Timothy, hay	0.5
Timothy, forage	0.5
Wheat, forage	0.05
Wheat, grain	0.05
Wheat, hay	0.05
Wheat, straw	0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on the following raw agricultural commodities as follows:

Commodity	Parts per million
Artichoke, globe	0.01
Beet, sugar, roots	0.04
Beet, sugar, tops	0.02

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999; 65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011]

§180.287 Amitraz; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N-[[(2,4-dimethylphenyl)imino]methyl]]-N-methylmethanimidamide), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring amitraz residues convertible to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, in or on the following raw agricultural commodities:

Commodity	Parts per million
Cattle, fat	0.1
Cattle, meat	0.02
Cattle, meat byproducts	0.2
Hog, fat	0.1
Hog, kidney	0.1
Hog, liver	0.1
Hog, meat	0.05
Hog, meat byproducts	0.3
Honey	0.2
Honeycomb	9
Milk	0.03
Milk, fat	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; 74 FR 47456, Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013; 80 FR 72598, Nov. 20, 2015]

§180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole in or on the following food commodities:

Commodity	Parts per million
Barley, grain	0.1(N)
Barley, straw	0.1(N)
Beet, sugar, roots	0.1(N)
Beet, sugar, tops	0.1(N)
Corn, field, forage	0.1(N)
Corn, field, grain	0.1
Corn, field, stover	0.1
Corn, pop, grain	0.1
Corn, pop, stover	0.1
Cotton, forage	0.1(N)
Cotton, undelinted seed	0.1(N)
Oat, forage	0.1(N)
Oat, grain	0.1(N)
Oat, hay	0.1(N)
Oat, straw	0.1(N)
Rice, grain	0.1(N)
Safflower, seed	0.1(N)
Sorghum, grain, forage	0.1(N)
Sorghum, grain, grain	0.1(N)
Sorghum, grain, stover	0.1(N)
Wheat, forage	0.1(N)
Wheat, grain	0.1(N)
Wheat, hay	0.1(N)
Wheat, straw	0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 74 FR 46374, Sept. 9, 2009; 80 FR 72598, Nov. 20, 2015]

§180.289 Methanearsonic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide methanearsonic acid, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methanearsonic acid, from application of the disodium and monosodium salts of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, in or on the commodity.

Commodity	Parts per million	Expiration/Revocation Date
Cotton, undelinted seed	0.7	None
Cotton, hulls	0.9	None
Fruit, citrus	0.35	12/31/12

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 77 FR 59126, Sept. 26, 2012]

§180.291 Pentachloronitrobenzene; tolerance for residues.

(a) General. Tolerances are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity	Parts per million
Bean	0.1
Brassica, head and stem, subgroup 5A	0.1
Cotton, undelinted seed	0.1
Garlic, bulb	0.1
Peanut	1.0
Potato	0.1
Soybean, forage	0.02
Soybean, hay	0.02
Soybean, seed	0.02
Vegetable, fruiting, group 8	0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity	Parts per million
Collards	0.2
Kale	0.2
Mustard, greens	0.2

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47456, Sept. 16, 2009]

§180.292 Picloram; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide picloram, 4-amino-3,5,6-trichloropicolinic acid, including its metabolites and degradates, in or on the commodities in the following table from its application in the acid form or in the form of its salts. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only picloram, 4-amino-3,5,6-trichloropicolinic acid, in or on the commodity.

Commodity	Parts per million
Barley, grain	0.5
Barley, pearled barley	3.0
Barley, straw	1.0
Cattle, fat	0.4
Cattle, meat	0.4
Cattle, meat byproducts	15
Egg	0.05
Goat, fat	0.4
Goat, meat	0.4
Goat, meat byproducts	15
Grain, aspirated fractions	4.0
Grass, forage	400
Grass, hay	225
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	0.4
Horse, meat	0.4
Horse, meat byproducts	15
Milk	0.25
Oat, forage	1.0
Oat, grain	0.5
Oat, groats/rolled oats	3.0
Oat, straw	1.0
Poultry, fat	0.05
Poultry, meat	0.05
Poultry, meat byproducts	0.05
Sheep, fat	0.4
Sheep, meat	0.4
Sheep, meat byproducts	15
Wheat, bran	3.0
Wheat, forage	1.0
Wheat, germ	3.0
Wheat, grain	0.5
Wheat, middlings	3.0
Wheat, shorts	3.0
Wheat, straw	1.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72 FR 41930, Aug. 1, 2007; 75 FR 60243, Sept. 29, 2010]

§180.293 Endothall; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of endothall, including its metabolites and degradates, in or on the commodities in the table, below. Compliance with the tolerance levels specified, below, is to be determined by measuring only endothall (7-oxabicylco [2.2.1] heptanes-2,3-dicarboxylic acid) and its mono-methyl ester.

Commodity	Parts per million
Apple	0.05
Apple, wet pomace	0.15
Cotton, undelinted seed	0.1
Fish	0.1
Hop, dried cones	0.1
Potato	0.1
Rice, grain	0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di-N, N-dimethylalkylamine, and mono-N-N,-dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potential sources of water, potable.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent combined residues of the herbicide, endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in potable water from use of its potassium, sodium, di-N, N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other potable water sources that may lead to endothall residues in or on the following commodities:

Commodity	Parts per million
Almond, hulls	15.0
Animal feed, nongrass, group 18, forage	4.0
Animal feed, nongrass, group 18, hay	10
Apple, wet pomace	0.15
Beet, sugar, molasses	1.5
Brassica, head and stem subgroup 5A	0.1
Brassica, leafy, subgroup 5B	2.0
Bushberry subgroup 13-07B	0.6
Caneberry subgroup 13-07A	0.6
Cattle, fat	0.05
Cattle, kidney	0.05
Cattle, kidney¹	0.20
Cattle, liver¹	0.10
Cattle, liver	0.05
Cattle, meat	0.05
Corn, field, grain	0.07
Corn, pop, grain	0.07
Corn, sweet, kernel plus cob with husks removed	0.3
Citrus, dried pulp	0.1
Egg	0.05
Feed commodities not otherwise listed	10.0
Food commodities not otherwise listed	5.0
Fruit, citrus group 10	0.05
Fruit, pome, group 11	0.05
Fruit, stone, group 12	0.3
Goat, fat	0.05
Goat, kidney¹	0.15
Goat, kidney	0.05
Goat, liver	0.05
Goat, meat	0.05
Grain, aspirated fractions	35.0
Grain cereal, forage, fodder and straw, group 16	10.0
Grain, cereal, group 15, except corn	4.0
Grape	1.0
Grape, raisin	5.0
Grass, forage, fodder, and hay group 17, forage	3.5
Grass, forage, fodder, and hay group 17, hay	18.0
Herb and spice, group 19	5.0
Hog, fat	0.05
Hog, kidney¹	0.10
Hog, kidney	0.05
Hog, liver	0.05
Hog, meat	0.05
Milk¹	0.03
Milk	0.01
Nut, tree, group 14	0.05
Okra	0.05
Pea and bean, dried shelled, subgroup 6C	0.2
Pea and bean, succulent shelled, subgroup 6B	2.0
Peppermint, tops	5.0
Pistachio	0.05
Poultry, fat	0.05
Poultry, liver	0.05
Poultry, meat	0.05
Poultry, meat byproducts¹	0.20
Poultry, meat byproducts	0.05
Rice, hulls	8.0
Sheep, fat	0.05
Sheep, kidney¹	0.15
Sheep, kidney	0.05
Sheep, liver	0.05
Sheep, meat	0.05
Soybean, hulls	0.5
Soybean, seed	0.2
Spearmint, tops	5.0
Tomato, paste	0.1
Tomato, puree	0.1
Vegetable, bulb, group 3-07	0.5
Vegetable, cucurbit, group 9	1.5
Vegetable, foliage of legume, group 7	4.0
Vegetable, fruiting, group 8	0.05
Vegetable, leafy, except brassica, group 4	2.0
Vegetable, leaves of root and tuber, group 2	3.0
Vegetable, legume, edible, podded, subgroup 6A	2.0
Vegetable, root and tuber, group 1	1.0
Wheat, milled byproducts	5.0

¹This tolerance expires on May 22, 2017.

[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63 FR 42249, Aug. 7, 1998; 67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; 74 FR 67097, Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013; 80 FR 72598, Nov. 20, 2015; 81 FR 83169, Nov. 21, 2016]

§180.297 N-1-Naphthyl phthalamic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide N-1-naphthyl phthalamic acid from application of its sodium salt in or on the following raw agricultural commodities:

Commodity	Parts per million
Cantaloupe	0.1(N)
Cucumber	0.1(N)
Muskmelon	0.1(N)
Watermelon	0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

§180.298 Methidathion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in or on the commodity.

Commodity	Parts per million	Expiration/revocation date
Almond, hulls	6.0	12/31/16
Artichoke, globe	0.05	12/31/16
Citrus, oil	420.0	12/31/16
Cotton, undelinted seed	0.2	12/31/16
Fruit, citrus, group 10, except tangerine	4.0	12/31/16
Fruit, pome, group 11	0.05	12/31/16
Fruit, stone, group 12	0.05	12/31/16
Mango	0.05	12/31/16
Nut, tree, group 14	0.05	12/31/16
Olive	0.05	12/31/16
Safflower, seed	0.5	12/31/16
Sorghum, forage, forage	2.0	12/31/16
Sorghum, grain, forage	2.0	12/31/16
Sorghum, grain, grain	0.2	12/31/16
Sorghum, grain, stover	2.0	12/31/16
Sunflower, seed	0.5	12/31/16
Tangerine	6.0	12/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in or on the commodity.

Commodity	Parts per million	Expiration/ revocation date
Kiwifruit	0.1	12/31/16
Longan	0.1	12/31/16
Starfruit	0.1	12/31/16
Sugar apple	0.2	12/31/16

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 44845, Sept. 29, 1978]

Editorial Note: For Federal Register citations affecting §180.298, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.299 Dicrotophos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of 3-hydroxy-N,N-dimethyl-cis-crotonamide, in or on the following food commodities:

Commodity	Parts per million
Cotton, gin byproducts	2.0
Cotton, undelinted seed	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52613, Sept. 10, 2008]

§180.300 Ethephon; tolerances for residues.

(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl) phosphonic acid] in or on food commodities as follows:

Commodity	Parts per million
Apple	5.0
Apple, juice	10.0
Barley, bran	5.0
Barley, grain	2.0
Barley, straw	10.0
Blackberry	30.0
Blueberry	20.0
Cantaloupe	2.0
Cattle, fat	0.02
Cattle, kidney	1.0
Cattle, meat	0.02
Cattle, meat byproducts, except kidney	0.2
Cherry	10.0
Coffee, bean, green	0.5
Cotton, gin byproducts	180.0
Cotton, undelinted seed	6.0
Egg	0.002
Goat, fat	0.02
Goat, kidney	1.0
Goat, meat	0.02
Goat, meat byproducts, except kidney	0.2
Grape	2.0
Grape, raisin	12.0
Hazelnut	0.80
Hog, fat	0.02
Hog, kidney	1.0
Hog, meat	0.02
Hog, meat byproducts, except kidney	0.2
Horse, fat	0.02
Horse, kidney	1.0
Horse, meat	0.02
Horse, meat byproducts, except kidney	0.2
Milk	0.01
Nut, macadamia	0.5
Pepper	30.0
Pineapple	2.0
Poultry, fat	0.02
Poultry, liver	0.05
Poultry, meat	0.01
Poultry, meat byproducts, except liver	0.01
Sheep, fat	0.02
Sheep, kidney	1.0
Sheep, meat	0.02
Sheep, meat byproducts, except kidney	0.2
Sugarcane, molasses	1.5
Tomato	2.0
Walnut	0.5
Wheat, bran	5.0
Wheat, germ	5.0
Wheat, grain	2.0
Wheat, middlings	5.0
Wheat, shorts	5.0
Wheat, straw	10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(m), of 0.1 part per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic acid] in or on the food commodity sugarcane.

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010; 80 FR 72598, Nov. 20, 2015]

§180.301 Carboxin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide carboxin (5,6-dihydro-2-methyl-1,4-oxathiin-3-carboxanilide) and its metabolites determined as aniline and expressed as parent compound, in or on food commodities as follows:

Commodity	Parts per million
Barley, grain	0.2
Barley, straw	0.2
Bean, dry, seed	0.2
Bean, succulent	0.2
Canola, seed	0.03
Cattle, fat	0.05
Cattle, meat byproducts	0.1
Cattle, meat	0.05
Corn, field, forage	0.2
Corn, field, grain	0.2
Corn, field, stover	0.2
Corn, pop, grain	0.2
Corn, pop, stover	0.2
Corn, sweet, forage	0.2
Corn, sweet, kernel plus cob with husks removed	0.2
Corn, sweet, stover	0.2
Cotton, undelinted seed	0.2
Egg	0.05
Goat, fat	0.05
Goat, meat byproducts	0.1
Goat, meat	0.05
Hog, fat	0.05
Hog, meat byproducts	0.1
Hog, meat	0.05
Horse, fat	0.05
Horse, meat byproducts	0.1
Horse, meat	0.05
Milk	0.05
Oat, forage	0.5
Oat, grain	0.2
Oat, straw	0.2
Onion, bulb	0.2
Peanut	0.2
Peanut, hay	0.2
Poultry, fat	0.1
Poultry, meat byproducts	0.1
Poultry, meat	0.1
Rice, grain	0.2
Safflower, seed	0.2
Sheep, fat	0.05
Sheep, meat byproducts	0.1
Sheep, meat	0.05
Soybean, seed	0.2
Wheat, forage	0.5
Wheat, grain	0.2
Wheat, straw	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR 4586, Jan. 30, 1998; 64 FR 11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9, 2002; 71 FR 56383, Sept. 27, 2006; 80 FR 72598, Nov. 20, 2015]

§180.303 Oxamyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide oxamyl, methyl N,N-dimethyl-N-[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N-dimethyl-N-hydroxy-1-thiooxamimidate calculated as oxamyl in or on the following food commodities:

Commodity	Parts per million
Apple	2
Banana	0.3
Cantaloupe	2.0
Carrot	0.1
Celery	10.0
Cotton, undelinted seed	0.2
Cucumber	2.0
Eggplant	2.0
Fruit, citrus, group 10	3
Garlic, bulb	0.2
Melon, honeydew	2.0
Onion, bulb	0.2
Peanut	0.05
Peanut, hay	2.0
Pear	2.0
Peppermint, tops	10.0
Pepper, bell	2.0
Pepper, nonbell	5.0
Pineapple	1
Pineapple, process residue	2.0
Pumpkin	2.0
Spearmint, tops	10.0
Squash, summer	2.0
Squash, winter	2.0
Tomato	2
Vegetable, tuberous and corm, subgroup 1C	0.1
Watermelon	2.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 72598, Nov. 20, 2015]

§180.304 Oryzalin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

Commodity	Parts per million
Almond, hulls	0.05
Avocado	0.05
Berry group 13	0.05
Cranberry	0.05
Fig	0.05
Fruit, citrus, group 10	0.05
Fruit, pome, group 11	0.05
Fruit, stone, group 12	0.05
Grape	0.05
Kiwifruit	0.05
Nut, tree, group 14	0.05
Olive	0.05
Pistachio	0.05
Pomegranate	0.05
Strawberry	0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural commodities:

Commodity	Parts per million
Guava	0.05
Papaya	0.05

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011]

§180.314 Triallate; tolerances for residues.

(a) General. Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl diisopropylthiocarbamate and its metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodity:

Commodity	Parts per million
Bermudagrass, hay	0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in 180.1(l),are established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its metabolite 2, 3, 3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:

Commodity	Parts per million
Barley, grain	0.05
Barley, hay	1.0
Barley, straw	0.3
Beet, sugar, dried pulp	0.2
Beet, sugar, roots	0.1
Beet, sugar, tops	0.5
Pea, dry	0.2
Pea, field, hay	1.0
Pea, field, vines	0.5
Pea, succulent	0.2
Wheat, forage	0.5
Wheat, grain	0.05
Wheat, hay	1.0
Wheat, straw	1.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24, 2009]

§180.316 Pyrazon; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the following food commodities:

Commodity	Parts per million
Beet, garden, roots	0.9
Beet, garden, tops	7.0
Beet, sugar, molasses	1.5
Beet, sugar, roots	0.2
Beet, sugar, tops	3.0
Cattle, fat	0.10
Cattle, liver	0.15
Cattle, meat	0.10
Cattle, meat byproducts, except liver	0.10
Goat, fat	0.10
Goat, liver	0.15
Goat, meat	0.10
Goat, meat byproducts, except liver	0.10
Horse, fat	0.10
Horse, liver	0.15
Horse, meat	0.10
Horse, meat byproducts, except liver	0.10
Milk	0.02
Sheep, fat	0.10
Sheep, liver	0.15
Sheep, meat	0.10
Sheep, meat byproducts, except liver	0.10

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for combined residues of the herbicide pyrazon, 5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone, and its metabolites (calculated as pyrazon), in or on the following food commodities:

Commodity	Parts per million
Corn, field, forage	0.5
Corn, field, stover	0.5
Soybean, forage	0.5
Soybean, hay	0.5
Wheat, forage	0.3
Wheat, hay	0.2
Wheat, straw	0.1

[68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008]

§180.317 Propyzamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity	Parts per million
Alfalfa, seed	10.0
Animal feed, nongrass, group 18	10.0
Apple	0.1
Artichoke, globe	0.01
Blackberry	0.05
Blueberry	0.05
Boysenberry	0.05
Cattle, fat	0.2
Cattle, kidney	0.4
Cattle, liver	0.4
Cattle, meat	0.02
Cattle, meat byproducts, except kidney and liver	0.02
Egg	0.02
Endive	1.0
Fruit, stone, group 12	0.1
Goat, fat	0.2
Goat, kidney	0.4
Goat, liver	0.4
Goat, meat	0.02
Goat, meat byproducts, except kidney and liver	0.02
Grape	0.1
Hog, fat	0.2
Hog, kidney	0.4
Hog, liver	0.4
Hog, meat	0.02
Hog, meat byproducts, except kidney and liver	0.02
Horse, fat	0.2
Horse, kidney	0.4
Horse, liver	0.4
Horse, meat	0.02
Horse, meat byproducts, except kidney and liver	0.02
Lettuce, head	1.0
Lettuce, leaf	1.0
Milk	0.02
Pear	0.1
Poultry, fat	0.02
Poultry, liver	0.2
Poultry, meat	0.02
Poultry, meat byproducts, except liver	0.02
Radicchio	2.0
Raspberry	0.05
Sheep, fat	0.2
Sheep, kidney	0.4
Sheep, liver	0.4
Sheep, meat	0.02
Sheep, meat byproducts, except kidney and liver	0.02

(b) Section 18 emergency exemptions. The time-limited tolerance specified in the table in this paragraph (b) is established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the specified agricultural commodity in the table in this paragraph (b), resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance level specified in the table in this paragraph (b) is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide in or on the commodity. The time-limited tolerance expires on the date specified in the table in this paragraph (b).

Commodity	Parts per million	Expiration/revocation date
Cranberry	1	December 31, 2022

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity	Parts per million
Pea, field, seed	0.05
Rhubarb	0.1

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity	Parts per million
Grain, cereal, forage, group 16	0.6
Grain, cereal, hay, group 16	0.2
Grain, cereal, straw, group 16	0.3

[72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011; 81 FR 1531, Jan. 13, 2016; 84 FR 60943, Nov. 12, 2019]

§180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.

(a) General. (1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or on the following food commodity:

Commodity	Parts per million
Pea	0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4-(4-chloro-2-methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic acid, in or on the following food commodities:

Commodity	Parts per million
Peppermint, tops	0.20
Spearmint, tops	0.20

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

§180.319 Interim tolerances.

(a) General. While petitions for tolerances for negligible residues are pending and until action is completed on these petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the following raw agricultural commodities:

Substances	Uses	Tolerance in parts per million	Raw agricultural commodity	Expiration/ revocation date
Endothall (7-oxabicyclo-(2,2,1)heptane 2,3-dicarboxylic acid	Herbicide	0.2	Beet, sugar	None
Methyl parathion	Herbicide	0.5	Rye	12/31/13

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014]

§180.324 Bromoxynil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide bromoxynil, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

Commodity	Parts per million
Alfalfa, forage	0.1
Alfalfa, hay	0.5
Barley, grain	0.05
Barley, hay	9.0
Barley, straw	4.0
Corn, field, forage	0.3
Corn, field, grain	0.05
Corn, field, stover	0.2
Corn, pop, grain	0.05
Corn, pop, stover	0.2
Flax, seed	0.1
Garlic	0.1
Grain, aspirated fractions	1.2
Grass, forage	18
Grass, hay	5.0
Oat, forage	0.3
Oat, grain	0.05
Oat, hay	9.0
Oat, straw	4.0
Onion, bulb	0.1
Peppermint, hay	0.1
Rye, forage	1.0
Rye, grain	0.05
Rye, straw	2.0
Sorghum, grain, forage	0.8
Sorghum, grain, grain	0.2
Sorghum, grain, stover	0.2
Spearmint, hay	0.1
Wheat, forage	1.0
Wheat, grain	0.05
Wheat, hay	4.0
Wheat, straw	2.0

(2) Tolerances are established for residues of the herbicide bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring only bromoxynil and its metabolite, 3,5-dibromo-4-hydroxybenzoic acid (DBHA), resulting from application of its octanoic and/or heptanoic acid ester, in or on the commodities.

Commodity	Parts per million
Cattle, fat	1
Cattle, meat byproducts	3.5
Cattle, meat	0.5
Cotton, gin byproducts	7.0
Cotton, hulls	5.0
Cotton, undelinted seed	1.5
Egg	0.05
Goat, fat	1
Goat, meat byproducts	3.5
Goat, meat	0.5
Hog, fat	1
Hog, meat byproducts	3.5
Hog, meat	0.5
Horse, fat	1
Horse, meat byproducts	3.5
Horse, meat	0.5
Milk	0.4
Poultry, fat	0.05
Poultry, meat byproducts	0.3
Poultry, meat	0.05
Sheep, fat	1
Sheep, meat byproducts	3.5
Sheep, meat	0.5

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001; 70 FR 7046, Feb. 10, 2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR 31491, June 1, 2011]

§180.328 Napropamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide napropamide, N,N-diethyl-2-(1-napthalenyloxy) propionamide, in or on the following food commodities:

Commodity	Parts per million	Expiration/revocation date
Almond, hulls	0.1	None
Asparagus	0.1	None
Basil	0.1	None
Berry group 13	0.1	None
Coffee, green bean	0.1	None
Cranberry	0.1	None
Grape	0.1	None
Kiwifruit	0.1	None
Marjoram	0.1	None
Nut, tree, group 14	0.1	None
Peppermint, tops	0.1	None
Persimmon	0.1	None
Rhubarb	0.1	None
Rosemary	0.1	None
Savory, summer	0.1	None
Savory, winter	0.1	None
Spearmint, tops	0.1	None
Strawberry	0.1	None
Sweet potato, roots	0.1	None
Vegetable, brassica, leafy, group 5	0.1	None
Vegetable, fruiting, group 8	0.1	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52614, Sept. 10, 2008, as amended at 76 FR 34885, June 15, 2011]

§180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	5.0
Alfalfa, hay	11.0
Bean, lima	0.2
Beet, sugar, roots	0.3
Beet, sugar, tops	0.5
Broccoli	1.0
Brussels sprouts	1.0
Cabbage	2.0
Cauliflower	1.0
Clover, forage	5.0
Clover, hay	10.0
Corn, sweet, forage	1.0
Corn, sweet, kernel plus cob with husks removed	0.5
Corn, sweet, stover	3.0
Cotton, undelinted seed	0.02
Cucumber	1.0
Eggplant	1.0
Grapefruit	1.0
Hazelnut	0.05
Lemon	1.0
Lettuce, head	2.0
Melon	0.2
Onion, bulb	0.05
Orange	1.0
Pepper	0.75
Peppermint, tops	12.5
Pumpkin	0.2
Safflower, seed	1.0
Sorghum, forage, forage	2.0
Sorghum, grain, forage	2.0
Sorghum, grain, grain	0.75
Spearmint, tops	12.5
Squash, summer	1.0
Squash, winter	0.3
Strawberry	2.0
Walnut	0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.01
Cattle, meat	0.01
Cattle, meat byproducts	0.01
Egg	0.01
Goat, fat	0.01
Goat, meat	0.01
Goat, meat byproducts	0.01
Hog, fat	0.01
Hog, meat	0.01
Hog, meat byproducts	0.01
Horse, fat	0.01
Horse, meat	0.01
Horse, meat byproducts	0.01
Milk	0.01
Poultry, fat	0.01
Poultry, meat	0.01
Poultry, meat byproducts	0.01
Sheep, fat	0.01
Sheep, meat	0.01
Sheep, meat byproducts	0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

Commodity	Parts per million
Broccoli raab	2.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

§180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid (2,4-DB), both free and conjugated, determined as the acid, in or on food commodities, as follows:

Commodity	Parts per million
Alfalfa, forage	0.7
Alfalfa, hay	2.0
Cattle, meat byproducts	0.05
Clover, forage	0.2
Clover, hay	0.2
Goat, meat byproducts	0.05
Hog, meat byproducts	0.05
Horse, meat byproducts	0.05
Peanut	0.2
Peppermint, tops	0.2
Sheep, meat byproducts	0.05
Soybean, forage	0.7
Soybean, hay	2.0
Soybean, seed	0.5
Spearmint, tops	0.2
Trefoil, forage	0.7
Trefoil, hay	2.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 74 FR 46374, Sept. 9, 2009]

§180.332 Metribuzin; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1-dimethyl- ethyl)-3-(methylthio)-;1,2,4-triazin-5(4H)-one) and its triazinone metabolites in or on food commodities:

Commodity	Parts per million
Alfalfa, forage	2.0
Alfalfa, hay	7.0
Asparagus	0.1
Barley, grain	0.75
Barley, hay	7.0
Barley, pearled barley	3.0
Barley, straw	1.0
Carrot, roots	0.3
Cattle, fat	0.7
Cattle, meat	0.7
Cattle, meat byproducts	0.7
Corn, field, forage	0.1
Corn, field, grain	0.05
Corn, field, stover	0.1
Corn, pop, grain	0.05
Corn, sweet, forage	0.1
Corn, sweet, kernel plus cob with husks removed	0.05
Corn, sweet, stover	0.1
Egg	0.01
Goat, fat	0.7
Goat, meat	0.7
Goat, meat byproducts	0.7
Grass, forage	2.0
Grass, hay	7.0
Hog, fat	0.7
Hog, meat	0.7
Hog, meat byproducts	0.7
Horse, fat	0.7
Horse, meat	0.7
Horse, meat byproducts	0.7
Lentil	0.05
Milk	0.05
Pea, dry, seed	0.05
Pea, field, hay	4.0
Pea, field, vines	0.5
Pea, succulent	0.1
Potato	0.6
Potato, chips	3.0
Potato, processed potato waste	3.0
Poultry, fat	0.7
Poultry, meat	0.7
Poultry, meat byproducts	0.7
Sainfoin, forage	2.0
Sainfoin, hay	7.0
Sheep, fat	0.7
Sheep, meat	0.7
Sheep, meat byproducts	0.7
Soybean, seed	0.3
Soybean, forage	4.0
Soybean, hay	4.0
Sugarcane, cane	0.1
Sugarcane, molasses	2.0
Tomato	0.1
Wheat, bran	3.0
Wheat, forage	2.0
Wheat, germ	3.0
Wheat, grain	0.75
Wheat, hay	7.0
Wheat, middlings	3.0
Wheat, shorts	3.0
Wheat, straw	1.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979; 52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR 63198, Dec. 5, 2001; 67 FR 49617, July 31, 2002]

§180.337 Oxytetracycline; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the commodity.

Commodity	Parts per million
Apple	0.35
Fruit, citrus, group 10-10	0.01
Peach	0.35
Pear	0.35

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for residues of the fungicide/bactericide oxytetracycline, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-naphthacenecarboxamide, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire on the dates specified in the table.

Commodity	Parts per million	Expiration/ revocation date
Fruit, citrus, group 10-10	0.40	12/31/19

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23493, Apr. 27, 2011, as amended at 82 FR 13251, Mar. 10, 2017; 83 FR 62493, Dec. 4, 2018]

§180.339 MCPA; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid), both free and conjugated, resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	0.5
Alfalfa, hay	2.0
Barley, grain	1.0
Barley, hay	40
Barley, straw	25
Clover, forage	0.5
Clover, hay	2.0
Flax, seed	0.1
Grain, aspirated fractions	3.0
Grass, forage	300
Grass, hay	20
Lespedeza, forage	0.5
Lespedeza, hay	2.0
Oat, forage	20
Oat, grain	1.0
Oat, hay	115
Oat, straw	25
Pea, dry	0.1
Pea, field, hay	0.1
Pea, succulent	0.1
Pea, field, vines	0.1
Rye, forage	20
Rye, grain	1.0
Rye, straw	25
Trefoil, forage	0.5
Trefoil, hay	2.0
Vetch, forage	0.5
Vetch, hay	2.0
Wheat, forage	20
Wheat, grain	1.0
Wheat, hay	115
Wheat, straw	25

(2) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid) resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.1
Cattle, meat	0.1
Cattle, meat byproducts	0.1
Goat, fat	0.1
Goat, meat	0.1
Goat, meat byproducts	0.1
Hog, fat	0.1
Hog, meat	0.1
Hog, meat byproducts	0.1
Horse, fat	0.1
Horse, meat	0.1
Horse, meat byproducts	0.1
Milk	0.1
Sheep, fat	0.1
Sheep meat	0.1
Sheep meat byproducts	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008]

§180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.

(a) General. Tolerances are established for combined negligible residues of a fungicide and insecticide that is a mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw agricultural commodities as follows:

Commodity	Parts per million
Apple¹	0.1
Grape¹	0.1

¹There are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

§180.342 Chlorpyrifos; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	3.0
Alfalfa, hay	13
Almond	0.2
Almond, hulls	12
Apple	0.01
Apple, wet pomace	0.02
Banana	0.1
Beet, sugar, dried pulp	5.0
Beet, sugar, molasses	15
Beet, sugar, roots	1.0
Beet, sugar, tops	8.0
Cattle, fat	0.3
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Cherry, sweet	1.0
Cherry, tart	1.0
Citrus, dried pulp	5.0
Citrus, oil	20
Corn, field, forage	8.0
Corn, field, grain	0.05
Corn, field, refined oil	0.25
Corn, field, stover	8.0
Corn, sweet, forage	8.0
Corn, sweet, kernel plus cob with husk removed	0.05
Corn, sweet, stover	8.0
Cotton, undelinted seed	0.2
Cranberry	1.0
Cucumber	0.05
Egg	0.01
Fig	0.01
Fruit, citrus, group 10	1.0
Goat, fat	0.2
Goat, meat	0.05
Goat, meat byproducts	0.05
Hazelnut	0.2
Hog, fat	0.2
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	0.25
Horse, meat	0.25
Horse, meat byproducts	0.25
Kiwifruit	2.0
Milk, fat (Reflecting 0.01 ppm in whole milk)	0.25
Nectarine	0.05
Onion, bulb	0.5
Peach	0.05
Peanut	0.2
Peanut, refined oil	0.2
Pear	0.05
Pecan	0.2
Pepper	1.0
Peppermint, tops	0.8
Peppermint, oil	8.0
Plum, prune, fresh	0.05
Poultry, fat	0.1
Poultry, meat	0.1
Poultry, meat byproducts	0.1
Pumpkin	0.05
Radish	2.0
Rutabaga	0.5
Sheep, fat	0.2
Sheep, meat	0.05
Sheep, meat byproducts	0.05
Spearmint, tops	0.8
Spearmint, oil	8.0
Sorghum, grain, forage	0.5
Sorghum, grain, grain	0.5
Sorghum, grain, stover	2.0
Soybean, seed	0.3
Strawberry	0.2
Sunflower, seed	0.1
Sweet potato, roots	0.05
Turnip, roots	1.0
Turnip, tops	0.3
Vegetable, brassica, leafy, group 5	1.0
Vegetable, legume, group 6. except soybean	0.05
Walnut	0.2
Wheat, forage	3.0
Wheat, grain	0.5
Wheat, straw	6.0

(2) Chlorpyrifos [O,O-diethyl O-(3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in accordance with the following prescribed conditions.

(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are held, processed, prepared or served. Contamination of food or food contact surfaces shall be avoided. Food must be removed or covered during treatment.

(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active ingredient by weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the spray.

(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active ingredient by weight.

(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by weight. Equipment capable of delivering a pin-stream of insecticide shall be used.

(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release product in food-handling establishments where food and food products are held, processed, prepared, or served. A maximum of 36 strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor space. The strips are not to be placed in exposed areas where direct contact with food, utensils, and food-contact surfaces would be likely to occur.

(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food commodities (other than those already covered by a higher tolerance as a result of use on growing crops) in food service establishments where food and food products are prepared and served, as a result of the application of chlorpyrifos in microencapsulated form.

(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where food and food products are prepared and served. All treatments shall be applied in such a manner as to avoid contamination of food or food contact surfaces.

(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight.

(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into cracks and crevices or capable of applying small amounts of insecticide into cracks and crevices shall be used.

(iv) For spot treatment, an individual spot shall not exceed 2 square feet.

(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in 180.1(l), are established for residues of the pesticide chlorpyrifos per se (O,O-diethyl- O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity	Parts per million
Asparagus	5.0
Grape	0.01

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 2008; 76 FR 56656, Sept. 14, 2011]

§180.345 Ethofumesate; tolerances for residues.

(a) General. Tolerance are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the following food commodities.

Commodity	Parts per million
Beet, garden, roots	0.5
Beet, garden, tops	5.0
Beet, sugar, molasses	2.0
Beet, sugar, roots	1.5
Beet, sugar, tops	4.0
Cattle, fat	0.05
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Garlic	0.25
Goat, fat	0.05
Goat, meat	0.05
Goat, meat byproducts	0.05
Grass, straw	1.0
Horse, fat	0.05
Horse, meat	0.05
Horse, meat byproducts	0.05
Onion, bulb	0.25
Shallot, bulb	0.25
Shallot, fresh leaves	0.25
Sheep, fat	0.05
Sheep, meat	0.05
Sheep, meat byproducts	0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in §180.1(l) are established for residues of the herbicide ethofumesate, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified is to be determined by measuring only the sum of ethofumesate, 2-ethoxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate, and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranylmethanesulfonate, calculated as the stoichiometric equivalent of ethofumesate, in or on the raw agricultural commodities.

Commodity	Parts per million
Carrot, roots	7.0

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007; 82 FR 57158, Dec. 4, 2017]

§180.349 Fenamiphos; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide/insecticide fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, and its cholinesterase inhibiting metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl 1-(methylethyl)phosphoramidate and ethyl 3-methyl-4-(methylsulfonyl)phenyl 1-(methylethyl)phosphoramidate, calculated as the stoichiometric equivalent of fenamiphos, in or on the commodity.

Commodity	Parts per million
Banana¹	0.1
Grape¹	0.1
Grape, raisin¹	0.3
Pineapple¹	0.3

¹There are no U.S. registrations as of May 31, 2007.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, 2010]

§180.350 Nitrapyrin; tolerances for residues.

(a) General. Tolerances are established for residues of the nitrification inhibitor nitrapyrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of nitrapyrin (2-chloro-6-(trichloromethyl) pyridine) and its 6-CPA metabolite (6-chloro-picolinic acid), calculated as the stoichiometric equivalent of nitrapyrin, in or on the commodity:

Commodity	Parts per million
Almond, hulls	0.06
Beet, sugar, molasses	0.5
Beet, sugar, roots	0.3
Beet, sugar, tops	0.7
Corn, field, forage	1.0
Corn, field, grain	0.1
Corn, field, milled byproducts	0.2
Corn, field, stover	1.0
Corn, pop, grain	0.1
Corn, pop, stover	1.0
Corn, sweet, forage	1.0
Corn, sweet, kernel plus cob with husks removed	0.1
Corn, sweet, stover	1.0
Fruit, citrus, group 10-10	0.06
Fruit, citrus, group 10-10, dried pulp	0.5
Fruit, citrus, group 10-10, oil	2
Leaf petiole vegetable subgroup 22B	0.5
Nut, tree, group 14-12	0.02
Rapeseed, seed	0.3
Sorghum, forage, forage	0.5
Sorghum, grain, forage	0.5
Sorghum, grain, grain	0.1
Sorghum, grain, stover	0.5
Vegetable, Brassica, head and stem, group 5-16	0.1
Vegetable, bulb, group 3-07	0.3
Vegetable, leafy, group 4-16	0.4
Vegetable, tuberous and corm, crop subgroup 1C	0.6
Wheat, bran	3.0
Wheat, forage	2.0
Wheat, grain	0.5
Wheat, milled byproducts, except flour	2.0
Wheat, straw	6.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993; 63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007; 82 FR 56744, Nov. 30, 2017; 84 FR 44712, Aug. 27, 2019; 85 FR 48654, Aug. 12, 2020]

§180.352 Terbufos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide terbufos (phosphorodithioic acid, S-(t-butylthio)methyl O,O-diethyl ester) and its phosphorylated (cholinesterase-inhibiting) metabolites (phosphorothioic acid, S-(t-butylthio)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester; phosphorodithioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; and phosphorodithioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester) in or on food commodities:

Commodity	Parts per million
Banana	0.025
Beet, sugar, roots	0.05
Beet, sugar, tops	0.1
Coffee, green bean¹	0.05
Corn, field, forage	0.5
Corn, field, grain	0.5
Corn, field, stover	0.5
Corn, pop, grain	0.5
Corn, pop, stover	0.5
Corn, sweet, kernel plus cob with husks removed	0.05
Corn, sweet, forage	0.5
Corn, sweet, stover	0.5
Sorghum, grain, forage	0.5
Sorghum, grain, grain	0.05
Sorghum, grain, stover	0.5

¹ There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 53740, Sept. 17, 2008]

§180.353 Desmedipham; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide desmedipham, (ethyl-m-hydroxycarbanilate carbanilate) in or on the following raw agricultural commodities in the table that follows:

Commodity	Parts per million
Beet, garden, roots	0.05
Beet, garden, tops	1.0
Beet, sugar, roots	0.1
Beet, sugar, tops	5.0
Spinach	6.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25, 1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

§180.355 Bentazon; tolerances for residues.

(a) General. (1) Tolerances are established for residues of bentazon, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring for only the sum of bentazon (3-(1-methylethyl)-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide), 6-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide, and 8-hydroxy-3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one 2,2-dioxide calculated as the stoichiometric equivalent of bentazon.

Commodity	Parts per million
Bean, dry, seed	0.05
Bean, succulent	0.5
Corn, field, forage	3.0
Corn, field, grain	0.05
Corn, field, stover	3.0
Corn, pop, grain	0.05
Corn, sweet, kernel plus cob with husks removed	0.05
Cowpea, forage	10.0
Cowpea, hay	3.0
Flax, seed	1.0
Pea, dry, seed	3
Pea, field, hay	8.0
Pea, field, vines	3.0
Pea, succulent	3.0
Peanut	0.05
Peanut, hay	3.0
Pepper, nonbell	0.05
Peppermint, tops	1.0
Rice, grain	0.05
Rice, hulls	0.25
Sorghum, forage	0.20
Sorghum, grain, grain	0.05
Sorghum, grain, stover	0.05
Soybean, forage	8.0
Soybean, hay	8.0
Soybean, seed	0.05
Spearmint, tops	1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl-1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl benzamide (AIBA) in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.05
Cattle, meat byproducts	0.05
Cattle, meat	0.05
Egg	0.05
Goat, fat	0.05
Goat, meat byproducts	0.05
Goat, meat	0.05
Hog, fat	0.05
Hog, meat byproducts	0.05
Hog, meat	0.05
Milk	0.02
Poultry, fat	0.05
Poultry, meat byproducts	0.05
Poultry, meat	0.05
Sheep, fat	0.05
Sheep, meat byproducts	0.05
Sheep, meat	0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(m), are established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

Commodity	Parts per million
Clover, forage	1.0
Clover, hay	2.0

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 26979, May 26, 1977]

Editorial Note: For Federal Register citations affecting §180.355, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.356 Norflurazon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro-5-(methylamino)-2-(alpha, alpha, alpha-trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its desmethyl metabolite 4-chloro-5-(amino)-2-alpha, alpha, alpha-trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural commodities:

Commodity	Parts per million
Alfalfa, forage	3.0
Alfalfa, hay	5.0
Alfalfa, seed	0.1
Almond, hulls	1.0
Almond	0.1
Apple	0.1
Apricot	0.1
Asparagus	0.05
Avocado	0.20
Blackberry	0.1
Blueberry	0.2
Cattle, fat	0.1
Cattle, liver	0.50
Cattle, meat	0.1
Cattle, meat byproducts, except liver	0.1
Cherry	0.1
Citrus, dried pulp	0.4
Citrus, molasses	1.0
Cotton, undelinted seed	0.1
Cranberry	0.1
Fruit, citrus	0.2
Goat, fat	0.1
Goat, liver	0.50
Goat, meat	0.1
Goat, meat byproducts, except liver	0.1
Grape	0.1
Hazelnut	0.1
Hog, fat	0.1
Hog, liver	0.50
Hog, meat	0.1
Hog, meat byproducts, except liver	0.1
Hop, dried cones	3.0
Hop, vines	1.0
Horse, fat	0.1
Horse, liver	0.50
Horse, meat	0.1
Horse, meat byproducts, except liver	0.1
Milk	0.1
Nectarine	0.1
Peach	0.1
Peanut	0.05
Peanut, hay	5.50
Peanut, hay	1.5
Pear	0.1
Pecan	0.1
Plum, prune, fresh	0.1
Poultry, fat	0.1
Poultry, meat	0.1
Poultry, meat byproducts	0.1
Raspberry	0.2
Sheep, fat	0.1
Sheep, liver	0.50
Sheep, meat	0.1
Sheep, meat byproducts, except liver	0.1
Soybean	0.1
Soybean, forage	1.0
Soybean, hay	1.0
Walnut	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 14909, Apr. 7, 1982]

Editorial Note: For Federal Register citations affecting §180.356, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.360 Asulam; tolerance for residues.

(a) General. Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate) and its sulfanilamide containing metabolites in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.05
Cattle, meat	0.05
Cattle, meat byproducts	0.2
Goat, fat	0.05
Goat, meat	0.05
Goat, meat byproducts	0.2
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.2
Horse, fat	0.05
Horse, meat	0.05
Horse, meat byproducts	0.2
Milk	0.05
Sheep, fat	0.05
Sheep, meat	0.05
Sheep, meat byproducts	0.2
Sugarcane, cane	1.0
Sugarcane, molasses	30

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

§180.361 Pendimethalin; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on the commodities. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine] and its metabolite, 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	80
Alfalfa, hay	150
Alfalfa, seed	0.10
Almond, hulls	6.0
Apple, wet pomace	0.20
Artichoke, globe	0.1
Asparagus	0.15
Beans	0.10
Beans, forage	0.10
Beans, hay	0.10
Berry, low growing subgroup 13-07G	0.1
Brassica head and stem, subgroup 5-A	0.1
Brassica, leafy greens, subgroup 5B	0.20
Bushberry subgroup 13-07B	0.10
Caneberry subgroup 13-07A	0.10
Carrot	0.5
Citrus, oil	0.5
Corn, field, forage	0.1
Corn, field, grain	0.1
Corn, field, stover	0.1
Corn, pop, grain	0.1
Corn, sweet, forage	0.1
Corn, sweet, kernel plus cob with husks removed	0.1
Corn, sweet, stover	0.1
Cotton, gin byproducts	3.0
Cotton, undelinted seed	0.1
Crayfish	0.05
Fruit, citrus, group 10-10	0.1
Fruit, pome, group 11-10	0.1
Fruit, small vine climbing, except grape, subgroup 13-07E	0.10
Fruit, stone, group 12-12	0.1
Grape	0.1
Grass, forage, fodder, and hay crop group 17, forage	1,000
Grass, forage, fodder, and hay crop group 17, hay	2,000
Hop, dried cones	0.1
Leaf petiole vegetable subgroup 22B	0.2
Lettuce, leaf	4.0
Melon subgroup 9A	0.10
Monarda, fresh leaves	0.2
Monarda, oil	1
Nut, tree, group 14-12	0.10
Olive	0.1
Onion, bulb subgroup 3-07A	0.1
Onion, green subgroup 3-07B	0.2
Peanut	0.1
Peanut, hay	0.1
Peas (except field peas)	0.10
Peppermint, oil	1.0
Peppermint, tops	0.2
Pomegranate	0.10
Potato	0.1
Rice, grain	0.1
Rosemary, fresh leaves	0.2
Rosemary, oil	1
Sorghum, forage	0.1
Sorghum, grain, grain	0.1
Sorghum, grain, stover	0.1
Soybean, forage	0.1
Soybean, hay	0.1
Soybean, seed	0.1
Spearmint, oil	1.0
Spearmint, tops	0.2
Sugarcane, cane	0.1
Sunflower subgroup 20B	0.1
Turnip greens	0.20
Vegetable, fruiting, group 8-10	0.1
Vegetable, soybean, succulent	0.10
Wheat, grain	0.10
Wheat, forage	3.0
Wheat, hay	0.60
Wheat, straw	0.30

(2) Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and degradates, in or on commodities listed in the following table. Compliance with the tolerance levels is to be determined by measuring only the sum of pendimethalin (N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine)) and its metabolite, 1-(1-ethylpropyl)-5, 6-dimethyl-7-nitro-1H-benzimidazole (metabolite 6), calculated as the stoichiometric equivalent of pendimethalin, in or on the commodity.

Commodity	Parts per million
Cattle, fat	0.30
Cattle, meat	0.10
Cattle, meat byproduct	3.0
Goats, fat	0.30
Goats, meat	0.10
Goats, meat byproduct	3.0
Horse, fat	0.30
Horse, meat	0.10
Horse, byproduct	3.0
Milk	0.04
Sheep, fat	0.30
Sheep, meat	0.10
Sheep, meat byproduct	3.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for combined residues of the herbicide pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the table.

Commodity	Parts per million	Expiration/revocation date
Bermuda grass, forage	25	12/31/10
Bermuda grass, hay	60	12/31/10

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 15293, Apr. 18, 1984]

Editorial Note: For Federal Register citations affecting §180.361, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.362 Fenbutatin-oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity	Parts per million
Almond, hulls	80.0
Apple	15.0
Apple, wet pomace	100.0
Cherry, sweet	6.0
Cherry, tart	6.0
Citrus, dried pulp	100.0
Citrus, oil	140.0
Cucumber	4.0
Eggplant	6.0
Fruit, citrus, group 10	20.0
Grape	5.0
Grape, raisin	20.0
Nut, tree, group 14	0.5
Papaya	2.0
Peach	10.0
Pear	15.0
Pistachio	0.5
Plum, prune, fresh	4.0
Plum, prune, dried	20.0
Strawberry	10.0

(2) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the animal commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, and its organotin metabolites, dihydroxybis(2-methyl-2-phenylpropyl) stannane and 2-methyl-2-phenylpropylstannoic acid, calculated as the stoichiometric equivalent of fenbutatin-oxide, in or on the commodity.

Commodity	Parts per million
Cattle, fat	0.5
Cattle, meat	0.5
Cattle, meat byproducts	0.5
Egg	0.1
Goat, fat	0.5
Goat, meat	0.5
Goat, meat byproducts	0.5
Hog, fat	0.5
Hog, meat	0.5
Hog, meat byproducts	0.5
Horse, fat	0.5
Horse, meat	0.5
Horse, meat byproducts	0.5
Milk, fat	0.1
Poultry, fat	0.1
Poultry, meat	0.1
Poultry, meat byproducts	0.1
Sheep, fat	0.5
Sheep, meat	0.5
Sheep, meat byproducts	0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity	Parts per million
Raspberry	10.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011]

§180.364 Glyphosate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine).

Commodity	Parts per million
Acerola	0.2
Alfalfa, seed	0.5
Almond, hulls	25
Aloe vera	0.5
Ambarella	0.2
Animal feed, nongrass, group 18	400
Artichoke, globe	0.2
Asparagus	0.5
Atemoya	0.2
Avocado	0.2
Bamboo, shoots	0.2
Banana	0.2
Barley, bran	30
Beet, sugar, dried pulp	25
Beet, sugar, roots	10
Beet, sugar, tops	10
Berry and small fruit, group 13-07	0.20
Betelnut	1.0
Biriba	0.2
Blimbe	0.2
Breadfruit	0.2
Cacao bean, bean	0.2
Cactus, fruit	0.5
Cactus, pads	0.5
Canistel	0.2
Carrot	5.0
Chaya	1.0
Cherimoya	0.2
Citrus, dried pulp	1.5
Coconut	0.1
Coffee, bean, green	1.0
Corn, pop, grain	0.1
Corn, sweet, kernel plus cob with husk removed	3.5
Cotton, gin byproducts	210
Custard apple	0.2
Date, dried fruit	0.2
Dokudami	2.0
Durian	0.2
Epazote	1.3
Feijoa	0.2
Fig	0.2
Fish	0.25
Fruit, citrus, group 10-10	0.50
Fruit, pome, group 11-10	0.20
Fruit, stone, group 12	0.2
Galangal, roots	0.2
Ginger, white, flower	0.2
Gourd, buffalo, seed	0.1
Governor's plum	0.2
Gow kee, leaves	0.2
Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover	100
Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice	30
Grass, forage, fodder and hay, group 17	300
Guava	0.2
Herbs subgroup 19A	0.2
Hop, dried cones	7.0
Ilama	0.2
Imbe	0.2
Imbu	0.2
Jaboticaba	0.2
Jackfruit	0.2
Kava, roots	0.2
Kenaf, forage	200
Leucaena, forage	200
Longan	0.2
Lychee	0.2
Mamey apple	0.2
Mango	0.2
Mangosteen	0.2
Marmaladebox	0.2
Mioga, flower	0.2
Noni	0.20
Nut, pine	1.0
Nut, tree, group 14	1.0
Oilseeds, group 20, except canola	40
Okra	0.5
Olive	0.2
Oregano, Mexican, leaves	2.0
Palm heart	0.2
Palm heart, leaves	0.2
Palm, oil	0.1
Papaya	0.2
Papaya, mountain	0.2
Passionfruit	0.2
Pawpaw	0.2
Pea, dry	8.0
Peanut	0.1
Peanut, hay	0.5
Pepper leaf, fresh leaves	0.2
Peppermint, tops	200
Perilla, tops	1.8
Persimmon	0.2
Pineapple	0.1
Pistachio	1.0
Pomegranate	0.2
Pulasan	0.2
Quinoa, grain	5.0
Rambutan	0.2
Rice, grain	0.1
Rice, wild, grain	0.1
Rose apple	0.2
Sapodilla	0.2
Sapote, black	0.2
Sapote, mamey	0.2
Sapote, white	0.2
Shellfish	3.0
Soursop	0.2
Spanish lime	0.2
Spearmint, tops	200
Spice subgroup 19B	7.0
Star apple	0.2
Starfruit	0.2
Stevia, dried leaves	1.0
Sugar apple	0.2
Sugarcane, cane	2.0
Sugarcane, molasses	30
Surinam cherry	0.2
Sweet potato	3.0
Tamarind	0.2
Tea, dried	1.0
Tea, instant	7.0
Teff, forage	100
Teff, grain	5.0
Teff, hay	100
Ti, leaves	0.2
Ti, roots	0.2
Ugli fruit	0.5
Vegetable, bulb, group 3-07	0.20
Vegetable, cucurbit, group 9	0.5
Vegetable, foliage of legume, subgroup 7A, except soybean	0.2
Vegetable, fruiting, group 8-10 (except okra)	0.10
Vegetable, leafy, brassica, group 5	0.2
Vegetable, leafy, except brassica, group 4	0.2
Vegetable, leaves of root and tuber, group 2, except sugar beet tops	0.2
Vegetable, legume, group 6 except soybean and dry pea	5.0
Vegetables, root and tuber, group 1, except carrot, sweet potato, and sugar beet	0.20
Wasabi, roots	0.2
Water spinach, tops	0.2
Watercress, upland	0.2
Wax jambu	0.2
Yacon, tuber	0.2

(2) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only glyphosate (N-(phosphonomethyl)glycine) and its metabolite N-acetyl-glyphosate (N-acetyl-N-(phosphonomethyl)glycine; calculated as the stoichiometric equivalent of glyphosate).

Commodity	Parts per Million
Canola, seed	20
Cattle, meat byproducts	5.0
Corn, field, forage	13
Corn, field, grain	5.0
Corn, field, stover	100
Egg	0.05
Goat, meat byproducts	5.0
Grain aspirated fractions	310.0
Hog, meat byproducts	5.0
Horse, meat byproducts	5.0
Poultry, meat	0.10
Poultry, meat byproducts	1.0
Sheep, meat byproducts	5.0
Soybean, forage	100.0
Soybean, hay	200.0
Soybean, hulls	120.0
Soybean, seed	20.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 64911, Oct. 1, 1980]

Editorial Note: For Federal Register citations affecting §180.364, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.

(a) General. A tolerance of 5 parts per million is established for residues of the insecticide synergist N-octyl bicycloheptene dicarboximide, including its metabolites and degradates, in or on all food items in food handling establishments where food and food products are held, processed, prepared and/or served, provided that the food is removed or covered prior to such use, except for bagged food in warehouse storage which need not be removed or covered prior to applications of formulations containing N-octyl bicycloheptene dicarboximide. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only N-octyl bicycloheptene dicarboximide, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 75 FR 60243, Sept. 29, 2010]

§180.368 Metolachlor; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2- ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

Commodity	Parts per million
Almond, hulls	0.30
Animal feed, nongrass, group 18	1.0
Cattle, fat	0.02
Cattle, kidney	0.20
Cattle, liver	0.05
Cattle, meat	0.02
Cattle, meat byproducts, except kidney and liver	0.04
Corn, field, forage	6.0
Corn, field, grain	0.10
Corn, field, stover	6.0
Corn, pop, grain	0.10
Corn, pop, stover	6.0
Corn, sweet, forage	6.0
Corn, sweet, kernel plus cob with husks removed	0.10
Corn, sweet, stover	6.0
Cotton, gin byproducts	4.0
Cotton, undelinted seed	0.10
Dillweed	0.50
Egg	0.02
Goat, fat	0.02
Goat, kidney	0.20
Goat, liver	0.05
Goat, meat	0.02
Goat, meat byproducts, except kidney and liver	0.04
Grass, forage	10
Grass, hay	0.20
Horse, fat	0.02
Horse, kidney	0.20
Horse, liver	0.05
Horse, meat	0.02
Horse, meat byproducts, except kidney and liver	0.04
Milk	0.02
Nut, tree, group 14	0.10
Okra	0.50
Peanut	0.20
Peanut, hay	20
Peanut, meal	0.40
Potato	0.20
Poultry, fat	0.02
Poultry, meat	0.02
Poultry, meat byproducts	0.05
Safflower, seed	0.10
Sheep, fat	0.02
Sheep, kidney	0.20
Sheep, liver	0.05
Sheep, meat	0.02
Sheep, meat byproducts, except kidney and liver	0.04
Sorghum, grain, forage	1.0
Sorghum, grain, grain	0.30
Sorghum, grain, stover	4.0
Soybean, forage	5.0
Soybean, hay	8.0
Soybean, seed	0.20
Tomato	0.10
Vegetable, foliage of legume, subgroup 7A, except soybean	15.0
Vegetable, legume, group 6	0.30

(2) Tolerances are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodity(s), as defined. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Table 2 to Paragraph (a)(2)

Commodity	Parts per million
Beet, sugar, molasses	2.0
Beet, sugar, roots	0.5
Beet, sugar, tops	15.0
Brassica, leafy greens, subgroup 4-16B	1.8
Bushberry subgroup 13-07B	0.15
Caneberry subgroup 13-07A	0.10
Carrot, roots	0.40
Cattle, fat	0.02
Cattle, kidney	0.20
Cattle, liver	0.05
Cattle, meat	0.02
Cattle, meat byproducts, except kidney and liver	0.04
Cilantro, leaves	8.0
Coriander, seed	0.13
Corn, field, forage	40
Corn, field, grain	0.10
Corn, field, stover	40
Corn, pop, grain	0.10
Corn, pop, stover	40
Corn, sweet, forage	40
Corn, sweet, kernel plus cob with husks removed	0.10
Corn, sweet, stover	40
Cotton, gin byproducts	4.0
Cottonseed subgroup 20C	0.10
Dill, seed	15
Dillweed	5
Dillweed, dried leaves	9
Egg	0.02
Goat, fat	0.02
Goat, kidney	0.20
Goat, liver	0.05
Goat, meat	0.02
Goat, meat byproducts, except kidney and liver	0.04
Grain, aspirated fractions	4
Grass, forage	10.0
Grass, hay	0.20
Horse, fat	0.02
Horse, kidney	0.20
Horse, liver	0.05
Horse, meat	0.02
Horse, meat byproducts, except kidney and liver	0.04
Kohlrabi	0.60
Leaf petiole vegetable subgroup 22B	0.10
Lettuce	1.5
Low growing berry subgroup 13-07G, except cranberry	0.40
Milk	0.02
Onion, bulb, subgroup 3-07A	0.10
Onion, green, subgroup 3-07B	2.0
Peanut	0.20
Peanut, hay	20.0
Peanut, meal	0.40
Poultry, fat	0.02
Poultry, meat	0.02
Poultry, meat byproducts	0.05
Rosemary, dried leaves	2
Rosemary, fresh leaves	1.5
Safflower, seed	0.10
Sesame, seed	0.13
Sheep, fat	0.02
Sheep, kidney	0.20
Sheep, liver	0.05
Sheep, meat	0.02
Sheep, meat byproducts, except kidney and liver	0.04
Sorghum, grain, forage	1.0
Sorghum, grain, grain	0.3
Sorghum, grain, stover	4.0
Sorghum, sweet, stalk	4.0
Soybean, forage	5.0
Soybean, hay	8.0
Soybean, meal	1.5
Soybean, seed	0.9
Spinach	0.50
Stalk and stem vegetable subgroup 22A, except kohlrabi	0.10
Stevia, dried leaves	15
Sugarcane, cane	0.20
Sugarcane, molasses	1.5
Sunflower, meal	1.0
Sunflower subgroup 20B	1.0
Swiss chard	0.15
Tomato, paste	0.30
Vegetable, Brassica, head and stem, group 5-16	0.60
Vegetable, cucurbit group 9	0.50
Vegetable, foliage of legume, except soybean, subgroup 7A	15.0
Vegetable, fruiting, group 8-10, except tabasco pepper	0.10
Vegetable, leaves of root and tuber, group 2, except sugar beet	2.0
Vegetable, legume, group 6	0.30
Vegetable, root, except sugar beet, subgroup 1B, except carrot	0.30
Vegetable, tuberous and corm, subgroup 1C	0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. (1) Tolerances with regional registration as defined in 180.1(l) are established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound, in or on the following raw agricultural commodities:

Commodity	Parts per million
Pepper, nonbell	0.50

(2) Tolerances with regional registration are established for residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity	Parts per million
Pepper, tabasco	0.50

(d) Indirect or inadvertent residues. (1) Tolerances are established for the indirect or inadvertent combined residues (free and bound) of the herbicide metolachlor, 2-chloro-N-(2-ethyl-6- methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

Commodity	Parts per million
Animal feed, nongrass, group 18	1.0
Barley, grain	0.10
Barley, hay	0.80
Barley, straw	0.80
Buckwheat, grain	0.10
Millet, forage	0.50
Millet, grain	0.10
Millet, hay	0.80
Millet, straw	0.80
Oat, forage	0.50
Oat, grain	0.10
Oat, hay	0.80
Oat, straw	0.80
Rice, grain	0.10
Rye, forage	0.50
Rye, grain	0.10
Rye, straw	0.80
Wheat, forage	0.50
Wheat, grain	0.10
Wheat, hay	0.80
Wheat, straw	0.80

(2) Tolerances for are established for the indirect or inadvertent residues of S-metolachlor, including its metabolites and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity	Parts per million
Animal feed, nongrass, group 18	1.0
Barley, grain	0.10
Barley, hay	0.50
Barley, straw	0.50
Buckwheat, grain	0.10
Millet, forage	0.50
Millet, grain	0.10
Millet, hay	0.50
Millet, straw	0.50
Oat, forage	0.50
Oat, grain	0.10
Oat, hay	0.50
Oat, straw	0.50
Rice, grain	0.10
Rye, forage	0.50
Rye, grain	0.10
Rye, straw	0.50
Wheat, forage	0.50
Wheat, grain	0.10
Wheat, hay	0.50
Wheat, straw	0.50

[73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15, 2012; 77 FR 59127, Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015; 83 FR 12274, Mar. 21, 2018; 84 FR 8617, Mar. 11, 2019; 85 FR 40131, July 6, 2020]

§180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole and its monoacid metabolite 3-carboxy-5-ethoxy-1,2,4-thiadiazole in or on the following raw agricultural commodities:

Commodity	Parts per million
Cotton, gin byproducts	0.1
Cotton, undelinted seed	0.1
Tomato	0.15

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 81 FR 34905, June 1, 2016]

§180.371 Thiophanate-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

Commodity	Parts per million
Almond	0.1
Almond, hulls	0.5
Apple	2.0
Apricot	15.0
Banana	2.0
Bean, dry, seed	0.2
Bean, snap, succulent	2.0
Beet, sugar, roots	0.2
Cherry, sweet	20.0
Cherry, tart	20.0
Grain, aspirated fractions	12
Grape	5.0
Onion, bulb	0.5
Onion, green	3.0
Peach	3.0
Peanut	0.1
Peanut, hay	5.0
Pear	3.0
Pecan	0.1
Pistachio	0.1
Plum	0.5
Potato	0.1
Soybean, hulls	1.5
Soybean, seed	0.2
Strawberry	7.0
Vegetable, cucurbit, group 9	1.0
Wheat, forage	1.1
Wheat, grain	0.1
Wheat, hay	0.1
Wheat, straw	0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis(iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the commodity.

Commodity	Parts per million
Canola, seed	0.1

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60244, Sept. 29, 2010]

§180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.

(a) General. A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in or on the following food commodity:

Commodity	Parts per million
Banana¹	1.0

¹There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008]

§180.373 [Reserved]

§180.377 Diflubenzuron; tolerances for residues.

(a) General. (1) Tolerances are established for residues of diflubenzuron, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

Commodity	Parts per million
Artichoke, globe	6.0
Cattle, fat	0.05
Cattle, meat	0.05
Cottonseed subgroup 20C	0.20
Egg	0.07
Goat, fat	0.05
Goat, meat	0.05
Hog, fat	0.05
Hog, meat	0.05
Horse, fat	0.05
Horse, meat	0.05
Milk	0.05
Mushroom	0.2
Poultry, fat	0.10
Poultry, meat byproducts	0.08
Poultry, meat	0.05
Sheep, fat	0.05
Sheep, meat	0.05
Soybean	0.05
Soybean, hulls	0.5

(2) Tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

Commodity	Parts per million
Almond, hulls	6.0
Barley, grain	0.06
Barley, hay	3.0
Barley, straw	1.8
Brassica, leafy greens, subgroup 5B	9.0
Carrot, roots	0.20
Cattle, meat byproducts	0.15
Citrus, oil	32
Fruit, citrus, group 10-10	3.0
Goat, meat byproducts	0.15
Grain, aspirated fractions	11
Grass, forage, fodder, and hay, group 17	6.0
Hog, meat byproducts	0.15
Horse, meat byproducts	0.15
Oat, forage	7.0
Oat, grain	0.06
Oat, hay	6.0
Oat, straw	3.5
Peanut	0.10
Peanut, hay	55
Peanut, refined oil	0.20
Peach subgroup 12-12B	0.50
Pear	0.50
Pepper/Eggplant subgroup 8-10B	1.0
Plum Subgroup 12-12C	0.50
Nut, tree, group 14-12	0.20
Rice, grain	0.02
Sheep, meat byproducts	0.15
Turnip greens	9.0
Wheat, forage	7.0
Wheat, grain	0.06
Wheat, hay	6.0
Wheat, straw	3.5

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6- difluorobenzamide) and its metabolites, in connection with use of the pesticide under section 18 emergency exemptions granted by EPA. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity. The tolerances are specified in the following table, and will expire and are revoked on the dates specified.

Commodity	Parts per million	Expiration/revocation date
Alfalfa, forage	6.0	12/31/17
Alfalfa, hay	6.0	12/31/17
Lemon	0.8	12/31/10

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of diflubenzuron, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	6.0
Alfalfa, hay	20
Alfalfa, seed	0.90

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33699, May 24, 2000]

Editorial Note: For Federal Register citations affecting §180.377, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.378 Permethrin; tolerances for residues.

(a) General. Tolerances are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	20
Alfalfa, hay	45
Almond	0.05
Almond, hulls	20
Artichoke, globe	5.0
Asparagus	2.0
Avocado	1.0
Broccoli	2.0
Brussels sprouts	1.0
Cabbage	6.0
Cattle, fat	1.5
Cattle, meat	0.10
Cattle, meat byproducts	0.10
Cauliflower	0.5
Celtuce	5
Cherry subgroup 12-12A	4
Corn, field, forage	50
Corn, field, grain	0.05
Corn, field, stover	30
Corn, pop, grain	0.05
Corn, pop, stover	30
Corn, sweet, forage	50
Corn, sweet, kernel plus cob with husks removed	0.10
Corn, sweet, stover	30
Egg	0.10
Eggplant	0.50
Fennel, Florence, fresh leaves and stalks	5
Fruit, pome, group 11	0.05
Garlic, bulb	0.10
Grain, aspirated fractions	0.50
Goat, fat	1.5
Goat, meat	0.10
Goat, meat byproducts	0.10
Hazelnut	0.05
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	1.5
Horse, meat	0.10
Horse, meat byproducts	0.10
Horseradish	0.50
Kiwifruit	2.0
Leaf petiole vegetable subgroup 22B	5
Leafy greens subgroup 4A	20
Lettuce, head	20
Milk, fat (reflecting 0.88 ppm in whole milk)	3.0
Mushroom	5.0
Onion, bulb	0.10
Peach subgroup 12-12B	2
Pepper, bell	0.50
Pistachio	0.10
Poultry, fat	0.15
Poultry, meat	0.05
Poultry, meat byproducts	0.05
Sheep, fat	1.5
Sheep, meat	0.10
Sheep, meat byproducts	0.10
Soybean, seed	0.05
Spinach	20
Swiss chard	5
Tea, plucked leaves¹	20
Tomato	2.0
Vegetable, cucurbit, group 9	1.5
Vegetable, tuberous and corm, subgroup 1C	0.05
Walnut	0.05
Watercress	5.0

¹There are no United States registrations for use of permethrin on tea, plucked leaves as of July 28, 2020.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are established for residues of permethrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only permethrin [(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate], as the sum of its cis- and trans- isomers in or on the commodity.

Commodity	Parts per million
Collards	15
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F	2
Grass, forage	15
Grass, hay	15
Papaya	1.0
Turnip, tops	10
Turnip, roots	0.20

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52019, Sept. 12, 2007, as amended at 85 FR 45335, July 28, 2020]

§180.380 Vinclozolin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5-dichlorophenyl)-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5-dichloroaniline moiety in or on the food commodities in the table below. There are no U.S. registrations for grape (wine) as of July 30, 1997.

Commodity	Parts per million	Expiration/Revocation Date
Bean, succulent	2.0	11/30/05
Canola, seed	1.0	11/30/08
Cattle, fat	0.05	11/30/08
Cattle, meat	0.05	11/30/08
Cattle, meat byproducts	0.05	11/30/08
Egg	0.05	11/30/08
Goat, fat	0.05	11/30/08
Goat, meat	0.05	11/30/08
Goat, meat byproducts	0.05	11/30/08
Grape, wine	6. 0	None
Hog, fat	0.05	11/30/08
Hog, meat	0.05	11/30/08
Hog, meat byproducts	0.05	11/30/08
Horse, fat	0.05	11/30/08
Horse, meat	0.05	11/30/08
Horse, meat byproducts	0.05	11/30/08
Lettuce, head	10.0	11/30/05
Lettuce, leaf	10.0	11/30/05
Milk	0.05	11/30/08
Poultry, fat	0.1	11/30/08
Poultry, meat	0.1	11/30/08
Poultry, meat byproducts	0.1	11/30/08
Sheep, fat	0.05	11/30/08
Sheep, meat	0.05	11/30/08
Sheep, meat byproducts	0.05	11/30/08

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities with residues of vinclozolin resulting from lawful use are subject to the channels of trade provisions of section 408(l)(5) of the FFDCA:

Commodity	Parts per million
Cucumber	1.0
Fruit, stone, except plum, prune, fresh	25.0
Pepper, bell	3.0
Strawberry	10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002; 68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005]

§180.381 Oxyfluorfen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity	Parts per million
Almond, hulls	0.1
Artichoke, globe	0.05
Avocado	0.05
Banana	0.05
Broccoli	0.05
Cabbage	0.05
Cacao bean, dried bean	0.05
Cattle, fat	0.01
Cattle, meat	0.01
Cattle, meat byproducts	0.01
Cauliflower	0.05
Coffee, bean, green	0.05
Corn, field, grain	0.05
Cotton, undelinted seed	0.05
Date, dried fruit	0.05
Egg	0.03
Feijoa	0.05
Fig	0.05
Fruit, pome, group 11	0.05
Fruit, stone, group 12	0.05
Goat, fat	0.01
Goat, meat	0.01
Goat, meat byproducts	0.01
Grape	0.05
Hog, fat	0.01
Hog, meat	0.01
Hog, meat byproducts	0.01
Horse, fat	0.01
Horse, meat	0.01
Horse, meat byproducts	0.01
Horseradish	0.05
Kiwifruit	0.05
Milk	0.01
Nut, tree, group 14	0.05
Olive	0.05
Onion, bulb	0.05
Peppermint, tops	0.05
Persimmon	0.05
Pistachio	0.05
Pomegranate	0.05
Poultry, fat	0.2
Poultry, meat	0.01
Poultry, meat byproducts	0.01
Sheep, fat	0.01
Sheep, meat	0.01
Sheep, meat byproducts	0.01
Soybean	0.05
Spearmint, tops	0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity	Parts per million
Blackberry	0.05
Chickpea, seed	0.05
Grass, forage	0.05
Grass, hay	0.05
Grass, seed screenings	0.05
Guava	0.05
Papaya	0.05
Raspberry	0.05
Taro, corm	0.05
Taro, leaves	0.05

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 85022, Dec. 24, 1980]

Editorial Note: For Federal Register citations affecting §180.381, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.383 Sodium salt of acifluorfen; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen, sodium 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding acid, methyl ester, and amino analogues) in or on the following raw agricultural commodities:

Commodity	Parts per million
Peanut	0.1
Rice, grain	0.1
Soybean, seed	0.1
Strawberry	0.05

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006; 80 FR 72598, Nov. 20, 2015]

§180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator mepiquat, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only mepiquat, N,N-dimethylpiperidinium, in or on the commodity.

Commodity	Parts per million
Cattle, meat byproducts	0.1
Cotton, gin byproducts	6.0
Cotton, undelinted seed	2.0
Goat, meat byproducts	0.1
Grape	1.0
Grape, raisin	5.0
Hog, meat byproducts	0.1
Horse, meat byproducts	0.1
Sheep, meat byproducts	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 3118, Jan. 23, 2002, as amended at 80 FR 72598, Nov. 20, 2015]

§180.385 Diclofop-methyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoic acid and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agricultural commodities:

Commodity	Parts per million
Barley, grain	0.1
Barley, straw	0.1
Wheat, grain	0.1
Wheat, straw	0.1

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51 FR 19176, May 28, 1986; 63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

§§180.388-180.389 [Reserved]

§180.390 Tebuthiuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity	Parts per million
Grass, forage	10.0
Grass, hay	10.0

(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino-1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity	Parts per million
Cattle, fat	1.0
Cattle, meat	1.0
Cattle, meat byproducts	5.0
Goat, fat	1.0
Goat, meat	1.0
Goat, meat byproducts	5.0
Horse, fat	1.0
Horse, meat	1.0
Horse, meat byproducts	5.0
Sheep, fat	1.0
Sheep, meat	1.0
Sheep, meat byproducts	5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity	Parts per million
Milk	0.8

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 53461, Sept. 19, 2007]

§180.395 Hydramethylnon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)hydrazone in or on the following raw agricultural commodities:

Commodity	Parts per million
Grass, forage	2.0
Grass, hay	2.0
Pineapple	0.05

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001; 68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug. 1, 2007]

§180.396 Hexazinone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant metabolites: metabolite A, 3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite D, 3-cyclohexyl-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity	Parts per million
Alfalfa, forage	2.0
Alfalfa, hay	4.0
Alfalfa, seed	2.0
Blueberry	0.6
Grass, forage	250
Grass, hay	230
Pineapple	0.6
Sugarcane, cane	0.6
Sugarcane, molasses	4.0

(2) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its animal tissue metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity	Parts per million
Cattle, fat	0.1
Cattle, meat	0.5
Cattle, meat byproducts	4.0
Goat, fat	0.1
Goat, meat	0.5
Goat, meat byproducts	4.0
Hog, fat	0.1
Hog, meat	0.5
Hog, meat byproducts	4.0
Horse, fat	0.1
Horse, meat	0.5
Horse, meat byproducts	4.0
Sheep, fat	0.1
Sheep, meat	0.5
Sheep, meat byproducts	4.0

(3) A tolerance is established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C-2, 3-(3-hydroxycyclohexyl)-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity	Parts per million
Milk	11

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, 2010]

§180.399 Iprodione; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide in or on the following food commodities:

Commodity	Parts per million
Almond, hulls	2.0
Almond	0.3
Apricot	20.0
Bean, dry, seed	2.0
Bean, forage	90.0
Bean, succulent	2.0
Blueberry	15.0
Boysenberry	15.0
Broccoli	25.0
Caneberry subgroup 13A	25.0
Carrot, roots	5.0
Cherry, sweet, postharvest	20.0
Cherry, tart	20.0
Cotton, undelinted seed	0.10
Cowpea, hay	90.0
Currant	15.0
Garlic	0.1
Ginseng	2.0
Ginseng, dried root	4.0
Grape	60.0
Grape, raisin	300
Kiwifruit	10.0
Lettuce	25.0
Nectarine, postharvest	20.0
Onion, bulb	0.5
Peach, postharvest	20.0
Peanut	0.5
Peanut, hay	150.0
Plum, postharvest	20.0
Plum, prune	20.0
Potato	0.5
Raspberry	15.0
Rice, bran	30.0
Rice, grain	10.0
Rice, hulls	50.0
Strawberry	15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide] and [N-(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as iprodione equivalents in or on the following food commodities of animal origin:

Commodity	Parts per million
Cattle, fat	0.5
Cattle, kidney	3.0
Cattle, liver	3.0
Cattle, meat	0.5
Cattle, meat byproducts, except kidney and liver	0.5
Egg	1.5
Goat, fat	0.5
Goat, kidney	3.0
Goat, liver	3.0
Goat, meat	0.5
Goat, meat byproducts, except kidney and liver	0.5
Hog, fat	0.5
Hog, kidney	3.0
Hog, liver	3.0
Hog, meat	0.5
Hog, meat byproducts, except kidney and liver	0.5
Horse, fat	0.5
Horse, kidney	3.0
Horse, liver	3.0
Horse, meat	0.5
Horse, meat byproducts, except kidney and liver	0.5
Milk	0.5
Poultry, fat	3.5
Poultry, liver	5.0
Poultry, meat	1.0
Poultry, meat byproducts, except liver	1.0
Sheep, fat	0.5
Sheep, kidney	3.0
Sheep, liver	3.0
Sheep, meat	0.5
Sheep, meat byproducts, except kidney and liver	0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide], and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide] in or on the following food commodity:

Commodity	Parts per million
Mustard greens	15.0

(d) Indirect or inadvertent residues. [Reserved]

[48 FR 40385, Sept. 7, 1983]

Editorial Note: For Federal Register citations affecting §180.399, see the List of CFR Sections Affected, which appears in the Finding Aids section of the printed volume and at www.govinfo.gov.

§180.401 Thiobencarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide thiobencarb (S-[(4-chlorophenyl)methyl]diethyl-carbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

Commodity	Part per million
Cattle, fat	0.2
Cattle, meat byproducts	0.2
Cattle, meat	0.2
Egg	0.2
Goat, fat	0.2
Goat, meat byproducts	0.2
Goat, meat	0.2
Hog, fat	0.2
Hog, meat byproducts	0.2
Hog, meat	0.2
Horse, fat	0.2
Horse, meat byproducts	0.2
Horse, meat	0.2
Milk	0.05
Poultry, fat	0.2
Poultry, meat byproducts	0.2
Poultry, meat	0.2
Rice, grain	0.2
Sheep, fat	0.2
Sheep, meat byproducts	0.2
Sheep, meat	0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the herbicide thiobencarb (S-[(4-chloro-phenyl)methyl]diethylcarbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

Commodity	Parts per million
Celery	0.2
Endive	0.2
Lettuce	0.2

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, 2011; 80 FR 72599, Nov. 20, 2015]

§180.403 Thidiazuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenyl-N-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.4
Cattle, meat	0.4
Cattle, meat byproducts	0.4
Cotton, gin byproducts	24.0
Cotton, undelinted seed	0.3
Goat, fat	0.4
Goat, meat	0.4
Goat, meat byproducts	0.4
Hog, fat	0.4
Hog, meat	0.4
Hog, meat byproducts	0.4
Horse, fat	0.4
Horse, meat	0.4
Horse, meat byproducts	0.4
Milk	0.05
Sheep, fat	0.4
Sheep, meat	0.4
Sheep, meat byproducts	0.4

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

§180.404 Profenofos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2-chlorophenyl)-O-ethyl-S-propyl phosphorothioate) in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.05
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Cotton, gin byproducts	55.0
Cotton, undelinted seed	2.0
Goat, fat	0.05
Goat, meat	0.05
Goat, meat byproducts	0.05
Horse, fat	0.05
Horse, meat	0.05
Horse, meat byproducts	0.05
Milk	0.01
Sheep, fat	0.05
Sheep, meat	0.05
Sheep, meat byproducts	0.05

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007]

§180.405 Chlorsulfuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5-hydroxy-N-[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the following raw agricultural commodities:

Commodity	Parts per million
Barley, grain	0.1
Barley, straw	0.5
Oat, forage	20.0
Oat, grain	0.1
Oat, straw	0.5
Wheat, forage	20.0
Wheat, grain	0.1
Wheat, straw	0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2- yl)aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities.

Commodity	Parts per million
Cattle, fat	0.3
Cattle, meat	0.3
Cattle, meat byproducts	0.3
Goat, fat	0.3
Goat, meat	0.3
Goat, meat byproducts	0.3
Grass, forage	11.0
Grass, hay	19.0
Hog, fat	0.3
Hog, meat	0.3
Hog, meat byproducts	0.3
Horse, fat	0.3
Horse, meat	0.3
Horse, meat byproducts	0.3
Milk	0.1
Sheep, fat	0.3
Sheep, meat	0.3
Sheep, meat byproducts	0.3

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 52873, Aug. 14, 2002]

§180.407 Thiodicarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl N,N′-[thiobis[[(methylimino)carbonyloxy]] bis[ethanimidothioate]) and its metabolite methomyl (S-methyl N-[(methylcarbamoyl) oxy]thioacetimidate) in or on the following food commodities or groups. The time-limited tolerances expire and are revoked on the dates listed in the following table:

Commodity	Parts per million	Expiration/revocation date
Broccoli	7.0	None
Cabbage	7.0	None
Cauliflower	7.0	None
Corn, sweet, kernel plus cob with husks removed	2.0	None
Cotton, undelinted seed	0.4	None
Soybean, hulls	0.8	None
Soybean	0.2	None
Vegetable, leafy, except brassica, group 4	35	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 44595, Aug. 22, 1997, as amended at 75 FR 60245, Sept. 29, 2010]

§180.408 Metalaxyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [N-(2,6-dmethylphyenyl)-N-(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methylphenyl)-N-(methoxyacetyl)-alanine methyl ester, each expressed as metalaxyl equivalents, in or on the following food commodities:

Commodity	Parts per million
Alfalfa, forage	6.0
Alfalfa, hay	20.0
Almond	0.5
Almond, hulls	10.0
Apple	0.2
Apple, wet pomace	0.4
Apricot, dried	4.0
Asparagus	7.0
Avocado	4.0
Beet, garden, roots	0.1
Beet, garden, tops	0.1
Beet, sugar	0.1
Beet, sugar, molasses	1.0
Beet, sugar, roots	0.5
Beet, sugar, tops	10.0
Blueberry	2.0
Broccoli	2.0
Brussels sprouts	2.0
Cabbage	1.0
Cattle, fat	0.4
Cattle, kidney	0.4
Cattle, liver	0.4
Cattle, meat	0.05
Cattle, meat byproducts, except kidney and liver	0.05
Cauliflower	1.0
Citrus, oil	7.0
Citrus, dried pulp	7.0
Clover, forage	1.0
Clover, hay	2.5
Cotton, undelinted seed	0.1
Cranberry	4.0
Egg	0.05
Fruit, citrus	1.0
Fruit, stone, group 12	1.0
Ginseng	3.0
Goat, fat	0.4
Goat, kidney	0.4
Goat, liver	0.4
Goat, meat	0.05
Goat, meat byproducts, except kidney and liver	0.05
Grain, cereal, group 15, except barley, oat and wheat	0.1
Grain, crop	0.1
Grape	2.0
Grape, raisin	6.0
Grass, forage	10.0
Grass, hay	25.0
Hog, fat	0.4
Hog, kidney	0.4
Hog, liver	0.4
Hog, meat	0.05
Hog, meat byproducts, except kidney and liver	0.05
Hop, dried cones	20
Hop, vines	2.0
Horse, fat	0.4
Horse, kidney	0.4
Horse, liver	0.4
Horse, meat	0.05
Horse, meat byproducts, except kidney and liver	0.05
Lettuce, head	5.0
Milk	0.02
Mustard greens	5.0
Onion, bulb	3.0
Onion, green	10.0
Peanut	0.2
Peanut, hay	20.0
Peanut, meal	1.0
Peanut, hulls	2.0
Pineapple	0.1
Pineapple, fodder	0.1
Pineapple, forage	0.1
Plum, prune, dried	4.0
Potato, chips	4.0
Potato, granules, flakes	4.0
Potato, processed potato waste	4.0
Potato, wet peel	4.0
Poultry, fat	0.4
Poultry, kidney	0.4
Poultry, liver	0.4
Poultry, meat	0.05
Poultry, meat byproducts, except kidney and liver	0.05
Potato	0.5
Raspberry	0.5
Sheep, fat	0.4
Sheep, kidney	0.4
Sheep, liver	0.4
Sheep, meat	0.05
Sheep, meat byproducts, except kidney and liver	0.05
Soybean, hulls	2.0
Soybean, meal	2.0
Soybean, seed	1.0
Spinach	10.0
Strawberry	10.0
Sunflower, seed	0.1
Sunflower, forage	0.1
Tomato, paste	3.0
Tomato, puree	3.0
Vegetable, brassica, leafy, group 5, except broccoli, cabbage, cauliflower, brussels sprouts, and mustard greens	0.1
Vegetable, cucurbit, group 9	1.0
Vegetable, foilage of legume, group 7	8.0
Vegetable, fruiting, group 8	1.0
Vegetable, leafy, except brassica, group 4, except spinach	5.0
Vegetable, leaves of root and tuber, group 2	15.0
Vegetable, legume, cannery waste	5.0
Vegetable, legume, group 6	0.2
Vegetable, root and tuber, group 1	0.5
Walnut	0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration (refer to §180.1(m)) are established for the combined residues of the fungicide metalaxyl [N-(2,6-dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N-(methoxyacetyl)-alanine methylester, each expressed as metalaxyl, in or on the following raw agricultural commodity:

Commodity	Parts per million
Papaya	0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of metalaxyl in or on the food commodities when present therein as a result of the application of metalaxyl to growing crops listed in paragraph (a) of this section and other non-food crops to read as follows:

Commodity	Part per million
Barley, bran	1.0
Barley, flour	1.0
Barley, grain	0.2
Barley, pearled barley	1.0
Barley, straw	2.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage	1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; stover	1.0
Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; straw	1.0
Oat, flour	1.0
Oat, forage	2.0
Oat, grain	0.2
Oat, groats, rolled oats	1.0
Oat, straw	2.0
Wheat, bran	1.0
Wheat, flour	1.0
Wheat, forage	2.0
Wheat, germ	1.0
Wheat, grain	0.2
Wheat, middlings	1.0
Wheat, shorts	1.0
Wheat, straw	2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, 2009; 75 FR 56015, Sept. 15, 2010]

§180.409 Pirimiphos-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2-diethylamino-6-methyl-4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural commodities:

Commodity	Parts per million
Cattle, fat	0.02
Cattle, meat byproducts	0.02
Corn, field, grain	8.0
Corn, pop, grain	8.0
Goat, fat	0.02
Goat, meat byproducts	0.02
Grain, aspirated fractions	20.0
Hog, fat	0.02
Hog, meat byproducts	0.02
Horse, fat	0.02
Horse, meat byproducts	0.02
Poultry, fat	0.02
Sheep, fat	0.02
Sheep, meat byproducts	0.02
Sorghum, grain, grain	8.0

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 72 FR 53462, Sept. 19, 2007]

§180.410 Triadimefon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:

Commodity	Parts per million	Expiration/Revocation Date
Pineapple	2.0	None

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 76 FR 34885, June 15, 2011]

§180.411 Fluazifop-P-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.

Commodity	Parts per million
Banana	0.01
Beans, dry, seed	50
Beet, sugar, dried pulp	1.0
Beet, sugar, molasses	3.5
Beet, sugar, roots	0.25
Bushberry subgroup 13-07B	0.30
Caneberry subgroup 13-07A	0.08
Carrot, roots	2.0
Cattle, fat	0.05
Cattle, meat	0.05
Cattle, meat byproducts	0.05
Citrus, dried pulp	0.40
Citrus, juice	0.06
Citrus, oil	30.0
Cotton, gin byproducts	1.5
Cotton, refined oil	1.3
Cotton, undelinted seed	1.0
Egg	0.05
Endive	6.0
Fruit, citrus, group 10	0.03
Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F	0.03
Fruit, stone	0.05
Goat, fat	0.05
Goat, meat	0.05
Goat, meat byproducts	0.05
Hog, fat	0.05
Hog, meat	0.05
Hog, meat byproducts	0.05
Horse, fat	0.05
Horse, meat	0.05
Horse, meat byproducts	0.05
Lettuce, head	3.0
Lettuce, leaf	5.0
Milk	0.05
Nut, macadamia	0.1
Onion, bulb, subgroup 3-07A	0.50
Onion, green	1.5
Peanut	1.5
Peanut, meal	2.2
Pecans	0.05
Poultry, fat	0.05
Poultry, meat	0.05
Poultry, meat byproducts	0.05
Potato¹	1.0
Potato, chips¹	2.0
Potato, granules/flakes¹	4.0
Rhubarb	0.50
Sheep, fat	0.05
Sheep, meat	0.05
Sheep, meat byproducts	0.05
Soybean, seed	2.5
Strawberry	3.0
Vegetable, tuberous and corm, except potato, subgroup 1D	1.5

¹No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.

Commodity	Parts per million
Asparagus	3.0
Coffee, bean	0.1
Fescue, forage	4.0
Fescue, hay	15
Pepper, tabasco	1.0

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33714, May 24, 2000, as amended at 74 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, 2009; 74 FR 47457, Sept. 16, 2009; 76 FR 5703, Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR 46822, Aug. 6, 2015; 82 FR 44942, Sept. 27, 2017]

§180.412 Sethoxydim; tolerances for residues.

(a) Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No. 74051-80-2) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

Table 1 to Paragraph (a)

Commodity	Parts per million
Alfalfa, forage	40
Alfalfa, hay	40
Almond, hulls	2.0
Apricot	0.2
Apple, wet pomace	0.8
Asparagus	4.0
Basil, dried leaves	20
Basil, fresh leaves	8
Bean, succulent	15
Beet, sugar, molasses	10
Beet, sugar, tops	3.0
Berry, low growing, subgroup 13-07H, except strawberry	2.5
Borage, meal	40
Buckwheat, flour	25
Buckwheat, grain	19
Bushberry subgroup 13-07B	4.0
Calendula, meal	20
Caneberry subgroup 13-07A	5.0
Canola, meal	40
Castor oil plant, meal	20
Cattle, fat	0.2
Cattle, meat	0.2
Cattle, meat byproducts	1.0
Cherry, sweet	0.2
Cherry, tart	0.2
Chinese tallowtree, meal	20
Citrus, dried pulp	1.5
Clover, forage	35
Clover, hay	55
Coriander, leaves	4.0
Corn, field, forage	2.0
Corn, field, grain	0.5
Corn, field, stover	2.5
Corn, sweet, forage	3.0
Corn, sweet, kernel plus cob with husk removed	0.4
Corn, sweet, stover	3.5
Cottonseed subgroup 20C	5.0
Cowpea, forage	15
Cowpea, hay	50
Crambe, meal	40
Cuphea, meal	40
Dillweed, fresh leaves	10
Echium, meal	40
Egg	2.0
Euphorbia, meal	20
Evening primrose, meal	20
Flax seed, meal	40
Fruit, citrus, group 10-10	0.5
Fruit, pome, group 11-10	0.2
Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F	1.0
Goat, fat	0.2
Goat, meat	0.2
Goat, meat byproducts	1.0
Gold of pleasure, meal	40
Grape, raisin	2.0
Hare's ear mustard, meal	40
Hog, fat	0.2
Hog, meat	0.2
Hog, meat byproducts	1.0
Horse, fat	0.2
Horse, meat	0.2
Horse, meat byproducts	1.0
Jojoba, meal	20
Juneberry¹	5.0
Lesquerella, meal	40
Lingonberry¹	5.0
Lunaria, meal	40
Meadowfoam, meal	40
Milk	0.5
Milkweed, meal	40
Mustard, meal	40
Nectarine	0.2
Niger seed, meal	20
Nut, tree, group 14	0.2
Oil radish, meal	40
Pea and bean, dried shelled, except soybean, subgroup 6C	25
Pea, field, hay	40
Pea, field, vines	20
Pea, succulent	10
Peach	0.2
Peanut	25
Peppermint, tops	30
Pistachio	0.2
Poppy seed, meal	40
Potato granules/flakes	8.0
Potato waste, processed	8.0
Poultry, fat	0.2
Poultry, meat	0.2
Poultry, meat byproducts	2.0
Radish, tops	4.5
Rapeseed, meal	40
Rapeseed subgroup 20A	35
Rose hip, meal	20
Safflower, seed	15
Salal¹	5.0
Sesame, meal	40
Sheep, fat	0.2
Sheep, meat	0.2
Sheep, meat byproducts	1.0
Soybean, hay	10
Soybean, seed	16
Spearmint, tops	30
Strawberry	10
Stokes aster, meal	20
Sunflower, meal	20
Sunflower subgroup 20B, except safflower	7.0
Sweet rocket, meal	40
Tallowwood, meal	20
Tea oil plant, meal	20
Turnip, tops	5.0
Vegetable, brassica, leafy, group 5	5.0
Vegetable, bulb, group 3-07	1.0
Vegetable, cucurbit, group 9	4.0
Vegetable, fruiting, group 8-10	4.0
Vegetable, leafy, except brassica, group 4	4.0
Vegetable, root and tuber, group 1	4.0
Vernonia, meal	20

¹The individual tolerances for Juneberry, Lingonberry, and Salal expire on December 15, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of sethoxydim, in or on the commodity.

Commodity	Parts per million
Artichoke, globe	5.0
Fescue, forage	7.0
Fescue, hay	4.0
Rhubarb	0.3

(d) Indirect and inadvertent residues. [Reserved]

[80 FR 34077, June 15, 2015, as amended at 85 FR 78002, Dec. 3, 2020]

§180.413 Imazalil; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1H-imidazole-1-yl)-1-ethanol, in or on the following food commodities:

Commodity	Parts per million
Banana	3.0
Barley, grain	0.1
Barley, hay	0.5
Barley, straw	0.5
Citrus, dried pulp	25.0
Citrus, oil	200.0
Fruit, citrus, postharvest	10.0
Wheat, forage	0.5
Wheat, grain	0.1
Wheat, hay	0.5
Wheat, straw	0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2-(2,3-dihydroxypropoxy)ethyl]-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]-2,4-imidazolidinedione (FK284), in or on the following food commodities:

Commodity	Parts per million
Cattle, fat	0.01
Cattle, meat	0.01
Cattle, meat byproducts	0.2
Goat, fat	0.01
Goat, meat	0.01
Goat, meat byproducts	0.2
Horse, fat	0.01
Horse, meat	0.01
Horse, meat byproducts	0.2
Milk	0.02
Sheep, fat	0.01
Sheep, meat	0.01
Sheep, meat byproducts	0.2

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

§180.414 Cyromazine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine.

Commodity	Parts per million
Bean, dry, except cowpea	3.0
Bean, lima	1.0
Bean, succulent	2.0
Brassica, leafy greens, subgroup 4-16B	35
Broccoli	1.0
Cattle, fat	0.05
Cattle, kidney	0.2
Cattle, meat	0.05
Cattle, meat byproducts, except kidney	0.05
Celtuce	10
Chickpea, edible podded	0.4
Chickpea, succulent shelled	0.3
Dwarf pea, edible podded	0.4
Edible podded pea, edible podded	0.4
Egg	0.25
English pea, succulent shelled	0.3
Fennel, Florence, fresh leaves and stalk	10
Garden pea, succulent shelled	0.3
Goat, fat	0.05
Goat, kidney	0.2
Goat, meat	0.05
Goat, meat byproducts, except kidney	0.05
Grass-pea, edible podded	0.4
Green pea, edible podded	0.4
Green pea, succulent shelled	0.3
Hog, fat	0.05
Hog, kidney	0.2
Hog, meat	0.05
Hog, meat byproducts, except kidney	0.05
Horse, fat	0.05
Horse, kidney	0.2
Horse, meat	0.05
Horse, meat byproducts, except kidney	0.05
Kohlrabi	35
Leaf petiole vegetable subgroup 22B	10
Leafy greens subgroup 4-16A	10
Lentil, edible podded	0.4
Lentil, succulent shelled	0.3
Mango¹	0.3
Milk	0.05
Mushroom	1.0
Onion, bulb, subgroup 3-07A	0.3
Onion, green, subgroup 3-07B	3
Onion, potato²	3.0
Pepper/eggplant subgroup 8-10B	3
Pigeon pea, edible podded	0.4
Pigeon pea, succulent shelled	0.3
Poultry, fat (from chicken layer hens and chicken breeder hens only)	0.05
Poultry, meat (from chicken layer hens and chicken breeder hens only)	0.05
Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only)	0.05
Sheep, fat	0.05
Sheep, kidney	0.2
Sheep, meat	0.05
Sheep, meat byproducts, except kidney	0.05
Snap pea, edible podded	0.4
Snow pea, edible podded	0.4
Sugar snap pea, edible podded	0.4
Tomato subgroup 8-10A	1
Vegetable, brassica, head and stem, group 5-16, except broccoli	35
Vegetable, cucurbit, group 9	1.0
Vegetable, tuberous and corm, subgroup 1C	0.8

¹There are no U.S. registrations on mango as of May 4, 2000.

²This tolerance expires on April 7, 2020.

(2) A tolerance of 5.0 parts per million is established for residues of the insecticide cyromazine, including its metabolites and degradates, in or on poultry feed when used as a feed additive only in feed for chicken layer hens and chicken breeder hens at the rate of not more than 0.01 pound of cyromazine per ton of poultry feed for control of flies in manure of treated chicken layer hens and chicken breeder hens, provided the feeding of cyromazine-treated feed must stop at least 3 days (72 hours) before slaughter. If the feed is formulated by any person other than the end user, the formulator must inform the end user, in writing, of the 3-day (72 hours) pre-slaughter interval. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph when present therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of this section. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

Commodity	Parts per million
Cotton, undelinted seed	0.1
Corn, sweet, kernel plus cob with husks removed	0.5
Corn, sweet, forage	0.5
Corn, sweet, stover	0.5
Radish, roots	0.5
Radish, tops	0.5

[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003; 75 FR 22256, Apr. 28, 2010; 76 FR 23494, Apr. 27, 2011; 84 FR 53322, Oct. 7, 2019]

§180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Commodity	Parts per million
Avocado	25
Banana	3.0
Bushberry subgroup 13B	40
Caneberry subgroup 13A	0.1
Cranberry	0.5
Fruit, citrus, group 10-10	9.0
Fruit, pome, group 11	10
Ginseng	0.1
Hop, dried cones	45
Juneberry	40
Lingonberry	40
Nut, macadamia	0.20
Onion, bulb	0.5
Onion, green	10.0
Pea, succulent	0.3
Pepper/eggplant, subgroup 8-10B¹	0.01
Pineapple	0.1
Salal	40
Strawberry	75
Tomato	3
Turnip, greens	40
Turnip, roots	15
Vegetable, brassica, leafy, group 5	60
Vegetable, cucurbit, group 9	15
Vegetable, leafy, except brassica, group 4	100

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Commodity	Parts per million
Asparagus	0.1
Grape	10

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002; 68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015; 83 FR 12265, Mar. 21, 2018]

§180.416 Ethalfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide ethalfluralin, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring only the residues of ethalfluralin, N-ethyl-N-(2-methyl-2-propenyl)-2,6-dinitro-4-(trifluoromethyl)benzenamine.

Commodity	Parts per million
Bean, dry, seed	0.05
Dill, dried leaves	0.05
Dill, fresh leaves	0.05
Peanut	0.05
Pea, dry, seed	0.05
Potato	0.01
Potato¹	0.05
Rapeseed subgroup 20A	0.05
Soybean	0.05
Sunflower subgroup 20B	0.05
Vegetable, cucurbit, group 9	0.05

¹This tolerance expires on January 28, 2021.

(b) Section 18 emergency exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR 66014, Dec. 17, 1997; 64 FR 5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, 2013; 85 FR 45341, July 28, 2020]

§180.417 Triclopyr; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide triclopyr, including its metabolites and degradates, in or on the commodities in the table below resulting from the application of the butoxyethyl ester of triclopyr, triethylamine salt of triclopyr, or choline salt of triclopyr. Compliance with the tolerance levels specified below is to be determined by measuring only triclopyr, 2-[(3,5,6-trichloro-2-pyridinyl)oxy]acetic acid.

Commodity	Parts per million
Egg	0.05
Fish	3.0
Grass, forage	700.0
Grass, hay	200.0
Milk	0.60
Poultry, fat	0.1
Poultry, meat	0.1